Devitrifying Glass Or Vitrifying Crystalline Glass (e.g., Starting With Or Forming Crystalline Glass, Etc.) Patents (Class 65/33.1)
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Patent number: 12053215Abstract: The present disclosure provides a bone-implantable device and methods of use. The bone-implantable device comprises a body having an exterior surface, wherein a portion of the exterior surface includes a cured osteostimulative material comprising MgO.Type: GrantFiled: December 28, 2022Date of Patent: August 6, 2024Assignee: Bone Solutions, Inc.Inventors: Frankie Morris, Drew Diaz, Brandon Roller
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Patent number: 11984555Abstract: Provided is a method for producing a sulfide-based solid electrolyte with a balance between the ion conductivity of the sulfide-based solid electrolyte and the heat generation amount of an electrode layer containing the sulfide-based solid electrolyte during an electrode reaction. Disclosed is a method for producing a sulfide-based solid electrolyte comprising a sulfide glass-based material that contains at least one lithium halide compound selected from the group consisting of LiI, LiBr and LiCl, the method comprising immersing the sulfide glass-based material, which is at least one sulfide glass-based material selected from the group consisting of a sulfide glass and a glass ceramic, in an organic solvent having a solubility parameter of 7.0 or more and 8.8 or less, for 1 hour to 100 hours.Type: GrantFiled: March 17, 2023Date of Patent: May 14, 2024Assignee: TOYOTA JIDOSHA KABUSHIKI KAISHAInventors: Naoki Osada, Ayano Kobayashi
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Patent number: 11952303Abstract: A quartz glass body and a process for the preparation of a quartz glass body is disclosed. One process includes providing a silicon dioxide granulate from a pyrogenic silicon dioxide powder, making a glass melt out of the silicon dioxide granulate and making a quartz glass body out of at least part of the glass melt. In at least one process a silicon component different from silicon dioxide is added. A quartz glass body is obtainable by this process. A light guide, an illuminant and a formed body, are each obtainable by further processing of the quartz glass body.Type: GrantFiled: December 16, 2016Date of Patent: April 9, 2024Assignee: Heraeus Quarzglas GmbH & Co. KGInventors: Nigel Robert Whippey, Marcus Constantin Göbel, Boris Gromann, Gerrit Scheich
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Patent number: 11540866Abstract: The present disclosure provides a bone-implantable device and methods of use. The bone-implantable device comprises a body having an exterior surface, wherein a portion of the exterior surface includes a cured osteostimulative material comprising MgO.Type: GrantFiled: July 24, 2020Date of Patent: January 3, 2023Assignee: Bone Solutions, Inc.Inventors: Frankie L. Morris, Drew Diaz
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Publication number: 20150111030Abstract: A process for producing a chemically strengthened glass is provided. The method for producing a chemically strengthened glass includes subjecting a phase-separated glass to an ion exchange treatment. A chemically strengthened glass which is obtained by the process and a phase-separated glass which has been subjected to the ion exchange treatment are also provided.Type: ApplicationFiled: October 27, 2014Publication date: April 23, 2015Applicant: ASAHI GLASS COMPANY, LIMITEDInventors: Junko MIYASAKA, Takahiro SAKAGAMI, Seiki OHARA, Kosho AKATSUKA, Manuel Diaz REYES, Kazutaka ONO, Hiroyuki HIJIYA
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Publication number: 20150110701Abstract: A low cost process is provided for creating high purity silicon from agricultural waste, particularly rice hull ash. The process uses a series of chemical and thermal steps to yield high purity silica while using less energy and more efficient chemical processes. The high purity silicon features fewer impurities that negatively affect the use of high purity for PV cells and reduces capital and operating costs of processes to yield ultra-pure silicon.Type: ApplicationFiled: October 20, 2014Publication date: April 23, 2015Inventors: Richard M. Laine, Julien C. Marchal
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Patent number: 8986841Abstract: A process for reinforcing a glass-ceramic article, into which a maximum tension is introduced beneath the surface of the glass-ceramic, advantageously in proximity to said surface. The invention also relates to an enamel that can be used for this reinforcement, this enamel being formed from a glass frit having the following composition, the proportions being expressed as weight percentages: SiO2 50-66% MgO 3-8% Na2O ?7-15% K2O 0-3% Li2O ?0-12% CaO ?0-10% BaO ?0-15% Al2O3 0-3% ZrO2 0-3% ZnO 0-5% B2O3 0-8% the sum of the alkaline-earth metal oxides CaO+BaO moreover being between 8 and 15%, and the sum of the alkali metal oxides Na2O+K2O+Li2O moreover being between 7 and 20%. The reinforced glass-ceramics obtained by the process.Type: GrantFiled: January 10, 2014Date of Patent: March 24, 2015Assignee: Eurokera S.N.C.Inventors: Stephanie Pelletier, Marie-Helene Chopinet, Caroline Faillat, Marie-Helene Rouillon, Pablo Vilato
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Patent number: 8959954Abstract: A process for producing proppants from waste mineralogical material. The process can include providing the waste mineralogical material in a form such as particles, fines, dust, powders, and the like, and forming a plurality of “green” pellets from the waste mineralogical material. Thereafter, the plurality of green pellets are fed into a provided flame drop tower that has a combustion flame, a hot zone, and a collection basin located downstream from the hot zone. The plurality of green pellets pass through the hot zone, are melted and subsequently solidified in the shape of a sphere downstream from the hot zone to form vitrified glass spheres. In some instances, the vitrified glass spheres are subjected to a devitrification step.Type: GrantFiled: January 17, 2013Date of Patent: February 24, 2015Assignee: The Penn State Research FoundationInventors: Ryan P. Koseski, John R. Hellmann, Barry E. Scheetz
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Patent number: 8936732Abstract: A white light emitting glass-ceramic. The chemical formula of the glass-ceramic is aSiO2.bAl2O3.cNaF.dCeF3.nDyF3.mAg, wherein a, b, c, d, n and m are, by mol part, 25-50, 15-30, 10-30, 10-25, 0.01-1 and 0.01-1, respectively, and a+b+c+d-100. A method for producing said glass-ceramic is also provided. Silver ion is doped in the glass-ceramic in the form of silver particles by means of sintering and reduction annealing treatment, and thus the luminescence properties of rare earth ion is improved.Type: GrantFiled: July 22, 2010Date of Patent: January 20, 2015Assignee: Ocean's King Lighting Science & Technology Co., Ltd.Inventors: Mingjie Zhou, Wenbo Ma, Fangyi Weng
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Patent number: 8893525Abstract: An apparatus for manufacturing tempered glass. A transportation unit transports a glass substrate that is intended to be tempered. An ionizer ionizes alkali oxides in the glass substrate by radiating energy onto the glass substrate. A dielectric heating unit increases the temperature of the inner portion of the glass substrate in which the alkali oxides are ionized by the ionizer.Type: GrantFiled: December 27, 2011Date of Patent: November 25, 2014Assignee: Samsung Corning Precision Materials Co., Ltd.Inventors: Hoikwan Lee, Seo-Yeong Cho, Yoon Young Kwon, Kyungwook Park, Kyungmin Yoon, Jongsung Lee, Jaeyoung Choi, Gennady Kizevich
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Patent number: 8883330Abstract: A glass for use in chemical reinforcement for use in a substrate of an information recording medium, having a composition comprising, denoted as mol %: SiO2 47 to 70%? Al2O3 1 to 10% (where the total of SiO2 and Al2O3 is 57 to 80%) CaO 2 to 25% BaO 1 to 15% Na2O 1 to 10% K2O 0 to 15% (where the total of Na2O and K2O is 3 to 16%) ZrO2 1 to 12% MgO 0 to 10% SrO 0 to 15% (where the ratio of the content of CaO to the total of MgO, CaO, SrO, and BaO is greater than or equal to 0.5) ZnO 0 to 10% (where the total of MgO, CaO, SrO, BaO, and ZnO is 3 to 30%) TiO2 0 to 10% and the total content of the above-stated components is greater than or equal to 95%. A glass for use in chemical reinforcement for use in the substrate of an information recording medium employed in a perpendicular magnetic recording system, in which the glass exhibits the glass transition temperature is greater than or equal to 600° C.Type: GrantFiled: February 7, 2011Date of Patent: November 11, 2014Assignee: Hoya CorporationInventors: Mikio Ikenishi, Xuelu Zou
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Publication number: 20140318184Abstract: Provided herein is a method for producing glass-ceramic sheets. The method includes texturing at least one surface of a first glass sheet, and stacking the first glass sheet and a second glass sheet. The first glass sheet and the second glass sheet are stacked so that the textured surface of the first glass sheet contacts a surface of the second glass sheet. The first and second glass sheets are cerammed. After cooling, the cerammed first and second glass sheets are separated. Also provided is a pre-form for producing glass-ceramic sheets. The pre-form includes a first glass sheet having a textured surface, and a second glass sheet contacting the first glass sheet. The textured surface of the first glass sheet is in contact with a surface of the second glass sheet.Type: ApplicationFiled: April 30, 2013Publication date: October 30, 2014Applicant: Corning IncorporatedInventors: Sumalee Likitvanichkul, William Edward Lock, Sophie Peschiera
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Patent number: 8815403Abstract: A method for producing a silica container having a rotational symmetry is provided. The method includes forming a preliminarily molded article by feeding a powdered substrate's raw material to an inner wall of an outer frame having aspiration holes with rotating the frame, and forming a silica substrate. The preliminarily molded article is aspirated from an outer peripheral side with controlling a humidity inside the outer frame by ventilating gases present in the outer frame with charging from inside the preliminarily molded article a gas mixture comprised of an O2 gas and an inert gas and made below a prescribed dew-point temperature by dehumidification, and at the same time heated from inside the preliminarily molded article by a discharge-heat melting method with carbon electrodes, thereby making an outer peripheral part of the preliminarily molded article to a sintered body while an inner peripheral part to a fused glass body.Type: GrantFiled: June 25, 2010Date of Patent: August 26, 2014Assignee: Shin-Etsu Quartz Products Co., Ltd.Inventors: Shigeru Yamagata, Tomomi Usui
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Publication number: 20140228196Abstract: Lithium silicate glass ceramics and glasses containing specific oxides of divalent elements are described which crystallize at low temperatures and are suitable in particular as dental materials.Type: ApplicationFiled: October 11, 2012Publication date: August 14, 2014Applicant: Ivoclar Vivadent AGInventors: Christian Ritzberger, Elke Apel, Wolfram Höland, Volker Rheinberger
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Publication number: 20140190211Abstract: A method of forming fused quartz glass is provided. The method includes the steps of: (a) providing a starting body made of fused quartz glass; (b) positioning the fused quartz glass starting body on a base plate; (c) inserting a first insert device into an interior cavity of the starting body to form an assembled structure; (d) heating the assembled structure to a predetermined temperature at which the fused quartz glass has a viscosity in a range of 105 to 1013 poise; and (e) deforming the fused quartz glass of the starting body at the predetermined temperature or in the viscosity range of 105 to 1013 poise around the first insert device to change a shape of the starting body. A method for making a large fused quartz glass vessel and a forming assembly for forming fused quartz glass are also provided.Type: ApplicationFiled: January 8, 2013Publication date: July 10, 2014Applicant: HERAEUS QUARTZ AMERICA LLCInventor: Matthew Donelon
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Patent number: 8771530Abstract: A method for producing a polarizing element includes: forming particulate materials of a metal halide on a glass substrate; forming a protective film that covers the particulate materials in a non-plasma environment; stretching the particulate materials by heating and stretching the glass substrate; and forming acicular metal particles by reducing the metal halide constituting the stretched particulate materials.Type: GrantFiled: February 22, 2013Date of Patent: July 8, 2014Assignee: Seiko Epson CorporationInventor: Yoshitomo Kumai
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Publication number: 20140141205Abstract: A method for producing a conversion element for an optical and/or optoelectronic component is provided. The method may include at least: providing a transparent substrate, applying a layer, which contains powdered glass solder, vitrifying the layer by a first temperature treatment, whereby the glass solder of the layer is vitrified and thus converted into a transparent glass material having little intrinsic coloration, applying a phosphor-containing material to the layer, and performing a second temperature treatment, whereby phosphor of the phosphor-containing material sinks into the glass material of the layer.Type: ApplicationFiled: July 4, 2012Publication date: May 22, 2014Applicant: OSRAM GMBHInventors: Angela Eberhardt, Christina Wille
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Patent number: 8728961Abstract: A method is described for making a float glass convertible into a glass ceramic, by which a largely crystal fault-free glass can be produced. In this method the glass is cooled from a temperature (TKGmax), at which a crystal growth rate is at a maximum value (KGmax), to another temperature (TUEG), at which practically no more crystal growth occurs, with a cooling rate, KR, in ° C. min?1 according to: KR UEG KGmax ? ? ? ? T UEG KGmax 100 · KG ? ? max , wherein ?T=TKGmax?TUEG, and KGmax=maximum crystal growth rate in ?m min?1. The float glass has a thickness below an equilibrium thickness, a net width of at least 1 m and has no more than 50 crystals with a size of more than 50 ?m, especially no crystals with a size of more than 10 ?m, per kilogram of glass within the net width.Type: GrantFiled: July 27, 2011Date of Patent: May 20, 2014Assignee: Schott AGInventors: Gerhard Lautenschlaeger, Andreas Langsdorf, Ulrich Lange, Bernd Ruedinger, Klaus Schneider, Michael Jacquorie, Friedrich Siebers, Wolfgang Schmidbauer
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Publication number: 20140128241Abstract: Glass-ceramics comprising Al2O3 and rare earth oxide, yttrium oxide, and/or alkaline earth oxide. Uses of the glass-ceramics include dental articles, orthodontic appliances, abrasive particles, cutting tools, infrared windows, and ceramic bearings.Type: ApplicationFiled: June 22, 2012Publication date: May 8, 2014Applicant: 3M INNOVATIVE PROPERTIES COMPANYInventors: Anatoly Z. Rosenflanz, Jean A. Tangeman
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LIGHT-DIFFUSING PLATE, METHOD OF FABRICATING THE SAME AND LED ILLUMINATION DEVICE INCLUDING THE SAME
Publication number: 20140119050Abstract: A light-diffusing plate, a method of fabricating the same and a light-emitting diode (LED) illumination device including the same. The light-diffusing plate allows incident light to pass through, with the incident light diffused and scattered by the light-diffusing plate. The light-diffusing plate is made of crystallized glass in which crystals that diffuse and scatter the incident light are formed.Type: ApplicationFiled: October 25, 2013Publication date: May 1, 2014Applicant: Samsung Corning Precision Materials Co., Ltd.Inventors: Kiyeon Lee, Jhee-Mann Kim, Jaeho Lee -
Patent number: 8650907Abstract: The method produces a reshaped glass-ceramic article by forced reshaping of a flat green glass part during a ceramicizing process with temporarily lowered viscosity due to crystallization heat. To perform the forced reshaping economically the forced reshaping takes place in a continuous oven for ceramicizing and in an oven section in which the viscosity of the green glass part is temporarily lowered as a result of crystallization heat. An apparatus for performing the process is provided in the continuous oven including different active reshaping devices and/or a hollow mold. The method produces glass-ceramic articles with undamaged surfaces corresponding to surfaces produced during the making of the green glass part (smooth or structured, e.g. knobbed).Type: GrantFiled: July 17, 2008Date of Patent: February 18, 2014Assignee: Schott AGInventors: Martin Taplan, Herwig Scheidler, Ioannis Kosmas, Friedrich-Georg Schroeder, Wolfgang Schmidbauer, Torsten Gabelmann, Dieter Schoenig
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Publication number: 20140000314Abstract: Lithium silicate glass ceramics and glasses are described which can advantageously be applied to zirconium oxide ceramics in particular by pressing-on in the viscous state and form a solid bond with these.Type: ApplicationFiled: September 6, 2013Publication date: January 2, 2014Applicant: Ivoclar Vivadent AGInventors: Christian Ritzberger, Ricardo Dellagiacomo, Marcel Schweiger, Harald Bürke, Wolfram Höland, Volker Rheinberger
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Publication number: 20130334957Abstract: The invention provides a tin phosphate glass containing embedded luminescent material particles, wherein the luminescent material particles comprise luminescent material from the class of CaAlSiN 3:Eu 2+ and optionally other luminescent material particles. The invention further provides a method for the production of such glass as well as a lighting unit using such glass as (part of) a light conversion unit.Type: ApplicationFiled: February 28, 2012Publication date: December 19, 2013Applicant: KONINKLIJKE PHILIPS N.V.Inventors: Lucas Johannes Anna Maria Beckers, Paulus Hubertus Gerardus Offermans
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Publication number: 20130283858Abstract: Methods for selecting titania-doped quartz glass which experiences a reduction in OH group concentration of less than or equal to 100 ppm upon heat treatment at 900° C. for 100 hours as suitable material for the EUV lithography member.Type: ApplicationFiled: June 18, 2013Publication date: October 31, 2013Applicant: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Shigeru Maida, Hisatoshi Otsuka, Tetsuji Ueda, Masanobu Ezaki
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Publication number: 20130274085Abstract: Crystallizable glasses, glass-ceramics, IXable glass-ceramics, and IX glass-ceramics are disclosed. The glass-ceramics exhibit ?-spodumene ss as the predominant crystalline phase. These glasses and glass-ceramics, in mole %, include: 62-75 SiO2; 10.5-17 Al2O3; 5-13 Li2O; 0-4 ZnO; 0-8 MgO; 2-5 TiO2; 0-4 B2O3; 0-5 Na2O; 0-4 K2O; 0-2 ZrO2; 0-7 P2O5; 0-0.3 Fe2O3; 0-2 MnOx; and 0.05-0.2 SnO2. Additionally, these glasses and glass-ceramics exhibit the following criteria: a. a ratio: [ Li 2 ? O + Na 2 ? O + K 2 ? O + MgO + ZnO ] [ Al 2 ? O 3 + B 2 ? O 3 ] ?between 0.7 to 1.5; b. a ratio: [ TiO 2 + SnO 2 ] [ SiO 2 + B 2 ? O 3 ] ?greater than 0.04. Furthermore, the glass-ceramics exhibit an opacity ?about 85% over the wavelength range of 400-700 nm for an about 0.Type: ApplicationFiled: March 15, 2013Publication date: October 17, 2013Inventors: George Halsey Beall, Marie Jacqueline Monique Comte, George Owen Dale, Linda Ruth Pinckney, Charlene Marie Smith, Ronald Leroy Stewart, Steven Alvin Tietje
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Patent number: 8536078Abstract: Lithium silicate glass ceramics and glasses containing at least 6.1 wt.-% ZrO2 are provided which can advantageously be applied to zirconium oxide ceramics in particular by pressing-on in the viscous state and forming a solid bond with the zirconium oxide ceramics.Type: GrantFiled: April 5, 2011Date of Patent: September 17, 2013Assignee: Ivoclar Vivadent AGInventors: Christian Ritzberger, Ricardo Dellagiacomo, Marcel Schweiger, Harald Burke, Wolfram Holand, Volker Rheinberger
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Publication number: 20130237400Abstract: A glass-ceramic having at least two crystal phases, wherein at least one crystal phase has a positive temperature dependence of the resonance frequency ?f, at least one crystal phase has a negative temperature dependence of the resonance frequency ?f and the glass-ceramic has a resulting temperature dependence of the resonance frequency ?f of 0 ppm/K with a maximum deviation of +/?20 ppm/K, is described. Furthermore, a process for producing such a glass-ceramic and the use of the glass-ceramic are described.Type: ApplicationFiled: March 12, 2012Publication date: September 12, 2013Applicant: SCHOTT AGInventors: Martin Letz, Stephan Knoener, Martina Dressler, Daniela Seiler, Bernd Hoppe, Michael Kluge
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Publication number: 20130224493Abstract: A lithium-containing, transparent glass-ceramic material is provided. The material has low thermal expansion and has an amorphous, lithium-depleted, vitreous surface zone. The zone is at least 50 nm thick on all sides and encloses a crystalline interior, which has high transmission. The material includes a transition region connecting the zone and the interior.Type: ApplicationFiled: July 7, 2011Publication date: August 29, 2013Applicant: SCHOTT AGInventors: Falk Gabel, Otmar Becker, Michael Glasenapp, Jan-Peter Ortmann, Petra Grewer, Veit Luther, Harald Striegler, Dietmar Wennemann, Thomas Schuler, Thoralf Johansson, Helga Goetz, Michael Bug, Guenther Benhaar, Gerhard Hahn, Friedrich-Georg Schroeder
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Patent number: 8516851Abstract: In order to obtain glass or glass ceramic materials having increased strength, the invention provides a method for producing glass or glass ceramic articles, which comprises the steps: producing an initial glass body (11), mounting the initial glass body (11) on a gas cushion (13) between a levitation support (1) and the initial glass body (11), and at least partially ceramizing the initial glass body (11) on the levitation support (1). The levitation support comprises at least one continuous surface region (3) having at least one gas feed region (151, 152, 153) where levitation gas for the gas cushion (13) is fed out from the levitation support, and at least one gas discharge region (171 172, 173) where gas from the gas cushion (13) is at least partially discharged into the levitation support.Type: GrantFiled: December 9, 2005Date of Patent: August 27, 2013Assignee: Schott AGInventors: Sybill Nuettgens, Wolfgang Schmidbauer, Roland Dudek, Friedrich Georg Schroeder, Gerhard Hahn, Markus Borrmann, Helga Goetz
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Publication number: 20130209963Abstract: Lithium silicate materials are described which can be easily processed by machining to dental products without undue wear of the tools.Type: ApplicationFiled: March 15, 2013Publication date: August 15, 2013Inventor: Ivoclar Vivadent AG
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Publication number: 20130167589Abstract: A fused silica body comprising a layer of vitreous silica adjacent at least a portion of an inner surface is described in embodiments herein. In other embodiments, a method of making a fused silica body with a layer of vitreous silica adjacent at least a portion of an inner surface is described herein, comprising heating at least a portion of the inner surface to the point of vitrification. In certain embodiments, the method involves passing a linear local heat source over the inner surface in a particular manner, such as a helical fashion transverse to the linear shape, and may involve creating on the inner surface of the body overlapping swaths of temporarily melted silica material.Type: ApplicationFiled: March 1, 2013Publication date: July 4, 2013Applicant: RAYTHEON COMPANYInventor: RAYTHEON COMPANY
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Patent number: 8461068Abstract: Described herein are glass ceramic compositions with bulk scattering properties that have improved light extraction properties due to high levels of diffuse transmission, and methods of making such glass ceramic compositions. The compositions are based on Li2O—Al2O3—SiO2 glass ceramics and with the proper crystal size, exhibit good volume scattering characteristic for visible light and enhance the outcoupling from the substrate to the air in optical devices, such as light emitting diodes.Type: GrantFiled: April 13, 2010Date of Patent: June 11, 2013Assignee: Corning IncorporatedInventors: Etienne Almoric, Marie Jacqueline Monique Comte, Micaela Nazaraly, Lothar Wondraczek
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Publication number: 20130133377Abstract: A known method for producing synthetic quartz glass comprises the method steps of: forming a stream of a SiO2 feedstock material which contains octamethylcyclotetrasiloxane (D4) as the main component which has a reference molecular mass assigned to it, feeding the stream to a reaction zone in which the feedstock material is converted under formation of amorphous SiO2 particles by pyrolysis or hydrolysis into SiO2, depositing the amorphous SiO2 particles on a deposition surface while forming a porous SiO2 soot body, and vitrifying the SiO2 soot body while forming the synthetic quartz glass.Type: ApplicationFiled: November 23, 2012Publication date: May 30, 2013Applicant: HERAEUS QUARZGLAS GMBH & CO. KGInventors: Heinz Fabian, Juergen Roeper
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Publication number: 20130130886Abstract: A matrix for a thermostructural fibrous composite material obtained by geopolymer synthesis based on nanocrystalline cristobalite resulting from the crystallization of geopolymer micelles of potassium polysiloxonate K—(Si—O—Si—O)n. The nanocrystalline cristobalite is in the form of micelles and/or microspheres having dimensions of less than 1 micron, preferably of less than 500 nanometers, connected together by an amorphous phase. The matrix 4 contains at least 85 percent by weight of oxide SiO2 with at most 15%, preferably at most 10%, by weight of alkali metal oxide K2O. The nanocrystalline cristobalite results from the crystallization of geopolymer micelles of potassium polysiloxonate by a heat treatment at a temperature preferably between 600° C. and 800° C., for a time of less than 30 minutes. The fibrous composite material impregnated with this matrix is thermostructural.Type: ApplicationFiled: March 28, 2011Publication date: May 23, 2013Applicant: PYROMERAL SYSTEMS S.A.Inventor: M. Michel Davidovics
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Publication number: 20130055764Abstract: A crystal growth furnace is disclosed herein and includes a top cover, a body and a bottom portion. The top cover is configured to be moved by a top cover shifting mechanism. The body is configured to be moved vertically by a body shifting mechanism. The bottom portion is configured to be moved from the bottom of the crystal growth furnace by a bottom portion shifting mechanism and used to carry a crucible. When the top cover, the body and the bottom portion are connected together to be the crystal growth furnace, a silicon material disposed within the crucible is grown to be an ingot.Type: ApplicationFiled: September 6, 2011Publication date: March 7, 2013Applicant: REAL GREEN MATERIAL TECHNOLOGY CORP.Inventor: Wen-Yuan Chang
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Patent number: 8359886Abstract: A process for increasing toughness of glass particulates is provided. The process includes providing an aluminosilicate glass particulate, the glass particulate generally having the form of a sphere, and heating the glass particulate to a temperature greater than 600° C. for a predetermined time. Thereafter, the glass particulate can be cooled to ambient temperature and the heating step can alter the failure mechanism of the glass particulate from a high energy failure that produces generally fine powder to a lower energy failure that produces generally large fragments. The glass particulate can be an amorphous glass particulate and may or may not have a nominal composition that corresponds to rhyolite, basalt, tholeiite, olivine and/or andesite.Type: GrantFiled: August 3, 2009Date of Patent: January 29, 2013Assignee: The Penn State Research FoundationInventors: Ryan P. Koseski, John R. Hellmann, Barry E. Scheetz
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Publication number: 20120297830Abstract: A method for improving the thermo-mechanical properties of an aluminum-titanate composite, the composite including at least one of strontium-feldspar, mullite, cordierite, or a combination thereof, including: combining a glass source and an aluminum-titanate source into a batch composition; and firing the combined batch composite composition to produce the aluminum-titanate composite. Another method for improving the thermo-mechanical properties of the composite dips a fired composite article into phosphoric acid, and then anneal the dipped composite article. The resulting composites have a thin glass film situated between the ceramic granules of the composite, which can arrest microcrack propagation.Type: ApplicationFiled: May 27, 2011Publication date: November 29, 2012Inventors: Monika Backhaus-Ricoult, Christopher Raymond Glose
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Publication number: 20120291492Abstract: A consecutive molding method for crystallized glass comprises: a melting process to obtain molten glass by melting glass raw materials; a molding process to obtain a band-shaped plate glass by roll forming the molten glass to become band-shaped; a crystallization process to obtain a band-shaped crystallized glass plate by conducting thermal treatment on the band-shaped plate glass to crystallize it; and a cutting process to cut the band-shaped crystallized glass plate, wherein the crystallization process includes: a temperature-raising process to produce the band-shaped crystallized glass plate by disposing the band-shaped plate glass obtained in the molding process, in the atmosphere of a crystal nucleus-formation temperature and raising the temperature to a crystal-growth temperature or above to grow crystals as well as form crystal nuclei; and a slow-cooling process to slowly cool down the band-shaped crystallized glass plate.Type: ApplicationFiled: March 9, 2012Publication date: November 22, 2012Applicants: Ta Hsiang Containers Ind. Co., Ltd., a Taiwan Corporation, Huzhou Ta Hsiang Glass Products Co., Ltd., a China CorporationInventors: Kuo-Chuan Hsu, Yan-Bin Jiang, Chao Qu
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Patent number: 8283060Abstract: To provide a substrate for information recording medium having various properties, in particular higher fracture toughness, required for application of the substrate for information recording medium of the next generation such as perpendicular magnetic recording system, etc. and a material with excellent workability for such purpose. A crystallized glass substrate for information recording medium, consisting of a crystallized glass which comprises one or more selected from RAl2O4 and R2TiO4 as a main crystal phase, in which R is one or more selected from Zn, Mg and Fe, and in which the main crystal phase has a crystal grain size in a range of from 0.5 nm to 20 nm, a degree of crystallinity of 15% or less, and a specific gravity of 3.00 or less.Type: GrantFiled: June 2, 2010Date of Patent: October 9, 2012Assignee: Ohara Inc.Inventors: Toshitaka Yagi, Naoyuki Goto
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Publication number: 20120247151Abstract: An apparatus for producing a layer of vitreous silica adjacent at least a portion of an inner surface of a fused silica body is described, comprising a heat source disposed to apply sufficient heat to at least a portion of the inner surface to cause a layer of said at least a portion of the inner surface to vitrify. In certain embodiments the heat source is configured to heat at one time a relatively small area of the inner surface, and the apparatus comprises a positioning mechanism for moving the heat source with respect to the inner surface. In certain embodiments the heat source is a hydrogen-oxygen surface-mix fueled torch that is moved helically with respect to the inner surface of the body under the control of a programmed CNC motion control system.Type: ApplicationFiled: March 31, 2011Publication date: October 4, 2012Inventors: Allen L. Kelly, Christopher K. Solecki, Kevin M. Chapla, William C. Strauss
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Publication number: 20120251745Abstract: A fused silica body comprising a layer of vitreous silica adjacent at least a portion of an inner surface is described in embodiments herein. In other embodiments, a method of making a fused silica body with a layer of vitreous silica adjacent at least a portion of an inner surface is described herein, comprising heating at least a portion of the inner surface to the point of vitrification. In certain embodiments, the method involves passing a linear local heat source over the inner surface in a particular manner, such as a helical fashion transverse to the linear shape, and may involve creating on the inner surface of the body overlapping swaths of temporarily melted silica material.Type: ApplicationFiled: March 31, 2011Publication date: October 4, 2012Inventors: Derrick J. Rockosi, Richard Gentilman, Chrostopher K. Solecki, Allen L. Kelly, William C. Strauss, Brian Gahan
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Publication number: 20120228561Abstract: Provided is the method for producing, by heat treating raw material powder, a lithium ion secondary battery positive electrode material which contains an olivine-structure crystal represented by general formula LiMxFe1-xPO4 (where 0?x<1 and M is at least one type selected from Nb, Ti, V, Cr, Mn, Co and Ni), wherein the raw material powder contains trivalent iron compound. The present invention allows for stably producing at reduced cost a lithium ion secondary battery positive electrode material which contains olivine-type LiMxFe1-xPO4 crystal.Type: ApplicationFiled: November 11, 2010Publication date: September 13, 2012Applicants: NATIONAL UNIVERSITY CORPORATION NAGAOKA UNIVERSITY OF TECHNOLOGY, NIPPON ELECTRIC GLASS CO., LTD.Inventors: Tomohiro Nagakane, Akihiko Sakamoto, Tsuyoshi Honma, Takayuki Komatsu
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Patent number: 8241395Abstract: Disclosed are processes for preparing conductive glass-ceramic membranes and methods of using them in hydrogen or proton separation.Type: GrantFiled: June 11, 2008Date of Patent: August 14, 2012Assignee: Schott CorporationInventors: Mark J. Davis, Samuel David Conzone, Paula Vullo
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Publication number: 20120198889Abstract: A manufacturing method of a glass strip, the method including a heating and drawing process of heating and softening a glass plate preform, drawing the glass plate preform to have a desired thickness, and forming a glass strip, wherein at the heating and drawing process, the glass plate preform is drawn so that an internal pressure of a heating furnace is kept positive relative to an atmospheric pressure and so that gas flows introduced to both surfaces of the glass plate preform, respectively are equal to each other within the heating furnace.Type: ApplicationFiled: April 20, 2012Publication date: August 9, 2012Applicant: THE FURUKAWA ELECTRIC CO., LTD.Inventors: Toshihiro Nakamura, Tetsuya Kumada, Yasuhiro Naka
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Publication number: 20120189918Abstract: A sulfide solid electrolyte with excellent ion conductivity and a method for producing a crystallized glass contained in the sulfide solid electrolyte. A sulfide solid electrolyte comprising a crystallized glass represented by the following chemical formula yLi2S.(100-x-y)P2S5.xP2O5, wherein 0<x<25 and 67<y<80.Type: ApplicationFiled: August 31, 2010Publication date: July 26, 2012Applicant: TOYOTA JIDOSHA KABUSHIKI KAISHAInventors: Masahiro Tatsumisago, Akitoshi Hayashi, Shigenori Hama, Koji Kawamoto, Takamasa Ohtomo
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Publication number: 20120167479Abstract: An abrasive element consisting substantially of a glass material that is at least partially devitrified.Type: ApplicationFiled: September 9, 2011Publication date: July 5, 2012Inventors: Steven Bradley Vaughan, Philip James Harrison
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Patent number: 8211817Abstract: Fused silica glass having an internal transmittance of UV with 245 nm wavelength, being at least 95% at 10 mm thickness, a OH content of not larger than 5 ppm, and a content of Li, Na, K, Mg, Ca and Cu each being smaller than 0.1 ppm. Preferably the glass has a viscosity coefficient at 1215° C. of at least 1011.5 Pa·s; and a Cu ion diffusion coefficient of not larger than 1×10?10 cm2/sec in a depth range of greater than 20 ?m up to 100 ?m, from the surface, when leaving to stand at 1050° C. in air for 24 hours. The glass is made by cristobalitizing powdery silica raw material; then, fusing the cristobalitized silica material in a non-reducing atmosphere. The glass exhibits a high transmittance of ultraviolet, visible and infrared rays, has high purity and heat resistance, and exhibits a reduced diffusion rate of metal impurities, therefore, it is suitable for various optical goods, semiconductor-production apparatus members, and liquid crystal display production apparatus members.Type: GrantFiled: September 11, 2007Date of Patent: July 3, 2012Assignees: Tosoh Corporation, Tosoh SGM CorporationInventors: Kazuyoshi Arai, Tsutomu Takahata, Shinkichi Hasimoto, Masahito Uchida, Nobusuke Yamada, Yoshinori Harada, Hideharu Horikoshi
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Patent number: 8201421Abstract: To obtain an optical component having excellent secondary optical nonlinear properties by irradiating a surface and/or inside of glass having at least one member selected from Ni, Fe, V, Cu, Cr and Mn as a heat source material for absorbing and converting a laser beam to heat, incorporated to a glass matrix comprising at least one glass-forming oxide-selected from SiO2, GeO2, B2O3, P2O5, TeO2, Ga2O3, V2O5, MoO3 and WO3 and at least one member selected from alkali metals, alkaline earth metals, rare earth elements and transition elements, with a laser beam with a wavelength to be absorbed by the heat source material, to convert the irradiated portion to a single crystal or a group of crystal grains comprising components contained in the glass matrix and not containing the heat source material, thereby to form a pattern.Type: GrantFiled: August 11, 2008Date of Patent: June 19, 2012Assignees: Asahi Glass Company, Limited, Nagaoka University of TechnologyInventors: Takayuki Komatsu, Tsuyoshi Honma, Takumi Fujiwara, Yasuhiko Benino
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Patent number: 8198201Abstract: Transparent ?-quartz glass-ceramics containing vanadium oxide. Such glass-ceramics have advantageous optical properties including good transmission in the infrared range, low transmission in the visible range, and significant transmission in the blue range for thicknesses of 3 mm. They can be used as materials for cooking top plates.Type: GrantFiled: May 28, 2010Date of Patent: June 12, 2012Assignee: EurokeraInventors: Marie Jacqueline Monique Comte, Philippe Lehuede, Isabelle Marie Chauvel-Melscoet, Daniel Louis Gabriel Ricoult
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Patent number: 8196429Abstract: In order to provide method and apparatus for manufacturing a vitreous silica crucible with little mixing of foreign matter and stable arc during arc melting, the method and apparatus for manufacturing a vitreous silica crucible have a device which blows off air from the side of arc electrodes toward a melting space of a mold, and air discharge ports which discharge the air within the heating furnace, and perform forced supply of air into the melting space during melting to make the atmospheric pressure of the melting space higher than the surroundings, and preferably, form an air pressure difference of 100 Pa or more between the melting space and the surroundings, thereby performing melting.Type: GrantFiled: July 25, 2008Date of Patent: June 12, 2012Assignee: Japan Super Quartz CorporationInventors: Takeshi Fujita, Minoru Kanda