Having Composition Or Density Gradient Or Differential Porosity Patents (Class 428/547)
  • Patent number: 8061580
    Abstract: A method of forming and assembling at least two parts together that may be metal, ceramic, or a combination of metal and ceramic parts. Such parts may have different CTE. Individual parts that are formed and sintered from particles leave a network of interconnecting porosity in each sintered part. The separate parts are assembled together and then a fill material is infiltrated into the assembled parts using a method such as capillary action, gravity, and/or pressure. The assembly is then cured to yield a bonded and fully or near-fully dense part that has the desired physical and mechanical properties for the part's intended purpose. Structural strength may be added to the parts by the inclusion of fibrous materials.
    Type: Grant
    Filed: November 23, 2010
    Date of Patent: November 22, 2011
    Assignee: Babcock & Wilcox Technical Services Y-12, LLC
    Inventor: Edward B. Ripley
  • Patent number: 8043716
    Abstract: Disclosed herein is a gradient thin film, formed on a substrate by simultaneously depositing different materials on the substrate using a plurality of thin film deposition apparatuses provided in a vacuum chamber, wherein the gradient thin film is formed such that the composition thereof is continuously changed depending on the thickness thereof by deposition control plates provided in the path through which the different materials move to the substrate. The gradient thin film is advantageous in that the thin film is formed by simultaneously depositing different materials using various deposition apparatuses, so that the composition thereof is continuously changed depending on the thickness thereof, with the result that the physical properties of a thin film are easily controlled and the number of deposition processes is decreased, and thus processing time and manufacturing costs are decreased, thereby improving economic efficiency.
    Type: Grant
    Filed: July 22, 2008
    Date of Patent: October 25, 2011
    Assignee: Korea Electrotechnology Research Institute
    Inventors: Ho Sup Kim, Sang Soo Oh, Tae Hyung Kim, Dong Woo Ha, Kyu Jung Song, Hong Soo Ha, Rock Kil Ko, Nam Jin Lee
  • Patent number: 7998238
    Abstract: A sintered sliding member comprises a back metal (21a) and a ferrous sintered sliding body (20) which is sintering-bonded to the back metal (21a). The ferrous sintered sliding body (20) has martensite phase having a solid soluble carbon concentration of 0.15 to 0.5 wt % and contains carbide in a content of 5 to 50% by volume. The sintered sliding member is excellent in abrasion resistance, seizing resistance and heat crack resistance.
    Type: Grant
    Filed: July 30, 2004
    Date of Patent: August 16, 2011
    Assignee: Komatsu Ltd.
    Inventors: Takemori Takayama, Tetsuo Ohnishi, Kazuo Okamura
  • Patent number: 7955706
    Abstract: A cermet armor material for highly effective ballistic performance which is comprised of a layer of base metal in which is deposited a layer or layers of ceramic and a compatible metal such that the deposited metal in combination with the base metal forms a continuous matrix around the ceramic particles. The body has a structure which is continuously graded from a highest ceramic content at the outer surface (strike face) decreasing to zero within the base substrate, and contained no abrupt interfaces.
    Type: Grant
    Filed: June 28, 2007
    Date of Patent: June 7, 2011
    Assignee: Materials & Electrochemical Research Corp.
    Inventors: James C. Withers, Roger S. Storm, Vladimir Shapovalov, Raouf Loutfy
  • Patent number: 7914903
    Abstract: In a layered composite including a substrate comprising a number of individual layers disposed on the substrate, at least one of the individual layers includes cubic boron nitride formed by material deposition, the cubic boron nitride including oxygen added during deposition of the material.
    Type: Grant
    Filed: February 12, 2007
    Date of Patent: March 29, 2011
    Assignee: Forschungszentrum Karlsruhe GmbH
    Inventors: Sven Ulrich, Jian Ye, Konrad Sell, Michael Stüber
  • Patent number: 7914629
    Abstract: The present invention provides high strength thick steel plate superior in crack arrestability high in strength, free of deterioration of HAZ toughness, and free of anisotropy, that steel plate containing, by mass %, C: 0.03 to 0.15%, Si: 0.1 to 0.5%, Mn: 0.5 to 2.0%, P: ?0.02%, S: ?0.01%, Al: 0.001 to 0.1%, Ti: 0.005 to 0.02%, Ni: 0.15 to 2%, and N: 0.001 to 0.008% and having a balance of iron and unavoidable impurities as chemical components, having a microstructure of a ferrite and/or pearlite structure with bainite as a matrix phase, and having an average circle equivalent diameter of crystal grains with a crystal misorientation angle of 15° or more of 15 ?m or less in the regions of 10% of plate thickness from the front and rear surfaces and of 40 ?m or less in the other region including the center part of plate thickness.
    Type: Grant
    Filed: April 13, 2007
    Date of Patent: March 29, 2011
    Assignee: Nippon Steel Corporation
    Inventors: Kiyotaka Nakashima, Masanori Minagawa, Kouji Ishida, Akira Ito
  • Patent number: 7910219
    Abstract: A cermet armor material for highly effective ballistic performance which is comprised of a layer of base metal in which is deposited a layer or layers of ceramic and a compatible metal such that the deposited metal in combination with the base metal forms a continuous matrix around the ceramic particles. The body has a structure which is continuously graded from a highest ceramic content at the outer surface (strike face) decreasing to zero within the base substrate, and contained no abrupt interfaces.
    Type: Grant
    Filed: June 28, 2007
    Date of Patent: March 22, 2011
    Assignee: Materials & Electrochemical Research Corp.
    Inventors: James C. Withers, Roger S. Storm, Vladimir Shapovalov, Loutfy Raouf
  • Publication number: 20110008639
    Abstract: The invention describes a method of producing a sinter-hardened component from a metallic powder containing chromium which is pre-alloyed in particular, comprising the steps of compacting the powder to form a green compact and then sintering the green compact in a reducing sintering atmosphere at a sintering temperature in excess of 1100° C. A gas containing carbon is added to the sintering atmosphere.
    Type: Application
    Filed: May 29, 2008
    Publication date: January 13, 2011
    Applicant: Miba Sinter Austria GmbH
    Inventors: Peter Orth, Gerold Stetina
  • Patent number: 7857193
    Abstract: A method of assembling two or more parts together that may be metal, ceramic, metal and ceramic parts, or parts that have different CTE. Individual parts are formed and sintered from particles that leave a network of interconnecting porosity in each sintered part. The separate parts are assembled together and then a fill material is infiltrated into the assembled, sintered parts using a method such as capillary action, gravity, and/or pressure. The assembly is then cured to yield a bonded and fully or near-fully dense part that has the desired physical and mechanical properties for the part's intended purpose. Structural strength may be added to the parts by the inclusion of fibrous materials.
    Type: Grant
    Filed: November 23, 2005
    Date of Patent: December 28, 2010
    Assignee: Babcock & Wilcox Technical Services Y-12, LLC
    Inventor: Edward B. Ripley
  • Patent number: 7854958
    Abstract: Thermal spray processing and cold spray processing are utilized to manufacture porous starting materials (such as tube stock, wire and substrate sheets) from biocompatible metals, metal alloys, ceramics and polymers that may be further processed into porous medical devices, such as stents. The spray processes are also used to form porous coatings on consolidated biocompatible medical devices. The porous substrates and coatings may be used as a reservoir to hold a drug or therapeutic agent for elution in the body. The spray-formed porous substrates and coatings may be functionally graded to allow direct control of drug elution without an additional polymer topcoat. The spray processes are also used to apply the drug or agent to the porous substrate or coating when drug or agent is robust enough to withstand the temperatures and velocities of the spray process with minimal degradation.
    Type: Grant
    Filed: March 18, 2009
    Date of Patent: December 21, 2010
    Assignee: Advanced Cardiovascular Systems, Inc.
    Inventor: Pamela A. Kramer
  • Publication number: 20100310895
    Abstract: A polycrystalline aluminum thin film is made of polycrystals of an alloy of aluminum. The polycrystalline aluminum thin film includes a first additive which is distributed with even concentration over an inside of each crystal grain and an interface of the crystal grain and a second additive which is distributed with higher concentration in the interface of the crystal grain than in the inside of the crystal grain.
    Type: Application
    Filed: June 18, 2010
    Publication date: December 9, 2010
    Applicant: Pioneer Corporation
    Inventors: Takanobu Higuchi, Yasuo Hosoda
  • Patent number: 7846554
    Abstract: The present invention discloses a method of making a functionally graded metal matrix composite (MMC) sheet having a central layer of particulate matter. The method includes providing a molten metal containing particulate matter to a pair of advancing casting surfaces. Solidifying the molten metal while advancing the molten metal between the advancing casting surfaces to form a product comprising a first solid outer layer, a second solid outer layer, and a semi-solid central layer having a higher concentration of particulate matter than either of the outer layers. Solidifying the central layer to form a solid metal product comprised of an inner layer sandwiched between the outer layers and withdrawing the metal product from between the casting surfaces. The method yields an MMC having a central layer enriched with particulate matter and sandwiched between metallic outer layers.
    Type: Grant
    Filed: April 11, 2007
    Date of Patent: December 7, 2010
    Assignee: Alcoa Inc.
    Inventors: David A. Tomes, Jr., Gavin F. Wyatt-Mair, David W. Timmons, Ali Unal
  • Patent number: 7842398
    Abstract: The dielectric device includes a substrate, a lower electrode, a dielectric layer, and an upper electrode. The lower electrode is bonded onto the substrate. The dielectric layer is bonded onto the lower electrode. The dielectric layer is obtained through thermal treatment of a film layer formed by spraying of a powdery dielectric material and a fine-particulate metal. In the thus-formed film layer, the metal is dispersed in the matrix of the dielectric material. Thermal treatment of the film layer causes migration of the metal in the film layer. This metal migration causes a lower-electrode-adjacent portion and upper-surface-adjacent portion of the dielectric layer to have different metal contents.
    Type: Grant
    Filed: April 7, 2009
    Date of Patent: November 30, 2010
    Assignee: NGK Insulators, Ltd.
    Inventors: Tsutomu Nanataki, Nobuyuki Kobayashi
  • Publication number: 20100276236
    Abstract: One exemplary embodiment includes a damped product. The damped product is composed of a sintered powder metallurgy material and has a first portion and a second portion. The first portion has a density that is greater in value that a density of the second portion. The different densities damp vibrations in the product when the product is vibrated.
    Type: Application
    Filed: May 1, 2009
    Publication date: November 4, 2010
    Applicant: GM GLOBAL TECHNOLOGY OPERATIONS, INC.
    Inventors: Chongmin Kim, Michael D. Hanna, James G. Schroth
  • Patent number: 7776449
    Abstract: A composite article that can be used as a substrate for coated conductors is disclosed. The composite substrate has at least three layers in which one or more inner layers of Ni—W alloys with 9 at. %-13 at. % W and two outer layers of Ni—W alloys with 3 at. %-9 at. % W. The content of W element gradually decreases from the inner layers to the outer layers. The composite substrate can be prepared using a process of designing and sintering composite ingot, rolling composite ingot and then annealing composite substrate. The composite substrate have a dominant cube texture on the outer layer of the whole substrate which have a weaker magnetism and higher strength than that of a single Ni-5 at. % W alloy substrate.
    Type: Grant
    Filed: June 5, 2009
    Date of Patent: August 17, 2010
    Assignee: Beijing University of Technology
    Inventors: Hongli Suo, Min Liu, Yue Zhao, Meiling Zhou, Lin Ma, Tieyong Zuo
  • Patent number: 7763356
    Abstract: A coated article includes an article having at least one surface and composed of a molybdenum based refractory metal alloy base substrate, a niobium based refractory metal alloy base substrate or a silicon base substrate. A bond coat layer is disposed upon the surface. The bond coat layer includes a molybdenum disilicide base compound and at least one of the following: silicon nitride, silicon carbide or tantalum oxide. A process for coating the article includes the steps of applying upon the article's surface the aforementioned bond coat layer. A functionally graded material layer is applied upon the bond coat layer. The functionally graded material layer comprising molybdenum disilicide, mullite and at least one of the following: silicon nitride, silicon carbide or tantalum oxide. A thermal barrier coating layer is then applied upon the functionally graded material layer.
    Type: Grant
    Filed: March 13, 2006
    Date of Patent: July 27, 2010
    Assignee: United Technologies Corporation
    Inventors: Douglas M. Berczik, David A. Litton, Melvin Freling, Kevin W. Schlichting
  • Patent number: 7749428
    Abstract: A manufacturing method of a clad material composed of a bronze alloy and a steel is provided, including: scattering a bronze alloy powder on a steel back metal; sintering the bronze alloy powder to obtain a bilayer material having a porous bronze alloy layer on the steel; dry-rolling and a sintering the bilayer material so that the bronze alloy layer has a porosity of 3% or less; and wet-rolling the bilayer material with supplying a rolling oil to surfaces of rolling rolls. The clad manufactured according to this method can be heat-treated without an disadvantage in a conventional wet-rolling that entering rolling oil vaporizes in the bronze alloy layer during the heat treatment to form new voids. Therefore, it becomes possible to make a bronze alloy layer high in density in small times of rolling, thus enabling an increase in production efficiency.
    Type: Grant
    Filed: March 27, 2007
    Date of Patent: July 6, 2010
    Assignee: Daido Metal Co Ltd.
    Inventors: Hiroyuki Sugawara, Yasuo Ido, Yoshiaki Sato, Yukio Ogita, Shigemasa Hakakoshi
  • Patent number: 7718273
    Abstract: The present invention provides a wiring material for forming wiring on a substrate by causing coalescence of conductive particles through heating, and including a binder layer and a wiring layer. The binder layer contains metal particles and having a binder function to be adhered to the substrate; and the wiring layer contains metal particles and laminated on the binder layer. The metal particles of the binder layer and the metal particles of the wiring layer are in contact with each other. With this arrangement, it is possible to provide a wiring material allowing use of a larger variety of materials, while also ensuring low resistance of wiring and improvement of adhesion between the wiring and the substrate.
    Type: Grant
    Filed: January 13, 2004
    Date of Patent: May 18, 2010
    Assignee: Sharp Kabushiki Kaisha
    Inventors: Akiyoshi Fujii, Toshio Tahira, Nobukazu Nagae
  • Publication number: 20100098964
    Abstract: The invention describes a process for the production of a coating (6) on the basis of at least one material selected from a group comprising silicon, germanium, and the oxides SiOx or GeOx of these elements, whereby these are doped where applicable and produced specifically amorphised, on at least a subsection of a surface (3) of a metallic substrate (2), whereby the concentration of nitrate is increased in the substrate (2) where applicable prior to precipitation of the coating (6) at least in the area of the subsection. This subsection is subjected to oxidation prior to precipitation of the coating (6).
    Type: Application
    Filed: February 29, 2008
    Publication date: April 22, 2010
    Inventor: Guenter Ruebig
  • Patent number: 7682704
    Abstract: A metal injection-molding feedstock is heated and plasticized. Supercritical carbon dioxide is injected into the feedstock to form micropores when the pressure is reduced and a parts mold is filled. The micropores are retained when the green parts are debindered and sintered.
    Type: Grant
    Filed: July 2, 2004
    Date of Patent: March 23, 2010
    Assignee: Southco, Inc.
    Inventor: Ratnesh K. Dwivedi
  • Patent number: 7632565
    Abstract: Metal foams are impregnated with resins. The metal foam/polymer composite formed upon curing has excellent acoustic dampening and structural properties. Foams of various metals, such as aluminum, titanium, nickel, copper, iron, zinc, lead, silver, gold, platinum, tantalum, and alloys based on these metals, may be used. The polymer component may be any polymeric resin, for example, epoxy, natural rubber, acrylic, or phenolic.
    Type: Grant
    Filed: April 28, 1997
    Date of Patent: December 15, 2009
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: M. Ashraf Imam, Bhakta B. Rath, Teddy M. Keller
  • Patent number: 7594325
    Abstract: An aerofoil (35) for example a fan blade (26) comprises a leading edge (36), a trailing edge (38), a concave pressure surface extending (40) from the leading edge (36) to the trailing edge (38) and a convex suction surface (42) extending from the leading edge (36) to the trailing edge (38). The aerofoil (35) comprises a metal foam (50) arranged within a cavity defined by metal workpieces (52, 54). The metal foam (50) of the aerofoil (26) ideally has a density of less than 1g/cm3, is cheaper to manufacture and has improved fatigue behaviour and impact capability.
    Type: Grant
    Filed: August 25, 2005
    Date of Patent: September 29, 2009
    Assignee: Rolls-Royce plc
    Inventor: Simon Read
  • Patent number: 7569284
    Abstract: A high k dielectric film and methods for forming the same are disclosed. The high k material includes two peaks of impurity concentration, particularly nitrogen, such as at a lower interface and upper interface, making the layer particularly suitable for transistor gate dielectric applications. The methods of formation include low temperature processes, particularly CVD using a remote plasma generator and atomic layer deposition using selective incorporation of nitrogen in the cyclic process. Advantageously, nitrogen levels are tailored during the deposition process and temperatures are low enough to avoid interdiffusion and allow maintenance of the desired impurity profile.
    Type: Grant
    Filed: July 3, 2008
    Date of Patent: August 4, 2009
    Assignee: ASM America, Inc.
    Inventors: Eric J Shero, Christophe Pomarede
  • Patent number: 7534287
    Abstract: The present invention is directed to porous composite materials comprised of a porous base material and a powdered nanoparticle material. The porous base material has the powdered nanoparticle material penetrating a portion of the porous base material; the powdered nanoparticle material within the porous base material may be sintered or interbonded by interfusion to form a porous sintered nanoparticle material within the pores and or on the surfaces of the porous base material. Preferably this porous composite material comprises nanometer sized pores throughout the sintered nanoparticle material. The present invention is also directed to methods of making such composite materials and using them for high surface area catalysts, sensors, in packed bed contaminant removal devices, and as contamination removal membranes for fluids.
    Type: Grant
    Filed: December 10, 2007
    Date of Patent: May 19, 2009
    Assignee: Entegris, Inc.
    Inventors: Robert Zeller, Christopher Vroman
  • Patent number: 7514122
    Abstract: Thermal spray processing and cold spray processing are utilized to manufacture porous starting materials (such as tube stock, wire and substrate sheets) from biocompatible metals, metal alloys, ceramics and polymers that may be further processed into porous medical devices, such as stents. The spray processes are also used to form porous coatings on consolidated biocompatible medical devices. The porous substrates and coatings may be used as a reservoir to hold a drug or therapeutic agent for elution in the body. The spray-formed porous substrates and coatings may be functionally graded to allow direct control of drug elution without an additional polymer topcoat. The spray processes are also used to apply the drug or agent to the porous substrate or coating when drug or agent is robust enough to withstand the temperatures and velocities of the spray process with minimal degradation.
    Type: Grant
    Filed: October 17, 2006
    Date of Patent: April 7, 2009
    Assignee: Advanced Cardiovascular Systems, Inc.
    Inventor: Pamela A. Kramer
  • Patent number: 7486020
    Abstract: A composite article comprises a substrate having at least a substrate surface and a graded-composition coating disposed on a substrate surface. The composition of the coating material varies substantially continuously across its thickness. The coating reduces the transmission rates of oxygen, water vapor, and other chemical species through the substrate such that the composite article can be used effectively as a diffusion barrier to protect chemically sensitive devices or materials. An organic light-emitting device incorporates such a composite article to provide an extended life thereto.
    Type: Grant
    Filed: December 2, 2005
    Date of Patent: February 3, 2009
    Assignee: General Electric Company
    Inventors: Marc Schaepkens, Kevin Warner Flanagan
  • Patent number: 7468089
    Abstract: A self-cleaning porous cermet material, filter and system utilizing the same may be used in filtering particulate and gaseous pollutants from internal combustion engines having intermetallic and ceramic phases. The porous cermet filter may be made from a transition metal aluminide phase and an alumina phase. Filler materials may be added to increase the porosity or tailor the catalytic properties of the cermet material. Additionally, the cermet material may be reinforced with fibers or screens. The porous filter may also be electrically conductive so that a current may be passed therethrough to heat the filter during use. Further, a heating element may be incorporated into the porous cermet filter during manufacture. This heating element can be coated with a ceramic material to electrically insulate the heating element. An external heating element may also be provided to heat the cermet filter during use.
    Type: Grant
    Filed: March 29, 2005
    Date of Patent: December 23, 2008
    Assignee: Battelle Energy Alliance, LLC
    Inventor: Peter C. Kong
  • Patent number: 7465500
    Abstract: Methods and apparatus are provided for a shield to protect a surface from the impact of hyper-velocity projectiles. The apparatus comprises a foam material that is configured to cover the surface to be protected and is attached directly to that surface. A coating material is typically disposed on the outer surface of the foam material and may penetrate the foam material to a predetermined depth. The foam material and the coating material are selected to form a composite having predetermined values of sonic velocity, toughness, and thermal conductivity. The composite of foam material and coating material can be significantly lighter in weight than a metal shield having equivalent protective characteristics.
    Type: Grant
    Filed: October 28, 2004
    Date of Patent: December 16, 2008
    Assignee: The Boeing Company
    Inventors: Sherwin Yang, Nathan J. Hoffman, Adon Delgado, Jr., Alan V. Von Arx, Michael P. Moriarty, Kathleen M. Sevener, Gerard D. Pelletier
  • Patent number: 7449043
    Abstract: A cemented carbide tool comprising hard constituents in a binder phase of Co and/or Ni and at least one surface portion and an interior portion in which surface portion the grain size is smaller than in the interior portion is disclosed. The surface portion with the fine grain size has a lower binder phase content than the interior portion. A method to form the cemented carbide cutting tool is also disclosed.
    Type: Grant
    Filed: December 15, 2004
    Date of Patent: November 11, 2008
    Assignee: Sandvik Intellectual Property Aktiebolag
    Inventors: Marianne Collin, Susanne Norgren, Håkan Engstrōm
  • Patent number: 7427310
    Abstract: A cemented carbide cutting tool insert/button for mining and construction comprising hard constituents in a binder phase of Co and/or Ni and at least one surface portion and an interior portion in which surface portion the grain size is smaller than in the interior portion is disclosed. The surface portion with the smaller grain size has a lower binder phase content than the interior portion. A method to form the cemented carbide cutting tool insert/button is also disclosed.
    Type: Grant
    Filed: December 15, 2004
    Date of Patent: September 23, 2008
    Assignee: Sandvik Intellectual Property AB
    Inventors: Mathias Tillman, Susanne Norgren, Marianne Collin
  • Publication number: 20080166579
    Abstract: A method for producing an at least partially surface-densified metallic toothed element comprising a densified sintering material, in order to improve a strength profile, a preform of the toothed element being produced with a locally selective oversize profile relative to a final size of the toothed element and being rolled to the final size by means of at least one rolling die, the toothed element being densified in locally varied manner at least in the region of at least one flank and/or one root of a tooth of the toothed element to produce a densified outer layer.
    Type: Application
    Filed: December 10, 2007
    Publication date: July 10, 2008
    Inventor: Gerhard Kotthoff
  • Patent number: 7390568
    Abstract: A semiconductor nanocrystal heterostructure has a core of a first semiconductor material surrounded by an overcoating of a second semiconductor material. Upon excitation, one carrier can be substantially confined to the core and the other carrier can be substantially confined to the overcoating.
    Type: Grant
    Filed: August 12, 2003
    Date of Patent: June 24, 2008
    Assignee: Massachusetts Institute of Technology
    Inventors: Sungjee Kim, Moungi G. Bawendi
  • Patent number: 7361203
    Abstract: A bearing is manufactured by filling iron-based material powder and copper-based material powder in a filling portion of a mold, compacting those material powder so as to form a green compact, and then sintering the green compact. The copper-based material powder contains flat powder particles, the flat powder particles having a large aspect ratio than particles of the iron-based material powder. The coppers-based powder particles segregate on a sliding surface by vibration. The sliding surface of a bearing is covered with copper, and a ratio of iron increases from the sliding surface toward the inside. Since a rotation shaft slides on the sliding surface covered with copper, a frictional coefficient between the rotation shaft and the sliding surface is reduced, thus enabling a smooth rotation thereof. Simultaneously the usage of iron imparts predetermined strength and durability.
    Type: Grant
    Filed: August 4, 2003
    Date of Patent: April 22, 2008
    Assignee: Mitsubishi Materials Corporation
    Inventors: Teruo Shimizu, Tsuneo Maruyama
  • Patent number: 7329311
    Abstract: The present invention is directed to porous composite materials comprised of a porous base material and a powdered nanoparticle material. The porous base material has the powdered nanoparticle material penetrating a portion of the porous base material; the powdered nanoparticle material within the porous base material may be sintered or interbonded by interfusion to form a porous sintered nanoparticle material within the pores and or on the surfaces of the porous base material. Preferably this porous composite material comprises nanometer sized pores throughout the sintered nanoparticle material. The present invention is also directed to methods of making such composite materials and using them for high surface area catalysts, sensors, in packed bed contaminant removal devices, and as contamination removal membranes for fluids.
    Type: Grant
    Filed: August 10, 2006
    Date of Patent: February 12, 2008
    Assignee: Entegris, In.
    Inventors: Robert Zeller, Christopher Vroman
  • Patent number: 7297271
    Abstract: Provided are a porous sintered compact suitable for a filter, a power feeder in a polymer electrolyte membrane type water electrolyzer, a current collector in a solid polymer fuel cell and in addition a liquid dispersion plate, especially an ink dispersion plate for an ink jet printer ink and the like. A titanium powder sintered compact made of a plate-like porous compact is obtained by sintering spherical powder made of titanium or a titanium alloy produced by means of a gas atomization method. A void ratio in the range of from 35 to 55% is realized by filling without applying a pressure and sintering without applying a pressure.
    Type: Grant
    Filed: August 10, 2006
    Date of Patent: November 20, 2007
    Assignee: Sumitomo Titanium Corporation
    Inventors: Takashi Onishi, Tadashi Ogasawara, Munetoshi Watanabe, Masamichi Kato
  • Publication number: 20070141374
    Abstract: An environmentally resistant gas turbine engine disk is disclosed. The disk includes a substrate metal having locally enriched surface regions, the locally enriched surface regions comprising alloying elements present in a higher percentage than found in the substrate metal. A method for making the disk and other articles is also disclosed. The method includes furnishing a plurality of powder particle substrates made of a substrate metal, providing a nonmetallic precursor of a metallic coating material, wherein the metallic coating material includes an alloying element that is thermophysically melt incompatible with the substrate metal, contacting the powder particle substrates with the nonmetallic precursor, and chemically reducing the nonmetallic precursor to form coated powder particles comprising the powder particle substrates having a surface-enriched layer of the metallic coating material thereon, wherein the step of chemically reducing is performed without melting the powder particle substrates.
    Type: Application
    Filed: December 19, 2005
    Publication date: June 21, 2007
    Applicant: GENERAL ELECTRIC COMPANY
    Inventors: David P. Mourer, Kenneth R. Bain
  • Patent number: 7137312
    Abstract: A method is disclosed for the manufacture of gear wheels having two axially adjacent gears (4,6) thereon. A blank is prepared with the two gears crudely formed thereon by compressing and sintering a shaped mass of substantially metal powder. The blank is then mounted for rotation about a first axis, and the gears are roll-formed on the blank by rotating the blank in meshing engagement with respective dies (10,12) mounted for rotation about second and third axes substantially parallel to the first axis.
    Type: Grant
    Filed: March 30, 2001
    Date of Patent: November 21, 2006
    Assignee: FormFlo Limited
    Inventor: Christopher John Cole
  • Patent number: 7112237
    Abstract: The present invention is directed to porous composite materials comprised of a porous base material and a powdered nanoparticle material. The porous base material has the powdered nanoparticle material penetrating a portion of the porous base material; the powdered nanoparticle material within the porous base material may be sintered or interbonded by interfusion to form a porous sintered nanoparticle material within the pores and or on the surfaces of the porous base material. Preferably this porous composite material comprises nanometer sized pores throughout the sintered nanoparticle material. The present invention is also directed to methods of making such composite materials and using them for high surface area catalysts, sensors, in packed bed contaminant removal devices, and as contamination removal membranes for fluids.
    Type: Grant
    Filed: December 11, 2003
    Date of Patent: September 26, 2006
    Assignee: Entegris, Inc.
    Inventors: Robert Zeller, Christopher Vroman
  • Patent number: 7097685
    Abstract: A cemented carbide comprises a binder phase consisting essentially of an iron family metal, a first hard phase consisting essentially of WC having a hexagonal crystal structure, and a second hard phase consisting essentially of one or more types of a compound of a metal or metals of group 4, 5 or 6 of the periodic table having an NaCl-type cubic crystal structure. The cemented carbide is formed by a surface region with a thickness of 2 to 50 ?m consisting of the binder phase and the first hard phase, and an inner region present underneath the surface region consisting of the binder phase, the first hard phase and the second hard phase. A ratio of an average grain size of the first hard phase in the surface region to an average grain size of the first hard phase in the inner region is 1 or less, and a ratio of an area of the binder phase in the surface region to an area of the binder phase in the inner region is greater than 1.
    Type: Grant
    Filed: August 25, 2004
    Date of Patent: August 29, 2006
    Assignee: Tungaloy Corporation
    Inventors: Hiroyuki Miura, Satoshi Kinoshita
  • Patent number: 7070643
    Abstract: There is disclosed a compositionally graded sintered alloy which comprises: 1 to 40% by weight of a iron group metal; 0.1 to 10% by weight of at least one type of a specific metal element selected from the group consisting of Cr, Au, Ge, Cu; Sn, Al, Ga, Ag, In, Mn and Pb; a hard phase containing, as a main component, at least one compound selected from the group consisting of a carbide, a nitride and a mutual solid solution of a metal(s) which belongs to Group 4 (Ti, Zr, Hf), 5 (V, Nb, Ta) or 6 (Cr, Mo, W) of the Periodic Table; and inevitable impurities, wherein the content of the specific metal element gradually increases from a surface of the sintered alloy toward an inner portion thereof, and a ratio of the average concentration of the specific metal element in a region which is at least 1 mm inside from the surface of the sintered alloy, to the average concentration of the specific metal element in a region between the surface and the position which is 0.
    Type: Grant
    Filed: March 26, 2004
    Date of Patent: July 4, 2006
    Assignee: Toshiba Tungaloy Co., Ltd.
    Inventor: Masaki Kobayashi
  • Patent number: 7014367
    Abstract: An oil-impregnated sintered sliding bearing formed of a porous iron-based sintered alloy with quenched structure and receiving a high surface pressure capable of reducing the number of finishing steps by cutting and grinding and providing a bearing performance equivalent to or higher than that of conventional bearings, wherein a plurality of ridge-and-groove lines having a height difference of 2 to 12.5 ?m and extending in circumferential direction are axially arranged in parallel with each other by boring the bearing surface thereof to form a wavy surface in axial direction, and the portion thereof deeper by 10 to 60 ?m from the outer layer of the bearing surface is formed dense to seal surface pores so as to reduce the pores opening to the outer surface to 1 to 10 percent by area, whereby the bearing can be used at a surface pressure of 6 kgf/mm2 (58.5 MPa) or higher and a sliding speed of 2 to 5 cm/s.
    Type: Grant
    Filed: January 20, 2003
    Date of Patent: March 21, 2006
    Assignees: Hitachi Powered Metals Co., Ltd., Hitachi Construction Machinery Co., Ltd.
    Inventors: Motohiro Miyasaka, Kazuo Maruyama, Michiharu Mogami, Junichi Kobayashi, Hideki Akita, Osamu Gokita
  • Patent number: 6972156
    Abstract: A body (5) of set, initially pasty material, such as concrete, includes an electrically conducting path formed by a concentrated layer (6) of electrically conducting magnetizable elements, such as fibers (F) or granules (G), embedded in the initially pasty material and extending through at least a portion of the body (5). Electrically conducting terminal members (9) may be connected to the electrically conducting layer (6) at spaced-apart positions along the layer (6). A method of providing such a body (5) includes the steps of: (a) forming a body of the pasty material in which electrically conducting magnetizable elements (F) are dispersed, (b) applying a magnetic field to the body of pasty material to form from the magnetizable elements an electrically conducting layer embedded in the body of pasty material and extending at least through a portion the body (5), and (c) causing the body of pasty material containing the layer (6) to set.
    Type: Grant
    Filed: December 21, 2000
    Date of Patent: December 6, 2005
    Assignee: Readymix Technologies Limited
    Inventor: Björn Svedberg
  • Patent number: 6955112
    Abstract: A lightweight armor system may comprise multiple reinforcement materials layered within a single metal matrix casting. These reinforcement materials may comprise ceramics, metals, or other composites with microstructures that may be porous, dense, fibrous or particulate. Various geometries of flat plates, and combinations of reinforcement materials may be utilized. These reinforcement materials are infiltrated with liquid metal, the liquid metal solidifies within the material layers of open porosity forming a dense hermetic metal matrix composite armor in the desired product shape geometry. The metal infiltration process allows for metal to penetrate throughout the overall structure extending from one layer to the next, thereby binding the layers together and integrating the structure.
    Type: Grant
    Filed: July 7, 2004
    Date of Patent: October 18, 2005
    Assignee: Ceramics Process Systems
    Inventors: Richard Adams, Mark Occhionero
  • Patent number: 6936339
    Abstract: A thermal protection system (TPM) for protecting a surface subject to high thermal load comprising a fiber substrate where the substrate is composed of woven or non-woven layers of fibers laminated together, or the substrate is formed by a process of three-dimensional weaving, wherein the fiber substrate has a variable density of fibers, with said density of fibers increasing across the thickness of the TPM, and further wherein the substrate is needled and coupled to an insulation backing.
    Type: Grant
    Filed: November 22, 2002
    Date of Patent: August 30, 2005
    Assignee: Albany International Techniweave, Inc.
    Inventor: Henry Moody
  • Patent number: 6918943
    Abstract: A machining surface of a machining tool such as a drill is composed of a metal-rich section. A ceramics-rich section is formed centrally in the drill. Further, a gradient section is provided between the ceramics-rich section and the metal-rich section. In the gradient section, the composition ratio of metal is gradually increased from the ceramics-rich section to the metal-rich section. That is, the drill is composed of the gradient composite material in which the composition ratio of ceramics is increased and the composition ratio of metal is decreased inwardly from the machining surface.
    Type: Grant
    Filed: December 12, 2001
    Date of Patent: July 19, 2005
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventors: Mitsuo Kuwabara, Masanori Ohtsuka
  • Patent number: 6895851
    Abstract: A lightweight armor system may comprise multiple reinforcement materials layered within a single metal matrix casting. These reinforcement materials may comprise ceramics, metals, or other composites with microstructures that may be porous, dense, fibrous or particulate. Various geometries of flat plates, and combinations of reinforcement materials may be utilized. These reinforcement materials are infiltrated with liquid metal, the liquid metal solidifies within the material layers of open porosity forming a dense hermetic metal matrix composite armor in the desired product shape geometry. The metal infiltration process allows for metal to penetrate throughout the overall structure extending from one layer to the next, thereby binding the layers together and integrating the structure.
    Type: Grant
    Filed: June 16, 2003
    Date of Patent: May 24, 2005
    Assignee: Ceramics Process Systems
    Inventors: Richard Adams, Mark Occhionero
  • Patent number: 6897123
    Abstract: A method for bonding materials with different thermal expansion coefficients is provided. An intermediary layer of glass, ceramics, polymers, metals or composites is inserted between the materials to be bonded; this intermediary layer has a compositional gradient that could have been formed through diffusion processes. The coefficient of thermal expansion changes across the intermediary layer and on each side it is not substantially different from the coefficient of thermal expansion of the material that the layer is facing. In that manner there is nowhere within the intermediate layer or on the interfaces to the materials being bonded that thermally induced stress will cause fractures or significant permanent plastic deformation. The thickness of the intermediary layer depends on the difference in the coefficient of thermal expansion between the two materials being bonded, the temperature range the bond will be exposed to and the elasticity.
    Type: Grant
    Filed: March 5, 2002
    Date of Patent: May 24, 2005
    Assignee: Agityne Corporation
    Inventor: Kaspar Tobias Winther
  • Patent number: 6869460
    Abstract: An eta-phase-free cemented carbide insert with improved surface hardness and wear resistance containing WC, and possibly cubic phases of a carbide and/or carbonitride, in a binder phase of Co, Ni, Fe or a combination thereof, with a binder phase gradient in the surface and near surface regions, is disclosed. The nominal binder phase content in the insert is 3-20 weight %. The surface, and near surface cobalt content is 50-100% of the binder phase content of the inner portion of the insert. The insert is formed by standard sintering practices, followed by the chemical removal of the binder phase from the surface and near surface regions of the insert. The insert is then heat treated at a temperature of 1300-1350° C. in a carburizing atmosphere, for a time of 5-400 minutes to cause diffusion of the binder phase from the interior into the binder depleted surface regions.
    Type: Grant
    Filed: September 22, 2003
    Date of Patent: March 22, 2005
    Assignee: Valenite, LLC
    Inventors: Stephen L. Bennett, Mark J. Jagner
  • Patent number: 6783696
    Abstract: A method for reducing the loss of particles from the surface of porous getter bodies is taught herein. The method consists in producing on the surface of the porous getter a thin layer of a metal or metal alloy with a deposition technique selected among the deposition of materials from arc generated plasma, ionic beam deposition and cathodic deposition. The deposition technique allows for granular or columnar surface of the covering material but still allowing access to the surface of the getter material, resulting in a reduced getter particle loss.
    Type: Grant
    Filed: March 14, 2003
    Date of Patent: August 31, 2004
    Assignee: SAES Getters S.p.A.
    Inventors: Andrea Conte, Marco Moraja
  • Patent number: 6776818
    Abstract: A projectile having a body of sintered metal powder and a sintered metal powder surface that faces toward the rifling in the bore of a firearm, and therewith co-acts with the rifling. At least the body layer that is deformed by the rifling has a porosity in the region of 5-25%. The powder may consist of a copper alloy, such as tombak.
    Type: Grant
    Filed: March 4, 2002
    Date of Patent: August 17, 2004
    Assignee: Norma Precision AB
    Inventor: Åke Nilsson