Oxide Of Aluminum(al), Beryllium(be), Magnesium(mg), Alkaline Earth Metal, Scandium(sc), Yttrium(y), Lanthanide Metal, Actinide Metal, Titanium (ti), Zirconium(zr), Or Hafnium(hf) Patents (Class 75/235)
  • Patent number: 5004714
    Abstract: The present invention relates to a novel method of manufacturing a composite body, such as a ZrB.sub.2 --ZrC--Z composite body, by utilizing a post-treatment technique. Moreover, the invention relates to novel products made according to the process. The novel process modifies at least a portion of a composite body by exposing said body to a source of second metal.
    Type: Grant
    Filed: January 13, 1989
    Date of Patent: April 2, 1991
    Assignee: Lanxide Technology Company, LP
    Inventors: Terry D. Claar, William B. Johnson, Robert A. Rapp
  • Patent number: 5004498
    Abstract: A dispersion strengthened copper alloy containing a copper matrix, and dispersion particles dispersed in the copper matrix within a range of 0.5 to 6 vol %. In this alloy, an average diameter of a matrix region where the dispersion particles are not present is 0.3 .mu.m or less, and the total amount of solid solution elements contained in the copper matrix is determined such that, when this amount of the solid solution elements is added to pure copper, the electric conductivity of the matrix is lowered by 5% IACS or less.
    Type: Grant
    Filed: October 10, 1989
    Date of Patent: April 2, 1991
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Keizo Shimamura, Kagetaka Amano, Tatsuyoshi Aisaka, Satoshi Hanai, Kohsoku Nagata
  • Patent number: 4999336
    Abstract: There is provided a substantially fully dense powdered metal composite comprising a highly conductive metal or metal alloy matrix having dispersed therein discrete microparticles of a refractory metal oxide and discrete macroparticles of a mechanical or physical property-conferring additive material. The respective components undergo minimal alloying or interdispersion because sintering is not utilized in forming the composite. These composites are characterized by high thermal or electrical conductivity and a desired property (controlled thermal expansion, high strength, wear and arc erosion resistance, or magnetic) attributable to the composite forming material, like refractory metal, alloy, or compound. The composites are useful in forming lead frames for integrated circuit chips, electric lamp lead wires, electrical contact members, and discrete component leads.
    Type: Grant
    Filed: June 17, 1988
    Date of Patent: March 12, 1991
    Assignee: SCM Metal Products, Inc.
    Inventors: Anil Nadkarni, Prasan K. Samal, James E. Synk
  • Patent number: 4999049
    Abstract: An electrically resistive track suitable for use as a heating element consists of a thick film including a base metal constituent and a glass constituent. The thick film has in the temperature range of from 20.degree. C. to 600.degree. C. a temperature coefficient of resistance (TCR) less than 0.0050 per degree C. Suitable metal constituents include tungsten, molybdenum, a mixture of nickel and tungsten and a mixture of nickel and chromium.
    Type: Grant
    Filed: July 18, 1988
    Date of Patent: March 12, 1991
    Assignee: Thorn EMI plc
    Inventors: Simon N. Balderson, Alan R. Atterbury
  • Patent number: 4985401
    Abstract: A superconductor is produced by electric discharge explosion flame spraying of a composite body of constituents of an immiscible alloy. The electrically discharged composite body is deposited on a substrate and the resultant alloy is oxidized to yield an oxide of the alloy having superconductive property. This process can be applied to the Ln-Ba-Cu system (Ln is at least one of the rare earth elements including Y), typically the Y.sub.1 Ba.sub.2 Cu.sub.3 - or Y.sub.2 Ba.sub.4 Cu.sub.8 system, or other immiscible alloy systems such as the Bi-(Ca, Sr)-Cu system to form an oxide thereof.
    Type: Grant
    Filed: February 24, 1989
    Date of Patent: January 15, 1991
    Assignee: Aisin Seiki Kabushiki Kaisha
    Inventors: Akira Sawaoka, Ryuichi Matsuda, Tadashi Kondo
  • Patent number: 4983572
    Abstract: A superconductive body of an oxidic superconductive material having good mechanical properties is characterized in that the oxidic material forms a matrix through which finely divided particles are mixed at least the surface of which consists of a metal or a metal alloy. Particles in the form of fibres are preferably used and the surface of the particles consists of silver or gold.
    Type: Grant
    Filed: August 25, 1988
    Date of Patent: January 8, 1991
    Assignee: U.S. Philips Corporation
    Inventor: Gijsbertus De With
  • Patent number: 4983574
    Abstract: Conductor in strip, sheet or wire form with an electrical conductivity of at least 0.85.times.10.sup.6 .OMEGA..sup.-1 cm.sup.-1 at 77.degree. K. composed of a composite material of a metal matrix (1) and particles (2) composed of a high-temperature superconductor of the type RE Ba.sub.2 Cu.sub.3 O.sub.6.5-7.5 embedded therein and arranged rectilinearly in the longitudinal direction, RE generally denoting a rare earth metal. Preferably RE=yttrium and specifically the substance YBa.sub.2 Cu.sub.3 O.sub.7 and the particle diameter=0.1-100 .mu.m, more narrowly 0.2-20 .mu.m. Optionally an additional metal sheath which envelops the body forming the matrix (1).
    Type: Grant
    Filed: July 20, 1988
    Date of Patent: January 8, 1991
    Assignee: BBC Brown Boveri AG
    Inventor: Gundolf Meyer
  • Patent number: 4981511
    Abstract: A compound or composite powder which includes metallic or ceramic whiskers embedded in a metallic or ceramic matrix as host material, the whiskers have a length between 5.times.10.sup.-6 m and 2.times.10.sup.-4 m and diameters between 2.times.10.sup.-7 m and 1.times.10.sup.-5 m, and are embedded in the matrix with a volume proportion of whisker content between 1 to 50% (by volume), the reference being to a pore-free compacted compound/composite material; the whiskers being made of SiC, Si.sub.-3 N.sub.-4, Al.sub.-2 O.sub.-3 or ZrO.sub.-2 and are embedded in a ceramic matrix being Al.sub.-2 O.sub.-3, Al.sub.-2 O.sub.-3 +from 5 to 40% ZrO.sub.-2 +from 0 to 5% Y.sub.-2 O.sub.-3 or ZrO.sub.-2 with 3 to 15% Y.sub.-2 O.sub.-3 or Si-nitride or Si-carbide. Alternatively the whiskers are made of Si.sub.-3 N.sub.-4, Al.sub.-2 O.sub.-3, ZrO.sub.-2 or W and the matrix is made of W, Mo, Fe, Ni, Co, Cu or an alloy thereof.
    Type: Grant
    Filed: May 16, 1988
    Date of Patent: January 1, 1991
    Assignee: Dornier System GmbH
    Inventors: Rainer Schmidberger, Tilman Haug, Reinhard Marquardt, Juergen Bocan
  • Patent number: 4973356
    Abstract: The present invention relates to a method of preparing an alloy for use as a cutting tool material comprising hard principles and binder phase by which a uniform distribution of the hard principles in the binder phase is obtained, and the resulting product.
    Type: Grant
    Filed: October 23, 1989
    Date of Patent: November 27, 1990
    Assignee: Sandvik AB
    Inventors: Peder von Holst, Hakan Morberg, Rolf Oskarsson
  • Patent number: 4966625
    Abstract: A composite comprises of a sintered matrix of spinel ferrite and an electrically conductive phase of elemental silver is produced by co-firing a laminated structure of ferrite powder-containing tapes containing a silver metallization-forming material having two end portions wherein only the end portions are exposed.
    Type: Grant
    Filed: June 5, 1989
    Date of Patent: October 30, 1990
    Assignee: General Electric Company
    Inventors: Richard J. Charles, Achuta R. Gaddipati
  • Patent number: 4964907
    Abstract: A process is provided for the production of a sintered body. The process includes the following consecutive steps: (i) mixing and kneading one or more metal powders and/or one or more alloy powder with a binder into a compound, said metal and alloy powders having an average particle size not greater than 30 .mu.m, (ii) injection-molding the compound into a green body; (iii) debinding the green body to form a debound body; and (iv) subjecting the debound body to first-stage sintering at 1,050.degree.-1,250.degree. C. in a reducing or reduced-pressure atmosphere and then to second-stage sintering at a temperature in a range of 1,100.degree.-1,400.degree. C. which is higher than that of the first-stage sintering. This process can provide sintered Ti bodies and sintered magnetic bodies of the Fe-Si type, which have a density ratio of at least 95%.
    Type: Grant
    Filed: August 14, 1989
    Date of Patent: October 23, 1990
    Assignee: Kawasaki Steel Corp.
    Inventors: Yoshisato Kiyota, Junichi Ohta, Hiroshi Ohtsubo, Shigeaki Takajo
  • Patent number: 4961778
    Abstract: Substantially dense, void-free ceramic-metal composites are prepared from components characterized by chemical incompatibility and non-wetting behavior. The composites have a final chemistry similar to the starting chemistry and microstructures characterized by ceramic grains similar in size to the starting powder and the presence of metal phase. A method for producing the composites requires forming a homogeneous mixture of ceramic-metal, heating the mixture to a temperature that approximates but is below the temperature at which the metal begins to flow and presssing the mixture at such pressure that compaction and densification of the mixture occurs and an induced temperature spike occurs that exceeds the flowing temperature of the metal such that the mixture is further compacted and densified. The temperature spike and duration thereof remains below that at which significant reaction between metal and ceramic occurs. The method requires pressure of 60-250 kpsi employed at a rate of 5-250 kpsi/second.
    Type: Grant
    Filed: January 13, 1988
    Date of Patent: October 9, 1990
    Assignee: The Dow Chemical Company
    Inventors: Aleksander J. Pyzik, Irving G. Snyder, Jr., Alexander Pechenik, Robert R. McDonald
  • Patent number: 4948676
    Abstract: The present invention provides a ceramic/metal composite material comprising cerium/aluminum mixed oxides as the ceramic phase and an alloy or intermetallic compond of cerium and at least one of aluminum, nickel, iron and cobalt as the metal phase. The ceramic phase may comprise interengaged crystal lattices of ceria and alumina. The material may be a self-sustaining body which may be used as substrate for a dimensionally stable anode in molten sale aluminum electrowinning cells, coated with a protective layer of cerium oxyfluoride in situ during electrolysis in molten cryolite containing cerium ions.
    Type: Grant
    Filed: February 15, 1989
    Date of Patent: August 14, 1990
    Assignee: Moltech Invent S.A.
    Inventors: Dominique Darracq, Jean-Jacques Duruz
  • Patent number: 4943320
    Abstract: A process for preparing ceramic-metal composites without melting the metal is disclosed. A compact or green body is made from a ceramic and a metal, and the compact is sealed in a vacuum in a container such as a glass envelope. The compact is then heated to a temperature below the melting point of the metal, but high enough so that the vapor pressure of the metal is significant, and the metal redistributes through the ceramic by evaporation and condensation. The composite thereby forms a body having ceramic particles uniformly coated by the metal. Products formed by the process and fabrication of a B.sub.4 C/Cr composite are also disclosed.
    Type: Grant
    Filed: December 15, 1988
    Date of Patent: July 24, 1990
    Assignee: The Regents of the University of California
    Inventors: Alexander Pechnik, M. Dean Matthews
  • Patent number: 4941919
    Abstract: The sintered sliding material according to the present invention consists of from 0.1 to 10% by of graphite, from 1 to 7% by of alumina, and balance of copper, and occasionally at least one member selected from the group consisting of from 1 to 10% of Sn and from 1 to 30% of Pb, and/or not more than 1% of P, and includes the alumina dispersed in the copper matrix. The alumina is held by the copper matrix so that the particles of alumina are not separated from the material during sliding under a boundary lubricating condition.
    Type: Grant
    Filed: June 15, 1988
    Date of Patent: July 17, 1990
    Assignee: Taiho Kogyo Co., Ltd.
    Inventors: Eiji Asada, Takashi Tomikawa, Tatsuhiko Fukuoka
  • Patent number: 4941918
    Abstract: A magnesium-based composite material having improved mechanical strength, and in particular an improved modulus of elasticity, and a relatively low density. The material is provided by pressing and sintering a mixture of magnesium or magnesium-based alloy particles or a particulate combination of magnesium particles and particles of one or more additional metals, with a reinforcement additive of boron, or boron-coated B.sub.4 C, Si.sub.3 N.sub.4, SiC, Al.sub.2 O.sub.3 or MgO particles.
    Type: Grant
    Filed: December 12, 1988
    Date of Patent: July 17, 1990
    Assignee: Fujitsu Limited
    Inventors: Eiji Horikoshi, Tsutomu Iikawa, Takehiko Sato
  • Patent number: 4939038
    Abstract: A light metallic composite material containing therein fine granular additives dispersed in a matrix of a light metallic material, which composite material has a light weight, high mechanical strength, and excellent characteristics such as high damping ability. The additives each have a density less than that of the matrix and heat resistance enough to withstand a heating temperature at which they are composited with the matrix. Preferably, the additives are each formed with a coating which increases mechanical strength and provides an electromagnetic characteristic different from that of the matrix. Preferably, the composite material is produced by heating a mixture of matrix powders and additives up to a temperature where only part of the mixture including no microspheres is softened but the mixture is adequately composited, an amount of additives being equal to 10% to 70% by volume of the matrix, and by forming the composited mixture into a desired shape and solidifying same.
    Type: Grant
    Filed: November 30, 1987
    Date of Patent: July 3, 1990
    Assignee: Inabata Techno Loop Corporation
    Inventor: Tadao Inabata
  • Patent number: 4933007
    Abstract: A heat-resistant aluminum-base composite which includes an aluminum matrix of not smaller than 99.0% purity, Si particles whose average diameter falls in the range of 0.1 to 100 .mu.m, and Al.sub.2 O.sub.3 and Al.sub.4 C.sub.3 particles, the particles being dispersed in the aluminum matrix at volume percents Vf(Si) and V.sub.f (Al.sub.2 O.sub.3 +Al.sub.4 C.sub.3) wherein Vf(Si).gtoreq.9%, Vf(Al.sub.2 O.sub.3 +Al.sub.4 C.sub.3).ltoreq.20% and Vf (Al.sub.2 O.sub.3 +Al.sub.4 C.sub.3)+Vf(Si).ltoreq.40%.
    Type: Grant
    Filed: October 19, 1989
    Date of Patent: June 12, 1990
    Assignee: Showa Aluminum
    Inventors: Tsunemasa Miura, Koichiro Fukui
  • Patent number: 4929418
    Abstract: A cathode is made from tungsten powder using as an impregnant the product rmed from adding about 1 mole of a member selected from the group consisting of zirconium, zirconium dioxide, hafnium, hafnium dioxide, uranium, uranium dioxide, titanium, and titanium dioxide to about 50 to about 100 moles of a compound selected from the group consisting of Ba.sub.3 Al.sub.2 O.sub.6, Ba.sub.3 WO.sub.6, and Ba.sub.4 Al.sub.2 O.sub.7.
    Type: Grant
    Filed: January 22, 1990
    Date of Patent: May 29, 1990
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventors: Louis E. Branovich, Bernard Smith, Gerard L. Freeman, Eckart Donald W.
  • Patent number: 4927473
    Abstract: A compressed powder core is made of a compressed body of a magnetic powder each particle of which has a surface covered with an insulating layer. The insulating layer is formed of an insulating material selected from the group consisting of an inorganic compound powder having an electronegativity of not less than 12.5, an inorganic compound powder having an electronegativity of less than 8.5, a metal alkoxide and a decomposition product of a metal alkoxide.
    Type: Grant
    Filed: October 20, 1988
    Date of Patent: May 22, 1990
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Kumi Ochiai, Hiromichi Horie, Itsuo Arima, Mikio Morita
  • Patent number: 4919734
    Abstract: A compressed powder core is made of a compressed body of a magnetic powder each particle of which has a surface covered with an insulating layer. The insulating layer is formed of an insulating material selected from the group consisting of an inorganic compound powder having an electronegativity of not less than 12.5, an inorganic compound powder having an electronegativity of less than 8.5, a metal alkoxide and a decomposition product of a metal alkoxide.
    Type: Grant
    Filed: September 14, 1987
    Date of Patent: April 24, 1990
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Kumi Ochiai, Hiromichi Horie, Itsuo Arima, Mikio Morita
  • Patent number: 4915899
    Abstract: The invention comprises a process for co-sintering of conductors of copper or copper-based alloy and a ceramic substrate, the substrate being produced from a ceramic powder of cordierite type, having a sintering temperature of lower than 950.degree. C.The process comprises the following steps:(a) shaping of the ceramic substrate from a powder of cordierite type,(b) deposit of copper on the ceramic substrate, and(c) co-sintering heat treatment, during which the organic compounds are removed, the copper is regenerated in a reducing atmosphere, and co-sintering of the conductors and the substrate is carried out in a flow of moist inert gas with a plateau at a temperature of between 1065.degree. and 1080.degree. C.The process according to the invention makes it possible to produce substrates of cordierite with internal and external conductors.
    Type: Grant
    Filed: January 23, 1989
    Date of Patent: April 10, 1990
    Assignee: Pechiney Recherche Groupement d'Interet Economique
    Inventors: Veronique Oliver, Jean-Louis Guille, Jean-Claude Bernier, Claude Drapier
  • Patent number: 4909841
    Abstract: A process of hot pressing of materials to form articles or compacts is characterized by the steps: (A) providing a compactable particulate mixture; (B) uniaxially pressing the particles without heating to provide article or compact (22); (C) placing at least one article or compact (22) in an open pan (31) having an insertable frame (32) with edge surfaces (34) that are not significantly pressure deformable, where the inside side surfaces of the frame are parallel to the central axis B--B of the open pan, and where each article or compact is surrounded by fine particles of a separating material; (D) evacuating air from the container and sealing the articles or compacts inside the container by means of top lid (36); (E) hot pressing the compacts at a pressure from 352.5 kg/cm.sup.2 to 3,172 kg/cm.sup.
    Type: Grant
    Filed: June 30, 1989
    Date of Patent: March 20, 1990
    Assignee: Westinghouse Electric Corp.
    Inventors: Natraj C. Iyer, Alan T. Male, William R. Lovic
  • Patent number: 4908158
    Abstract: An electrical contact material consists of Ag in which a metallic oxide is produced and dispersed through an internal oxidation and containing as metallic elements Cd, Mn and Al. With this contact material of this composition, there can be shown a high anti-welding property and a stably low contact resistance.
    Type: Grant
    Filed: February 13, 1989
    Date of Patent: March 13, 1990
    Assignee: Matsushita Electric Works, Ltd.
    Inventors: Koji Tsuji, Shuji Yamada, Yoshinobu Takegawa
  • Patent number: 4894273
    Abstract: Bonding additives for refractory metallization compositions allow for circuit traces having good resistivities and adhesion values in excess of 6 kpsi, generally between about 10 and 20 kpsi. The inks are provided in formulations devoid of a glass component, and are suitable for co-sintering circuit traces and vias with 96% alumina substrates, and especially for 99% alumina substrates. Suitable bonding additives are the oxides of molybdenum, tungsten, niobium, manganese, yttrium, and titanium, or mixtures of such oxides.
    Type: Grant
    Filed: June 16, 1988
    Date of Patent: January 16, 1990
    Assignee: Ceramics Process Systems Corp.
    Inventors: Sheldon I. Lieberman, Eric A. Barringer, Brian C. Foster
  • Patent number: 4892861
    Abstract: Disclosed is a cermet exhibiting superconducting properties with improved mechanical properties comprising a mixture of a superconducting ceramic and one or more metals, the cermet resulting from liquid phase sintering at a temperature at which one of the metals is molten and below the melting temperature of the superconducting ceramic.
    Type: Grant
    Filed: August 14, 1987
    Date of Patent: January 9, 1990
    Assignee: Aluminum Company of America
    Inventor: Siba P. Ray
  • Patent number: 4891078
    Abstract: Compositions for the production of rare earth-ferromagnetic-metal permanent magnets comprise mixtures of rear earth-ferromagnetic metal alloy powder and a lesser amount of a powdered second-phase sintering aid, wherein there is added up to about 2 percent by weight of a particulate refractory oxide, carbide, or nitride additive. Permanent magnets are prepared by mixing the components, aligning the mixture in a magnetic field, pressing and sintering. The refractory material inhibits grain growth in the second phase during sintering, improving the magnetic properties of the major phase.
    Type: Grant
    Filed: January 25, 1988
    Date of Patent: January 2, 1990
    Assignee: Union Oil Company of California
    Inventor: Mohammad H. Ghandehari
  • Patent number: 4888054
    Abstract: The invention is directed to a process for producing metal composites from low-cost earth products and articles manufactured thereby. Fly ash from burned coal and oil is bonded with low-melting metals or alloys to produce economical composite materials with modified strength, conductivity and wear resistance.
    Type: Grant
    Filed: January 21, 1988
    Date of Patent: December 19, 1989
    Inventor: Robert B. Pond, Sr.
  • Patent number: 4885029
    Abstract: A thin section fibrous, unrecrystallized dispersion strengthened copper body suitable for use in the manufacture of lead frames for integrated circuits and a method for making same.
    Type: Grant
    Filed: April 1, 1988
    Date of Patent: December 5, 1989
    Assignee: SCM Metal Products, Inc.
    Inventors: Thomas B. Buerkle, Jack D. Troxell
  • Patent number: 4871394
    Abstract: Sintered copper friction facing suitable for operation in oil and quieter in operation than current facing of this type has a void volume not less than 30% of the total volume. It can be made by employing, as the copper to form the facing matrix, copper powder which is in dendritic form and of apparent density not greater than 1.3 gram/cm.sup.3.
    Type: Grant
    Filed: November 8, 1988
    Date of Patent: October 3, 1989
    Assignee: Ferodo Limited
    Inventors: Ralph Baker, Stephen N. Foulkes
  • Patent number: 4867788
    Abstract: To control grain size during recrystallization annealing of a consolidated metallurgical, dispersion-strengthened powder allow material, the initial powder is seeded with a powder alloy in which the dispersoid is absent or is in a coarser form or is present in a lesser quantity so that the seeds provide sites at which nucleation of recrystallization is promoted.
    Type: Grant
    Filed: September 26, 1988
    Date of Patent: September 19, 1989
    Assignee: United Kingdom Atomic Energy Authority
    Inventor: Andrew R. Jones
  • Patent number: 4863514
    Abstract: There is provided a material for dentures having metallic matrix, containing 0.5-30 volume % glass having a softening temperature above 650.degree. C. and/or ceramic particles having a maximum grain size of 40 .mu.m.
    Type: Grant
    Filed: February 8, 1989
    Date of Patent: September 5, 1989
    Assignee: Degussa Atiengesellschaft
    Inventors: Werner Groll, Josef Rothaut
  • Patent number: 4859239
    Abstract: An electrode, and method of producing same, including tungsten which has been heated in wet hydrogen at 1050.degree. C. for 5 to 10 minutes, then heated at about 1500.degree. C. for about three hours in a vacuum, and then further heated at about 2800.degree. C. for about 5 minutes in a vacuum.
    Type: Grant
    Filed: December 20, 1988
    Date of Patent: August 22, 1989
    Assignee: GTE Products Corporation
    Inventor: Edmund M. Passmore
  • Patent number: 4838936
    Abstract: Spiral parts, such as orbiting and fixed scroll plates having involute wraps, for use in scroll compressors, the parts having low coefficient of thermal expansion and high tensile strength and Young's modulus, are formed by combining a self-lubricating power into aluminum raw material powder prior to compression and forging. As an alternative to and in conjunction with the foregoing, temperatures during preform heating and in the die for forging are controlled to be in respective ranges of 300.degree. to 500.degree. C. and 150.degree. to 500.degree. C. Aluminum alloy fine powder preferably has a particle diameter no larger than 350 .mu.m. The self-lubricating powder preferably forms 1 to 25% of the mix by volume, and contains at least one member selected from the group consisting of graphite, BN, and MoS.sub.2.
    Type: Grant
    Filed: May 23, 1988
    Date of Patent: June 13, 1989
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventor: Kiyoaki Akechi
  • Patent number: 4837232
    Abstract: The invention concerns self-supporting ceramic structures, including ceramic composite structures embedding a filler, and methods of making them. The ceramic structures comprise a polycrystalline material made by oxidation of a body of molten parent metal with an oxidant. The polycrystalline material has a first region substrate surmounted by a terminal region stratum which is integral with the first region. The terminal region stratum is harder and of denser, finer crystalline structure than the first region substrate and is formed in a reaction stage subsequent to the reaction stage in which the first region of polycrystalline material is formed. Growth of the first stage is attained by attenuating or interrupting the transport of molten parent metal to the first region under conditions which nonetheless leave or maintain therein enough oxidizable molten parent metal to form the polycrystalline material of the terminal region.
    Type: Grant
    Filed: September 16, 1986
    Date of Patent: June 6, 1989
    Assignee: Lanxide Technology Company, LP
    Inventors: Stanley J. Luszcz, Harry R. Zwicker
  • Patent number: 4833106
    Abstract: A fluid-permeable article which permits fluid to pass therethrough includes a porous ceramic structure having a multiplicity of hollow members made of ceramic material which are concatenated with each other to form a framework having a continuous capillary passageway system. A continuous space is formed outside of the framework and is defined by the outer surfaces of the hollow members. A continuous matrix material fills the continuous space outside of the framework and cooperates with the porous ceramic structure to provide an integral composite structure consisting of the ceramic material and the matrix material. The continuous passageway system is open in at least a portion of the exposed surfaces of the article and permits fluids to pass therethrough.
    Type: Grant
    Filed: October 14, 1987
    Date of Patent: May 23, 1989
    Assignee: Nabeya Iron & Tool Works, Ltd.
    Inventor: Takao Horie
  • Patent number: 4832893
    Abstract: A method for producing PLZT generally expressed as (Pb.sub.1-x La.sub.x) (Zr.sub.1-y Ti.sub.y).sub.1-x/4 O.sub.3 (0<x.ltoreq.0.3, 0.ltoreq.y.ltoreq.1.0) comprises the steps of forming a coprecipitated body by reacting solution containing at least one of Pb, La and Ti with a zirconium-containing solution and a precipitation-forming solution, or (a) forming a solution containing at least one of Pb, La and Ti forming PLZT generally expressed as (Pb.sub.1-x La.sub.x) (Zr.sub.1-y Ti.sub.y).sub.1-x/4 O.sub.3 (0<x.ltoreq.0.3, 0.ltoreq.y.ltoreq.1.0) and a zirconium-containing solution and carrying out a hydrolysis reaction to produce a sol body, (b) drying and then presintering the coprecipitated body at a temperature of from 700.degree. to 1300.degree. C. to form a modified zirconia powder, (c) mixing the presintered body with a compound having a remaining component composition of a required PLZT composition, (d) presintering the mixture at a temperature of from 500.degree. to 1000.degree. C.
    Type: Grant
    Filed: December 16, 1987
    Date of Patent: May 23, 1989
    Assignees: Nippondenso Co., Ltd., Science and Technology Agency National Institute
    Inventors: Michio Hisanaga, Kazunori Suzuki, Masataka Naito, Shinichi Shirasaki
  • Patent number: 4826808
    Abstract: A method of preparing a superconducting oxide by combining the metallic elements of the oxide to form an alloy, followed by oxidation of the alloy to form the oxide. Superconducting oxide-metal composites are prepared in which a noble metal phase intimately mixed with the oxide phase results in improved mechanical properties. The superconducting oxides and oxide-metal composites are provided in a variety of useful forms.
    Type: Grant
    Filed: March 27, 1987
    Date of Patent: May 2, 1989
    Assignee: Massachusetts Institute of Technology
    Inventors: Gregory J. Yurek, John B. VanderSande
  • Patent number: 4808223
    Abstract: This invention relates to a silver/metal oxide material for electrical contacts containing no Cd which essentially consists of Ag and 5 to 30% by weight of at least one of oxides of Sb, Sn, Zn, In, Cu, Mn, Bi and Pb, and further, if necessary, 0.05 to 2% by weight of at least one of oxides of Mg, Al, Fe, Ni, Co, Si, Ga, Ge, Te, Ca and Li, the total amount of said metal oxides being 5 to 32% by weight, wherein fine particles of said metal oxides are substantially uniformly distributed in a matrix whose main component is Ag in a sintered state, and wherein there are no grain boundaries formed by agglomerations or agglomerated layers of said metal oxides.
    Type: Grant
    Filed: July 7, 1987
    Date of Patent: February 28, 1989
    Assignees: Fuji Electric Co., Ltd., Tokuriki Honten Co., Ltd.
    Inventors: Ryoji Ozaki, Hisaji Shinohara, Hironobu Yamamoto, Takashi Nara, Hajime Yoshida
  • Patent number: 4798625
    Abstract: Superalloy with oxide dispersion hardening having improved corrosion and oxidation resistance and based on nickel with the following composition:Cr=17-18% by weight,Al=6-7% by weight,Mo=2-2.5% by weight,W=3-3.5% by weight,Ta=2-2.5% by weight,Zr<0.2% by weight,B<0.02% by weight,C<0.1% by weight,Y.sub.2 O.sub.3 =1-1.5% by weight,Ni=Remainder.
    Type: Grant
    Filed: August 28, 1987
    Date of Patent: January 17, 1989
    Assignee: BBC Brown Boveri AG
    Inventors: Peter Jongenburger, Robert Singer
  • Patent number: 4793967
    Abstract: The present invention is directed to a cermet material comprising a matrix of aluminum alloy with ceramic particles distributed therein. The cermet is adapted for use as a semiconductor substrate and is manufactured using powder technology procedures. The cermet comprises from about 40 to about 60 volume % of aluminum or aluminum alloy, from an effective amount up to about 10 volume % of binder for enhancing bonding between the aluminum alloy and ceramic particles, and the balance essentially ceramic particles.
    Type: Grant
    Filed: December 31, 1987
    Date of Patent: December 27, 1988
    Assignee: Olin Corporation
    Inventors: Michael J. Pryor, Eugene Shapiro, Deepak Mahulikar
  • Patent number: 4792353
    Abstract: A consolidated metal-ceramic composite comprises a first phase of particles of aluminum oxide or a solid solution based on aluminum oxide uniformly distributed in a second matrix phase wherein the second matrix phase is non-reactive with aluminum oxide and contains a sufficient amount of titanium carbide at the interface between the first and second phase to prevent a chemical reaction at the interface during consolidation at the liquidus temperature and which exhibits good mechanical properties with regard to strength and toughness at high temperatures up to about 1200.degree. C.
    Type: Grant
    Filed: October 10, 1986
    Date of Patent: December 20, 1988
    Assignee: Massachusetts Institute of Technology
    Inventors: Bruce M. Kramer, David M. Dombrowski, Dennis Gonseth, Minyang Yang, Stephen P. Kohler
  • Patent number: 4770701
    Abstract: Amorphous metal-ceramic and microcrystalline metal-ceramic composites are synthesized by solid state reaction-formation methods. These metal-ceramic composites are characterized by a composition that ranges from about 75 to about 99.9 percent ceramic in about 0.1 to about 25 percent amorphous or microcrystalline metal binder phase.
    Type: Grant
    Filed: April 30, 1986
    Date of Patent: September 13, 1988
    Assignee: The Standard Oil Company
    Inventors: Richard S. Henderson, Michael A. Tenhover
  • Patent number: 4756752
    Abstract: A method for forming a high density body from a powder material of metallic and non-metallic compositions and combinations thereof comprising confining a quantity of the powder material in a flexible mold structure, subjecting the powder material in the mold structure to a predetermined pressure along one axis while confining the material against movement in directions normal to the axis so as to form a compact body of the powder material and subsequently heating the compact body to a predetermined temperature so as to further compact the body. A quantity of glass is heated so that it will flow and transmit pressure following which the heated body is immersed in the heated glass and the flowable glass is subjected to a pressure high enough to further compact the body. The resulting densified body is uniformly compressed in the directions of three mutually perpendicular axes extending through the body.
    Type: Grant
    Filed: November 4, 1987
    Date of Patent: July 12, 1988
    Assignee: Star Cutter Company
    Inventor: Lewis J. Barnard
  • Patent number: 4756754
    Abstract: The present invention relates to a composite formed of a mixture of ceramic particles and at least two metallic components adhered together with a glassy phase. A first of the metallic components, in particle form, enhances the flow characteristics of the mixture where the second metallic component and the glass are in the molten condition. The final composite is a continuous phase of the second metallic component having particles of the first metallic component and glass coated ceramic particles distributed therein.
    Type: Grant
    Filed: March 6, 1987
    Date of Patent: July 12, 1988
    Assignee: Olin Corporation
    Inventor: Narendra N. SinghDeo
  • Patent number: 4755220
    Abstract: A material resistant to high temperature melts of metal and salt which comprises a composite material containing silicon nitride, silicon oxynitride, silicon dioxide and silicon prepared by(a) suspending silicon powder in SiO.sub.2 sol to form a pourable mass,(b) molding a workpiece from said mass,(c) hardening the molded workpiece, and(d) nitriding the hardened workpiece in a nitrogen atmosphere to form silicon nitride and silicon oxynitride to a degree that SiO.sub.2 and elemental silicon remain detectable in the nitrided workpiece,is useful as the material of construction for crucibles and tools for confining, handling and treating melts of metals or salts.
    Type: Grant
    Filed: November 6, 1987
    Date of Patent: July 5, 1988
    Assignee: Bayer Aktiengesellschaft
    Inventors: Peter Woditsch, Werner Kannchen, Horst Lange, Ingo Schwirtlich
  • Patent number: 4752334
    Abstract: There is provided a substantially fully dense powdered metal composite comprising a highly conductive metal or metal alloy matrix having dispersed therein discrete microparticles of a refractory metal oxide and discrete macroparticles of an additive metal or metal alloy, such as a nickel/iron alloy. The respective components undergo minimal alloying because sintering is not utilized in forming the composite. These composites are characterized by high thermal or electrical conductivity and a desired property attributable to the composite forming additive metal or metal alloy. The composites are useful in forming lead frames for integrated circuit chips, electric lamp lead wires, and electrical contact members.
    Type: Grant
    Filed: December 13, 1983
    Date of Patent: June 21, 1988
    Assignee: SCM Metal Products Inc.
    Inventors: Anil V. Nadkarni, Prasanna K. Samal, James E. Synk
  • Patent number: 4749545
    Abstract: This invention relates to metal matrix composites containing at least 40% v/v of a hard material such as SiC and a matrix of aluminium, magnesium or alloys of either. The invention also covers a method of making such composites by ball milling powders of the respective components. Other mixing techniques do not enable such a high proportion of hard material to be incorporated into the composite. The composites are useful to produce components resistant to wear.
    Type: Grant
    Filed: March 26, 1987
    Date of Patent: June 7, 1988
    Assignee: British Petroleum Co. p.l.c.
    Inventors: Alan R. Begg, Andrew D. Tarrant
  • Patent number: 4743299
    Abstract: The present invention is directed to a cermet material comprising a matrix of aluminum alloy with ceramic particles distributed therein. The cermet is adapted for use as a semiconductor substrate and is manufactured using powder technology procedures. The cermet comprises from about 40 to about 60 volume % of aluminum or aluminum alloy, from an effective amount up to about 10 volume % of binder for enhancing bonding between the aluminum alloy and ceramic particles, and the balance essentially ceramic particles.
    Type: Grant
    Filed: March 12, 1986
    Date of Patent: May 10, 1988
    Assignee: Olin Corporation
    Inventors: Michael J. Pryor, Eugene Shapiro, Deepak Mahulikar
  • Patent number: RE32942
    Abstract: A composite is provided which is adaptable to be a substrate for an electronic application. The composite comprises first material particles having a coefficient of thermal expansion in the range of about -20.times.10.sup.-7 to about 50.times.10.sup.-7 in/in/.degree.C. Second material particles having a coefficient of thermal expansion in the range of about 100.times.10.sup.-7 to about 200.times.10.sup.-7 in/in/.degree.C. are mixed with the first material particles. A bonding agent adheres the first and second material particles into a coherent composite having a coefficient of thermal expansion in the range of about 1.times.10.sup.-7 to about 50.times.10.sup.-7 in/in/.degree.C.
    Type: Grant
    Filed: May 15, 1986
    Date of Patent: June 6, 1989
    Assignee: Olin Corporation
    Inventor: Sheldon H. Butt