Diatomite Or Diatomaceous Earth, E.g., Kieselguhr, Infusorial Earth, Etc. Patents (Class 524/448)
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Patent number: 6455029Abstract: A composition for use as a dental impression material including a polymerizable telechelic oligomer or polymer curable by ring-opening metathesis polymerization, a filler system, and a ruthenium carbene complex catalyst, whereby the catalyst initiates ring-opening metathesis polymerization of the composition. The invention includes a paste/paste system in which a base paste includes the polymerizable telechelic oligomer or polymer and a filler system and in which a catalyst paste includes the catalyst dissolved in an inert solvent and a filler system. The telechelic oligomer or polymer may be, for example, a polydimethylsiloxane end-functionalized with norbornenyl groups. The catalyst may be, for example, a ruthenium carbene complex with a ligand having a basicity higher than tricyclohexylphosphine. The composition of the present invention exhibits reduced sensitivity to sulfur impurities.Type: GrantFiled: October 17, 2000Date of Patent: September 24, 2002Assignee: Kerr CorporationInventors: Christos Angeletakis, Mingfei Chen
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Patent number: 6441079Abstract: A curable fluoropolyether base rubber composition contains (A) 100 parts by weight of a linear fluoropolyether compound having at least two alkenyl groups in a molecule and a perfluoroalkyl ether structure in its backbone, (B) 10-40 parts by weight of a silica filler having a specific surface area of at least 50 m2/g, (C) 5-35 parts by weight of diatomaceous earth, (D) an organosilicon compound having at least two Si—H groups, and (E) a hydrosilylation catalyst. The inclusion of diatomaceous earth is effective for preventing the composition from outgassing and from changing its curing behavior with time.Type: GrantFiled: January 5, 2001Date of Patent: August 27, 2002Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Makoto Sato, Takashi Matsuda, Shinichi Sato, Masatoshi Arai
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Publication number: 20020103283Abstract: A method of inhibiting the loss of solar reflectivity over time of an exterior elastomeric coating composition comprising an organic binder and at least one inorganic additive comprises: replacing at least a part of the at least one inorganic additive with a solid, particulate, organic polymer having a Tg greater than 70° C. An improved exterior elastomeric coating composition is also disclosed.Type: ApplicationFiled: May 1, 2001Publication date: August 1, 2002Inventors: William Henry Elfring, Donald Alfred Winey
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Patent number: 6413354Abstract: A silicone composition that is oil resistant when cured is described. More particularly, this composition includes a silanol terminated silicone fluid, an organic plasticizer, a filler and a crosslinker, wherein the cured composition remains adhesive after exposure to oil. The present compositions provide superior adhesive properties after exposure to oil than conventional RTV silicone adhesives having M-stopped silicone plasticizers. Methods of making and using cured elastomeric products made from the present compositions are also provided.Type: GrantFiled: February 17, 2000Date of Patent: July 2, 2002Assignee: Loctite CorporationInventors: Hans E. Haas, Frank L. Kovacs
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Patent number: 6410630Abstract: A high solids content composition containing a fluoroelastomer, a solvent, and a low solvent absorptine filler is workable to fill voids, coat, adhere, seal, and protect various substrates from chemical permeation, corrosion, abrasion, etc. in horizontal or vertical applications. The fluoroelastomer component comprises copolymers of hexafluoropropylene and vinylidene flouride and/or terpolymers of hexafluoropropylene, vinylidene fluoride, and tetrafluoroethylene. The solids content of the composition is at least about 75%. The composition may include a curing agent to solidify the composition.Type: GrantFiled: December 29, 1999Date of Patent: June 25, 2002Assignee: Pelseal Technologies, LLCInventors: Gary Scott Hoover, Edwin William Ross, Jr.
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Patent number: 6391958Abstract: A novel wallboard composition is disclosed comprising a unique combination of synthetic binders selected for their ability to establish a strengthened permanent bond in the final dry state in combination with an expanded mineral such as Perlite which largely reduces the amount of gypsum over current gypsum wallboard formulations, thus reducing the weight while maintaining the strength of the wallboard structure. In a preferred embodiment, the lightweight, strengthened wallboard of the present invention also comprises a covering veneer that is applied to the top ply of the face paper to provide increased strength, moisture resistance, and fire retardency, and the back paper top ply is treated to provide increased flexural strength.Type: GrantFiled: October 26, 2000Date of Patent: May 21, 2002Assignee: Advanced Construction Materials Corp.Inventor: Joseph S. Luongo
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Patent number: 6391449Abstract: This invention relates to a polymer-clay intercalates, exfoliates, nanocomposites and methods of manufacturing comprising (i) a melt-processible matrix polymer, and incorporated therein (ii) a mixture of at least two layered clay materials. The invention also relates to articles produced from a nanocomposite and a process for preparing a nanocomposite.Type: GrantFiled: December 1, 1999Date of Patent: May 21, 2002Assignee: AMCOL International CorporationInventors: Tie Lan, Vasiliki Psihogios, Robert Boyd Barbee, James Christopher Matayabas, Jr., John Walker Gilmer
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Patent number: 6359052Abstract: The present invention relates to a polyester-platelet particle composite comprising at least one polyester having dispersed therein a platelet particle dispersion comprising chalcogen or platelet particles and at least one water dissipatible polymer.Type: GrantFiled: August 1, 2000Date of Patent: March 19, 2002Inventors: Jack Wesley Trexler, Jr., Rodney Layne Piner, Sam Richard Turner, Robert Boyd Barbee
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Patent number: 6355732Abstract: A packaging film or sheet which is capable of forming peel seals having acceptable seal strengths, is disclosed which includes a polymer mixture consisting of a blend having proportionate amounts of from about 60 percent by weight to about 70 percent by weight of LDPE; from about 15 percent by weight to about 25 percent by weight of mLLDPE; and from about 10 percent by weight to about 20 percent by weight of 1-polybutylene.Type: GrantFiled: October 13, 2000Date of Patent: March 12, 2002Assignee: Fres-Co System USA, Inc.Inventor: Jeffrey Scott Beer
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Patent number: 6355717Abstract: The present invention provides barrier composite resin compositions and moulded bodies, comprising (a) aromatic polyamide resins or polyamide resin compositions containing at least one aromatic polyamide resin, and (b) a layered silicate modified by a triazine compound derivative.Type: GrantFiled: August 4, 2000Date of Patent: March 12, 2002Assignee: EMS-Chemie AGInventors: Kenji Tamura, Hirofumi Inoue, Junichi Nakamura, Masayuki Noguchi, Tsuguo Ebata
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Publication number: 20020022678Abstract: This invention relates to a polymer-clay intercalates, exfoliates, nanocomposites and methods of manufacturing comprising (i) a melt-processible matrix polymer, and incorporated therein (ii) a mixture of at least two layered clay materials. The invention also relates to articles produced from a nanocomposite and a process for preparing a nanocomposite.Type: ApplicationFiled: December 1, 1999Publication date: February 21, 2002Inventors: TIE LAN, VASILIKI PSHIHOGIOS, ROBERT BOYD BARBEE, JAMES CHRISTOPHER MATAYABAS, JOHN WALKER GILMER
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Patent number: 6323262Abstract: In a continuous process for producing filler-containing silicone compositions (P), a silicone composition (E) comprising filler (F1) is mixed with filler (F2).Type: GrantFiled: February 25, 2000Date of Patent: November 27, 2001Assignee: Wacker-Chemie GmbHInventors: Frank Achenbach, Manfred Heisler, Armin Fehn, Christof Wörner
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Patent number: 6306946Abstract: Disclosed is a select class of liquid crystalline polyesters and molding compositions comprising the polyesters and glass fiber. The liquid crystalline polyesters consist essentially of (1) diacid residues consisting essentially of (i) cyclohexanedicarboxylic acid residues and (ii) other diacid residues selected from terephthalic acid residues, 2,6-naphthalenedicarboxylic acid residues, or a mixture thereof; (2) diol residues consisting essentially of hydroquinone residues, 4,4′-biphenol residues or a mixture thereof; and, optionally, (3) p-hydroxybenzoic acid residues. In the above definition, the moles of diol residues are equal to the moles of diacid residues and the total of the (1), (2) and (3) mole percentages is equal to 100. The liquid crystalline polyesters have melting points determined by differential scanning calorimetry equal to or less than 360° C.Type: GrantFiled: November 8, 2000Date of Patent: October 23, 2001Assignee: Eastman Chemical CompanyInventors: Timothy Edward Long, William Ronald Darnell
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Patent number: 6284819Abstract: The present invention provides a recording medium comprising a substrate having a glossy coating thereon, wherein the glossy coating comprises a binder and first and second groups of particles, wherein: (a) the first group comprises metal oxide particles, wherein the metal oxide particles are aggregates of smaller, primary particles, (b) the mean diameter of the primary particles is less than about 100 nm, (c) the mean diameter of the aggregates is from about 100 nm to about 500 nm, (d) the mean diameter of the particles in the second group is less than about 50% of the mean diameter of the aggregates in the first group, and (e) the ratio of particles in the first group to particles in the second group is from about 0.1:1 to about 10:1 by weight. The glossy coating of the inventive recording medium has an excellent rate of liquid absorption, a relatively high liquid absorption capacity, excellent adhesiveness, and a non-brittle, crack-resistant, glossy surface.Type: GrantFiled: July 1, 1999Date of Patent: September 4, 2001Assignee: Cabot CorporationInventors: Michael S. Darsillo, David J. Fluck, Rudiger Laufhutte
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Patent number: 6268432Abstract: A filler/adhesive agent for display units containing a condensation reaction curable silicone composition including air oxidation-curable unsaturated compounds and for use as a filler or adhesive in display units whose construction is such that the cured product of said composition is exposed in the display section, which composition is capable of forming matte finished cured products with insignificant surface tact, is disclosed.Type: GrantFiled: September 30, 1999Date of Patent: July 31, 2001Assignee: Dow Corning Toray Silicone Co. Ltd.Inventors: Toshiki Nakata, Masayuki Onishi
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Publication number: 20010009936Abstract: A method of manufacturing an insulating film-forming material comprising a curable composition comprisING (A) an inorganic polymer compound or an organic polymer compound and (B) an organic solvent, which comprises treating the curable composition with a zeta potential-producing filter material. Because the curable composition has a very small content of alkali metals and heavy metals, the composition is suitably used for the manufacture of materials for forming insulating films which have a wide variety of applications in the electronic field.Type: ApplicationFiled: January 17, 2001Publication date: July 26, 2001Applicant: JSR CorporationInventors: Hidenori Suzuki, Katsuyuki Kakinoki, Yoshihisa Nakase, Michinori Nishikawa, Takashi Okada, Kinji Yamada
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Publication number: 20010008916Abstract: A curable fluoropolyether base rubber composition contains (A) 100 parts by weight of a linear fluoropolyether compound having at least two alkenyl groups in a molecule and a perfluoroalkyl ether structure in its backbone, (B) 10-40 parts by weight of a silica filler having a specific surface area of at least 50 m2/g, (C) 5-35 parts by weight of diatomaceous earth, (D) an organosilicon compound having at least two Si—H groups, and (E) a hydrosilylation catalyst. The inclusion of diatomaceous earth is effective for preventing the composition from outgassing and from changing its curing behavior with time.Type: ApplicationFiled: January 5, 2001Publication date: July 19, 2001Inventors: Makoto Sato, Takashi Matsuda, Shinichi Sato, Masatoshi Arai
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Patent number: 6262162Abstract: Intercalated layered materials prepared by co-intercalation of a multi-charged onium ion spacing/coupling agent and a matrix polymer between the planar layers of a swellable layered material, such as a phyllosilicate, preferably a smectite clay. The spacing of adjacent layers of the layered materials is expanded at least about 3 Å, preferably at least about 5 Å, usually to about 15-20 Å, e.g., 18 Å with the di-charged onium ion spacing/coupling agent. The intercalation of the matrix polymer then increases the spacing between adjacent layers to at least about 15 Å, preferably to about 20 Å to about 30 Å.Type: GrantFiled: March 19, 1999Date of Patent: July 17, 2001Assignee: AMCOL International CorporationInventors: Tie Lan, Erin K. Westphal, Vasiliki Psihogios, Ying Liang
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Publication number: 20010003766Abstract: An aromatic polyamide resin composition is obtained by blending an inorganic filler and an impact modifier. The ratio of the weight M of the inorganic filler to the weight T of the impact modifier is preferably 2.0≦M/T≦6.5. The aromatic polyamide resin has a melting point of at least 290° C., and preferably a glass transition temperature of at least 60° C. The composition has an excellent balance of toughness and stiffness.Type: ApplicationFiled: November 18, 1998Publication date: June 14, 2001Inventor: MASAHIRO NOZAKI
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Patent number: 6245849Abstract: A method is provided for fabricating ceramic microstructures, i.e., microcomponents of micron or submicron dimensions. A polymer composition is prepared containing a polymer, typically a thermally or chemically curable polymer, and nanometer size (1 to 1000 nm in diameter) ceramic particles. A mold, such as a lithographically patterned mold, preferably a LIGA mold, is filled with the polymer composition and the polymer is then cured or otherwise hardened. The elevated segments of the mold are then removed. The surface-attached ceramic microstructures so provided may then be removed from the substrate and, if desired, pyrolyzed and sintered.Type: GrantFiled: June 2, 1999Date of Patent: June 12, 2001Assignee: Sandia CorporationInventors: Alfredo Martin Morales, Z. John Zhang, Douglas Chinn
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Publication number: 20010002412Abstract: An easily shaped evacuated porous stonelike body is impregnated in a consistent manner with a fluid polymer forming composition or molten polymer composition and solidified to form a polymeric matrix stone product bearing a striking resemblance to a natural rock in texture, structure, and formation exhibited throughout any substantial cross section. The polymeric composition is decoratively enhanced by the labyrinthic skeletal framework of the porous body and the skeletal framework is structurally enhanced by the polymeric composition. The method of forming the product closely duplicates the natural formation of most of the rocks exposed at the surface of the earth. Therefore, a wide range of stonelike textures are now available in a dimensional stock product of pre-determined size and shape. A wide range of chemical and physical properties are also possible depending upon the specific combination of porous bodies and solidified polymeric compositions.Type: ApplicationFiled: November 6, 1997Publication date: May 31, 2001Inventor: JOHN P. KOLARIK
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Patent number: 6239194Abstract: The present invention relates to surface-modified fillers obtained by mixing a filler with water, adding an water-based organosiloxane composition with very thorough mixing, wherein the organosiloxanes are soluble in water and contain, in addition to OH groups, at least one amino-functional group and optionally a functional group from the series consisting of alkyl, haloalkyl, alkenyl, glycidyl ether alkyl, acryloxyalkyl and methacryloxyalkyl, and wherein a functional group is bonded to each silicon atom of the organosiloxane, and drying the mixture. The present invention also provides a process for the surface modification of fillers, their use and ethylene-vinyl acetate copolymer compositions which include the surface-modified fillers.Type: GrantFiled: April 28, 1999Date of Patent: May 29, 2001Assignee: Huels AktiengesellschaftInventors: Burkhard Standke, Jaroslaw Monkiewicz, Albert-Johannes Frings, Ralf Laven, Roland Edelmann, Peter Jenkner, Helmut Mack, Dieter Barfurth, Michael Horn
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Patent number: 6232389Abstract: Applications of barrier coating mixtures containing in a carrier liquid, (a) an elastomeric (preferably butyl-containing) polymer; (b) a dispersed exfoliated layered filler having an aspect ratio greater than 25; and (c) at least one surfactant, wherein the solids content of the mixture is less than 30% and the ratio of polymer (a) to filler (b) is between 20:1 and 1:1 include coated articles, which are elastomeric, e.g., sports balls and inflatable articles. Methods of manufacturing such coated products are also encompassed.Type: GrantFiled: June 10, 1999Date of Patent: May 15, 2001Assignees: InMat, LLC, Michelin Recherche et Technique S.A.Inventors: Carrie A. Feeney, Michele Farrell, Klaus Tannert, Harris A. Goldberg, Mengshi Lu, Michael D. Grah, William G. Steiner, Paul B. Winston
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Patent number: 6218495Abstract: A three-stage process for the continuous preparation of RTV-1 compositions comprises, in a first step, preparing a raw mixture of &agr;,&ohgr;-dihydroxypolydiorganosiloxane, filler and, if desired, further constituents, in a second step, freeing the raw mixture of gas inclusions under reduced pressure and, if desired, mixing it with further constituents and, in a third step, mixing the degassed raw mixture with a crosslinker, a condensation catalyst and, if desired, additional constituents not yet added in the first and second steps.Type: GrantFiled: February 24, 1999Date of Patent: April 17, 2001Assignee: Wacker-Chemie GmbHInventors: Rudolf Braun, Helmut Wöhrl, Werner Trajer, Johann Steiner, Thomas Felber
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Patent number: 6194508Abstract: Peroxidically crosslinkable silicone rubber compositions containing a filler which has covalently bound Si—H-containing groups exhibit lower tendency toward yellowing while maintaining or increasing other elastomer physical properties and processing properties.Type: GrantFiled: February 10, 1999Date of Patent: February 27, 2001Assignee: Wacker-Chemie GmbHInventors: Frank Achenbach, Herbert Barthel, Christian Finger
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Patent number: 6162857Abstract: The present invention relates to polyester-platelet particle composite comprising; at least one polyester having dispersed therein a platelet particle dispersion comprising about 0.01 to about 25 weight percent platelet particles and at least one water dissipatible polymer in a concentration which is at least about 1 part water dissipatible polymer to 1 part said polyester wherein said platelet particles primarily comprise individual platelet particles and tactoids. The composites of the present invention are prepared by dispersing at least one clay material in a water dissipatible polymer to form a platelet particle dispersion; introducing said platelet particle dispersion to a polyester and extrusion mixing said dispersion and polyester.Type: GrantFiled: December 22, 1997Date of Patent: December 19, 2000Assignee: Eastman Chemical CompanyInventors: Jack Wesley Trexler, Jr., Rodney Layne Piner, Sam Richard Turner, Robert Boyd Barbee
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Patent number: 6162852Abstract: A hot alkaline liquid soluble or dispersable composition made from a first polymer of an ethylene-acrylic acid copolymer having an acrylic acid portion, an ethylene-methacrylic acid copolymer having a methacrylic acid portion, or a mixture thereof, where the acrylic acid portion and the methacrylic acid portion each, independently, comprise from 10 to 30 wt. % of the total copolymer weight and also including an Ionomer-type copolymer having an acrylic acid portion, a methacrylic acid portion, or a combination thereof, comprising from 10 to 30 wt. % of the total Ionomer copolymer weight. Methods of making articles from such compositions. Methods of disposal of such compositions in hot liquid and alkaline conditions.Type: GrantFiled: September 4, 1997Date of Patent: December 19, 2000Assignee: Isolyser Company, Inc.Inventors: Travis W. Honeycutt, Baosheng Lee, Feng Qin, Robert S. Woody
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Patent number: 6140406Abstract: A coating composition for an ink jet recording medium comprises an aqueous suspension of absorptive pigment, a binder, a sizing agent, and a cationic fixing agent. The coating composition combines solids content of greater than 30% with good runnability. The composition may preferably be dispersed at pH values in the range of 4.5 to 7.0. The pigment is preferably a mixture of 75% or more silica gel having a pore volume of 0.5-2.0 cc/g, and 10% or more alumina or alumina hydrate. A method for making down the coating composition includes the sequential steps of dispersing a polyvinyl alcohol binder in water, cooling the binder dispersion, dispersing a sizing agent, and mixing the suspension thoroughly before addition of a cationic fixing agent and pigment.Type: GrantFiled: June 12, 1998Date of Patent: October 31, 2000Assignee: Consolidated Papers, Inc.Inventors: Leonard J. Schliesman, Leland O. Tritz, Karen K. Spreda
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Patent number: 6121362Abstract: A monophase silicone impression composition which crosslinks by an addition reaction, includes the following components:(a) organopolysiloxanes with at least two unsaturated groups in the molecule,(b) organohydrogenpolysiloxanes with at least 2 SiH groups in the molecule,(c) optionally, organopolysiloxane without reactive groups,(d) a platinum catalyst,(e) a hydrophilizing agent,(f) diatomaceous earth,(g) a filler, and(h) optionally further customary additives, auxiliaries and dyestuffs, the amount of component (f) is 8 to 25 wt. %, based on the total weight of the cured composition, and the composition has a Shore hardness A to be determined in accordance with DIN 53505, of less than 45--measured after 30 minutes--, and a viscosity, determined in accordance with ISO 4823, of 31 to 39 mm. The impression composition is suitable for the production of provisional bridges and crowns.Type: GrantFiled: July 16, 1998Date of Patent: September 19, 2000Assignee: ESPE Dental AGInventors: Erich Wanek, Joachim Zech
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Patent number: 6121361Abstract: A composite clay material with the interlayer distance sufficiently expanded by dispersing clay mineral in a low polar polymer on a molecular level and the method for producing the same, blend material and composite clay rubber material using the same and the production method thereof.The composite clay material is formed of a clay mineral rendered compatible with an organic material through ionic bonding to an organic onium ion having 6 or more carbon number and a main guest molecule having a polar group in its main chain and side chain and molecular length equal to or larger than that of said organic onium ion. The main guest molecule is incorporated at least partially into an interlayer section of the clay mineral which has a hydrogen bonding with the polar group of the main guest molecule. The main guest molecule preferably has a molecular weight ranging from about 100 to 100000.Type: GrantFiled: January 7, 1999Date of Patent: September 19, 2000Assignee: Kabushiki Kaisha Toyota Chuo KenkyushoInventors: Arimitsu Usuki, Makoto Kato, Akane Okada
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Patent number: 6107387Abstract: Provided are acidified aqueous stable dispersions of an exfoliated silicate derived from a silicate having a layer lattice structure in which the silicate layer units have a thickness of 5 to 25 Angstroms, wherein the exchange capacity ranges from 30 to 200 millequivalents per gram of silicate having a layer lattice structure, and wherein the silicate materials have been exfoliated with a cationic group-containing polymer or polymer having functional groups which can be post-reacted to form cationic groups. These silicate dispersions are useful in coating compositions, particularly in electrodepositable coating compositions, where they impart improved crater control.Type: GrantFiled: February 22, 1999Date of Patent: August 22, 2000Assignees: PPG Industries Ohio, Inc., Amcol International Corp.Inventors: Alan J. Kaylo, Richard F. Karabin, Tie Lan, Michael G. Sandala
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Patent number: 6106956Abstract: A polymer film comprising at least first and second contiguous and coextruded portions, wherein the first portion is extruded from a first polymer composition containing a filler material in an amount sufficient to increase the water vapor permeability of the first portion relative to the second portion, and the second portion is extruded from a second polymer composition such that a tensile strength of the second portion is greater than the tensile strength of the first portion. Such polymer films allow for highly vapor permeability, while providing portions with sufficient strength to allow for taping or attachment of fastening devices.Type: GrantFiled: January 26, 1998Date of Patent: August 22, 2000Assignee: Exxon Chemical Patents, Inc.Inventors: Hans E. Heyn, Kevin A. Brady
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Patent number: 6103817Abstract: A composite clay material with the interlayer distance sufficiently expanded by dispersing clay mineral in a low polar polymer on a molecular level and the method for producing the same, blend material and composite clay rubber material using the same and the production method thereof. The composite clay material is formed of a clay mineral rendered compatible with an organic material through ionic bonding to an organic onium ion having 6 or more carbon number and a main guest molecule having a polar group in its main chain and side chain and molecular length equal to or larger than that of said organic onium ion. The main guest molecule is incorporated at least partially into an interlayer section of the clay mineral which has a hydrogen bonding with the polar group of the main guest molecule. The main guest molecule preferably has a molecular weight ranging from about 100 to 100000.Type: GrantFiled: January 7, 1999Date of Patent: August 15, 2000Assignees: Kabushiki Kaisha Toyota Chuo Kenkyusho, Denso CorporationInventors: Arimitsu Usuki, Makoto Kato, Akane Okada
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Patent number: 6087016Abstract: Barrier coating mixtures contain in a carrier liquid, (a) an elastomeric (preferably butyl-containing) polymer; (b) a dispersed exfoliated layered filler having an aspect ratio greater than 25; and (c) at least one surfactant, wherein the solids content of the mixture is less than 30% and the ratio of polymer (a) to filler (b) is between 20:1 and 1:1. Coated articles, which are rigid or flexible and elastomeric, and free-standing films and membranes, which are flexible and elastomeric, are produced using the barrier coating mixtures.Type: GrantFiled: June 8, 1998Date of Patent: July 11, 2000Assignees: InMat, LLC, Michelin Recherche et Technique S.A.Inventors: Carrie A. Feeney, Michele Farrell, Klaus Tannert, Harris A. Goldberg, Mengshi Lu, Michael D. Grah, William G. Steiner, Paul B. Winston
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Patent number: 6084005Abstract: An antimicrobial caries-detecting composition, which comprises(i) water, a water-miscible solvent or a combination thereof, (ii) a dye capable of staining the caries-infected portions of teeth, and (iii) at least one antimicrobial agent.Type: GrantFiled: February 24, 1998Date of Patent: July 4, 2000Assignee: Kuraray Co., Ltd.Inventors: Kyoko Fukunishi, Kenichi Hino
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Patent number: 6056897Abstract: Solid form of a stabilizer for organic polymers consisting of one or more tocopherols, as such or in formulation, absorbed on porous polypropylene with a high crystallinity, in a quantity ranging from 30% to 85% by weight. The above tocopherols, as such or in formulation, can also be used in a mixture with other stabilizers such as, for example, secondary antioxidants containing phosphorous or sulfur, sterically hindered phenols and sterically hindered amines.Type: GrantFiled: February 18, 1998Date of Patent: May 2, 2000Assignee: Great Lakes Chemical (Europe) GmbHInventors: Luciano Pallini, Silvestro Costanzi, Carlo Neri, Francesco Groppelli
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Patent number: 6034163Abstract: The present invention relates to a composition comprising a polymer having dispersed therein at least one layered clay material which has been cation exchanged with an organic cation salts represented by Formula I: ##STR1## wherein M represents either nitrogen or phosphorous; X.sup.- represents an anion selected from the group consisting of halogen, hydroxide, or acetate anions, preferably chloride and bromide; R.sub.1 is selected from the group consisting of straight and branched alkyl groups having at least 8 carbon atoms; R.sub.2, R.sub.3, and R.sub.4 are independently selected from straight or branched alkyl groups having 1 to four carbon atoms; and at least one expanding agent which is compatible with said polymer. Preferred polymers include polyesters. The compositions of the present invention show vastly improved platelet separation as evidenced by higher than previously reported basal spacing.Type: GrantFiled: December 22, 1997Date of Patent: March 7, 2000Assignee: Eastman Chemical CompanyInventors: Robert Boyd Barbee, James Christopher Matayabas, Jr., Jack Wesley Trexler, Jr., Rodney Layne Piner
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Patent number: 6017991Abstract: This invention concerns a mixture of a first component selected from talcs and one or more second component(s) selected from diatomaceous earth, natural and synthetic silica, clay, ceramic spheres, volcanic ash and glass cullet wherein the ratio of the component to the second component(s) provides an enhanced abrasiveness property, an enhanced die pressure character, and a reduced melt fracture character. The invention further relates to an antiblock agent made from such mixture that significantly reduces or eliminates the need to provide polymer processing additives. This invention also relates to a masterbatch composition having an admixture such that enhanced die pressure character and/or reduced melt fracture character are obtained.Type: GrantFiled: August 10, 1998Date of Patent: January 25, 2000Assignee: Minerals Technologies Inc.Inventors: Donald Kendall Drummond, Joseph Anthony Radosta, Donald Richard Deutsch
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Patent number: 6013724Abstract: The present invention relates to a paint film embodying a new parameter representing the resistance to raindrop fouling and having very satisfactory fouling resistance, particularly resistance to raindrop fouling, even ultra-low foulability, as well as high water resistance, acid resistance, alkali resistance, and crack resistance; a coating composition capable of providing said paint film; a method for forming a satisfactory paint film using said coating composition; and an article coated with said paint film. A coating composition comprising (I) a tetramethoxysilane partial hydrolyzed condensate and at least one member selected from (A) a film-forming resin and (B) an inorganic binder containing alkoxysilyl as a reactive curing group and having a water dynamic reverse tension (Tr) of not less than 55 dyn/cm; and an antifouling paint film containing the coating composition is provided.Type: GrantFiled: March 5, 1998Date of Patent: January 11, 2000Assignee: Nippon Paint Co., Ltd.Inventors: Keita Mizutani, Yoichi Tozaki, Toshihiro Okai, Hozumi Endou, Takeshi Sawai, Nobuyuki Matsuzoe
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Patent number: 6008295Abstract: Diene polymers or copolymers having improved balance between raw polymer viscosity and mixed compound viscosity, useful in tire tread compositions having highly balanced wet traction, rolling resistance, and traction in ice and snow, and fracture properties in the cured and white carbon reinforced states are provided. These diene polymers or copolymers comprise a mixture of diene polymer or copolymer chains containing carbon-tin bonds in the main polymer or copolymer chains and diene polymer or copolymer chains containing terminals derived from hydrocarboxysilane compounds. The diene polymer or copolymers are prepared by first coupling a portion of the living diene polymer or copolymer chains obtained by anionic polymerization using a tin polyhalide coupling agent and then terminating the remaining living diene polymer or copolymer chains using hydrocarboxysilane compounds.Type: GrantFiled: July 11, 1997Date of Patent: December 28, 1999Assignee: Bridgestone CorporationInventors: Hideo Takeichi, Daniel F. Graves, Sunil B. Sarkar, David F. Lawson
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Patent number: 5998528Abstract: Intercalates formed by contacting the layer material, e.g., a phyllosilicate, with an intercalant to sorb or intercalate the between adjacent platelets of the layered material. Sufficient intercalant polymer is sorbed between adjacent platelets to expand the adjacent platelets at least about 5 .ANG. (as measured after water removal to 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. A monovalent, divalent and/or trivalent cation is added to the intercalating composition, or after intercalation for surprising increases in viscosity. The intercalated complex is combined with an organic liquid into an unexpectedly viscous carrier material, for delivery of the carrier material, or for delivery of an active compound, e.g., a pharmaceutical, or cosmetic, or lubricant, e.g., food grade lubricants dissolved or dispersed in the carrier material.Type: GrantFiled: February 2, 1998Date of Patent: December 7, 1999Assignee: Amcol International CorporationInventors: Semeon Tsipursky, Vladimir Dolinko, Vasiliki Psihogios, Gary W. Beall
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Patent number: 5998506Abstract: The invention provides novel compositions and golf balls formed from those compositions. The compositions generally include a cured blend of an elastomer, a peroxide polymerization agent, a co-agent, and an unsaturated polycarboxylic acid. More particularly, the cured composition includes a cured blend of cis 1,4 polybutadiene, dicumyl peroxide, zinc diacrylate, and fumaric acid. One piece golf balls formed of these compositions have improved durability.Type: GrantFiled: September 12, 1997Date of Patent: December 7, 1999Assignee: Spalding Sports Worldwide, Inc.Inventor: Robert Dennis Nesbitt
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Patent number: 5990234Abstract: The invention provides a liquid composition for coating surfaces, comprising: polymer droplets dispersed in a liquid component, ultraviolet light (UV) absorber, and defoamer. The liquid component comprises water, and volatile organic solvent. The organic solvent comprises a first and a second ether. The first and the second ether are miscible with water. The UV absorber and the defoamer are dispersed in the liquid component. A preferred embodiment of the invention provides the liquid composition with a particulate composition to provide a material for superior non-skid surface coatings, such as non-skid flooring surface coatings. Thus, the invention provides a material for making non-skid coatings, comprising: a particulate composition including wollastonite particles, cellulose particles, and diatomaceous earth particles.Type: GrantFiled: July 30, 1998Date of Patent: November 23, 1999Assignee: BTG, a PartnershipInventors: Robert Stahovic, Anthony J. Pecora
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Patent number: 5973053Abstract: A composite clay material with the interlayer distance sufficiently expanded by dispersing clay mineral in a low polar polymer on a molecular level and the method for producing the same, blend material and composite clay rubber material using the same and the production method thereof.The composite clay material is formed of a clay mineral rendered compatible with an organic material through ionic bonding to an organic onium ion having 6 or more carbon number and a main guest molecule having a polar group in its main chain and side chain and molecular length equal to or larger than that of said organic onium ion. The main guest molecule is incorporated at least partially into an interlayer section of the clay mineral which has a hydrogen bonding with the polar group of the main guest molecule. The main guest molecule preferably has a molecular weight ranging from about 100 to 100000.Type: GrantFiled: May 30, 1996Date of Patent: October 26, 1999Assignee: Kabushiki Kaisha Toyota Chuo KenkyushoInventors: Arimitsu Usuki, Makoto Kato, Akane Okada
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Patent number: 5955517Abstract: The invention relates to a composition comprising a thermoplastic, structurally crosslinked elastomeric or thermosetting polymer, which comprises(a) a polar, adsorptive inorganic or organic material in the form of fibres or particles which are in mutual contact, onto which is adsorptively bound(b) a polar antistatic agent comprising a mixture ofb1) at least one polar organic compound having at least 5 carbon atoms and at least 3 heteroatoms, andb2) the salt of an inorganic protic acid, which is solvated or complexed in the polar organic compound. The invention also relates to a second composition comprising b) a polar inorganic or organic material, b1) a polar organic compound having at least 5 carbon atoms and at least 3 heteroatoms and b2) an inorganic salt, to the use of this second composition for the antistatic treatment of polymers, and to a process for preparing antistatically treated polymers.Type: GrantFiled: July 29, 1998Date of Patent: September 21, 1999Assignee: Ciba Specialty Chemicals CorporationInventors: Bruno Hilti, Markus Burkle, Jurgen Pfeiffer, Ernst Minder, Markus Grob
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Patent number: 5918413Abstract: The present invention is characterized by coating a seed with from 0.1 to 25% by weight of a powder (A) composed of one or both of montmorillonite and bentonite and having an average particle diameter of 30 .mu.m or less and from 99.9 to 75% by weight of a powder (B) composed of a material other than montmorillonite and bentonite and having an average particle diameter of at least 10 .mu.m and at most 30 .mu.m using a polyvinyl alcohol aqueous solution having an aqueous solution viscosity at 25.degree. C. of 50 mPa.multidot.s or less as a binder. Consequently, a coated seed obtained by coating a seed, especially a light-favoured seed, easily absorbs water in sowing and is easily cracked in absorbing water. Further, the easy cracking thereof remains unchanged with the course of time. In the coating, formation of by-product seedless spherical pellets is little observed.Type: GrantFiled: June 9, 1998Date of Patent: July 6, 1999Assignees: Dai-Ichi Kogyo Seiyaku Co., Ltd., Takii Shubyo Kabushiki KaishaInventors: Takamitsu Otani, Hiroyuki Nakata, Toshikazu Akao, Yoshihiro Maeda
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Patent number: 5916944Abstract: Disclosed is a method of forming tamper-proof coatings on electronic devices. The method comprises applying a coating of a silica precursor resin and a filler onto the electronic device, wherein the filler is one which reacts in an oxidizing atmosphere to liberate enough heat to damage the electronic device. The coated electronic device is then heated at a temperature sufficient to convert the silica precursor resin to a silica containing ceramic matrix.Type: GrantFiled: September 29, 1997Date of Patent: June 29, 1999Assignee: Dow Corning CorporationInventors: Robert Charles Camilletti, Loren Andrew Haluska, Keith Winton Michael
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Patent number: 5908890Abstract: The invention relates to the production and use of an agent for use in polymers as an antiblock agent. Pumice with very low amounts of crystalline silica is processed from pumice stone to produce a fine ground pumice with a narrow particle size range. When incorporated into a polyolefin film, the fine ground pumice acts as an antiblock agent while not significantly contributing to haze.Type: GrantFiled: August 8, 1997Date of Patent: June 1, 1999Assignee: CR Minerals CorporationInventor: Arlen C. Cornett
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Patent number: 5902848Abstract: Disclosed are polyolefin films suitable for packaging having Elmendorf values lower than 0.8N in both machine direction and cross direction are obtained from compositions comprising (percentages by weight):A) from 70% to 90% of a polyolefin matrix containing 30% of one or more crystalline propylene homopolymers and/or copolymers having a flexural modulus greater than or equal to 1800 MPa;B) from 10% to 30% of one or more mineral fillers.Type: GrantFiled: March 4, 1997Date of Patent: May 11, 1999Assignee: Montell North America Inc.Inventors: Emanuele Burgin, Nello Pasquini
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Patent number: H1955Abstract: Films, made of polyethylenes and fillers, and articles made therefrom greater WVTR than previously available films based on conventional Ziegler-Natta based polyethylenes. The polyethylenes are produced in a metallocene-catalyzed production process. The films may be made by a cast film process, and may be made in widely varying filler content, generally polyethylene to filler ratios of 30/70 to 70/30. The metallocene based polyethylenes when combined with filler also permit the extrusion of thinner films leading to lighter weight and softer films. The m-polyethylenes utilized for making such films typically have a Composition Distribution Breadth Index above 50%, a Mw/Mn below 3, and a Mz/Mw below 2.Type: GrantFiled: July 31, 1996Date of Patent: April 3, 2001Assignee: Exxon Chemical Patents Inc.Inventors: Jeffrey Alan Middlesworth, Kevin Arthur Brady