Removing A Liquid To Form A Cellular Product Patents (Class 521/64)
  • Patent number: 11957556
    Abstract: An absorbent structure comprising one or more absorbent layers wherein the absorbent structure exhibits a first cycle Peak Force compression between about 30 grams and about 150 grams. The absorbent structure further exhibits a fifth cycle dry recovery energy between 0.1 mJ and 2.8 mJ.
    Type: Grant
    Filed: April 30, 2020
    Date of Patent: April 16, 2024
    Assignee: The Procter & Gamble Company
    Inventors: Christopher Philip Bewick-Sonntag, Clint Adam Morrow, Wade Monroe Hubbard, Jr.
  • Patent number: 11920304
    Abstract: The present invention describes a method for preparing graphene by mixing graphite and carbon nanofibrils. The prepared graphene can be used to form nanopaper. The present invention also provides a method of preparing nanopaper by suspending cellulose nanofibrils and graphene, followed by vacuum filtering of the suspension.
    Type: Grant
    Filed: October 28, 2019
    Date of Patent: March 5, 2024
    Assignee: The Regents of the University of California
    Inventors: You-Lo Hsieh, Xuezhu Xu
  • Patent number: 11857946
    Abstract: The present disclosure relates to a preparing method of a super absorbent polymer sheet and a super absorbent polymer sheet prepared therefrom. The preparing method of a super absorbent polymer sheet of the present disclosure may prepare a porous flexible super absorbent polymer sheet exhibiting high flexibility and fast absorption rate.
    Type: Grant
    Filed: December 14, 2018
    Date of Patent: January 2, 2024
    Inventors: Kiyoul Yoon, Hyeon Choi, Hyosook Joo, Gicheul Kim, Ju Eun Kim
  • Patent number: 11846645
    Abstract: In a method of measuring parameters of superabsorbents, the absorption capacity of superabsorbents is determined under pressure, by reducing the pressure applied to a sample of the superabsorbent stepwise and determining the absorption capacity at each pressure. In addition, the rise in absorption capacity after a reduction in pressure is measured as a function of time and this is used to calculate the swelling constant k or the characteristic swelling time ?. Swelling constant or characteristic swelling time or the magnitude of the difference in absorption capacity at two different pressures are used to determine further parameters of the superabsorbent.
    Type: Grant
    Filed: June 24, 2020
    Date of Patent: December 19, 2023
    Assignee: BASF SE
    Inventors: Thomas Daniel, Markus Toennessen, Christophe Bauduin
  • Patent number: 11839869
    Abstract: The present disclosure discloses a method of preparing a Ni active site-loaded C—Si aerogel catalyst, and a product and use thereof, belonging to the technical field of catalyst preparation. The method includes the following steps: (1) dissolving absolute ethanol, trimethoxymethylsilane, cetyltrimethylammonium bromide and HCl in deionized water, conducting hydrolysis to obtain a hydrolyzate, followed by adjusting a pH value of the hydrolyzate to 7 to 8.5, and drying to obtain a C—Si aerogel; and (2) in the absolute ethanol, mixing NiCl2.6H2O with the C—Si aerogel obtained in step (1) uniformly, and conducting ultrasonication, impregnation and drying, followed by calcination to obtain the Ni active site-loaded C—Si aerogel catalyst. In the present disclosure, the prepared Ni active site-loaded C—Si aerogel catalyst is capable of conducting catalytic degradation of aromatic volatile organic compounds (VOCs) at room temperature.
    Type: Grant
    Filed: March 21, 2022
    Date of Patent: December 12, 2023
    Assignee: TIANJIN UNIVERSITY
    Inventors: Hui Ding, Dan Zhao, Rui Liu
  • Patent number: 11805821
    Abstract: The present application discloses a method for preparing porous glass for an electronic cigarette, comprising the following steps: heating quartz glass to a molten state for granulation; mixing boron-silicon powder and quartz glass granules, and heating a mixture to a temperature between 600° C. to 900° C. to cover peripheries of the quartz glass granules with the boron-silicon powder; and sintering the quartz glass granules covered with boron-silicon in a preset mold to obtain the porous glass for the electronic cigarette. The technical solution according to the present application can greatly improve the smoking taste of the electronic cigarette.
    Type: Grant
    Filed: December 8, 2021
    Date of Patent: November 7, 2023
    Inventor: Lantian Guo
  • Patent number: 11773189
    Abstract: The present invention relates to citrus pectin characterized by a low degree of methyl esterification yet a high intrinsic viscosity, a process for producing pectin using citrus peel and use of an enzyme endogenous to citrus peel to produce pectin.
    Type: Grant
    Filed: March 18, 2019
    Date of Patent: October 3, 2023
    Assignee: CP KELCO APS
    Inventors: Claus Rolin, Mette Enøe Hansen
  • Patent number: 11760647
    Abstract: Provided is a hydrophobic silica aerogel precursor, and a hydrophobic silica aerogel produced using the same. In the methods, a linear silane crosslinking agent containing a PEG-derived unit is introduced when preparing a hydrophobic aerogel precursor, resulting in the production of a hydrophobic silica aerogel having improved high-temperature thermal stability and improved physical properties.
    Type: Grant
    Filed: December 7, 2018
    Date of Patent: September 19, 2023
    Assignee: LG Chem, Ltd.
    Inventors: Hee Jung Choi, Se Hyun Kwon, Yeong Rae Chang, Seok Hoon Jang
  • Patent number: 11753517
    Abstract: A method for manufacturing a patterned polyimide aerogel film on a substrate includes: dispensing a polyimide prepolymer sol onto a first portion of a surface of a substrate, a second portion of the surface of the substrate being substantially free of the polyimide prepolymer sol; forming a patterned film of a polyimide prepolymer gel on the substrate from the polyimide prepolymer sol; drying the polyimide prepolymer gel to form a patterned film of a polyimide prepolymer aerogel on the substrate; and curing the polyimide prepolymer aerogel on the substrate to form the patterned polyimide aerogel film on the first portion of the surface of the substrate, the second portion of the surface of the substrate being substantially free of the patterned polyimide aerogel film.
    Type: Grant
    Filed: December 12, 2019
    Date of Patent: September 12, 2023
    Assignee: RAYTHEON COMPANY
    Inventor: Thomas A. Hanft
  • Patent number: 11746465
    Abstract: A process of making a synthetic leather includes (i) first, contacting a textile with an aqueous solution containing a cationic hydroxyethylcellulose polymer to form a modified textile component; (ii) subsequently, impregnating the modified textile component with an aqueous polyurethane dispersion externally stabilized with an anionic surfactant; and (iii) precipitating the polyurethane in the modified textile component. And a synthetic leather formed by the process.
    Type: Grant
    Filed: August 21, 2018
    Date of Patent: September 5, 2023
    Assignee: The Dow Chemical Company
    Inventors: Xiangyang Tai, Zhaohui Qu, Ruijun Zhao, Yunlong Guo, Xiaoyi Pang
  • Patent number: 11744784
    Abstract: A series of particles, in which each particle contains at least 3 wt. % of pigment(s) in relation to the weight of the particle, a method for producing the series of particles, and uses thereof in cosmetic compositions, particularly in make-up for keratinous materials.
    Type: Grant
    Filed: March 30, 2018
    Date of Patent: September 5, 2023
    Assignee: CAPSUM
    Inventors: Julie Cani, Cassia Michel, Morgane Forest
  • Patent number: 11730793
    Abstract: Non-aqueous emulsion methods for producing polymeric or polymer-coated microparticles are provided. One method produces a sustained release microparticle composition by combining protein powder and a polymer into a hydrocarbon solvent to form a non-aqueous first solution and adding the first solution to a second solution, wherein the second solution comprises a fluorocarbon liquid and a fluorosurfactant to form a non-aqueous emulsion comprising multiple emulsion hydrocarbon droplets in the fluorocarbon liquid. The subsequent microparticle hardening process includes the steps of removing the hydrocarbon solvent from the formed emulsion droplets, which can be achieved through evaporation the hydrocarbon at ambient condition under stirring, or accelerated hardening through vacuum, or through adding hydrofluoroester into the fluorocarbon as a cosolvent.
    Type: Grant
    Filed: November 25, 2020
    Date of Patent: August 22, 2023
    Assignee: Regeneron Pharmaceuticals, Inc.
    Inventors: Yiming Zhao, Hunter Chen
  • Patent number: 11724006
    Abstract: A method of producing a cryogel-based multicompartment 3D scaffold is herein disclosed. The method comprises the steps of: a) providing a first frozen polymeric layer on a refrigerated support kept at subzero temperature; b) providing subsequent polymeric layers to obtain a stack of polymeric layers by possibly modulating the subzero temperature of the refrigerated support; c) optionally incubating the final polymeric structure at subzero temperature; and d) placing the produced cryogel at a temperature above 0° C., the method being characterized in that each subsequent layer i) is deposited on the previous one after freezing of this latter; ii) is deposited on the previous one before the complete polymerization of this latter; and iii) is deposited with a temperature higher than the freezing temperature of the previously deposited layer. Cryogel scaffolds obtained from the method of the invention are also disclosed.
    Type: Grant
    Filed: January 10, 2018
    Date of Patent: August 15, 2023
    Assignee: École Polytechnique Fédérale de Lausanne (EPFL)
    Inventors: Amélie Barbara Hildegarde Béduer, Thomas Braschler, Philippe Renaud
  • Patent number: 11718716
    Abstract: An aerogel and drying method, the aerogel having a larger size, good productivity, and high transparency. The aerogel has a silsesquioxane structure and exhibits two exothermic peaks observed in a temperature range of 300 to 600° C. as measured by TG-DTA (thermogravimetry-differential thermal analysis) under an inert gas atmosphere containing 80% by volume of an inert gas and 20% by volume of oxygen. A method for producing aerogel includes a drying step including a first step in which an aerogel which has undergone condensation of a hydrolysate is placed in a liquid phase system having a first liquid phase and a second liquid phase; a second step in which a first solvent constituting the first liquid phase is evaporated from the first liquid phase at a temperature greater than room temperature; and a third step in which heating is still continued after the first liquid phase is evaporated off.
    Type: Grant
    Filed: April 6, 2020
    Date of Patent: August 8, 2023
    Assignee: TIEM FACTORY INC.
    Inventors: Noboru Kawase, Mamoru Aizawa
  • Patent number: 11661490
    Abstract: A molded body is produced from a molding material including a continuous phase and a dispersed phase by a three-dimensionalization step, a curing step, and a peeling step. The continuous phase of the molding material is a water phase containing a curable compound. In the three-dimensionalization step, the molding material is placed in a container. In the curing step, the curable compound is cured to form a cured product after the three-dimensionalization step. In the peeling step, the container and the cured product are separated after the curing step. In the dispersed phase removal step, the dispersed phase of the cured product is removed after the curing step.
    Type: Grant
    Filed: July 22, 2020
    Date of Patent: May 30, 2023
    Assignee: FUJIFILM Corporation
    Inventors: Keisuke Oku, Koju Ito, Hiroshi Yabu, Yoshiaki Uchida
  • Patent number: 11639400
    Abstract: An active energy ray curable liquid contains an unsaturated acid monomer and a metal salt.
    Type: Grant
    Filed: August 21, 2019
    Date of Patent: May 2, 2023
    Assignee: Ricoh Company, Ltd.
    Inventors: Takashi Matsumura, Tatsuya Niimi, Takuya Saito
  • Patent number: 11629435
    Abstract: An electrospun nanofiber membrane and a method for preparing the electrospun nanofiber membrane are provided to solve problems of poor mechanical properties, short service life, poor uniformity and consistency of orientation of fibers and poor stability of fiber networks in current electrospun composite nanofiber materials. The electrospun nanofiber membrane is prepared by spinning solution through a high-voltage electrospinning device. The spinning solution is blending solution of regenerated silk fibroin:polyvinyl alcohol:polylactic acid with a mass ratio being 75-85:10-20:5 dissolved in a mixed solvent of trifluoroacetic acid and dichloromethane with a volume ratio being 7:3. The method establishes a reasonable mass ratio parameter of the regenerated silk fibroin, the polyvinyl alcohol and the polylactic acid to blending spinning to improve spinnability of silk fibroin, as well as prepare the electrospun composite nanofiber membrane with good mechanical properties.
    Type: Grant
    Filed: August 29, 2022
    Date of Patent: April 18, 2023
    Assignees: SHAANXI ENVIRONMENTAL PROTECTION RESEARCH INST., SHAANXI RONGNA MATERIAL TECHNOLOGY CO., LTD.
    Inventors: Feng Ji, Min Zhang, Dong Li, Yifan Lei, Qingyi Wang, Jundong Wang, Hongbo Li
  • Patent number: 11629239
    Abstract: Mesoporous poly (aryl ether ketone) articles are formed from blends of poly (aryl ether ketones) with pore forming additives by melt processing, and can be in the form of a monofilament, disc, film, microcapillary or other complex shapes. The method of formation provides for preparation of poly (aryl ether ketone) articles with high degree of surface area and uniform nanometer pore size. The preferred poly (aryl ether ketone)s are poly (ether ketone) and poly (ether ether ketone). The mesoporous articles formed by the method of the present invention are useful for a broad range of applications, including molecular separations and organic solvent filtration.
    Type: Grant
    Filed: October 14, 2022
    Date of Patent: April 18, 2023
    Assignee: Avanpore LLC
    Inventor: Benjamin Bikson
  • Patent number: 11584843
    Abstract: The invention provides an olefin-olefinic alcohol copolymer and a preparation method thereof, said copolymer comprising a spherical and/or spherical-like polymer. The copolymer provided by the invention exhibits a good morphology and has good prospects in industrial use.
    Type: Grant
    Filed: October 24, 2018
    Date of Patent: February 21, 2023
    Assignees: CHINA PETROLEUM & CHEMICAL CORPORATION BEIJING RESEARCH INSTITUTE OF CHEMICAL INDUSTRY, CHINA PETROLEUM & CHEMICAL CORPORATION
    Inventors: Rong Gao, Zifang Guo, Junling Zhou, Dongbing Liu, Jie Fu, Jingjing Lai, Tingjie Huang, Shiyuan Xu, Xinyang Li
  • Patent number: 11563256
    Abstract: A method for producing a microporous material comprising the steps of: providing an ultrahigh molecular weight polyethylene (UHMWPE); providing a filler; providing a processing plasticizer; adding the filler to the UHMWPE in a mixture being in the range of from about 1:9 to about 15:1 filler to UHMWPE by weight; adding the processing plasticizer to the mixture; extruding the mixture to form a sheet from the mixture; calendering the sheet; extracting the processing plasticizer from the sheet to produce a matrix comprising UHMWPE and the filler distributed throughout the matrix; stretching the microporous material in at least one direction to a stretch ratio of at least about 1.5 to produce a stretched microporous matrix; and subsequently calendering the stretched microporous matrix to produce a microporous material which exhibits improved physical and dimensional stability properties over the stretched microporous matrix.
    Type: Grant
    Filed: October 3, 2017
    Date of Patent: January 24, 2023
    Assignee: Celgard, LLC
    Inventors: Eric H. Miller, Joseph G. Yaritz, Mark T. Demeuse, J. Kevin Whear
  • Patent number: 11505662
    Abstract: The invention relates to an elastic membrane comprising an elastomer having an elongation at break of greater than 150% measured according to DIN 53504, wherein the thermoplastic elastomer (P1) comprises a polyurethane elastomer based on the following components: 11 % to 79% by weight of a mixture of at least one diol (D1) and at least one isocyanate (I1), 21% to 89% by weight of at least one compound (C1) having at least two isocyanate-reactive groups.
    Type: Grant
    Filed: October 8, 2018
    Date of Patent: November 22, 2022
    Assignee: BASF SE
    Inventors: Frank Prissok, Juergen Ahlers, Martin Weber, Oliver Gronwald
  • Patent number: 11505671
    Abstract: Mesoporous poly (aryl ether ketone) articles are formed from blends of poly (aryl ether ketones) with pore forming additives by melt processing, and can be in the form of a monofilament, disc, film, microcapillary or other complex shapes. The method of formation provides for preparation of poly (aryl ether ketone) articles with high degree of surface area and uniform nanometer pore size. The preferred poly (aryl ether ketone)s are poly (ether ketone) and poly (ether ether ketone). The mesoporous articles formed by the method of the present invention are useful for a broad range of applications, including molecular separations and organic solvent filtration.
    Type: Grant
    Filed: May 10, 2022
    Date of Patent: November 22, 2022
    Assignee: Avanpore LLC
    Inventor: Benjamin Bikson
  • Patent number: 11447743
    Abstract: This invention provides a cell culture substrate comprising on its surface a fluorine-containing polymer that enables three-dimensional tissue culture. The cell culture substrate of the invention has a surface at least a part of which is composed of a resin composition comprising a fluorine-containing polymer having one or more fluorine atoms in a repeating unit and exhibits the oxygen gas permeability of 219 cm3 (STP)/(m2·24 h·atm) or higher. Three-dimensional tissue can be formed via cell culture with the use of the cell culture substrate of the invention.
    Type: Grant
    Filed: March 17, 2015
    Date of Patent: September 20, 2022
    Assignee: Nippon Shokubai Co., Ltd.
    Inventors: Tomomi Makino, Hiroshi Horikawa
  • Patent number: 11370856
    Abstract: The present invention relates to super absorbent polymer and a method for preparing the same. According to the super absorbent polymer and preparation method for the same of the present invention, super absorbent polymer having improved rewet property and vortex time can be provided.
    Type: Grant
    Filed: March 20, 2019
    Date of Patent: June 28, 2022
    Inventors: Dae Woo Nam, Ki Hyun Kim, Jun Kyu Kim, Young Jae Hur
  • Patent number: 11118173
    Abstract: A method of collecting a nucleic acid(s) from a biological sample includes step a) mixing an aluminum oxide support with a water-soluble neutral polymer adsorbed on a surface thereof and a solution containing a nucleic acid(s), thereby adsorbing the nucleic acid(s) to the support; step b) separating the support on which the nucleic acid(s) is/are adsorbed from the solution mixed in step a); and step c) collecting the nucleic acid(s) by adding an eluent to the support on which the nucleic acid(s) is/are adsorbed and which is separated in step b).
    Type: Grant
    Filed: March 18, 2016
    Date of Patent: September 14, 2021
    Assignee: Toray Industries, Inc.
    Inventors: Shota Sekiguchi, Shinjiro Sawada
  • Patent number: 11103845
    Abstract: Disclosed herein is a polysaccharide aerogel comprising cotton cellulose fibres and a method of preparing the polysaccharide aerogel. The method comprises: mixing cotton cellulose fibres and a cross-linker to form a mixture; sonicating the mixture; freezing the sonicated mixture; and freeze drying the frozen mixture to form an aerogel. A further embodiment provides a polysaccharide aerogel comprising cotton cellulose fibres and paper cellulose fibres in a weight ratio of 1:1 to 1:6 and a method of preparation thereof wherein in the mixing step, the paper cellulose fibres are added to the cotton cellulose fibres to form a mixture.
    Type: Grant
    Filed: December 7, 2017
    Date of Patent: August 31, 2021
    Assignee: National University of Singapore
    Inventors: Hai Minh Duong, Nhan Phan-Thien, Bowen Gu, Mark Pyne Pennefather, Thanh Xuan Nguyen
  • Patent number: 10913834
    Abstract: A polymer matrix composite comprising a porous polymeric network; and a plurality of indicator particles distributed within the polymeric network structure; wherein the indicator particles are present in a range from 1 to 99 weight percent, based on the total weight of the indicator particles and the polymer (excluding the solvent); and wherein the polymer matrix composite has a density of at least 0.05 g/cm3; and methods for making the same. The polymer matrix composites are useful, for example, as sensors.
    Type: Grant
    Filed: November 15, 2018
    Date of Patent: February 9, 2021
    Assignee: 3M Innovative Properties Company
    Inventors: Derek J. Dehn, Clinton P. Waller, Jr., Bharat R. Acharya, Satinder K. Nayar
  • Patent number: 10882750
    Abstract: In the present invention are provided a method for preparing a silica aerogel-containing blanket, and a blanket which includes a silica aerogel and is manufactured using the same, wherein the method includes a step for preparing a reaction solution by reacting a silazane-based surface modification agent with an alcohol-based compound, a step for preparing a silica gel-base material composite by adding a silica precursor, water, and a polar organic solvent to the reaction solution to prepare a silica sol, and then immersing a base material for a blanket in the prepared silica sol to gelate the silica sol, and a step for drying the silica gel-base material composite.
    Type: Grant
    Filed: March 28, 2016
    Date of Patent: January 5, 2021
    Assignee: LG CHEM, LTD.
    Inventors: Kyoung Shil Oh, Mi Ri Kim, Je Kyun Lee
  • Patent number: 10815316
    Abstract: A continuous process for manufacturing macroporous beads, the process comprising: providing an aqueous carrier phase flowing through a pipe at a carrier phase flow velocity; providing an emulsion of a UV-polymerisable or thermally polymerisable continuous phase in an aqueous dispersed phase; injecting the emulsion into the carrier phase at an injection speed to create polymerisable droplets flowing in the carrier phase; forming macroporous beads by irradiating the droplets with UV light, or by heating the droplets to a temperature sufficient to decompose a thermal initiator in the continuous phase, to polymerise the droplets; and removing the macroporous beads from the carrier phase; wherein the ratio of carrier phase flow velocity/injection speed is at least 1.
    Type: Grant
    Filed: October 31, 2017
    Date of Patent: October 27, 2020
    Assignee: University of Vienna
    Inventors: Juan Ferrer, Angelika Menner, Alexander Bismarck
  • Patent number: 10729592
    Abstract: An absorbent structure comprising a single stratum exhibiting a Capillarity Work Potential greater than the Capillarity Work Potential trade-off Boundary.
    Type: Grant
    Filed: November 4, 2016
    Date of Patent: August 4, 2020
    Assignee: The Procter & Gamble Company
    Inventors: Christopher Philip Bewick-Sonntag, Vito Carla, Wade Monroe Hubbard, Jr., John Lee Hammons
  • Patent number: 10729600
    Abstract: An absorbent structure comprising one or more absorbent layers wherein the absorbent structure exhibits a first cycle Peak Force compression between about 30 grams and about 150 grams. The absorbent structure further exhibits a fifth cycle dry recovery energy between 0.1 mJ and 2.8 mJ.
    Type: Grant
    Filed: November 4, 2016
    Date of Patent: August 4, 2020
    Assignee: The Procter & Gamble Company
    Inventors: Christopher Philip Bewick-Sonntag, Clint Adam Morrow, Wade Monroe Hubbard, Jr.
  • Patent number: 10654959
    Abstract: The present invention provides a method for preparing a superabsorbent polymer, the method comprising the steps of: forming a function gel polymer by cross-linked polymerization of a monomer mixture under the presence of an internal cross-linking agent, the monomer mixture including a water-soluble ethylene-based unsaturated monomer having an acid group at least part of which is neutralized, a carbonate, a volatile organic solvent, a surfactant, and a bubble promoting agent; forming a base resin powder by drying, grinding, and classifying the function gel polymer; and forming a surface cross-linked layer by additional cross-linking of the surface of the base resin powder under the presence of a surface cross-linking agent. The method for preparing a superabsorbent polymer may provide a superabsorbent polymer which has a porous structure, thereby exhibiting an excellent absorption rate while exhibiting excellent gel strength.
    Type: Grant
    Filed: April 11, 2016
    Date of Patent: May 19, 2020
    Assignee: LG Chem, Ltd.
    Inventors: Soo Jin Lee, Hye Mi Nam, Sang Gi Lee, Min Ho Hwang, Tae Hwan Jang
  • Patent number: 10637100
    Abstract: A method of making a passively impact resistant composite electrolyte and separator layer includes providing a suspension composition including electrically non-conducting particles that enable shear thickening. The particles can have a polydispersity index of no greater than 0.1, an average particle size in a range of from 50 nm to 1 um, and an absolute zeta potential of greater than ±40 mV. A particle suspension solvent is provided for suspending the particles. The suspension composition is applied to a porous separator material. A portion of the particles and suspension solvent penetrate the pores and the remainder of the particles in the suspension composition are distributed across the surface of the separator material. The suspension solvent is evaporated from the separator material to provide a shear thickening particle loaded separator. A separator assembly and a passivated battery are also disclosed.
    Type: Grant
    Filed: April 20, 2018
    Date of Patent: April 28, 2020
    Assignee: UT-BATTELLE, LLC
    Inventors: Beth L. Armstrong, Gabriel M. Veith, Sergiy Kalnaus, Hsin Wang, Katie L. Browning, Kevin M. Cooley
  • Patent number: 10626214
    Abstract: A reaction system for forming a viscoelastic polyurethane foam includes an isocyanate component that has at least one isocyanate and an isocyanate-reactive component that is a mixture formed by adding at least a polyol component, an additive component, and a preformed aqueous polymer dispersion. The mixture includes, based on the total weight of the mixture, from 50.0 wt % to 99.8 wt % of a polyol component including at least one polyether polyol, from 0.1 wt % to 50.0 wt % of an additive component including at least one catalyst, and from 0.1 wt % to 6.0 wt % of a preformed aqueous polymer dispersion. The preformed aqueous polymer dispersion has a solids content from 10 wt % to 80 wt %, based on the total weight of the preformed aqueous polymer dispersion, and is one of an aqueous acid polymer dispersion or an aqueous acid modified polyolefin polymer dispersion in which the polyolefin is derived from at least one C2 to C20 alpha-olefin.
    Type: Grant
    Filed: December 15, 2015
    Date of Patent: April 21, 2020
    Assignees: Dow Global Technologies LLC, Rohm and Haas Company
    Inventors: Kaoru Aou, Joseph Jacobs, Qinghao Meng, Paul Cookson
  • Patent number: 10376420
    Abstract: A personal hygiene article includes a chassis with a topsheet, a backsheet, and an absorbent component between the topsheet and the backsheet. At least one portion of the personal hygiene article includes a microporous film having an opaque, microporous region and at least one see-through region of lower porosity within the opaque, microporous region. The microporous film can include a beta-nucleating agent or can have thermally induced phase separation caused by a diluent. A container includes a microporous film enclosing at least one personal hygiene article. The microporous film has an opaque, microporous region and at least one see-through region of lower porosity forming a window within the opaque, microporous region. Methods of making the personal hygiene article and container are also described.
    Type: Grant
    Filed: June 12, 2014
    Date of Patent: August 13, 2019
    Assignee: 3M Innovative Properties Company
    Inventors: Neelakandan Chandrasekaran, Robert L. W. Smithson, Leigh E. Wood, Timothy V. Stagg
  • Patent number: 10059597
    Abstract: The present invention relates to a method for manufacturing an aerogel sheet. The method for manufacturing an aerogel sheet includes: a step (a) of immersing a blanket in an impregnation vessel in which silica sol is stored to impregnate the silica sol; and a step (b) of injecting a gelling catalyst to a surface of the blanket in which the silica sol is impregnated to gelate the silica sol.
    Type: Grant
    Filed: October 31, 2016
    Date of Patent: August 28, 2018
    Assignee: LG CHEM, LTD.
    Inventors: Ye Hon Kim, Je Kyun Lee, Jung Uk Choi
  • Patent number: 9840443
    Abstract: A general procedure applied to a variety of sol-gel precursors and solvent systems for preparing and controlling homogeneous dispersions of very small particles within each other. Fine homogenous dispersions processed at elevated temperatures and controlled atmospheres make a ceramic powder to be consolidated into a component by standard commercial means: sinter, hot press, hot isostatic pressing (HIP), hot/cold extrusion, spark plasma sinter (SPS), etc.
    Type: Grant
    Filed: October 16, 2014
    Date of Patent: December 12, 2017
    Assignee: Lawrence Livermore National Laboratory, LLC
    Inventors: Richard Landingham, Robert A. Reibold, Joe Satcher
  • Patent number: 9840605
    Abstract: Polymer foam bodies are made from phosphorus-containing thermoplastic random copolymers of a dialkyl (meth)acryloyloxyalkyl phosph(on)ate. Foam bodies made from these copolymers exhibit increased limiting oxygen indices and surprisingly have good properties. In certain embodiments, the phosphorus-containing thermoplastic copolymer is blended with one or more other polymers and formed into nanofoams.
    Type: Grant
    Filed: December 27, 2013
    Date of Patent: December 12, 2017
    Assignee: Dow Global Technologies LLC
    Inventors: Yudong Qi, Yan Li, Shana P. Bunker, Stephane Costeux, Ted A. Morgan
  • Patent number: 9777078
    Abstract: A process for producing water-absorbing polymer particles by polymerizing droplets of a monomer solution, where the monomer solution comprises at least two initiators, one of the initiators is a peroxide with the exception of persulfate, and the molar ratio of peroxide to further initiator is at least 1:8, the water-absorbing polymer particles themselves, and hygiene articles comprising these water-absorbing polymer particles.
    Type: Grant
    Filed: July 12, 2007
    Date of Patent: October 3, 2017
    Assignee: BASF SE
    Inventors: Dennis Loesch, Volker Seidl, Matthias Weismantel
  • Patent number: 9707000
    Abstract: The present invention is directed to the compositions and methods of preparing hydrogel-grafted nerve guides for peripheral nerve regeneration. Particularly, the present invention describes the nerve guides and methods for preparation of hydrogel-grafted nerve guides with encapsulated neurotrophic factors and a nanofiber mesh lining the inner surface of the guide. The present invention also provides methods for peripheral nerve repair using these hydrogel-grafted nerve guides.
    Type: Grant
    Filed: November 15, 2013
    Date of Patent: July 18, 2017
    Assignee: The Johns Hopkins University
    Inventors: Ahmet Hoke, Shawn H. Lim, Xingyu Liu, Hai-Quan Mao
  • Patent number: 9434832
    Abstract: An aerogel and process of making the aerogel is provided. The aerogel is a polyimide aerogel having polyamide cross-links formed using a triacid chloride cross-linker.
    Type: Grant
    Filed: March 17, 2015
    Date of Patent: September 6, 2016
    Assignee: The United States of America as Represented by the Administrator of National Aeronautics and Space Administration
    Inventor: Mary Ann B. Meador
  • Patent number: 9394384
    Abstract: The invention provides fabricated tough hydrogels, hydrogel-containing compositions, and methods of making the same. The invention also provides methods of implanting or administering the tough hydrogels, or the hydrogel-containing compositions to treat a subject in need. Methods of cross-linking pre-solidified or pre-gelled hydrogel particles and making crosslinked tough hydrogels, and crosslinked tough hydrogel-containing compositions also are disclosed herein.
    Type: Grant
    Filed: September 27, 2005
    Date of Patent: July 19, 2016
    Assignee: The General Hospital Corporation
    Inventors: Orhun K. Muratoglu, Jeeyoung Choi, Hatice Bodugoz-Senturk, Gavin J. C. Braithwaite, Stephen H. Spiegelberg
  • Patent number: 9345667
    Abstract: A process for preparing particles having a hydrophobic material therein is disclosed. The process comprises providing a multiple emulsion comprising a first emulsion dispersed in a hydrophobic medium, said first emulsion comprising a hydrophobic phase dispersed in a hydrophilic phase, wherein the hydrophobic phase comprises the hydrophobic material and the hydrophilic phase comprises a precursor which is capable of reacting to form a non-fluid matrix and reacting the precursor in the multiple emulsion to form the matrix in the form of the particles having the hydrophobic material therein wherein the precursor is added prior to formation of the multiple emulsion. Also disclosed are particles having a hydrophobic material therein, which may be releasable, as well as particles having a hydrophobic material therein, which may be releasable, made by the process and methods of using the particles.
    Type: Grant
    Filed: June 19, 2006
    Date of Patent: May 24, 2016
    Assignee: Australian Nuclear Science and Technology Organisation
    Inventors: Linggen Kong, Christophe Jean Alexandre Barbe, Kim Suzanne Finnie
  • Patent number: 9323102
    Abstract: There are provided a resin composition and an optical film using the same. The resin composition includes a copolymer (A) formed by polymerizing a (meth)acryloyl morpholine-based monomer (a), a maleimide-based monomer (b), and an alkyl(meth)acrylate-based monomer (c), and the optical film is manufactured using the same. The resin composition may provide a film having excellent optical properties and optical transparency, reduced haze, excellent mechanical strength, a relatively low level of thermal expansion coefficient leading to a relatively small change in a dimension, and a relatively low level of alteration in a retardation value due to external stress.
    Type: Grant
    Filed: September 24, 2013
    Date of Patent: April 26, 2016
    Assignee: LG CHEM, LTD.
    Inventors: Jun-Geun Um, Nam-Jeong Lee
  • Patent number: 9324571
    Abstract: A method and apparatus for depositing a low K dielectric film with one or more features is disclosed herein. A method of forming a dielectric layer can include positioning a substrate in a processing chamber, delivering a deposition gas to the processing chamber, depositing a dense organosilicon layer using the deposition gas on the surface of the substrate, the dense organosilicon layer comprising a porogenic carbon, transferring a pattern into the dense organosilicon layer, forming a pore-forming plasma from a reactant gas, exposing the dense organosilicon layer to the pore-forming plasma to create a porous organosilicon layer, wherein the pore-forming plasma removes at least a portion of the porogenic carbon and exposing the porous organosilicon layer to a desiccating post treatment.
    Type: Grant
    Filed: February 4, 2014
    Date of Patent: April 26, 2016
    Assignee: APPLIED MATERIALS, INC.
    Inventors: Kang Sub Yim, Pendar Ardalan, Sure Ngo, Alexandros T. Demos
  • Patent number: 9296851
    Abstract: The invention relates to a process for the preparation of polymers and to an apparatus for performing this process. The apparatus comprises devices and reactors that are combined in the sequence of first a mixing device, second a flow microwave and optionally third one or more additional reactors.
    Type: Grant
    Filed: April 1, 2011
    Date of Patent: March 29, 2016
    Assignee: DPx Holdings B.V.
    Inventor: Karsten Luettgen
  • Patent number: 9255198
    Abstract: The invention provides a method of preparing an aqueous dispersion of polymer encapsulated particulate material, the method comprising: providing a dispersion of the particulate material in a continuous aqueous phase, the dispersion comprising RAFT agent as a stabiliser for the particulate material; and polymerising ethylenically unsaturated monomer under the control of the RAFT agent to form polymer at the surface of the dispersed particulate material, thereby providing the aqueous dispersion of polymer encapsulated particulate material; wherein polymerisation of the ethylenically unsaturated monomer comprises: (a) polymerising a monomer composition that includes ionisable ethylenically unsaturated monomer so as to form a base responsive water swellable RAFT polymer layer that encapsulates the particulate material; and (b) polymerising a monomer composition that includes non-ionisable ethylenically unsaturated monomer so as to form an extensible, water and base permeable RAFT polymer layer that encapsulate
    Type: Grant
    Filed: December 1, 2010
    Date of Patent: February 9, 2016
    Assignee: The University of Sydney
    Inventors: Matthew P. Baker, Timothy W. Davey, Brian S. Hawkett, Duc N. Nguyen, Caitlin C. O'Brien, Christopher H. Such
  • Patent number: 9219264
    Abstract: A separator for a rechargeable lithium battery including a tungsten-doped vanadium oxide (VO2) phase transition material and the rechargeable lithium battery including the separator. Here, an explosion possibility of the rechargeable lithium battery including the separator may be prevented and delayed when the battery is excessively heated.
    Type: Grant
    Filed: January 8, 2013
    Date of Patent: December 22, 2015
    Assignee: Samsung SDI Co., Ltd.
    Inventors: Tae-Hyun Bae, Woo-Cheol Shin, Sang-Il Han, Jung-Yi Yu, Mi-Hyun Lee
  • Patent number: 9200154
    Abstract: The present invention provides porous resin particles made of a polymer of a monomer mixture, wherein the monomer mixture contains, as monomers, at least methyl methacrylate and a (meth)acrylic-based cross-linkable monomer, a content of the methyl methacrylate in the monomer mixture is 1 to 50% by weight, a content of the (meth)acrylic-based cross-linkable monomer in the monomer mixture is 50 to 99% by weight, the porous resin particles have a specific surface area of 130 to 180 m2/g, a pore volume of 0.3 to 0.7 ml/g, and an average pore size of 13 to 16 nm, an amount of unreacted methyl methacrylate remaining in the porous resin particles is 20 ppm or less, and the porous resin particles have a thermal decomposition starting temperature of 260° C. or more.
    Type: Grant
    Filed: March 26, 2013
    Date of Patent: December 1, 2015
    Assignee: SEKISUI PLASTICS CO., LTD.
    Inventors: Kenzo Teramoto, Junko Hiroi, Masaaki Nakamura
  • Patent number: 9181634
    Abstract: The invention concerns a particle having a code from a library of codes embedded in its physical structure by refractive index changes between different regions of the particle. In preferred embodiments, a thin film possesses porosity that varies in a manner to produce a code detectable in the reflectivity spectrum. An assay detection method uses such a particle and detects a spectral shift in the presence of an analyte. Additional embodiments are disclosed including additional features.
    Type: Grant
    Filed: December 21, 2004
    Date of Patent: November 10, 2015
    Assignee: The Regents of the University of California
    Inventors: Michael J. Sailor, Shawn O. Meade