Aluminum Compound (e.g., Clay, Aluminium Oxide, Etc.) Patents (Class 501/127)
  • Patent number: 5698485
    Abstract: A process for producing a ceramic having a microstructured surface with a surface profile depth of less than 1 micron, measured by the atomic force microscopy, comprising preparing a polymeric precursor material, shaping the precursor material into a structured mold insert of an inherently stable mold insert material having a structured surface geometry corresponding with the microstructured surface of the ceramic to form a shaped precursor material, the shaped precursor material being rendered infusible by chemical crosslinking, and wherein the inherently stable mold insert material is selected from materials having sufficient strength for structuring and high molding accuracy, and pyrolyzing the shaped precursor material, whereby the ceramic having the microstructured surface is obtained.
    Type: Grant
    Filed: January 22, 1996
    Date of Patent: December 16, 1997
    Assignees: Hoechst Aktiengesellschaft, Institut Fuer Mikrotechnik GmbH
    Inventors: Martin Bruck, Tilo Vaahs, Wolfgang Bocker, Wolfgang Ehrfeld, Manfred Lacher, Ludwig Giebel
  • Patent number: 5691259
    Abstract: A shaped ceramic article capable of being cut manually into selected sizes and process is based on a mixture of high-temperature resistant ceramic fibers and fibers which soften at temperatures below 2000.degree. F., particles of a ceramic material stable to temperatures exceeding 2000.degree. F., particles of a ceramic material which sinter at temperatures below 2000.degree. F., and a binder which provides green strength to shapes formed by vacuum formation from a slurry. The vacuum formed shape is dried at about 400.degree. F., thereby dried to form a shape which is preferably dipped in colloidal alumina or silica and dried again. The shape is sinterable by contact with flowing molten metal or by being sujected to radiant heat to form a hardened shape-stable ceramic form.
    Type: Grant
    Filed: November 8, 1996
    Date of Patent: November 25, 1997
    Assignee: Fiber Ceramics, Inc.
    Inventors: Clifford E. Couture, Paul A. Schumacher, Orville C. Clemmons
  • Patent number: 5688730
    Abstract: Gamma-aluminum oxynitride ground powders, white in color and well suited for conversion into optically transparent ceramic shaped articles, 100% of the particles of which being less than 10 .mu.m in size and exhibiting a transmittance of at least 8%, are prepared by grinding particulate gamma-aluminum oxynitride agglomerates having a porosity of greater than 75%, such agglomerates themselves being produced by interreacting dry powdery admixture of aluminum nitride, alpha-alumina, and an alumina of high specific surface area or precursor thereof.
    Type: Grant
    Filed: July 19, 1996
    Date of Patent: November 18, 1997
    Assignee: Elf Atochem S.A.
    Inventors: Roland Bachelard, Jean-Pierre Disson, Bruno Morlhon
  • Patent number: 5686366
    Abstract: A platelet .alpha.-Al.sub.2 O.sub.3 based ceramic composite consists of Al.sub.2 O.sub.3 powder, promoters and controllers. The composite is prepared by mixing aluminum oxide powder with promoters and controllers. The mixture is shaped and sintered to form an object. In one embodiment of the invention, the promoters are either salts or oxides of alkaline metals and alkaline earth metals. The salts are oxidized during sintering.
    Type: Grant
    Filed: August 3, 1994
    Date of Patent: November 11, 1997
    Assignee: Mitsubishi Materials Corporation
    Inventors: Takashi Koyama, Koichi Niihara
  • Patent number: 5676745
    Abstract: Composites in the form of a three-dimensional framework or skeleton of ceic particles are formed by a low cost, low temperature sintering process which decomposes a pre-ceramic inorganic or organic precursor. Upon heating, preferably in air, the precursor decomposes to form a ceramic phase in the form of necks between the individual ceramic particles. The properties of the resulting porous ceramic bodies can be modified, such as toughened by impregnation with monomers, oligomers or polymers which are polymerized or cured in situ. Such composites find use as cosmetic products or protheses for humans and animals, such as dental restoratives and bone implants. Methods of fabrication are disclosed which include the use of a pre-ceramic polymer as a binder for the ceramic particles which forms the necks of material between the individual ceramic particles upon firing.
    Type: Grant
    Filed: June 7, 1995
    Date of Patent: October 14, 1997
    Assignee: The United States of America, as represented by the Secretary of Commerce
    Inventors: John Robert Kelly, Joseph M. Antonucci
  • Patent number: 5672554
    Abstract: An alumina composition, an alumina molded article, prepared from the alumina composition, an alumina ceramic prepared by sintering the alumina molded article, and a process for producing the ceramic; the alumina composition comprising .alpha.-alumina particles having a ratio of the shortest diameter to the longest diameter of from 0.3 to 1; and a size distribution of not more than 5, as expressed in terms of a D.sub.90 /D.sub.10 ratio, wherein D.sub.10 and D.sub.90 represent a cumulative 10% diameter and a cumulative 90% diameter, respectively, of a cumulative distribution depicted from the small diameter side, or comprising .alpha.-alumina particles having a polyhedral shape; a D/H ratio of from 0.5 to 3.0, wherein D represents a maximum particle diameter parallel to a hexagonal lattice plane of a hexagonal close-packed lattice of .alpha.-alumina, and H represents a particle diameter perpendicular to the lattice plane; and a size distribution of not more than 5, as expressed in terms of a D.sub.90 /D.sub.
    Type: Grant
    Filed: May 28, 1996
    Date of Patent: September 30, 1997
    Assignee: Sumitomo Chemical Company, Limited
    Inventors: Masahide Mohri, Norio Matsuda, Shinichiro Tanaka, Yoshio Uchida
  • Patent number: 5670253
    Abstract: A composite ceramic wafer including a beta silicon carbide layer. The composite ceramic wafer is useful for making thin film magnetic heads.
    Type: Grant
    Filed: December 20, 1995
    Date of Patent: September 23, 1997
    Assignee: Minnesota Mining and Manufacturing Company
    Inventors: Raymond C. Chiu, Robert G. Smith, Billy Lee Weaver
  • Patent number: 5665127
    Abstract: Microcrystalline bodies based on .alpha.-Al.sub.2 O.sub.3 are made by drying sub-micron powders, press compacting and shock sintering at an intermediate sinter temperature range of 1,300.degree. to 1,550.degree. C., i.e. bringing the compact up to such range in under 60 seconds, preferably under 10.
    Type: Grant
    Filed: January 24, 1996
    Date of Patent: September 9, 1997
    Assignee: H.C. Starck GmbH & Co. KG
    Inventors: Paul Moltgen, Pirmin Wilhelm, Josef Schmoll
  • Patent number: 5658838
    Abstract: The present invention relates to novel alumina-based ceramic composition containing a compound capable of forming a spinel-type aluminate phase detectable by x-ray diffraction, the composition having particular advantage for use as a water faucet seal.
    Type: Grant
    Filed: March 15, 1996
    Date of Patent: August 19, 1997
    Assignee: Norton Desmarquest Fine Ceramics
    Inventor: Ridha Trabelsi
  • Patent number: 5656562
    Abstract: A method for improving the properties of ceramic green bodies is provided. In particular, ceramic green bodies having improved green strength are provided. Incorporating certain acid-containing polymers as binders at a level of at least about 1 to about 15, preferably at least about 3 to about 10 percent by weight based on the weight of ceramic particles improves the green strength of the resulting ceramic green bodies.
    Type: Grant
    Filed: June 5, 1996
    Date of Patent: August 12, 1997
    Inventor: Xianliang Wu
  • Patent number: 5652189
    Abstract: A ceramic composition for sintering into sliding parts contains:at least 90% by weight alumina,1.7% by weight to 2% by weight Mn.sub.3 O.sub.4,0.8% by weight to 1% by weight TiO.sub.2,0.5% by weight to 1.5% by weight SiO.sub.2,0.6% by weight to 1.2% by weight CoO,not more than 1% by weight MgO,not more than 0.4% by weight Fe.sub.2 O.sub.3,the remainder, up to 0.5% in total, comprising impurities.After sintering, this composition produces sliding parts containing manganese aluminate and/or cobalt aluminate phases.
    Type: Grant
    Filed: June 7, 1995
    Date of Patent: July 29, 1997
    Assignee: Norton Desmarquest Fine Ceramics
    Inventor: Ridha Trabelsi
  • Patent number: 5650121
    Abstract: The disclosed invention provides a method of forming refractory linings for maintaining refractory linings against attack by corrosive materials such as those present in steel manufacture. The method entails spraying an aqueous mixture of a refractory composition that includes at least one refractory material onto the working surface of a refractory lining. Spraying is performed to provide one or more layers of the refractory composition on the refractory lining after each exposure of the lining to corrosive materials such as those incurred in steel manufacture.
    Type: Grant
    Filed: June 6, 1995
    Date of Patent: July 22, 1997
    Assignee: Minerals Technologies, Inc.
    Inventors: Julie Annette Dody, Charles R. Rumpeltin, Jr.
  • Patent number: 5648303
    Abstract: Non-magnetic ceramics for recording/reproducing heads comprising an alumina and any one of a compound selected from silicon carbide, boron carbide, zirconium carbide, titanium oxide, aluminum boride or zirconium boride, said ceramics having a Young's modulus of not smaller than 370 Gpa and a surface coarseness Ra after milling of not larger than 100 nm, and a method of producing the same.
    Type: Grant
    Filed: February 27, 1995
    Date of Patent: July 15, 1997
    Assignee: Kyocera Corporation
    Inventor: Tsunehiko Nakamura
  • Patent number: 5641720
    Abstract: A corundum porcelain composition containing from 60 to 94% by weight of a component A and from 6 to 40% by weight of a component B, wherein component A contains from 0 to 70% by weight of alumina, from 20 to 70% by weight of clay material, from 10 to 50% by weight of glass formers and from 0 to 30% by weight of quartz, and component B comprises comminuted broken porcelain, the chemical composition of the mixture of the components A and B comprises from 20 to 75% by weight of SiO.sub.2, from 15 to 80% by weight of Al.sub.2 O.sub.3 and from 2 to 10% by weight of flux selected from the group consisting of K.sub.2 O, Na.sub.2 O, FeO, MgO, CaO, Li.sub.2 O; BaO, SrO, ZnO and fluoride, and the comminuted broken porcelain has a mean particle size between 25 and 800 .mu.m, useful, for example, in sintered bodies, such as insulators.
    Type: Grant
    Filed: November 29, 1995
    Date of Patent: June 24, 1997
    Assignee: Hoechst CeramTec Aktiengesellschaft
    Inventor: Gunter Fassbinder
  • Patent number: 5639704
    Abstract: The present invention relates to ceramics and a method for making ceramics having very little dimensional change after sintering and high dimensional accuracies, so that the characteristics of inorganic functional material are fully maintained and utilized. The ceramics of the present invention comprise grains of inorganic functional material and grains of complex oxide. The pores existing between said grains of inorganic functional material are filled with said grains of complex oxide produced by a sintering reaction between an oxidized metal and an inorganic compound.
    Type: Grant
    Filed: February 7, 1995
    Date of Patent: June 17, 1997
    Assignee: Matsushita Electric Industrial Co., Ltd.
    Inventors: Tsutomu Inuzuka, Shinji Harada, Yuji Mido, Tadashi Tojyo, Satoshi Tomioka
  • Patent number: 5637543
    Abstract: A ceramic composition for thermistor exhibiting stable resistance values over a wide temperature range and capable of being used for a prolonged time. The composition is represented by (M.sup.1 M.sup.2 O.sub.3).sub.1-x .multidot.(M.sup.1 AlO.sub.3).sub.x, wherein M.sup.1 is an element selected from the elements of the group 3A excluding La and M.sup.2 is an element of the groups 4A, 5A, 6A, 7A and 8, and wherein the mixing ratio between an electrically conductive substance stable at elevated temperatures and an insulating substance stable at elevated temperatures, may be adjusted. A thermistor formed of the composition is superior in high-temperature stability and can be used over a broad temperature range because its resistance value can be selected to an optimum value.
    Type: Grant
    Filed: December 18, 1995
    Date of Patent: June 10, 1997
    Assignee: NGK Spark Plug Co., Ltd.
    Inventors: Masaki Iwaya, Kyohei Hayashi, Hiroshi Matsuzaki, Yoshirou Suematsu
  • Patent number: 5633084
    Abstract: Fused alumina particles are covered with a coating of aluminum titanate which is formed by applying a Ti-containing compound to the surface of the fused alumina particles and firing the same to cause a reaction between the Ti-containing compound and the alumina.
    Type: Grant
    Filed: April 28, 1994
    Date of Patent: May 27, 1997
    Assignee: Showa Denko K.K.
    Inventors: Tadashi Hiraiwa, Fumiyoshi Ono
  • Patent number: 5627116
    Abstract: A sintered, translucent ceramic article comprises alpha alumina and up to 0.050 wgt. percent magnesia and between 0.001 to 0.100 wgt. percent lutetium oxide. In a preferred embodiment, the lutetium oxide is at 0.050 wgt. percent and in a second preferred embodiment half the lutetium oxide is replaced by yttrium oxide. A method of making a translucent ceramic article comprises the steps of: forming an aqueous slurry to yield one of the composition described above; adding nitric acid to adjust the pH to 4.6; adding an aqueous binder and plasticizer in the amount of 2.5 solids wgt. percent; spray-drying the slurry; forming an article by wet-bag isopressing; prefiring said article in air at about 1325.degree. C. for about 2 hours; and sintering said air-fired article in hydrogen for about 3 hours at 1800.degree. C.
    Type: Grant
    Filed: September 24, 1996
    Date of Patent: May 6, 1997
    Assignee: Osram Sylvania Inc.
    Inventor: Karlene J. Zuk
  • Patent number: 5625256
    Abstract: A ceramic discharge vessel (6) for a high-pressure discharge lamp (1) made from a sintered body of optically translucent polycrystalline alumina ceramic which is doped with only 100-800 ppm MgO, only 200-1200 ppm ZrO.sub.2 and only 10-300 ppm Y.sub.2 O.sub.3 (by weight). This improves the loading capacity and operating characteristics of the vessel and of the lamp.
    Type: Grant
    Filed: November 29, 1994
    Date of Patent: April 29, 1997
    Assignees: Patent-Treuhand-Gesellschaft F. Elektrische Gluehlampen mbH, NGK Insulators, Ltd.
    Inventors: Rita Tiedt, Helmut Weske, Koichiro Maekawa, Junichi Doi
  • Patent number: 5618762
    Abstract: An antibacterial ceramic contains an antibacterial material produced by loading an antibacterial metal such as silver on a calcium ceramic carrier and an inorganic material such as cordierite, and has a bulk density of 0.6-1.2 g/cm.sup.3. An antibacterial ceramic filter contains an antibacterial material produced by loading an antibacterial metal such as silver on a calcium ceramic carrier, an aggregate such as mullite, and a binder such as frit, and has a porosity of 20% or more. The light-weight antibacterial ceramic is suitably applicable to a roof garden or the like. The antibacterial ceramic filter can remove and extirpate various bacteria and suspensions.
    Type: Grant
    Filed: May 11, 1995
    Date of Patent: April 8, 1997
    Assignees: NGK Insulators, Ltd., NGK Adrec Co. Ltd., Sangi Co. Ltd.
    Inventors: Hiroshi Shirakawa, Osamu Yamakawa, Hiroaki Nihonmatsu, Kiminori Atsumi
  • Patent number: 5616526
    Abstract: There is now provided a ceramic material comprising of alumina, 10-50% by volume, preferably 20-35% by volume, silicon carbide whiskers, 1-25% by volume, preferably 5-20% by volume, most preferably 7-15% by volume, zirconia and 1-20% by volume, preferably 3-15% by volume, titanium compound-containing cubic phase. If this cubic phase has a lattice spacing of 4.29 to 4.40 .ANG. and a zirconium content of 3-65 weight %, a material with improved performance when turning heat resistant material such as aged Iconel 718, is obtained.
    Type: Grant
    Filed: June 20, 1995
    Date of Patent: April 1, 1997
    Assignee: Sandvik AB
    Inventors: Mats Andersson, Marianne Collin
  • Patent number: 5612267
    Abstract: Ceramic preforms comprising monocrystalline hexagonal platelets of .alpha.-alumina, well adopted for conversion into refractory bricks or ceramic composites, are prepared by crystallizing a settled fine powder of amorphous alumina, transition alumina or alumina hydrate, advantageously in the presence of a fluoro-compound flux, into a coherent mass of such hexagonal platelets of .alpha.-alumina.
    Type: Grant
    Filed: June 5, 1995
    Date of Patent: March 18, 1997
    Assignee: Atochem
    Inventors: Roland Bachelard, Annick Faure
  • Patent number: 5607630
    Abstract: A ceramic moulded body containing at least 10 vol. % fine-grained Al.sub.2 O.sub.3, and a process for its production(a) milling aluminium metal in powder form alone or together with Al.sub.2 O.sub.3 or/and if desired further suitable inorganic substances for ceramic formation in a non-aqueous liquid in the presence of oxygen until 10 to 80% of the metallic aluminium powder has reacted to form one or several aluminium oxidation precursors from the group amorphous Al.sub.2 O.sub.3, .gamma.-Al.sub.2 O.sub.3 and aluminium-organic compounds and the powder has a maximum oxidation rate between 510.degree. and 610.degree. C. according to differential thermoanalytical measurement;(b) molding the powder of step (a) into a green body;(c) slowly heating the green body in an atmosphere containing oxygen to a temperature which is below the melting temperature of aluminium until at least 50% of the metallic aluminium powder remaining after the milling has reacted to Al.sub.2 O.sub.
    Type: Grant
    Filed: September 30, 1994
    Date of Patent: March 4, 1997
    Inventor: Nils Claussen
  • Patent number: 5607887
    Abstract: The present invention provides a method for preparing a ceramic mixed-oxide of at least two metals including mixing an alloy with a ceramic oxide. The alloy including a metal selected from the group consisting of aluminum, calcium, lithium, magnesium, silicon, titanium, yttrium, and zirconium. The alloy also includes an element that is to be present in the ceramic mixed-oxide. The element is different from the metal and is selected from the group consisting of aluminum, calcium, lithium, magnesium, a combination of magnesium and silicon, silicon, titanium, yttrium, and zirconium. The ceramic oxide includes a metal that is to be present in the ceramic mixed oxide. The alloy and ceramic oxide are co-milled. The mixed and co-milled alloy and ceramic oxide are reaction-sintered, thereby oxidizing the metal and element of the alloy to produce the ceramic mixed-oxide.
    Type: Grant
    Filed: February 15, 1995
    Date of Patent: March 4, 1997
    Assignee: Volvo Aero Aktiebolag
    Inventors: Lars Pejryd, Robert Lundberg, Jesper Brandt
  • Patent number: 5603738
    Abstract: The present invention pertains to a process for preparing an abrasive based on corundum with a grain shape factor exceeding 0.6.
    Type: Grant
    Filed: November 14, 1994
    Date of Patent: February 18, 1997
    Assignee: Treibacher Schleifmittel AG
    Inventors: Hans Zeiringer, Peter Janz
  • Patent number: 5599867
    Abstract: A composition for manufacturing a fiber-reinforced molded ceramic body comprises a ceramic powder composed primarily of silicon nitride, inorganic fibers and a binder which are added to the ceramic powder. A fiber-reinforced molded ceramic body is manufactured by producing a slurry from such a composition, pouring the slurry into a mold to produce a fiber-reinforced molded ceramic body, and drying the fiber-reinforced molded ceramic body.
    Type: Grant
    Filed: March 28, 1995
    Date of Patent: February 4, 1997
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventors: Naoki Ito, Yuji Miki, Atsushi Koizumi, Hiroshi Ichikawa
  • Patent number: 5599756
    Abstract: A sintered high-toughness alumina-based composite body consisting essentially of a plate- or rod-shaped corundum or alumina-based compound structure, a fine granular corundum structure, and inevitable impurities.
    Type: Grant
    Filed: April 7, 1995
    Date of Patent: February 4, 1997
    Assignee: Yoshida Kogyo K.K.
    Inventor: Youji Matsuo
  • Patent number: 5593930
    Abstract: An object of the present invention is to shorten the working time for high pressure slip casting. There is provided a composition for high pressure casting slip including a first starting powder forming a frame of a mold body and second starting powder forming the frame of the mold body and acting as a plastic agent, wherein the first and second starting powders are uniformly mixed in a dry condition. "Slip" of a minimum water content is easily prepared by the composition to effect optimal fluidity of the slip so that the water is removed from the slip in a short time during a casting process.
    Type: Grant
    Filed: September 13, 1995
    Date of Patent: January 14, 1997
    Assignee: NGK Insulators, Ltd.
    Inventor: Ritsu Sato
  • Patent number: 5593468
    Abstract: The use of purified process materials in the production of a seeded sol-gel alumina abrasive results in an abrasive of superior properties.
    Type: Grant
    Filed: July 26, 1995
    Date of Patent: January 14, 1997
    Assignee: Saint-Gobain/Norton Industrial Ceramics Corporation
    Inventors: Arup K. Khaund, Ajay K. Garg, Ralph Bauer
  • Patent number: 5589426
    Abstract: This invention provides monolithic refractories comprising 100% by weight of refractory aggregate powders, and in addition thereto, based on the weight of refractory aggregate powers, 0.05 to 5% by weight of a binder which is phosphate glass and/or hydroxycarboxylates and 0.01 to 1% by weight of a thickener, characterized in that said monolithic refractories have been kneaded with water or other kneading liquid. The monolithic refractories are capable of being applied without being kneaded at working sites.
    Type: Grant
    Filed: July 9, 1993
    Date of Patent: December 31, 1996
    Assignee: Taikorozai Co., Ltd.
    Inventors: Itsutoshi Iwasaki, Tatsuo Yamasaki, Hideaki Sawada
  • Patent number: 5587010
    Abstract: The present invention provides a process for producing fine flaky alumina particles suitable as a raw material for ceramics, a pigment for paint and etc., wherein aluminum hydroxide or alumina hydrate having a particle size regulated to the order of submicron is subjected to a hydrothermal treatment in water or an aqueous alkali solution at a temperature of 350.degree. C. or above under a pressure of 200 kg/cm.sup.2 or below. The present invention further provides an alumina-based plastic material which is produced by kneading the aforesaid fine flaky particles with an organic water holding material and water. Methylcellulose, polyvinyl alcohol, carboxymethylcellulose, polyethylene glycol, etc. are preferably used as the organic water holding agent. The alumina-based plastic material has a high plasticity, so that there is no need of using a large amount of a binder. Thus a dense molded article having stable properties can be prepared.
    Type: Grant
    Filed: June 16, 1995
    Date of Patent: December 24, 1996
    Assignees: Agency Of Industrial Science And Technology, Ministry Of International Trade And Industry, YKK Corporation
    Inventors: Yasuo Shibasaki, Kiichi Oda, Takeshi Fukuda
  • Patent number: 5587346
    Abstract: A sintered, translucent ceramic article comprises alpha alumina and up to 0.050 wgt. percent magnesia and between 0.001 to 0.100 wgt. percent lutetium oxide. In a preferred embodiment, the lutetium oxide is at 0.050 wgt. percent and in a second preferred embodiment half the lutetium oxide is replaced by yttrium oxide. A method of making a translucent ceramic article comprises the steps of: forming an aqueous slurry to yield one of the composition described above; adding nitric acid to adjust the pH to 4.6; adding an aqueous binder and plasticizer in the amount of 2.5 solids wgt. percent; spray-drying the slurry; forming an article by wet-bag isopressing; prefiring said article in air at about 1325.degree. C. for about 2 hours; and sintering said air-fired article in hydrogen for about 3 hours at 1800.degree. C.
    Type: Grant
    Filed: June 16, 1995
    Date of Patent: December 24, 1996
    Assignee: Osram Sylvania, Inc.
    Inventor: Karlene J. Zuk
  • Patent number: 5580832
    Abstract: A method of forming a highly dispersed ceramic powder slurry is provided prising forming an aqueous based slurry of a ceramic powder and a polyelectrolyte at an acidic pH and adjusting the pH of the slurry to an alkaline value.
    Type: Grant
    Filed: April 26, 1995
    Date of Patent: December 3, 1996
    Assignee: The United States of America as represented by the Secretary of Commerce
    Inventors: Subhaschandra G. Malghan, Ramannair S. Premachandran
  • Patent number: 5580834
    Abstract: A self-sintered silicon carbide/carbon-graphite composite material having interconnected pores which may be impregnated, and a raw batch and process for producing the composite material, is provided. The composite material comprises a densified, self-sintered matrix of silicon carbide, carbon-graphite inclusions and small amounts of any residual sintering aids, such as boron and free carbon, and has interconnected pores which may be impregnated with resin, carbon, TEFLON, metal or other compounds or materials selected for their particular properties to achieve desired tribological characteristics for a specific application. The composite material is produced from a raw batch which includes silicon carbide, sintering aids, a temporary filler and coated graphite particles. The raw batch is then molded/shaped into a green body and heated to carbonize any carbonizable materials and to decompose and volatilize the organic filler to form a matrix of interconnected pores.
    Type: Grant
    Filed: February 25, 1994
    Date of Patent: December 3, 1996
    Assignee: The Morgan Crucible Company plc
    Inventor: Mark E. Pfaff
  • Patent number: 5569320
    Abstract: This invention provides a process for preparing a refractory molded article comprising the steps of (a) forming a molded article matrix from an aggregate and the first binder, (b) impregnating the molded article matrix formed in step (a) with the second binder consisting of an alcoholic solution of one kind or two or more kinds of metal alkoxides selected from alkoxides of metals of Group 4A or Group 4B (excepting carbon) and Group 3A or Group 3B of the periodic table and their partial hydrolysates and an alkaline compound of alkali metal or alkaline earth metal (one kind or a mixture of two or more kinds selected from alkoxides, hydroxides and salts of the metal) and (c) drying and firing the molded article matrix at high temperature and also provides a binder for the preparation of such refractory molded article.
    Type: Grant
    Filed: December 28, 1994
    Date of Patent: October 29, 1996
    Assignees: Cadic Corporation, KSP Inc., Tama Chemicals Co., Ltd.
    Inventors: Nobuyoshi Sasaki, Tetsuya Yokokawa, Yoshikazu Hashimoto, Yoshiro Ohta, Hideo Sekiguchi
  • Patent number: 5569547
    Abstract: A ceramic composite material consisting of single crystal .alpha.-Al.sub.2 O.sub.3 and single crystal Y.sub.3 Al.sub.5 O.sub.12 is provided. This composite material has high mechanical strength and creep behavior particularly at high temperatures.
    Type: Grant
    Filed: October 4, 1994
    Date of Patent: October 29, 1996
    Assignee: Ube Industries, Ltd.
    Inventors: Yoshiharu Waku, Hideki Ohtsubo, Yasuhiko Kohtoku
  • Patent number: 5569631
    Abstract: The present invention pertains to a refractory ceramic mass, consisting of 50 to 97 wt. % of sintered MgO as well as 3 to 50 wt. % of a spinel of the hercynite type.
    Type: Grant
    Filed: February 7, 1995
    Date of Patent: October 29, 1996
    Assignee: Veitsch-Radex Aktiengesellschaft Fur Feuerfeste Erzeugnisse
    Inventors: Harald Harmuth, Roland Heindl, Josef Deutsch
  • Patent number: 5565245
    Abstract: Mg.sub.x Al.sub.2-2x Ti.sub.1+x O.sub.5 (x.ltoreq.0.2) protective coatings have been developed for both dense and porous substrates, such as SiC and Si.sub.3 N.sub.4, using a chemical solution processing method involving the hydrolysis and condensation of magnesium, aluminum and titanium precursors. The solution viscosities, pH values, H.sub.2 O/alkoxide molar ratios, and dip coating withdrawal rates which are optimum for crack-free Mg.sub.x Al.sub.2-2x Ti.sub.1+x O.sub.5 (x.ltoreq.0.2) are 1.0 to 6.2 cP, pH 1-4.5, molar ratio 1.5-10, and withdrawal rate of 2.2-8.0 cm/min, respectively. Conversion of the amorphous coating to crystalline Mg.sub.x Al.sub.2-2x Ti.sub.1+x O.sub.5 (x.ltoreq.0.2) is achieved by a succession of calcination below 450.degree. C. and a final heat treatment above 1000.degree. C. for ten hours with controlled heating and cooling rates.
    Type: Grant
    Filed: March 1, 1995
    Date of Patent: October 15, 1996
    Assignee: Virginia Tech Intellectual Properties, Inc.
    Inventors: Tawei Sun, Nancy R. Brown, Jesse J. Brown, Jr., Min Kang
  • Patent number: 5565392
    Abstract: A method for making a high strength porcelain for use as an insulator or a structural ceramic, comprising:A) forming a mixture comprising alumina, clay and a fluxing material;B) forming the mixture into a shaped article; andC) firing the shaped article.
    Type: Grant
    Filed: June 1, 1995
    Date of Patent: October 15, 1996
    Assignee: Raychem Corporation
    Inventors: Karin M. Kinsman, Ryan W. Dupon, Martha L. McCrum, Linas Mazeika, Amy S. Chu
  • Patent number: 5560876
    Abstract: A process for producing strong, essentially dust-free agglomerates from dust created by an industrial operation carried out, for example, on an ore or mineral, e.g. during the thermal conversion of a material containing predominantly gibbsite to sub-alpha alumina by a multistage thermal process having at least one intermediate stage. The process comprises grinding particles of binder material containing undercalcined alumina to a median particle size of less than 30 microns and to a specific surface area in the range of 90-300 m.sup.2 /g; combining about 1-4 parts by weight of the dust with one part by weight of the ground binder material to form combined solids; mixing the combined solids with water to produce agglomerates, the total amount of added water being about 0.8-1.2 parts by weight for every part by weight of the ground binder material, plus about 0.08 to 0.
    Type: Grant
    Filed: May 4, 1995
    Date of Patent: October 1, 1996
    Assignee: Alcan International Limited
    Inventors: Claude Boulanger, Andrew N. Carruthers, Robert L. Clegg, Kwat I. The
  • Patent number: 5552354
    Abstract: The present invention pertains to a refractory brick based on at least one refractory metal oxide in a particle fraction of <8 mm containing 4 to 30 wt. % of a very fine refractory fraction, prepared by firing below a temperature at which the particles of the very fine refractory fraction sinter by recrystallization with grain growth.
    Type: Grant
    Filed: March 16, 1995
    Date of Patent: September 3, 1996
    Assignee: Veitsch-Radex Aktiengesellschaft fur Feuerfeste Erzeugnisse
    Inventors: Harald Harmuth, Roland Heindl, Josef Deutsch
  • Patent number: 5552356
    Abstract: The present invention relates to boron subphosphide/aluminum oxide composite materials, to processes for the production of these materials and to the use thereof.
    Type: Grant
    Filed: June 29, 1995
    Date of Patent: September 3, 1996
    Assignee: Bayer AG
    Inventor: Nils Perchenek
  • Patent number: 5545598
    Abstract: Disclosed is a high heat conductive body which consists of 30-99 wt. % of at least one of molybdenum and tungsten and 1 or more wt. % ceramic. A wiring base substrate fitted with such a high heat conductive body is also disclosed. Methods of producing such a high heat conductive body and a wiring base substrate are further disclosed.
    Type: Grant
    Filed: February 14, 1994
    Date of Patent: August 13, 1996
    Assignee: NGK Spark Plug Co., Ltd.
    Inventors: Kouki Ogawa, Kozo Yamasaki, Naomiki Kato
  • Patent number: 5538926
    Abstract: A mixed powder containing: 5-30 wt % of SiC whiskers; 3-30 wt % of a sintering auxiliary agent composed of one kind or more of oxides of Mg, Si, Ca, Ti, Zr, Cr, Ni, Y and rare earth elements; and an Al.sub.2 O.sub.3 powder as a base material; or further containing 0.5-40 wt % of one kind or more of compounds composed of one kind or more of transient elements in the groups IVa, Va, and VIa of the periodic table and one kind or more of C, N and B, are compacted and subjected to pressureless-sintering in a nitrogen containing inert gas atmosphere at a temperature between 1500.degree. and 1900.degree. C. With this method, the SiC whiskers containing Al.sub.2 O.sub.3 based ceramic material, which is densified and has a sufficient strength and toughness, can be formed in a complex shape and a large size.
    Type: Grant
    Filed: December 20, 1994
    Date of Patent: July 23, 1996
    Assignee: Kabushiki Kaisha Seiko Sho
    Inventors: Takehiro Tsuchida, Tsuneo Tatsuno, Moriyoshi Kanamaru
  • Patent number: 5536686
    Abstract: A binder for binding reinforcement materials is provided in which an aluminum and/or Group IIa-containing compound is combined, in a liquid, with a phosphorus-containing compound wherein said binder has a ratio of phosphorus to aluminum and/or Group IIa ions of 14 to 34, preferably 20 to 30. The binder is useful in binding reinforcement materials, particularly suited for preparing preforms for making metal matrix composite materials.
    Type: Grant
    Filed: October 20, 1992
    Date of Patent: July 16, 1996
    Assignee: The Research Foundation of State University of New York at Buffalo
    Inventor: Deborah D. L. Chung
  • Patent number: 5534470
    Abstract: This invention is directed to the production of thermally crystallizable glasses which, upon heat treatment in contact with alumina particulates, will form a strong glass-ceramic-bonded composite body, the excellent bonding being attributed to the presence of lithium aluminoborate crystals. The glass-ceramic composition consists essentially, in weight percent, of______________________________________ SiO.sub.2 25-55 MgO 0-12 B.sub.2 O.sub.3 35-65 Li.sub.2 O + MgO 4-16. Li.sub.
    Type: Grant
    Filed: October 27, 1994
    Date of Patent: July 9, 1996
    Assignee: Corning Incorporated
    Inventors: Ronald l. Andrus, John F. MacDowell
  • Patent number: 5527746
    Abstract: An aluminum oxide based sintered body and a method for manufacturing the same are disclosed. The aluminum oxide based sintered body is composed of silicon compounds of from about 5 to about 40 mole %, calculated as a carbide, at least one metal or metal compound of from 0.5 to about 25 mole %, calculated as metals, selected from Ti, Nb, Ta, Cr and Mo, and the remainder of Al.sub.2 O.sub.3, and a molar ratio of the metals with respect to the silicon compounds, calculated as a carbide is about 4 or less.
    Type: Grant
    Filed: April 5, 1995
    Date of Patent: June 18, 1996
    Assignee: NGK Spark Plug Co., Ltd.
    Inventors: Jun Otsuka, Satoshi Iio, Yo Tajima
  • Patent number: 5525561
    Abstract: The invention provides a method of making a magnesium/aluminium spinel compound having the formula Mg.sub.(1+x) Al.sub.(2+y) O.sub.4 in which 0.ltoreq.x.ltoreq.0.2 and 0.ltoreq.y.ltoreq.0.35. Particulate aluminium metal and a magnesium-containing component selected from magnesium oxide and precursors thereof are mixed together and heated to 800.degree.-1150.degree. C. in an oxidising environment to cause oxidation of at least part of the aluminium. Further heating then takes place to a temperature of 1150.degree.-1350.degree. C. in the oxidizing environment to cause aluminium oxide and magnesium oxide in the admixture to react together.
    Type: Grant
    Filed: October 28, 1994
    Date of Patent: June 11, 1996
    Assignee: Programme 3 Patent Holdings
    Inventor: Arnold Van Zyl
  • Patent number: 5523270
    Abstract: The present invention broadly relates to novel complex oxidation reaction products such as perovskite bodies, including shaped complex oxidation reaction products. This invention also includes complex oxidation reaction products which exhibit superconducting properties.
    Type: Grant
    Filed: June 16, 1994
    Date of Patent: June 4, 1996
    Assignee: Lanxide Technology Company, LP
    Inventors: Robert A. Rapp, Andrew W. Urquhart, Alan S. Nagelberg, Marc S. Newkirk
  • Patent number: 5523267
    Abstract: A silicon nitride-silicon carbide composite sintered material which comprises 100 parts by weight of a silicon nitride component containing 92 to 99.5 mol % of silicon nitride including excessive oxygen and 0.5 to 8 mol % of the elements of Group IIIa in the Periodic Table as corresponding oxides thereof and 1 to 100 parts by weight of a silicon carbide component in a dispersed state, wherein the silicon nitride component has an average particle size of 1 .mu.m or less and an average aspect ratio of 2 to 10, and the silicon carbide component has an average particle size of 1 .mu.m or less, moreover, the total amount of Al, Mg, Ca respectively contained in the sintered material as calculated as oxides thereof is 0.5% by weight or less, and a manufacturing method thereof.According to the above-mentioned composite sintered material, it becomes possible to suppress deterioration of strength at 1400.degree. C. and realize excellent creep properties.
    Type: Grant
    Filed: July 18, 1994
    Date of Patent: June 4, 1996
    Assignee: Kyocera Corporation
    Inventors: Kouichi Tanaka, Masaki Terazono, Masahiro Satoh, Masahito Nakanishi, Hideki Uchimura, Shoji Kousaka