Abstract: An improved method for isolating the impacts of flow-altering events in corrosion transport from those due to steady state corrosion in boiler/steam cycle processes. The method includes monitoring, in real time, with a particle counter or particle monitor levels of suspended particles in a fluid flow stream and of automatically collecting insoluble particulates large enough to be captured on a 0.45 micron filter when, and only when, these levels exceed an “event threshold”. For use in subsequently characterizing flow-altering events without necessarily weighing the collected particulates for each excursion above this threshold, an average particle count/particle index is obtained and compared with the actual weight of insoluble particulates captured. When excursions are highly infrequent, concentrations of insoluble metal oxides likely to be present in the flow stream and capable of producing above-threshold PC/PIs can be determined and used to identify anomalies when particulates are captured.

Abstract: An optical gas concentration sensor and method for measuring blood gas based on the light adsorption sensing technique are disclosed. The optical gas concentration sensor comprises a light source, a photo detector, and a gas filtering membrane for separating the indicator and a liquid. A gas in the liquid diffuses to the indicator through the gas filtering membrane so as to change the color of the indicator due to the chemical reaction occurred between the indicator and the gas. Then, the photo detector receives the light passing though the reacted indicator from the light source. The gas concentration is determined based on pH-sensitive absorbance spectrum of the indicator.

Abstract: A membrane-introduction mass spectrometer (MIMS) device has a sample inlet assembly provided with a membrane held by an outer retaining ring across the entrance of a central passage, a porous metal frit backing the membrane, and a cylindrical support piece supporting the frit. In a preferred embodiment, the membrane is a 10-micron thickness layer of silicone evenly coated upon an inert polymer backing material. The porous frit is a titanium or steel sponge metal. The cylindrical support piece is made of titanium with small, drilled thru-holes to allow passage of gases and volatile organics into the mass spectrometer. The sample inlet assembly includes a high-pressure temperature probe for sensing fluid temperature to correct for temperature variations in membrane diffusion rates. The sample inlet assembly is provided as a front end to an underwater sampling probe.

Abstract: A detector for the detection for trace vapors and particles in the air that includes a housing; a well formed in the housing; a heated filter positioned across the well; a source delivering sampled air substantially perpendicular to the open end of the well on a first side of the filter; a source to supply dry air across the first side of the filter; a detector line in communication with the at least one well on a second side of the filter; and a second dry air source for supplying air to the second side of the filter at a pressure below atmospheric pressure. An automatic inspection station that includes a vibrator for vibrating articles to be inspected. An automatic inspection station that includes a heating element positioned below an upper surface of the floor and an inlet positioned above the floor.

Abstract: A device for sampling drill cuttings includes a frame, an inclined perforated member mounted on the frame, a sprayer for washing cuttings down over the perforations, and a removable open-topped cuttings collector mounted under the perforated member, the perforated member cooperating with the downstream end of a vibratory screen over which the cuttings pass before translating onto the perforated screen.

Abstract: A portable microbial gaseous-fluid sampler includes a gaseous-fluid flow system at least partially supported by a structure. The gaseous-fluid flow system includes a gaseous-fluid intake portion having an intake port, a blower in fluid communication with the intake port, and a gaseous-fluid exhaust portion having an exhaust port. The sampler can further include an exhaust filter operable to substantially filter a totality of the gaseous fluid flowing through the sampler prior to exhausting the gaseous fluid. The sampler also can include a control system operable to control at least gaseous-fluid flow through the sampler, and a remote sampling head.

Abstract: The invention provides a system and method comprising an apparatus for removing contaminants from a gas in a semiconductor processing device, which can include a filter unit having at least two parallel filter stages located therein. The filter stages are designed to remove a least a portion of the contaminants present in the gas flowing through them. The apparatus can also include a flow controller for distributing the gas flow among the filter stages. In one embodiment, the controller may consist of a diffuser plate. The invention also provides a sampling tube orifice for gas flow control in a system or method of the invention. In another embodiment, an apparatus for removing contaminants from a gas in a clean room comprises a filter unit having at least two parallel filter stages, which are used to remove a portion of the contaminants in the gas as it passes through the apparatus.

Abstract: A sampling and analysis device comprises a housing, a sampling region and an analysis region being defined within the housing. The housing has at least one aperture to allow fluid ingress to and egress from the sampling region. A filter is disposed within the housing, and is movable inside the housing between a sampling position, located in the sampling region, and an analysis position, located in the analysis region.

Abstract: The invention relates to a sorbent collector material based on polyorganosiloxane for the microextraction of substances to be analysed, the collector material having an open-cell foam structure, and to a collector and a liner which include this collector material.

Abstract: The present invention is a filter apparatus with methods to capture a desired amount of material suspended in a liquid or gas for monolayer deposition, analysis or other uses. Novel filter devices are employed to capture material which may be used for the purification or enrichment of various sample constituents or captured material may be observed or analyzed. Alternatively, particulate material may be used as a transport mechanism for proteins or chemicals which in turn may be assessed or used. The filter device employs sensors to sense pressure and adjust, halt or otherwise control sample flow. The pressure sensor essentially monitors the flow rate of sample suspension through a filter, typically responding at a predetermined pressure associated with capture of a desired amount of material on the filter. A separate valve or valve integrated with pressure sensing provides a means to adjust sample flow.

Abstract: A sampling system for separating gaseous samples from a gas stream containing particulate matter and transporting the gaseous samples to a location outside of the flowing gas stream comprises an inertial filter mounted on the end of a hollow probe, the inertial filter positioned within the flowing gaseous stream. The inertial filter comprises a filter media mounted within a tube such that a portion of the particulate-containing gaseous steam flows through an annular space between the filter media and the tube wall, the gas to be sampled passes through the filter media into an inner space and the filtered gas is then delivered through the hollow probe to analytical devices external to the space containing the flowing gas stream, such as a flue stack.

Abstract: A method for analyzing particulate contaminant on a part comprises: applying a pressurized liquid onto the part on which the particulate contaminant is to be analyzed, wherein applying the pressurized liquid provides a dispersed spray of pressurized liquid; collecting an applied volume of the pressurized liquid; providing the applied volume onto a filter apparatus; and providing the filter apparatus for performing analysis of the particulate contaminant.

Abstract: A device and a method for measuring fluid flow and solute mass transport in flow systems includes a casing (1) having inlet (3) and outlet (9) openings and a fluid passageway therebetween, the casing containing at least one fluid permeable insoluble adsorbent matrix (7) and at least one tracer material (5, 5?) located in the fluid passageway. The tracer material (5,5?) is a fluid permeable partially soluble material which at least prior to installation is not physically or chemically bonded to the adsorbent matrix (7) and is either mixed with the adsorbent matrix or is located in at least one section (4,4?) of the casing (1) separate from but in contact with at least one section (6,6?) of the casing holding the insoluble adsorbent matrix (7,7?). The device is intended to be installed in a medium having a fluid path therein.

Abstract: A device and method for detecting anthrax or other pathogens are disclosed. Individual self-contained monitoring devices of a monitoring system can be portable or stationary (e.g. installed in air ducts or plumbing of buildings) and can be part of a network of devices. Monitoring devices may be used for the detection of a variety of airborne or surface pathogens, including but not limited to anthrax, smallpox, and Salmonella. Bioamplification-coupled proteomics assays provide rapid and reliable detection of pathogens, with self-checking capabilities reducing or eliminating false positives and false negatives. Sample preservation capability allows pathogen samples to be preserved after detection for further testing. The device of the invention can be remotely operated by minimally trained technicians or security personnel.

Abstract: A monitoring device for use in monitoring the life of a filter used in the operating unit of an air conditioning system. The monitoring device has a support for use in attaching the device to the housing of the operational unit in the air conditioning system, the unit having a least one air conditioning filter holding filter material. At least one tubular arm attached to the support, each arm having an air inlet and an air outlet. The support is mounted in a manner to have a portion of the air passing through the air conditioning unit pass through the arm on the support as well. A sample filter is provided along with mounting means for removably mounting the sample filter on the arm to have air passing through the arm also pass through the sample filter. The sample filter holds the same filter material as the air conditioning filter.

Abstract: A sampling system that contains filter components for collecting and concentrating vapor and particles in high-volume flows. The sample is then vaporized and delivered to a detector at a low-volume flow. The invention also has a sampling probe that contains an air-jet to help dislodge particles from surfaces and a heating lamp to help vaporize compounds on surfaces or objects. The sampling system is especially useful for screening for explosives and other illicit chemicals and toxins on people, baggage, cargo, and other objects.

Abstract: A method and system for controllably releasing contaminants from a contaminated porous metallic mesh by thermally desorbing and releasing a selected subset of contaminants from a contaminated mesh by rapidly raising the mesh to a pre-determined temperature step or plateau that has been chosen beforehand to preferentially desorb a particular chemical specie of interest, but not others. By providing a sufficiently long delay or dwell period in-between heating pulses, and by selecting the optimum plateau temperatures, then different contaminant species can be controllably released in well-defined batches at different times to a chemical detector in gaseous communication with the mesh. For some detectors, such as an Ion Mobility Spectrometer (IMS), separating different species in time before they enter the IMS allows the detector to have an enhanced selectivity.

Abstract: Solid phase extraction articles, well-less filtration devices, and methods of manufacturing the articles and devices are disclosed. Methods of extracting analytes from samples using the articles and devices are also disclosed. The articles, devices and methods include a solid phase extraction medium (SPE medium) that incorporates thermoplastic material, e.g., in the form of thermoplastic particles enmeshed within a fibril matrix.

Abstract: A probe for sampling a soil gas comprising a body having a cavity to which is connected an inlet and an outlet, and a gas permeable waterproof membrane wrapped around the body and sealing the cavity. The membrane allows the soil gas to flow across the membrane from the soil to the cavity. A method for measuring soil gas diffusivity comprising the step of circulating in a closed loop a carrier gas substantially at an atmospheric pressure through a diffusion gas sampling probe inserted in the soil and through a sensor used for the measurement of a concentration of at least a component of the soil gas.

Abstract: A device for sampling drill cuttings includes a frame, an inclined perforated member mounted on the frame, a sprayer for washing cuttings down over the perforations, and a removable open-topped cuttings collector mounted under the perforated member, the perforated member cooperating with the downstream end of a vibratory screen over which the cuttings pass before translating onto the perforated screen.

Abstract: An assembly for monitoring and locating leaks in an installation includes a collecting line formed of a material that is impermeable to a substance to be monitored. The collecting line has a multiplicity of openings spaced apart in its longitudinal direction. The openings are closed with a filter element of a sintered metallic material that is permeable to the substance and has been subjected to a heat treatment in an oxidizing atmosphere.

Abstract: A method that allows an individual to personally test for contaminants in an air supply. The method consists of purchasing the test kit, placing the test kit on a device that produces air circulation and blowing air through the test kit. The test kit is then removed from the device, repackaged and sent to a laboratory for analysis. The air quality test kit comprises a test filter, a filter backing pad and a support, which together form a device that captures and retains particles carried in an airflow.

Abstract: The present invention provides a funnel collector for use with a sample testing device. The funnel collector collects and holds a fluid sample in order to place the sample in immediate contact with a diagnostic test strip, which reacts with the sample in a known fashion.

Abstract: A method for characterizing contaminants within sediment comprising positioning a sampler in a continuous manner within the sediment, exposing the sampler to the sediment for a dwell time, retrieving the sampler, and analyzing the sampler. The sampler is exposed to the sediment for a sufficient period of time to allow at least one analyte of interest to permeate the sampler. The sampler may be analyzed using fluorescence and/or gas chromatography/mass spectrometry to determine contamination versus sampler length. The contamination versus sampler length may be converted to contamination versus depth or contamination versus horizontal position.

Abstract: A filter housing assembly for exhaust applications and method of testing the same is provided. In one embodiment, the filter housing assembly includes a housing having a filter receiving aperture, a first air flow port configured to couple the housing to an exhaust system and a second air flow port sized to deliver a flow capable of providing at least 75 feet per minute of air flow through the filter receiving aperture. A filter element is sealingly disposed in the filter receiving aperture of the housing. A cap is provided that operably seals the second air flow port when not in use. In another embodiment, a method for testing a filter housing assembly for exhaust applications includes providing air through a filter element disposed in the housing in a direction opposite an operational air flow direction, leak testing the filter element from a roomside of the filter element, and, flowing air through the filter element after leak testing in the operational direction.

Abstract: A method for withdrawing and filtering a partial volume of a particle-containing process fluid enclosed in a container, a combination of a container enclosing a process fluid and an assembly for continuously withdrawing and filtering a partial volume of a process fluid and a cross-flow filtering device are disclosed. The method, the assembly and the filtering device can be used in connection with biological process systems, in which the removal of sand, sludge, fibers and alike from partial volumes of the process fluid is necessary before additional filtration and subsequent sample analysis.

Abstract: A sampling system for detecting an analyte, comprising a diaphragm pump, a buffer chamber, a sensor head and intake port. The pump includes a chamber for receiving fluids via first and second ports. A buffer chamber is located at the second port for holding a quantity of air, and a sensor head is adapted to identify the presence of a desired analyte and produce a signal in response to the quantity identified. Preferably the diaphragm pump has a volume of gas per stroke capacity slightly larger than the volume of the sensor head such that the pump chamber has a greater volume than the buffer chamber and the buffer chamber has about the same volume as the sensor head. A sensor intake port intakes a sample potentially containing the analyte for contact with the sensor head upon operation of the diaphragm pump and out of the sensor head by jet-action caused by rapid movement of the diaphragm pump. A filter may be used for filtering air drawn through the pump chamber.

Abstract: A sampling device is disclosed. The sampling device is portable and capable of taking two samples in parallel. The sampling device can include two filter locations that are subjected to similar environmental conditions. The sampling device design facilitates easy assembly and disassembly, and can be designed so that a single filter holder design can be used in both filter locations.

Abstract: A method and apparatus for testing formations surrounding an earth borehole. The method includes the following steps: providing a tool movable through the borehole; providing a flow line in the tool; establishing fluid communication between the formations and the flow line of the tool; and providing a sand trap in communication with the flow line of the tool for trapping sand flowing with fluid from the formations.

Abstract: An adapter for use with a low volume PUF sampler is described. The adapter is affixed over the open end of a PUF (polyurethane foam) sample cartridge. Sample tubing is affixed to an aperture in the adapter, and the free end of the sample tubing is then positioned at a desired sample location such as within an aircraft interior. As a vacuum is applied to the PUF cartridge, the adapter allows air collected at the sample point to pass through the tubing and through the interior of the PUF cartridge while preventing air surrounding the PUF cartridge from being drawn into the PUF cartridge except through the sample tubing. In this manner the sample point of a desired air sample can be selected at a point remote from the PUF cartridge. Additionally, use of multiple PUF cartridges and adapters allows the simultaneous collection of separate air samples.

Abstract: A sheet form membrane probe, an apparatus and method, wherein the probe includes a probe body, a sheet-form membrane secured to the probe body and including an open surface exposed to the exterior of the probe; a channel formed between the probe body and the membrane through which a collector fluid can flow; an inlet port opening to the channel to conduct collector fluid to the channel; and an outlet port spaced from the inlet port such that the collector fluid passes through the channel from the inlet port to the outlet port in a flow direction substantially parallel to the membrane. The channel may be formed to provide broad surface contact of the collector fluid with the membrane. The membrane open surface may include an active area open to a sample fluid and open on an opposite side for contact with collector fluid flow in the channel. The active area may be large relative to the total membrane area to provide for an effective use of the expensive membrane material.

Abstract: A container for receiving fluids comprises a body having opposite ends and at least one wall defining an interior space. At least one seal defines a sealed chamber within the interior space of the body. Each seal is recessed from one of the ends of the body and has a sealing connection with the wall of the body. A cap sealingly closes each end of the body having a seal recessed therefrom.

Abstract: A device having a processing chamber, for electroelution and/or dialysis of a substance carried in a sample with respect to an external liquid medium. The chamber has a closed end and an opening at the other end, sufficiently large to permit a sample, particularly a gel contained sample, to be inserted thereto. The chamber has two portals, each laterally disposed with respect to the opening. A tubular membrane covers the portals, and is sealingly fixed onto an outside surface of the housing. The device provides high yield recovery, saves time and allows for easy handling, especially regarding loading an unloading of small volume samples for dialysis, or inserting the gel slice containing the macromolecule sample. The device may be partially immersed in the liquid medium, with the opening above the liquid surface. Optionally, the device may be hermetically sealed via a cap, and fully immersed in the liquid medium.

Abstract: The present invention is for processing fluids, especially waste streams from nuclear power plants, and other fluid media that may be carrying valuable or useful substances, in order to collect the substances. The system uses sequential filtering and multiple passes to concentrate the substances, which allows the system to collect virtually all of the substances of interest to the user while reducing the volume of both the unwanted materials as well as the desired materials desired without affecting the purity of the fluid after processing. Additionally, the collected substances can be processed in-place, and without requiring any thermal processing prior to disposal of unwanted substances, or for the recovery and/or reuse of valuable substances.

Abstract: An apparatus for collecting biological aerosols from an air sample is provided comprising an air intake assembly adapted to draw the air sample into the apparatus, a separation section coupled to the intake assembly and adapted to separate aerosol particles from the air sample, a capture section coupled to the separation section and adapted to transport the aerosol particles in a stream of liquid, and a hydrophobic membrane disposed between the separation section and the capture section and adapted to establish a controllable air/fluid boundary therebetween.

Abstract: An aquatic passive sampling device is disclosed comprising a diffusion-limiting membrane and a receiving phase itself comprising an immobilised solid phase material supported by a solid support. The solid support and membrane features enable the device to be adapted for use forcontinuously monitoring a variety of micropollutants, including polar organic, non-polar organic and inorganic analytes. Furthermore, the analytes may be collected by short column extraction rather than batch extraction.

Abstract: A closed fluidic sampling system. The system includes a first port for receiving a sample of fluid and a sampling chamber in fluid communication with the first port. A a one-way valve allows fluid to flow from the first port towards the sampling chamber while preventing backflow of fluid towards the first port. A second port in fluid communication with the sampling chamber enables fluid to be withdrawn from the sampling chamber. The fluid may be a blood component, such as platelets, plasma, whole blood, or red blood cells.

Abstract: A system for the collection and initial conditioning of sample gas for “on-line” analyzers, or filling of gas sample cylinders. The preferred embodiment of the present invention contemplates a system configured to obtain a representative gas phase sample from a process gas containing entrained liquid, or a process gas which generally is susceptible to partial condensation of some gas phase components. The preferred embodiment of the present invention teaches a sample probe assembly including a heat pipe configured for maintaining sample gas drawn through said sample probe at or near the source gas temperature and pressure. Accuracy of the analysis of source gas stream is enhanced and compositional changes of the gas phase are avoided by preventing the partial condensation of gas components or vaporization of entrained liquid.

Abstract: The present invention relates to apparatus for sampling and analysis of gas phase molecules. A source of negative pressure is used to draw gas phase molecules through a gas-permeable membrane. The gas phase molecules are then directed into an analyzer, suitably a gas chromatograph.

Abstract: A system for the retrieval and initial conditioning of sample gas for “on line” analyzers or filling of gas sample cylinders. The preferred embodiment of the present invention contemplates a system configured to obtain a representative gas phase sample from a process gas containing entrained liquid, or a process gas which generally is highly susceptible to partial condensation of some gas phase components. The preferred embodiment of the present invention teaches an assembly including a phase separation membrane and housing configured to facilitate the removal of entrained liquid from a sample gas stream. Accuracy of the sample is enhanced, and compositional changes are avoided by first extracting a sample from the process gas followed by removal of entrained liquid it may contain, with the entrained liquid removal being conducted at the prevailing process gas pressure and temperature. Thereafter the liquid free sample may be desaturated by lowering its pressure to reduce its susceptibility to condensation.

Abstract: The invention relates to a filtering device for taking a filtrate sample from liquid matter containing solid particles. The filtering device comprises two filter parts and at least one filtering slot between the filter parts. The filter parts are adapted to move in relation to each other in such a manner that the width of the filtering slot changes when the filter parts move in relation to each other. When taking a sample from a process, the filtering slot between the filter parts is at its smallest, and it is adapted to filter the sample while the liquid matter being measured flows from the process to the measurement. When rinsing the filtering device against the sampling direction, the filter parts are adapted to move away from each other, whereby the filtering slot widens.

Abstract: A slurry monitoring system is provided. A filter encompasses a filter chamber containing a purge piston. During a monitor operation, the purge piston is retracted, and slurry enters the filter chamber through the filter, then passes into an outlet pipe, where a characteristic of the slurry is monitored by a monitoring device. During a purge operation, a flush valve is opened to allow water to pass into the filter chamber through an inlet pipe. The purge piston is extended to force filtered slurry from the filter chamber. The water dilutes filtered slurry remaining in the filter chamber. The flush valve is then closed and the purge piston retracted. This forces diluted slurry to pass out of the filter. This purges the filter. Diluted slurry also passes into the outlet pipe, which purges the outlet pipe and monitoring device.

Abstract: A fluid stream sampler enables variable flow rate controlled air sampling, as an attachment to a vacuum source, typically a household vacuum cleaner. The fluid stream sampler includes a housing body having a vacuum outlet opening and a sampling port inlet. A volumetric flow rate indicator is disposed in the flowpath between the vacuum outlet opening and the sampling port inlet. An adjustable damper panel interposed in the flowpath regulates the vacuum pressure within the housing body. In operation, a vacuum imparted by the vacuum source directs a fluid stream along the flowpath between the vacuum outlet opening and the sampling port inlet such that, upon moving the damper panel to a desired position within the flowpath, a desired volumetric flow rate is achieved as measured by the indicator. The desired volumetric flow rate corresponds to a preferred flow rate specified for a fluid constituent sampling medium interposed in the flowpath at the sampling port inlet.

Abstract: The device and methods relate to a sampling device for obtaining samples of analytes in a difficult-to-reach sampling location, such as below ground or underwater, and transporting the sample to an accessible delivery or collection site. The sampling device comprises a semipermeable membrane-based sampling chamber, which can be positioned under the ground or water surface where analytes of interest can permeate into the chamber through the semipermeable membrane. Transfer channels, which communicate with the sampling chamber, is used to transport the sample to the surface for analysis without removing the chamber from the sampling location.

Abstract: A portable system for the detection of chemical particles such as explosive residue utilizes a metal fiber substrate that may either be swiped over a subject or placed in a holder in a collection module which can shoot a jet of gas at the subject to dislodge residue, and then draw the air containing the residue into the substrate. The holder is then placed in a detection module, which resistively heats the substrate to evolve the particles, and provides a gas flow to move the particles to a miniature detector in the module.

Abstract: A self sealing air sampling apparatus includes a body with a filter therein and an air moving device, such as a fan, mounted therein for moving air through the filter. There is an air inlet communicating with the filter. There is also a air outlet communicating with the filter. A manually operable control simultaneously opens the air inlet and the air outlet and operates the air moving device for moving air from the air inlet, through the filter and out through the air outlet. For example, the body may be cylindrical and have a cylindrical shell rotatably mounted thereon. The shell and the body have air inlet openings and air outlet openings which are aligned when the shell is rotated in one direction and become unaligned when the shell is rotated in an opposite direction thus sealing off the filter compartment from the outside environment. Rotation of the shell also closes a switch to operate the fan when the shell is rotated in the one direction.

Abstract: A suction lysimeter for sampling subsurface liquids includes a lysimeter casing having a drive portion, a reservoir portion, and a tip portion, the tip portion including a membrane through which subsurface liquids may be sampled; a fluid conduit coupled in fluid flowing relation relative to the membrane, and which in operation facilitates the delivery of the sampled subsurface liquids from the membrane to the reservoir portion; and a plurality of tubes coupled in fluid flowing relation relative to the reservoir portion, the tubes in operation facilitating delivery of the sampled subsurface liquids from the reservoir portion for testing. A method of sampling subsurface liquids comprises using this lysimeter.

Abstract: A liquid separator for a respiratory gas sample analyzer includes a closed container having a liquid trap filter chamber integral with the container. The liquid trap filter chamber includes an inlet compartment and an outlet compartment. The inlet compartment is interposed between a sample inlet port and a sample outlet port and includes a gas permeable, liquid impermeable filter element for separating liquid from a gas sample, the liquid separated from the gas sample passing to a collection chamber. The outlet compartment includes a further gas permeable, liquid impermeable trap filter element which is interposed between the collection chamber and a low pressure port, for preventing the flow of liquid through the output compartment to the low pressure port.

Abstract: A method and apparatus are provided for adsorbing surface-active compounds, such as corrosion inhibitors and water, from pressurized gas streams utilizing existing gas pipeline sampling valves. The apparatus includes an adsorption trap assembly containing an adsorption material packing, such as silica gel, fixedly positioned to selectively adsorb any surface-active compound(s)or water in the gas stream passing through the trap. After sampling, the adsorption material packing is removed and treated to desorb any entrained compound(s) for recovery, testing and identification. The method and apparatus have particular utility in determining the presence of corrosion inhibitors that have been added to petroleum pipelines upstream of the sampling point(s).

Abstract: An apparatus and method for preconcentrating particles and vapors. The preconcentrator apparatus permits detection of highly diluted amounts of particles in a main gas stream, such as a stream of ambient air. A main gas stream having airborne particles entrained therein is passed through a pervious screen. The particles accumulate upon the screen, as the screen acts as a sort of selective particle filter. The flow of the main gas stream is then interrupted by diaphragm shutter valves, whereupon a cross-flow of carrier gas stream is blown parallel past the faces of the screen to dislodge the accumulated particles and carry them to a particle or vapor detector, such as an ion mobility spectrometer. The screen may be heated, such as by passing an electrical current there through, to promote desorption of particles therefrom during the flow of the carrier gas. Various types of screens are disclosed.