Abstract: Process and apparatus for producing vinyl chloride monomer characterized by conjoint chlorination and dehydrochlorination reactions carried out in the presence of fluidized solids which provide efficient heat transfer within and between the two reaction zones.
Type:
Grant
Filed:
February 19, 1976
Date of Patent:
October 28, 1980
Assignee:
The Badger Company, Inc.
Inventors:
Harold R. Sheely, F. Frederick Oricchio, Domenic C. Ferrari
Abstract: A method is disclosed for using a pendulum viscometer having damped torsional oscillations, in a laboratory catalytic fluid-bed reactor, to monitor a propensity to stick which is exhibited by certain supported catalysts. A fluid-bed of such catalysts has been found to become suddenly more sticky just before a point at which a change in pressure drop across the fluid-bed can be measured due to a process "upset". At this point ("the inversion point"), the upset is usually irremediable. The method includes correlating data on catalyst stickiness from a laboratory reactor operating at atmospheric pressure, with an expected level of catalyst stickiness in a commercial reactor operating at elevated pressure.A pendulum viscometer and related auxiliary apparatus is disclosed for magnetically and electrically measuring and recording the rate at which the pendulum's torsional oscillations are damped.
Type:
Grant
Filed:
October 6, 1978
Date of Patent:
October 7, 1980
Assignee:
The B. F. Goodrich Company
Inventors:
Joseph A. Cowfer, Dane E. Jablonski, Ronald M. Kovach, Angelo J. Magistro