Mixture Of Solid Polymers Present During Cell Formation Patents (Class 521/62)
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Patent number: 11961998Abstract: Provided is a method of producing multiple particulates, the method comprising: (a) dispersing multiple primary particles of an anode active material, having a particle size from 2 nm to 20 ?m, and particles of a polymer foam material, having a particle size from 50 nm to 20 ?m, and an optional adhesive or binder in a liquid medium to form a slurry; and (b) shaping the slurry and removing the liquid medium to form the multiple particulates having a diameter from 100 nm to 50 ?m; wherein at least one of the multiple particulates comprises a polymer foam material having pores and a single or a plurality of the primary particles embedded in or in contact with the polymer foam material, wherein the primary particles have a total solid volume Va, and the pores have a total pore volume Vp, and the volume ratio Vp/Va is from 0.1/1.0 to 10/1.Type: GrantFiled: May 6, 2019Date of Patent: April 16, 2024Assignee: Honeycomb Battery CompanyInventors: Yi-Jun Lin, Yen-Po Lin, Sheng-Yi Lu, Bor Z. Jang
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Patent number: 11637311Abstract: A separator, a method of manufacturing the same, and a lithium secondary battery including the same are disclosed herein. In some embodiments, a separator includes a non-crosslinked polyolefin layer; and a crosslinked polyolefin layer disposed on one surface of the non-crosslinked polyolefin layer and having at least one crosslinking bond represented by the following Chemical Formula 1, wherein the separator is configured such that the non-crosslinked polyolefin layer of the separator faces a positive electrode. In some embodiments, a lithium secondary battery includes a positive electrode, a negative electrode and the separator interposed between the positive electrode and the negative electrode. The lithium secondary battery has a high melt-down temperature and shows high oxidation stability under high-voltage/high-temperature environment.Type: GrantFiled: January 31, 2019Date of Patent: April 25, 2023Inventor: Joo-Sung Lee
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Patent number: 10517372Abstract: A wiper assembly includes a non-porous base configured for attachment to an open end of a container body and a porous wiper overmolded onto the base that is configured to wipe formulation from an applicator when removed from the container body. A wiper assembly includes a collar configured to be positioned within an open end of a container body. The collar includes a substantially cylindrical shaped base portion having a top opening and a substantially dome-shaped secondary wiper portion extending from the base portion that has a bottom opening defining at least one secondary wiper edge. A sponge is configured to be disposed beneath the secondary wiper portion of the collar that has an opening in substantial axial alignment with the top and bottom openings of the collar.Type: GrantFiled: August 31, 2017Date of Patent: December 31, 2019Assignee: L'OrealInventor: Christopher Tarling
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Patent number: 10463131Abstract: A cosmetic device and related methods of manufacturing and using a cosmetic device. The device may comprise a porous part formed using a soluble filler and a non-porous part molded to the porous part.Type: GrantFiled: July 31, 2018Date of Patent: November 5, 2019Assignee: INOAC PACKAGING GROUP, INC.Inventor: Yutaka Matsui
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Patent number: 10259907Abstract: The present invention relates to a novel block copolymer of structure 1, wherein, A- is a block polymer chain, B is a block polymer chain, wherein, A- and B- are chemically different, covalently connected polymer chains, which are phase separable and the moiety X(Y(Z)b)a is a junction group, which comprises a surface active pendant moiety Y(Z)b wherein: a is an integer from 1 to 4 denoting the number of surface active pendant moieties Y(Z)b on X, b is an integer from 1 to 5 denoting the number of Z moieties on the linking moiety Y, X is a linking group between the A polymer block, the B polymer block and the moiety Y, Y is a linking group or a direct valence bond between X and Z; and Z is a moiety independently selected from, a fluorine containing moiety, a Si1-Si8 siloxane containing moiety or a hydrocarbon moiety with at least 18 carbons, and further wherein the junction group X(Y(Z)b)a has a surface energy less than that that of the block A and less than that of the block B.Type: GrantFiled: February 20, 2015Date of Patent: April 16, 2019Assignees: AZ Electronic Materials (Luxembourg) S.à r.l., IBM CorporationInventors: Ankit Vora, Eri Hirahara, Joy Cheng, Durairaj Baskaran, Orest Polishchuk, Melia Tjio, Margareta Paunescu, Daniel Sanders, Guanyang Lin
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Patent number: 9598545Abstract: A process includes casting a solution including poly(phenylene oxide), inorganic nanoparticles, a solvent, and a non-solvent on a substrate; and removing the solvent to form a porous film; wherein: the porous film is configured for use as a porous separator for a lithium ion battery.Type: GrantFiled: January 31, 2013Date of Patent: March 21, 2017Assignee: UCHICAGO ARGONNE, LLCInventors: Zhengcheng Zhang, Jung-Je Woo, Khalil Amine
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Patent number: 9441147Abstract: The present invention relates to methods and compositions useful for isolating a portion of a wellbore. In one embodiment, a method includes preparing a sealant composition containing two phases. The sealant composition is placed into the wellbore where one phase sets upon subjecting the sealant composition to a thermal source followed by the setting of the other phase.Type: GrantFiled: July 9, 2010Date of Patent: September 13, 2016Assignee: Halliburton Energy Services, Inc.Inventors: Natasha Shirshova, Alexander Bismarck, Angelika Menner, Gary Funkhouser
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Patent number: 9259848Abstract: Methods are disclosed that include forming selected perforation designs and patterns in web substrates. The perforation designs and patterns can be formed in linear or nonlinear fashion, can extend in the cross direction or the machine direction and can be formed to complement or match an embossed or printed design on the web. The perforation designs and patterns can be formed utilizing various mechanical perforating techniques.Type: GrantFiled: June 21, 2010Date of Patent: February 16, 2016Assignee: The Procter & Gamble CompanyInventors: Matthew Todd Hupp, James Michael Singer
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Patent number: 9120249Abstract: Medical implant devices are prepared from a polymeric material and a release agent, where the device is a molded, reservoir implant, and the release agent has a molecular weight (MW) of at least 1000. The release agent may be a non-ionic surfactant such as Brij 35, polyoxyetheylene(20)sorbitan trioleate, Tween 20, Tween 80, vitamin E TPGS, and a mixture of any two or more thereof. Hydrated implants may have a surface area of about 500 mm2 or greater.Type: GrantFiled: April 25, 2008Date of Patent: September 1, 2015Assignee: ENDO PHARMACEUTICALS SOLUTIONS INC.Inventors: Petr Kuzma, Stephanie Decker, Harry Quandt
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Patent number: 9102771Abstract: A method is disclosed for producing a water-absorbent resin by a reversed-phase suspension polymerization method, wherein an odor originating from a raw material component, in particular, a petroleum hydrocarbon dispersion medium, is further reduced as compared with a water-absorbent resin obtained by a conventional method, and a water-absorbent resin obtained by the method. More specifically, a method is disclosed for producing a water-absorbent resin by performing a reversed-phase suspension polymerization of a water-soluble ethylenically unsaturated monomer in a petroleum hydrocarbon dispersion medium, comprising adding and dispersing an aqueous solution of a water-soluble ethylenically unsaturated monomer containing a hydrophilic polymeric dispersion agent to a petroleum hydrocarbon dispersion medium in the presence of a surfactant under stirring, and performing a reversed-phase suspension polymerization using a radical polymerization initiator, and a water-absorbent resin obtained by the method.Type: GrantFiled: July 20, 2011Date of Patent: August 11, 2015Assignee: SUMITOMO SEIKA CHEMICALS CO., LTD.Inventors: Hideki Yokoyama, Atsushi Heguri, Nobuhiro Maeda
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Patent number: 9096746Abstract: There are provided a polyolefin resin composition having excellent mechanical properties and thermal resistance; a film formed of the polyolefin resin composition, which has excellent mechanical properties and thermal resistance and which is less likely to suffer from fisheyes; a microporous membrane having excellent permeability and shutdown properties in addition to the above-mentioned physical properties; and applications thereof. Such objects are accomplished by a polyolefin resin composition containing an ultra-high molecular weight ethylene polymer (A), a 4-methyl-1-pentene polymer or 3-methyl-1-pentene polymer (B), and a polymer of an olefin having 2 to 12 carbon atoms (C) at an intended ratio.Type: GrantFiled: August 29, 2012Date of Patent: August 4, 2015Assignee: MITSUI CHEMICALS, INC.Inventors: Nobuhisa Mikawa, Motoyasu Yasui, Akiyoshi Taguchi, Kazuto Sugiyama, Yasuhiro Kai, Kenji Sugimura
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Patent number: 9090018Abstract: A crosslaminate is formed from two oriented plies of thermoplastic polymer material, arranged so that their orientation directions cross one another, the plies being heat sealed together. Each ply is semi-fibrillated, that is consist of linear thin regions of biaxially oriented material and thicker linear bosses between the thinner regions. The webs are sealed primarily through bonds formed at the intersection of the bosses (thicker regions). The array of bosses has a division less than 2 mm. The laminate has improved aesthetic and strength properties. A method for forming the crosslaminate involves segmental stretching of the material to form the thinner regions, and apparatus comprising intermeshing grooved stretching rollers having sharp-edged crests is described.Type: GrantFiled: June 13, 2012Date of Patent: July 28, 2015Assignee: The Glad Products CompanyInventor: Ole-Bendt Rasmussen
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Patent number: 8980964Abstract: A film that is formed from a thermoplastic composition is provided. The thermoplastic composition contains a rigid renewable polyester and a polymeric toughening additive. The toughening additive can be dispersed as discrete physical domains within a continuous matrix of the renewable polyester. An increase in deformation force and elongational strain causes debonding to occur in the renewable polyester matrix at those areas located adjacent to the discrete domains. This can result in the formation of a plurality of voids adjacent to the discrete domains that can help to dissipate energy under load and increase tensile elongation. To even further increase the ability of the film to dissipate energy in this manner, the present inventors have discovered that an interphase modifier may be employed that reduces the degree of friction between the toughening additive and renewable polyester and thus reduces the stiffness (tensile modulus) of the film.Type: GrantFiled: February 10, 2012Date of Patent: March 17, 2015Assignee: Kimberly-Clark Worldwide, Inc.Inventors: Vasily A. Topolkaraev, Ryan J. McEneany, Neil T. Scholl, Thomas A. Eby
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Patent number: 8975305Abstract: A thermoplastic composition that contains a rigid renewable polyester and a polymeric toughening additive is provided. The toughening additive can be dispersed as discrete physical domains within a continuous matrix of the renewable polyester. An increase in the deformation force and elongational strain causes debonding to occur in the renewable polyester matrix at those areas located adjacent to the discrete domains. This can result in the formation of a plurality of voids adjacent to the discrete domains that can help to dissipate energy under load and increase impact strength. To even further increase the ability of the composition to dissipate energy in this manner, an interphase modifier may be employed that reduces the degree of friction between the toughening additive and renewable polyester and thus enhances the degree and uniformity of debonding.Type: GrantFiled: February 10, 2012Date of Patent: March 10, 2015Assignee: Kimberly-Clark Worldwide, Inc.Inventors: Vasily A. Topolkaraev, Neil T. Scholl, Ryan J. McEneany, Thomas A. Eby
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Publication number: 20150056492Abstract: A cross-linkable polyolefin composition (polyethylene, polypropylene or an ethylene-propylene copolymer) is coextruded with ultrahigh molecular weight polyethylene to form two-layer separator membranes, or three-layer separator membranes, for lithium-ion battery cells. In three-layer separator membranes, the cross-linkable polyolefin is formed as the outer faces of the separator for placement against facing surfaces of cell electrodes. The polymer materials initially contain plasticizer oil, which is removed from the extruded membranes, and the extruded membranes are also stretched to obtain a suitable open pore structure in the layered membranes to provide for suitable infiltration with a liquid electrolyte. The cross-linked polyolefin layer provides strength at elevated temperatures and the lower-melting, ultrahigh molecular weight polyethylene layer provides the separator membrane with a thermal shutdown capability.Type: ApplicationFiled: August 21, 2013Publication date: February 26, 2015Applicant: GM GLOBAL TECHNOLOGY OPERATIONS LLCInventor: XIAOSONG HUANG
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Patent number: 8916619Abstract: A porosity is freely controlled in preparation of a porous polymer film by a phase separation method. A solvent absorption sheet is used for a solvent in a polymer solution so that the coating film of the polymer solution may be covered with the sheet. After that, the solvent in the film is selectively removed. Then, the resultant is immersed in a poor solvent. Thus, a porous polymer film can be produced.Type: GrantFiled: June 16, 2010Date of Patent: December 23, 2014Assignee: Canon Kabushiki KaishaInventors: Naotake Sato, Toshihiro Kikuchi, Yuichi Hashimoto, Yohei Miyauchi
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Publication number: 20140357743Abstract: A method is presented for forming a collapsed foam film-like structure, the method including positioning a composition applicator adjacent to a hot non-permeable dryer surface, producing a first frothed dispersion or frothed solution from a first dispersion or solution, applying the first frothed dispersion or frothed solution to the dryer surface, allowing the first frothed dispersion or frothed solution to convert to a collapsed foam film-like structure, and scraping the collapsed foam film-like structure from the dryer surface. The method can further include producing a second dispersion or solution, blending the first dispersion or solution and the second dispersion or solution, frothing the blended dispersion or solution, applying the blended frothed dispersion or frothed solution to the dryer surface, and allowing the frothed dispersion or frothed solution to convert to a collapsed foam film-like structure.Type: ApplicationFiled: May 30, 2013Publication date: December 4, 2014Applicant: Kimberly-Clark Worldwide, Inc.Inventors: Keyur Desai, Jian Qin, Jeffrey Frank Jurena, Frank Paul Abuto, Susan Elaine Shawver, Donald Eugene Waldroup, Deborah Joy Calewarts
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Publication number: 20140243439Abstract: Techniques, mixtures and improved porous materials (interconnected porous constructs) that are capable of maintaining a sufficient porosity while conferring improved mechanical and physical strength to the final construct. A sacrificial construct (for example, a sacrificial material such as polymethyl methacrylate (PMMA)) is used to obtain an inverse porosity of the construct it was molded into. The process provides a less porous end material that may be used as an arthroplasty device or surgical implant (for example, an interference screw of suture anchor) among many other applications. The process employs a sacrificial material to reduce the porosity of the final construct to about 35%.Type: ApplicationFiled: January 10, 2014Publication date: August 28, 2014Applicant: Arthrex, Inc.Inventors: Christopher G. Papangelou, G. Joshua Karnes
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Publication number: 20140154491Abstract: Described herein are foam-like materials having substantially the same physical structure of polyurethane foams but with properties that can be tailored for a particular application. Methods of forming these foam-like materials are also described.Type: ApplicationFiled: February 6, 2014Publication date: June 5, 2014Applicant: ALLERGAN, INC.Inventors: Alexei Goraltchouk, Jordan Thompson, Miriam M. Abiad, Kevin Ma, Dennis Van Epps, Nicholas J. Manesis
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Publication number: 20140148523Abstract: Porous particles can be prepared using an evaporative limited coalescence process in which one or more discrete cavities are stabilized within the continuous polymeric solid phase of the porous particles. The one or more discrete cavities have inner walls and are dispersed within the continuous polymeric solid phase. The porous particles further comprise a cavity stabilizing hydrocolloid on the inner walls of the one or more discrete cavities, and an amphiphilic (low HLB) block copolymer that is disposed at the interface of the discrete cavities and the continuous polymeric solid phase.Type: ApplicationFiled: November 28, 2012Publication date: May 29, 2014Inventors: Mridula Nair, Tamara K. Jones, Mark R. Mis
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Patent number: 8722749Abstract: A method for producing foams, such as sponges, from hydrocolloids is described. A solid or semi-solid gel is formed by dissolving polymeric material in an aqueous solvent. The gel formed is allowed to set, and may optionally then be cut into the desired shape. The gel may be frozen to allow formation of ice crystals to act as porogens. Subsequently, the gel is exposed to a radiant energy field for drying under vacuum. This causes the solvent to boil and the foam or sponge is formed. Medicinally active ingredients may be included in the process, so that the sponge or foam formed contains the active ingredient dispersed within the structure. The method described provides an alternative to the conventional methods of particulate leaching or freeze drying.Type: GrantFiled: July 29, 2005Date of Patent: May 13, 2014Assignee: Enwave CorporationInventors: Timothy D. Durance, Jaya Sundaram, Mareike Ressing
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Patent number: 8691883Abstract: An aerogel-foam composite includes an open cell foam and an aerogel matrix polymer disposed in the open cell foam. The aerogel-foam composite has compression strength of about 15 megaPascals (MPa) or more. The open cell foam may be a polyurethane foam including a carbonate group (—OC(O)O—).Type: GrantFiled: June 21, 2011Date of Patent: April 8, 2014Assignee: Samsung Electronics Co., Ltd.Inventors: Myung-Dong Cho, Sang-Ho Park, Kwang-Hee Kim, Sung-Woo Hwang
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Patent number: 8629193Abstract: Thin porous moldings of silicone copolymers, suitable for use as membranes in separation processes, are prepared by forming a solution or suspension of silicone copolymer in two solvents L1 and L2, casting the suspension or solution, and removing solvent L1 to form a silicone copolymer rich phase A, effecting structure formation, and then removing solvent L2 and residues of solvent L2 to form a thin porous molding.Type: GrantFiled: January 19, 2011Date of Patent: January 14, 2014Assignee: Wacker Chemie AGInventors: Manfred Hoelzl, Frauke Kirschbaum, Robert Maurer, Juergen Pfeiffer, Konrad Alfons Wierer
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Patent number: 8603681Abstract: The present invention relates to a novel porous film material which comprises at least one carbonaceous semimetal oxide phase, and to a process for production thereof. The invention also relates to the use of these porous film materials as a separator layer or for production of such separator layers in electrochemical cells, particularly in lithium cells and especially in lithium secondary cells.Type: GrantFiled: June 28, 2010Date of Patent: December 10, 2013Assignee: BASF SEInventors: Nicole Hildebrandt, Arno Lange, Klaus Leitner, Phillip Hanefeld, Claudia Staudt
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Patent number: 8569062Abstract: The present invention relates to a cryogel which contains a polyol selected from polyvinyl alcohol or galactomannan and a co-polymer of Formula I: The cryogel is formed by mixing the monomers of the co-polymer of Formula I at a temperature of less about 5 degrees C. with the polyol and a free radical initiator in an aqueous solution and polymerizing the solution to form the cryogel. The cryogel is used for culturing cells and can be decomposed by contact with a monosaccharide.Type: GrantFiled: August 8, 2011Date of Patent: October 29, 2013Assignee: Indian Institute of Technology KanpurInventor: Ashok Kumar
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Patent number: 8563620Abstract: The process for the synthesis of a silica monolith comprises the following steps: hydrolysis of a silicon alkoxide in order to form a hydrolysis precursor followed by a condensation of said hydrolysis precursor in the presence of an organic solvent, in the presence of water and of a basic catalyst in order to form oligomeric clusters containing several silicon atoms; dispersion of said oligomeric clusters in a solution in order to form a sol; polymerization of the sol in order to obtain a gel via a first heat treatment, at a temperature below the boiling point of the constituents of the sol; drying of the gel via a second heat treatment; conversion of the gel to a xerogel via a third heat treatment; dehydration and densification of the xerogel until the silica monolith is obtained via a fourth heat treatment.Type: GrantFiled: October 1, 2009Date of Patent: October 22, 2013Assignees: Universite des Sciences et Technologies de Lille, Centre National de la Recherche Scientifique (CNRS)Inventors: Mohamed Bouazaoui, Bruno Capoen, Hicham El-Hamzaoui, Laurent Bigot, Géraud Bouwmans
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Patent number: 8552076Abstract: Disclosed herein is a method of preparing a fused aerogel-polymer composite in which aerogel and an organic polymer is mixed in a dry state to adsorb polymer particles on the surface of the aerogel and are then subjected to thermal treatment, thus forming a polymer coating on the aerogel. The fused aerogel-polymer composite can be used for thermal insulation in a variety of applications. The fused aerogel-polymer composite exhibits high thermal insulation properties and superior physical strength and processability while still maintaining the properties of an aerogel that does not have a polymer coated on its surface.Type: GrantFiled: April 10, 2008Date of Patent: October 8, 2013Assignee: Samsung Electronics Co., Ltd.Inventor: Myung Dong Cho
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Patent number: 8487013Abstract: The present invention relates to a method for producing a porous resin particle containing an aromatic vinyl compound-aromatic divinyl compound copolymer having a hydroxyl group, the method including: dissolving a monomer mixture containing an aromatic vinyl compound, an aromatic divinyl compound and a (meth)acrylic acid ester having one hydroxyl group within the molecule thereof, and a polymerization initiator in an organic solvent to obtain a solution containing the monomer mixture and the polymerization initiator; suspending the solution in water in the presence of a dispersion stabilizer; and performing a suspension copolymerization. The method of the invention is capable of easily producing a porous resin particle containing an aromatic vinyl compound-aromatic divinyl compound copolymer having a hydroxyl group, that is used as a support for solid phase synthesis and enables efficient nucleic acid synthesis.Type: GrantFiled: November 5, 2008Date of Patent: July 16, 2013Assignee: Nitto Denko CorporationInventors: Kenjiro Mori, Tatsuya Konishi
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Patent number: 8487012Abstract: Described herein are open celled foams including a matrix of interconnected spheres. Also described herein are methods of making open celled foams as well as making composite members with open celled foam coatings covering at least a portion of the composite member. The open celled foams described herein are silicone based materials and can be used to coat implants such as breast implants and function to encourage tissue ingrowth and reduce capsular formation.Type: GrantFiled: January 25, 2011Date of Patent: July 16, 2013Assignee: Allergan, Inc.Inventors: Alexei Goraltchouk, Jordan M. Thompson, Dennis E. Van Epps
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Patent number: 8420704Abstract: A process for preparing a polymer composite that includes reacting (a) a multi-functional monomer and (b) a block copolymer comprising (i) a first block and (ii) a second block that includes a functional group capable of reacting with the multi-functional monomer, to form a crosslinked, nano-structured, bi-continuous composite. The composite includes a continuous matrix phase and a second continuous phase comprising the first block of the block copolymer.Type: GrantFiled: July 18, 2008Date of Patent: April 16, 2013Assignee: Regents of the University of MinnesotaInventors: Marc Hillmyer, Liang Chen
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Patent number: 8389589Abstract: A nanoporous material exhibiting a lamellar structure is disclosed. The material comprises three or more substantially parallel sheets of an organosilicate material, separated by highly porous spacer regions. The distance between the centers of the sheets lies between 1 nm and 50 nm. The highly porous spacer regions may be substantially free of condensed material. For the manufacture of such materials, a process is disclosed in which matrix non-amphiphilic polymeric material and templating polymeric material are dispersed in a solvent, where the templating polymeric material includes a polymeric amphiphilic material. The solvent with the polymeric materials is distributed onto a substrate. Organization is induced in the templating polymeric material. The solvent is removed, leaving the polymeric materials in place. The matrix polymeric material is cured, forming a lamellar structure.Type: GrantFiled: December 18, 2008Date of Patent: March 5, 2013Assignee: International Business Machines CorporationInventors: Jennifer Nam Cha, Geraud Jean-Michel Dubois, James Lupton Hedrick, Ho-Cheol Kim, Victor Yee-Way Lee, Teddie Peregrino Magbitang, Robert Dennis Miller, Willi Volksen
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Publication number: 20130011744Abstract: The present invention relates to a method for producing a film containing a thermoplastic resin, the method comprising: a step of feeding a material containing a thermoplastic resin and having a pair of opposed flat portions to between a pair of rollers with the thermoplastic resin in a molten state, and a step of rolling, with the pair of rollers, the pair of flat portions being stacked, thereby welding the flat portions to each other to form a united film, wherein the material to be fed to between the rollers is two separate films each having a flat portion or one flat cylindrical film having a pair of opposed flat portions linked together by connecting portions at their end portions.Type: ApplicationFiled: March 29, 2011Publication date: January 10, 2013Applicant: SUMITOMO CHEMICAL COMPANY, LIMITEDInventors: Atsuhiro Takata, Toshihiko Suzuki, Takanari Yamaguchi
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Publication number: 20120252912Abstract: A process for producing a microporous polymeric object to improve the degree of freedom for its various properties, compared to conventional processes, includes: mixing a block copolymer made of three or more kinds of segments with a polymer, wherein one or more of the segments are made of monomer units having a first functional group forming ionic and/or hydrogen bond, the segments constitute a co-continuous structure having mutually-independent and continuous regions due to a phase separation based on incompatibility between the segments, and the polymer has, at other than polymer chain terminals, a second functional group forming such bond with the first functional group, thereby allowing the segments to associate with the polymer at many points; forming a co-continuous structure including a region composed of the polymer and the segments due to the phase separation; and removing the polymer from the region by weakening the bond between the functional groups.Type: ApplicationFiled: May 8, 2012Publication date: October 4, 2012Applicant: NITTO DENKO CORPORATIONInventors: Takahisa KONISHI, Takuji SHINTANI, Yushu MATSUSHITA, Atsushi TAKANO, Takeshi ASARI
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Publication number: 20120238652Abstract: The present invention provides a method for producing stereo complex crystals of polylactic acid, with which a polylactic acid having excellent heat resistance and containing stereo complex crystals at a high ratio can be efficiently produced, the method including: a step of dissolving in a solvent a block copolymer, which includes polylactic acid containing an L-lactic acid unit or poly lactic acid containing a D-lactic acid unit together with at least one kind of an organic polymer having a different structure from that of polylactic acid, and a polylactic acid homopolymer containing a D-lactic acid unit or a polylactic acid homopolymer containing an L-lactic acid unit, the lactic acid unit being an optical isomer that is not contained in the block copolymer, to prepare a polymer mixture solution; and a step of removing the solvent from the polymer mixture solution.Type: ApplicationFiled: September 7, 2010Publication date: September 20, 2012Applicant: National University Corporation Gunma UniversityInventors: Hiroki Uehara, Takeshi Yamanobe, Yusuka Karaki
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Publication number: 20120095121Abstract: Disclosed is a hydrophilic polyolefin sintered material which is a water-absorbing sintered material of a polyolefin resin ice having a graft chain composed of at least one molecular chain selected from hydrophilic ethylenically unsaturated group-containing monomers and their polymers. This hydrophilic polyolefin sintered material has an average porosity of 20-80% by volume and an open cell having an average pore diameter of 1-150 ?m.Type: ApplicationFiled: July 24, 2008Publication date: April 19, 2012Inventors: Naoki Matsuoka, Minoru Yamamoto, Shigeru Nakajima, Takahiro Deguchi
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Publication number: 20120065283Abstract: A composition for the manufacture of a porous, compressible article, the composition comprising a combination of: a plurality of reinforcing fibers; a plurality of polyimide fibers; and a plurality of polymeric binder fibers; wherein the polymeric binder fibers have a melting point lower than the polyimide fibers; methods for forming the porous, compressible article; and articles containing the porous, compressible article. An article comprising a thermoformed dual matrix composite is also disclosed, wherein the composite exhibits a time to peak release, as measured by FAR 25.853 (OSU test), a 2 minute total heat release, as measured by FAR 25.853 (OSU test), and an NBS optical smoke density of less than 200 at 4 minutes, determined in accordance with ASTM E-662 (FAR/JAR 25.853).Type: ApplicationFiled: September 14, 2011Publication date: March 15, 2012Applicant: SABIC INNOVATIVE PLASTICS IP B.V.Inventors: Thomas ADJEI, Benny Ezekiel DAVID, Dennis LOCKYER, Craig MILNE, Erich Otto TEUTSCH
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Patent number: 8097274Abstract: Provided herein are skin substitutes suitable for use in a living subject for purpose of repairing damaged tissues, methods of producing the skin substitutes and their uses. A biocomposite membrane comprising poly(?-caprolactone) (PCL) and at least one material selected from collagen and gelatin is provided. In one embodiment, the biocomposite is a 2-component membrane of PCL and gelatin. In another embodiment, the biocomposite is a 3-component membrane of PCL, collagen and gelatin. The bio-composite membrane may be used directly in vivo as a wound dressing, or as a support for cell growth on each side of the membrane to produce an in vitro cultivated artificial skin for future in vivo and/or in vitro applications.Type: GrantFiled: October 27, 2006Date of Patent: January 17, 2012Assignee: National Defense Medical CenterInventors: Allan Gerald Arthur Coombes, Eric Frank Adams, Niann-Tzyy Dai, Tsung-Hsun Liu, Ming-Kung Yeh
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Patent number: 8080590Abstract: A porous polymeric matrix containing at least one natural polymer and at least one synthetic polymer and optionally at least one cation. Furthermore, a method of making a porous polymeric matrix involving mixing at least one natural polymer and inorganic salts with a solution comprising at least one solvent and at least one synthetic polymer to form a slurry, casting the slurry in a mold and removing the solvent to form solid matrices, immersing the solid matrices in deionized water to allow natural polymer cross-linking and pore creation to occur simultaneously, and drying the matrices to create a porous polymeric matrix; wherein the matrix contains a cation.Type: GrantFiled: June 9, 2008Date of Patent: December 20, 2011Assignee: The United States of America as represented by the Secretary of AgricultureInventors: LinShu Liu, Marshall L. Fishman, Kevin B. Hicks
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Patent number: 8076383Abstract: The present invention relates to a method for producing a porous resin particle having a functional group X, the method including: dissolving a radical polymerizable aromatic monovinyl monomer and a radical polymerizable aromatic divinyl monomer together with a polymerization initiator in an organic solvent to prepare a monomer solution, dispersing the monomer solution in water in the presence of a dispersion stabilizer to obtain a suspension polymerization reaction mixture, and performing a suspension copolymerization while adding, when 0 to 80% of the entire polymerization time of the suspension copolymerization is passed, a mercapto compound represented by the formula (I): HS—R—X??(I) in which R represents an alkylene group having a carbon number of 2 to 12, and the functional group X represents a functional group selected from a hydroxy group and a primary amino group, to the suspension polymerization reaction mixture; and the porous resin particle obtained by the method.Type: GrantFiled: November 5, 2008Date of Patent: December 13, 2011Assignee: Nitto Denko CorporationInventors: Tatsuya Konishi, Kenjiro Mori
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Publication number: 20110276133Abstract: The present specification discloses porous materials, methods of forming such porous materials, biocompatible implantable devices comprising such porous materials, and methods of making such biocompatible implantable devices.Type: ApplicationFiled: May 10, 2011Publication date: November 10, 2011Applicant: Allergan, Inc.Inventors: Futian Liu, Nicholas J. Manesis, Alexei Goraltchouk, Dimitrios Stroumpoulis
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Publication number: 20110207840Abstract: The present invention provides a polyolefin resin composition which is excellent in mechanical properties and dimensional stability and is particularly excellent in heat resistance, a film which is excellent in mechanical properties, dimensional stability and heat resistance because it is obtained from the polyolefin resin composition and which is particularly excellent in meltdown properties, a macroporous membrane which is excellent in permeability and shutdown properties in addition to the above properties, and uses thereof. The polyolefin resin composition of the present invention (C) comprises 85 to 50% by mass of ultrahigh-molecular weight polyethylene (A) having a specific intrinsic viscosity and 15 to 50% by mass of a polymer (B) containing a repeating unit derived from 4-methyl-1-pentene, in 100% by mass of the polyolefin resin composition (C).Type: ApplicationFiled: November 18, 2009Publication date: August 25, 2011Applicant: Mitsui Chemicals, Inc.Inventors: Shota Abe, Atsushi Morita, Kazuto Sugiyama, Mineo Kubo
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Publication number: 20110165308Abstract: A porous membrane with the membrane wall constructed of a hydrophobic polymer and a hydrophilic polymer, wherein when the membrane wall is divided into 3 sections in the film thickness direction to form region “a” containing one wall surface A of the membrane wall, region “c” containing the other wall surface C and region “b” between region “a” and region “c”, the hydrophilic polymer content ratio Ca in region “a” is greater than the hydrophilic polymer content ratio Cc in region “c”, and the mean pore size of the wall surface C is larger than the mean pore size of the wall surface A.Type: ApplicationFiled: September 24, 2009Publication date: July 7, 2011Applicant: ASAHI KASEI CHEMICALS CORPORATIONInventor: Satoshi Shiki
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HOLLOW BIODEGRADABLE NANOSPHERES AND NANOSHELLS FOR DELIVERY OF THERAPEUTIC AND/OR IMAGING MOLECULES
Publication number: 20110123456Abstract: A polymeric hollow nanoshell or nanosphere for release of an agent is described, wherein the hollow nanosphere comprises at least one biodegradable polymer, characterised in that the polymer is cross-linked. The biodegradable mono-disperse nanospheres described are suitable for use as carriers of biomolecules, therapeutic agents and/or imaging agents.Type: ApplicationFiled: September 20, 2010Publication date: May 26, 2011Inventors: Abhay Pandit, Gildas Rethore, Hemantkumar Naik, Yvonne Lang, David Finn -
Patent number: 7947752Abstract: Disclosed is a microporous high density polyethylene film for a battery separator and a method of producing the same. The microporous high density polyethylene film includes high density polyethylene with a weight average molecular weight of 2×105-5×105, containing 5 wt % or less molecule with a molecular weight of 1×104 or less. The microporous high density polyethylene film has tensile strengths of 1,100 kg/cm2 or more in transverse and machine directions respectively, a puncture strength of 0.22 N/?m or more, a gas permeability (Darcy's permeability constant) of 1.3×10?5 Darcy or more, and shrinkages of 5% or less in machine and transverse directions, respectively. Particularly, the microporous high density polyethylene film has an excellent extrusion-compoundabiliy and stretchability and a high productivity, and can improve the performances and stability of a battery produced using the same.Type: GrantFiled: February 12, 2008Date of Patent: May 24, 2011Assignee: SK Energy Co., Ltd.Inventors: Young Keun Lee, Jang Weon Rhee, Won Young Cho, Jung Moon Sung, Byoung Cheon Jo, Chol Ho Lee, In Hwa Jung, Byung Rae Jung
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Publication number: 20110091706Abstract: Porous infusible polymer (IP) parts are made by incorporating 0.2 to 10 volume percent organic fibers, preferably with short lengths, into the particulate IP, consolidating the mixture under pressure and optionally heating, and then “burning off” the fibers. After the fibers are burned off the resulting part has porosity in which the pores are elongated, usually retaining the shape of the organic fibers. When these parts are exposed to moisture (which they usually absorb) and then suddenly heated they tend not to blister from vaporization of the water. This makes them useful as parts for aircraft (jet) and other engines and other applications where sudden temperature increase may occur.Type: ApplicationFiled: December 21, 2010Publication date: April 21, 2011Applicant: E. I. DU PONT DE NEMOURS AND COMPANYInventor: Thomas P. Gannett
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Patent number: 7887727Abstract: The present invention relates to a process for manufacturing a microporous polyolefin film which can be used for various battery separators, separating filters and membranes for microfiltration. The process for manufacturing a microporous polyolefin film according to the invention comprises mixing/extrusion through efficient and separate injection of 15-55% by weight of polyolefin (Component I), and 85-45% by weight of a diluent (Component II) which forms thermodynamic single phase with the polyolefin and a diluent (Component III) which can undergo thermodynamic liquid-liquid phase separation with the polyolefin, into an extruder.Type: GrantFiled: December 12, 2007Date of Patent: February 15, 2011Assignee: SK Energy Co., Ltd.Inventors: Young-keun Lee, Jang-weon Rhee, Gwi-gwon Kang, In-hwa Jung
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Patent number: 7850942Abstract: A method of making mesoporous carbon beads comprises steps of providing a nucleophilic component such as phenolic compound or phenol condensation prepolymer, dissolving the nucleophilic component in a pore former, together with at least one electrophilic cross-linking agent such as formaldehyde, paraformaldehyde, furfural and hexamethylene tetramine, dispersing the resulting solution into a mineral oil to form beads, condensing both the component and the agent in the presence of the pore former to form beads of porous resin, removing the beads from the mineral oil and carbonizing the beads to form mesoporous carbon beads.Type: GrantFiled: May 7, 2007Date of Patent: December 14, 2010Assignee: British American Tobacco (Investments) Ltd.Inventors: Stephen Robert Tennison, Oleksundr Prokopovych Kozynchenko, Volodymyr Vasyljovych Strelko, Andrew John Blackburn
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Patent number: 7838567Abstract: Foams composed of water-absorbing basic polymers, obtainable by (I) foaming a crosslinkable aqueous mixture including (a) at least one basic polymer whose basic groups have optionally been neutralized, (b) at least one crosslinker, (c) at least one surfactant, (d) optionally at least one solubilizer, (e) optionally thickeners, foam stabilizers, fillers, fibers and/or cell nucleators, and (f) optionally particulate water-absorbing acidic polymers, by dissolving a gas which is inert toward free radicals in the crosslinkable aqueous mixture under a pressure from 2 to 400 bar and subsequently decompressing the crosslinkable aqueous mixture to atmospheric or by dispersing fine bubbles of a gas which is inert toward free radicals, and (II) crosslinking the foamed mixture to form a hydrogel foam and if applicable adjusting the water content of the polymer foam to 1-60% by weight.Type: GrantFiled: January 30, 2003Date of Patent: November 23, 2010Assignee: Basf AktiengesellschaftInventors: Samantha Champ, Hans-Joachim Hähnle, Martin Beck, Rüdiger Funk
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Publication number: 20100292077Abstract: A process for preparing a polymer composite that includes reacting (a) a multi-functional monomer and (b) a block copolymer comprising (i) a first block and (ii) a second block that includes a functional group capable of reacting with the multi-functional monomer, to form a crosslinked, nano-structured, bi-continuous composite. The composite includes a continuous matrix phase and a second continuous phase comprising the first block of the block copolymer.Type: ApplicationFiled: July 18, 2008Publication date: November 18, 2010Inventors: Marc Hillmyer, Liang Chen
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Patent number: 7799839Abstract: Disclosed are porous material having hierarchical pore structure and preparation method thereof. A method of synthesizing a nanoporous material having high functionality as a support for bioactive material is combined with a three-dimensional rapid prototyping technique. Thereby, the porous material of the invention has interconnected pores of respective size regions and uneven surface corresponding to each size region, and thus conditions favorable for adhesion, division, proliferation, movement, and differentiation of cells are provided, thereby exhibiting efficient applications in various fields, in addition to bone fillers, restorative materials, and scaffolds.Type: GrantFiled: July 10, 2007Date of Patent: September 21, 2010Assignee: Korea Institute of Machinery & MaterialsInventors: Hui-suk Yun, Seung-Eon Kim