With Vapor-treating Devices Patents (Class 202/182)
  • Publication number: 20030132097
    Abstract: A desalination device includes a saltwater input line and a desalinator having a water input connected to the input line, a fresh water output and a brine output. A fuel cell generates electricity and is connected to an energy source for the desalinator. A heat exchanger transfers waste heat from the fuel cell to desalinator.
    Type: Application
    Filed: January 15, 2002
    Publication date: July 17, 2003
    Inventors: Brian Kenet, Pedro Joaquin Sanchez Belmar
  • Publication number: 20030132095
    Abstract: A method for distilling water includes the steps of entering brine to be distilled into a sub-atmospheric boiler having a brine section with a brine output and a water vapor output; concentrating brine in the brine section to a concentration of at least 250 grams of salt or contaminants per liter; stirring the brine in the brine section; and exiting the brine through the brine output. A distiller with a subatmospheric boiler having a stirring device is also provided.
    Type: Application
    Filed: January 15, 2002
    Publication date: July 17, 2003
    Inventors: Brian Kenet, Pedro Joaquin Sanchez Belmar
  • Publication number: 20030132096
    Abstract: An evaporator and condenser unit for use in distilling a liquid, such as water, includes a rotary heat exchanger plate having a plurality of folds or pleats. Adjacent panels of the folded plate define spaces between their oppositely facing surfaces, and these spaces are alternatingly configured as evaporating and condensing chambers. The evaporating chambers, moreover, are defined between adjacent panels that are joined at an outer diameter fold, while the condensing chambers are defined between adjacent panels that are joined at an inner diameter fold. The evaporating chambers are thus closed at their outer diameter ends and open at their inner diameter ends, while the condensing chambers are closed at their inner diameter ends and open at their outer diameter ends.
    Type: Application
    Filed: January 17, 2002
    Publication date: July 17, 2003
    Inventor: William H. Zebuhr
  • Patent number: 6589395
    Abstract: The distillation plant comprises a column (1) and a heat pump (4, 5) which operates between a sump vaporizer (3) and an exhaust vapor compressor (2) of the column. The heat pump is substitutable by devices (6, 7) which can be switched to the sump vaporizer and the exhaust vapor compressor when required. These substituting devices comprise devices (6 and 7 respectively) for the production of vapor or the provision of a coolant respectively as well as connection means (63, 63′, 72, 72′). The coolants can be liquids (water) or gases (air).
    Type: Grant
    Filed: May 15, 1999
    Date of Patent: July 8, 2003
    Assignee: Sulzer Chemtech AG
    Inventor: Albert Meili
  • Publication number: 20030092876
    Abstract: The invention pertains to a device (1) for the condensation of water from an aqueous liquid by means of a temperature gradient, which device comprises, (a) a vapor chamber (5) that can be brought in contact with a condensation compartment (4) wherein at least part of the water vapor from the aqueous liquid condenses, and wherein inside of said vapor chamber is located, (b) an evaporation compartment (2) having a least a wall with an outer surface and comprising a closed, hollow and water permeable membrane, and which vapor chamber has an outer surface that comprises a substantially water-impermeable insulation skirt (3) with an inner and an outer surface, such that there is a gap between the inner surface of the insulation skirt and the outer surface of the evaporation compartment, and wherein the vapor chamber has a lower surface of an active width (w) which is at least 10% of the effective diameter (d) of the evaporation compartment.
    Type: Application
    Filed: September 23, 2002
    Publication date: May 15, 2003
    Inventors: Arnoldus Paulus Maria Ter Beek, Carel Theo Jozef Wreesmann
  • Patent number: 6517686
    Abstract: A system and method for purifying liquefied corrosive gases of metallic impurities is described. The principle for this purification method relies on vapor-phase transfilling the vapor phase from a source container into a receiving container. This method has been observed to decrease metal concentrations by a factor of at least 1000 and, decreases the metallic impurity levels in the resulting condensate. The vapor transfer is accomplished by controlled differential pressure rather than mechanical pumping, thereby generating no particle or metal impurities.
    Type: Grant
    Filed: March 13, 2001
    Date of Patent: February 11, 2003
    Assignees: L'Air Liquide - Societe Anonyme A Directoire et Conseil de Surveillance pour l'Etude et l'Exploitation des Procedes Georges Claude, American Air Liquide, Air Liquide America Corporation
    Inventors: John Borzio, Tracey Jacksier
  • Patent number: 6514406
    Abstract: A water treatment apparatus comprises a first housing having an inlet, an outlet, and a chamber defined therebetween wherein the inlet is connected to an upstream water pipe. A series of magnets are arranged for attachment about the upstream water pipe for directing a magnetic field onto water flowing downstream into the first housing chamber. First and second electrodes of a copper and silver alloy are positioned in the first housing chamber for releasing copper and silver ions into the water therein to reduce bacteria levels of the water. A heating coil is disposed in the first housing for boiling the water in the first housing chamber. The apparatus includes a second housing having an inlet, an outlet, and a chamber defined therebetween. A conduit connects the outlet of the first housing with the inlet of the second housing for supplying water vapor from the first housing chamber to the second housing chamber.
    Type: Grant
    Filed: October 24, 2000
    Date of Patent: February 4, 2003
    Inventor: James E. Katehis
  • Patent number: 6436242
    Abstract: A water distiller has a sub-atmospheric boiler having a non-recirculating brine section, an input, a brine output and a vapor output. The input is for water to be distilled, the brine output for brine, and the vapor output for water vapor. A compressor is connected to the vapor output for heating the water vapor, and an heated vapor line is connected to an output of the compressor, the heated vapor line heating the brine section.
    Type: Grant
    Filed: February 10, 2000
    Date of Patent: August 20, 2002
    Inventor: Pedro Joaquin Sanchez Belmar
  • Publication number: 20020092762
    Abstract: A distillation unit (10) includes a filter (116) through which feed water passes before it is introduced into a rotary heat exchanger (32) for evaporation and subsequent condensation. During a normal mode of operation, liquid that has not evaporated as a result of passage through the rotary heat exchanger's evaporation chambers (56) is recirculated for reintroduction into those chambers, together with a minor amount of feed liquid from the filter to make up for evaporation. At the same time, some filtered feed water is fed into one side of a transfer pump (166), where it slowly accumulates. Periodically, though, during short flushing-mode periods, the erstwhile recirculating liquid is redirected at a relatively high flow rate through the filter (116) in the reverse direction, thereby flushing it.
    Type: Application
    Filed: January 18, 2001
    Publication date: July 18, 2002
    Inventor: William H. Zebuhr
  • Publication number: 20020092757
    Abstract: A distiller (10) that employs a rotary heat exchanger (32) introduces water to be evaporated into evaporation chambers (56). During most of its operation, it collects the water that has passed through the evaporation chamber (56) without evaporating, and it reintroduces the thus-collected liquid back into the evaporation chamber, where it also adds a minor amount of unrecirculated feed liquid to make up for evaporation and concentrate removal. Simultaneously, a minor amount of feed liquid is fed into one side of a transfer pump (116). During this mode of operation, the impurities concentration in the recirculating liquid tends to increase as a result of the evaporation of pure water vapor. Periodically, the erstwhile recirculating liquid is redirected to the other side of the transfer pump (116), where it causes the feed liquid stored in the transfer pump's first side to be fed without accompanying recirculant liquid into the rotary heat exchanger's evaporation chambers.
    Type: Application
    Filed: January 18, 2001
    Publication date: July 18, 2002
    Inventor: William H. Zebuhr
  • Publication number: 20020092624
    Abstract: In a distillation unit (10) a rotary heat exchanger (32) receives from a radially inward position feed liquid to be purified and collects on the inner surface of a rotating exterior shell (36) liquid that has passed through its evaporation chambers (56). Stationary scoop tubes (122 and 124) scoop liquid from the resultant liquid layer that forms on the shell (36)'s inner surface, and the kinetic energy of the liquid scooped from the thus-spinning layer drives it radially inward through the scoop tubes (122 and 124) into spray arms (58) for reintroduction into the rotary heat exchanger's evaporation chambers (56).
    Type: Application
    Filed: January 18, 2001
    Publication date: July 18, 2002
    Inventor: William H. Zebuhr
  • Publication number: 20020092758
    Abstract: A distillation unit (10) employs counterflow-heat-exchanger modules (102, 104, 106, 108, and 110) to use the heat from water that has come from a rotary heat exchanger (32) to heat feed water that is being sent to it for distillation. In one of the modules the feed water is heated only by concentrate that results from the distillation process, whereas only condensate heats the feed water in the other modules. By thus employing four different flows in two sets of heat-exchanger modules rather than three flows in a single set, the distillation unit can employ relatively simple counterflow-heat-exchanger modules and easily adjust flows to achieve a desired output concentration in response to different expected feed concentrations while maintaining optimum feed flows.
    Type: Application
    Filed: January 18, 2001
    Publication date: July 18, 2002
    Inventor: William H. Zebuhr
  • Publication number: 20020092759
    Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.
    Type: Application
    Filed: January 18, 2001
    Publication date: July 18, 2002
    Inventor: William H. Zebuhr
  • Patent number: 6402897
    Abstract: A combination liquid distillation unit and heater, where the distilled liquid is heated to an elevated temperature to effect distillation, and then stored and maintained at an elevated temperature in a hot liquid tank. Thermal communication between the distillation unit portion and the storage tank allow heat from the distillation unit to be recovered in the hot distilled liquid in the tank to be transferred back to the feed water and/or to help maintain the hot distilled liquid in the tank at an appropriate elevated temperature. A start-up chamber in the distillation unit stores a reservoir of feed liquid during periods of inactivity, and allows the hot distilled liquid in the tank to preheat this feed liquid so that the feed liquid boils more quickly upon start-up.
    Type: Grant
    Filed: October 24, 1997
    Date of Patent: June 11, 2002
    Inventor: Charles L. Gunn
  • Publication number: 20020066663
    Abstract: Apparatus and method for desolventizing particulate material having a solvent carried thereby wherein an upper indirect heating zone and a lower direct heating zone is provided. Each of the zones has a plurality of spaced apart horizontal trays for receiving particulate material. The trays define a vertical series of compartments through which the particulate material passes. Steam is provided to the particulate material indirectly in said indirect heating zone and directly in said direct heating zone are also included. An integral air tight flash chamber below the compartments enhances solvent recovery via vaporization of residual solvent from the condensed steam adhered to the particulate material traveling through the direct heating zone prior to discharge of the particulate material. The recovered residual solvent is delivered under pressure to a predetermined compartment in the direct heating zone provide heat for desolventizing the solvent-laden particulate material.
    Type: Application
    Filed: August 28, 2001
    Publication date: June 6, 2002
    Applicant: Crown Iron Works Company
    Inventor: George E. Anderson
  • Publication number: 20020038555
    Abstract: A vapor-compression distiller includes a rotary heat exchanger. A reciprocating compressor (26) maintains a pressure difference between the compressor's evaporation chambers (46) and its condensation chambers (44). The compressor is assembled in a common rotating assembly with the compressor, so the distiller does not need rotating seals between the compressor and heat exchanger. The compressor includes two pistons (56 and 58) driven in opposite directions in a rotating piston chamber (54). The directions in which they thereby reciprocate are substantially parallel to the rotating assembly's axis.
    Type: Application
    Filed: November 30, 2001
    Publication date: April 4, 2002
    Inventor: William H. Zebuhr
  • Patent number: 6365006
    Abstract: The present invention pertains to the alcohol processing industry and relates to a method that includes feeding a mixture into a distillation column which is fitted with contact devices for discharging the vapors through the top of said column. This method further includes boiling a bottom product and supplying the vapor thus formed back into the column. A part of the vapor to be processed using one of said contact devices is then fed back into the vapor flow or liquid flow towards one at least of said devices located upstream relative to the flow direction. In another or the same embodiment, a part of the vapor is fed back into the liquid flow under the level thereof and towards the same contact device in a place that is located upstream from its discharge relative to the flow direction of said vapor. The vapor feedback is preformed without complete condensation thereof.
    Type: Grant
    Filed: May 27, 1999
    Date of Patent: April 2, 2002
    Assignee: General Electric Company
    Inventors: Valery J. Aristovich, Jury V. Aristovich, Andrey J. Sokolov, Elena V. Sokolova
  • Patent number: 6365005
    Abstract: An improved design of a vapor compression distiller which makes use of a rapid, highly turbulent flow through the heat-of-evaporation recovery, or primary, heat exchanger. The distiller may also include the use of turbulators to increase turbulence and mixing within the primary heat exchanger. The increased level of turbulence and mixing dramatically reduces fouling inside the primary heat exchanger and increases the heat transfer efficiency. The improvements in the distiller are maximized by recirculating the liquid to be evaporated at a high multiple of the flow rate of the liquid feed to the distiller. The distiller may also include a feed circulation loop with a secondary heat exchanger to increase the efficiency of heat-of-evaporation recovery in the evaporation/condensation cycle. Applications of the vapor compression distiller include purification of waste liquids, concentration of dilute liquid mixtures, and separation of liquid/liquid, liquid/gas, and liquid/solid mixtures.
    Type: Grant
    Filed: February 9, 1999
    Date of Patent: April 2, 2002
    Inventor: James W. Schleiffarth
  • Patent number: 6350351
    Abstract: A plant for the vacuum distillation of liquids has a vacuum rectification column and a vacuum-producing device based on a liquid-gas jet apparatus. The plant is furnished additionally with a jet pump. A nozzle of the jet pump is connected to a pipeline for bleeding a liquid fraction from the column, an evacuated medium inlet of the jet pump is connected to an outlet of the liquid-gas jet apparatus and an outlet of the jet pump is connected to a separator of the vacuum-producing device. The plant provides more effective vacuum distillation of liquids.
    Type: Grant
    Filed: October 12, 1999
    Date of Patent: February 26, 2002
    Inventors: Serguei A. Popov, Mikhail V. Akimov
  • Publication number: 20020017450
    Abstract: A liquid having certain undesired elements therein is distilled in a distillation column to form a vapor stream. This vapor stream is fed by means of an inert gas drive to a first container having an array of semi-permeable screens which are rotated at a speed of 3,000-10,000 rpm to generate vertical spiral vortexes which act on the vapor to separate out heavier impurities. An inert gas is employed to drive the vapor stream from the first container to the bottom of a second container having a narrower diameter array of semi-permeable screens, these screens being driven at a velocity of 6000-100,000 rpm. In the second container, the molecular species is separated from the main vapor stream by virtue of the exposure of the vapor to large centrifugal gravity forces generated by the horizontal velocity vectors of the rotating screens.
    Type: Application
    Filed: August 1, 2001
    Publication date: February 14, 2002
    Inventor: Ernest Csendes
  • Publication number: 20020000365
    Abstract: A water distiller includes a shell, a container, a heater, a thermal conductive plate, a thermostat, a cover, a condenser coil, and a fan. The shell provides a compartment for receiving the container, the heater, the thermal conductive plate, and the thermostat. The container includes a bottom wall with an inclined surface to which the heater is connected. A higher end of the inclined surface is connected to the thermal conductive plate and the thermostat. The thermostat is mounted in a room provided between the shell and the container, and a first spring is provided to bias the thermostat to be in an intimate contact with cylindrical side wall of the container. A cap is mounted outside the room and a push button is mounted in the cap with an end exposed outside the cap for manual operation. A second spring is mounted in the cap for biasing the push button to a position for the manual operation. The cover mounted on top of the shell provides a compartment for receiving the condenser coil and the fan.
    Type: Application
    Filed: April 14, 1999
    Publication date: January 3, 2002
    Inventor: MR LONG-MING WANG
  • Patent number: 6303006
    Abstract: A vacuum type distilling system includes a sealed container including a vaporization chamber for containing a liquid and a condensation chamber, a pressure-reducing device, a condensing device, a heating device, and a vapor-collecting device including a floating piston for separating liquid and vapor and a guide tube for guiding vapor generated in the vaporization chamber into the condensation chamber. Liquid to be distilled is filled into the vaporization chamber and the pressure of the sealed container is reduced such that the boiling point of the liquid in the vaporization chamber is lowered. The heating device heats and thus vaporizes the liquid in the vaporization chamber into vapor which is immediately conveyed into the condensation chamber where vapor is condensed into distilled liquid by a condensing tube of the condensing device that is mounted in the condensation chamber.
    Type: Grant
    Filed: June 16, 1999
    Date of Patent: October 16, 2001
    Inventors: Chia-Wei Chang, Charlie S. F. Chang, Shen Tsung-Lin
  • Patent number: 6277247
    Abstract: The invention pertains to the field of the petrochemical industry. The invention essentially relates to a system and method that includes feeding of a liquid having molecular weight more than 100 (in atomic mass units) into a nozzle of an ejector as a motive liquid, and delivery of a mixed medium from the ejector into a shaped reservoir, where flow velocity is reduced and static pressure is boosted. The outlet of the ejector is connected to the inlet of the shaped reservoir, the inlet of a separator is connected to the outlet of the shaped reservoir. The introduced method and the system for its embodiment ensure a more efficient operation.
    Type: Grant
    Filed: December 21, 1998
    Date of Patent: August 21, 2001
    Inventor: Serguei A. Popov
  • Patent number: 6277246
    Abstract: A system and method for purifying liquefied corrosive gases of metallic impurities is described. The principle for this purification method relies on vapor-phase transfilling the vapor phase from a source container into a receiving container. This method has been observed to decrease metal concentrations by a factor of at least 1000 and decreases the metallic impurity levels in the resulting condensate. The vapor transfer is accomplished by controlled differential pressure rather than mechanical pumping, thereby generating no particle or metal impurities.
    Type: Grant
    Filed: January 28, 1999
    Date of Patent: August 21, 2001
    Assignees: Air Liquide America Corporation, American Air Liquide Inc.
    Inventors: John Borzio, Tracey Jacksier
  • Patent number: 6153802
    Abstract: A system and process for producing a fluorinated organic compound, said process comprising (a) reacting an organic compound with a fluorinations agent in the presence of a liquid-phase fluorinations catalyst to produce a product stream; (b) scrubbing said product stream to remove a substantial portion of said catalyst to form a low-catalyst content product stream; and (c) recovering said fluorinated organic compound from said low-catalyst content stream.
    Type: Grant
    Filed: May 8, 1998
    Date of Patent: November 28, 2000
    Assignee: AlliedSignal Inc.
    Inventor: Yuon Chiu
  • Patent number: 6022453
    Abstract: A compact apparatus of the distillation of solvent from a mixture of the solvent with oil seed for the extraction thereof according to the invention, the primary module includes a vapor scrubber forming a vapor contactor, a main evaporator and a first condenser while the secondary module has an after evaporator combined in a unit with the stripping column and the second condenser.
    Type: Grant
    Filed: August 6, 1998
    Date of Patent: February 8, 2000
    Assignee: Fried. Krupp AG Hoesch Krupp
    Inventor: Klaus Weber
  • Patent number: 5980695
    Abstract: A system for the vacuum distillation of contaminated solvents incorporates a tank for holding a liquid contaminated solvent, a heating chamber surrounding the tank for heating the liquid contaminated solvent into an evaporated solvent, a drift elimination and fractionation device for separating contaminants out of the evaporated solvent, a heat exchanger circuit for cooling the evaporated solvent from the drift elimination and fractionation device, a pump circuit connected to receive the evaporated solvent from the drift elimination and fractionation device and to circulate the evaporated solvent through the heat exchanger circuit, and a control circuit connected to at least the heating element and the pump so as to control operation their based on parameters of a solvent selected to be processed. The control circuit includes a plurality of sensors for monitoring operating conditions of at least the tank, the heating chamber and the heat exchanger circuit.
    Type: Grant
    Filed: November 14, 1996
    Date of Patent: November 9, 1999
    Assignee: TransGlobal Industrial Services, Inc.
    Inventors: Jeffory David Cox, Robert Grayson Martin
  • Patent number: 5980698
    Abstract: A method for vacuum distillation includes separation of a liquid product delivered to a reservoir under vacuum into a vapour-gaseous phase and at least one liquid fraction, withdrawal of the vapour-gaseous phase from the reservoir using a vacuum-creating device, and subsequent separation of the vapour-gaseous phase into gas and a liquid phase by condensing performed directly in the vacumm-creating device. A portion of the liquid phase is used as a fluid working medium in the vacuum-creating device.An equipment for vacuum distillation includes a reservoir under vacuum conditions equipped with mains and a vacuum-creating device, which has an ejector, a separator and a pump, interconnected by mains.
    Type: Grant
    Filed: January 7, 1997
    Date of Patent: November 9, 1999
    Assignee: Valery Grigorievich Tsegelsky
    Inventors: Alexandr Alexeevich Abrosimov, Alexandr Mikhailovich Kochemasov, Ivan Alexandrovich Kochergin, Valery Grigorievich Tsegelsky
  • Patent number: 5968321
    Abstract: Distillation system having an evaporator/condenser core with heat transfer plates welded together along their edges to form alternate boiling and condensing chambers. Feed liquid is supplied to the boiling chambers through a pair of heat exchangers which preheats the liquid and a steam stripper utilizing ceramic pieces to remove gasses from the liquid. Vapor from the boiling chambers is compressed and delivered to the condensing chambers where it is condensed and gives up its heat to the liquid in the boiling chambers. Pumps positioned between the two heat exchangers draw the condensed product and unvaporized feed liquid containing dissolved solids from the evaporator/condenser and circulate them through the heat exchangers to transfer heat to the feed liquid.
    Type: Grant
    Filed: February 13, 1996
    Date of Patent: October 19, 1999
    Assignee: Ridgewood WaterPure Corporation
    Inventor: Stephan B. Sears
  • Patent number: 5964986
    Abstract: A distillation plant contains a column with packings as well as a vaporizer. The elements of the column are arranged along a vertical axis and assembled as a constructional unit. They are executed in such a manner that a slight pressure drop sets in during the operation of the plant between a sump and a head. At least two vaporizers are provided, namely a first vaporizer, which is arranged in or directly above the sump, and an intermediate vaporizer which is arranged above the first vaporizer and a lower packing section; and/or at least two liquefiers are provided, namely a first liquefier, which is arranged in the head of the column, and an intermediate liquefier, which is arranged below the first liquefier and an upper packing section.
    Type: Grant
    Filed: August 29, 1997
    Date of Patent: October 12, 1999
    Assignee: Sulzer Chemtech AG
    Inventor: Albert Meili
  • Patent number: 5955041
    Abstract: This invention relates to a reactor 1 for the continuous production of linear or cyclic acetals, in particular trioxane, dioxolane, tetroxane, dimethoxymethane, diethoxymethane, diethoxyethane and dibutoxyethane. This reactor has internal adjacently arranged evaporator elements 2, which allow for flow-through of a heat transport medium, and which are at least two meters high so as to generate a thermosiphon flow. The clear cross section between the evaporator elements is 20 to 80% of the overall cross section. Using the reactor, circulation ratios of up to 250 can be achieved. Thus, the reliability and availability of a production plant is increased while the susceptibility to breakdown decreases.
    Type: Grant
    Filed: September 27, 1995
    Date of Patent: September 21, 1999
    Assignee: Hoechst AG
    Inventors: Dieter Arnold, Bernhard Hierholzer, Hubert Wloch, Karl-Friedrich Muck
  • Patent number: 5935388
    Abstract: A distillation plant includes a heat pump whose working fluid is compressed by a vapor jet compressor. A collection location for a liquid is arranged in the stripper part of a distillation column of the plant. At least a portion of the collected liquid is provided in the vaporized form as strip vapor. Connections lead from the collection location to a first vaporizer and to a second vaporizer. The liquid can be vaporized in these vaporizers at an elevated and at a reduced pressure respectively. The vapor jet compressor is connected to the two vaporizers and to the column in such a manner that the vapor from the second vaporizer can be compressed under a driving jet action of the vapor from the first vaporizer and used in the column as strip vapor. A pump is arranged in the connection to the first vaporizer and at least one restrictor member is contained in the connection to the second vaporizer.
    Type: Grant
    Filed: October 20, 1997
    Date of Patent: August 10, 1999
    Assignee: Sulzer Chemtech AG
    Inventor: Istvan Meszaros
  • Patent number: 5922174
    Abstract: Distilling equipment including evaporation apparatus having a boiling chamber and equipment and conduits for supplying raw liquid to the boiling chamber, a plurality of cells with the first cell being connected to the top of the boiling chamber to receive gas therefrom and condense the gas by contact with cold recycled distillate from the first cell, with each stage having vertical vacuum producing bubble tubes through which distillate and gas bubbles pass downward to a collection chamber through the bubble tubes. Cell recycle conduits and pumps recycle fluid from collection chamber to condensing chamber. Distillate is drawn from the condensing chamber of the first cell only. Gas by-pass tubes connect the collecting chamber of a cell to the condensing chamber of the next cell and provide the only connection between the cells to sum the vacuum generated by each cell's bubble tubes.
    Type: Grant
    Filed: November 25, 1996
    Date of Patent: July 13, 1999
    Assignee: Eco-Still Corporation
    Inventor: Philip G. Youngner
  • Patent number: 5906714
    Abstract: A method of separating water from an aqueous emulsion using a minimum of energy includes heating the aqueous emulsion in a sump, conveying concentrated emulsion from the sump to a heat exchanger so as to pass therethrough back to the sump, circulating water vapor and non-condensable gases from the sump through a compressor to raise its temperature and passing the heated water vapor and non-condensable gases through the heat exchanger to condense and heat the concentrated emulsion therein and evaporate water therefrom, a thermostat filled with water and water vapor, together with first and second pressure switches respectively communicating with the sump and the external atmosphere and the heat exchanger and the external atmosphere, maintaining a temperature differential between 0.5.degree. and 3.degree. C. between the aqueous emulsion in the sump and the temperature of the compressed water vapor and noncondensable gases.
    Type: Grant
    Filed: October 15, 1996
    Date of Patent: May 25, 1999
    Assignees: Agro Milj.o slashed. A/S, OHM Electric Co., Ltd.
    Inventors: Asger Gramkow, Jeppe Christian Bastholm, Finn Erik Christensen
  • Patent number: 5846387
    Abstract: Highly purified HCl for use in semiconductor manufacturing is prepared on-site by drawing HCl vapor from a liquid HCl reservoir, and scrubbing the filtered vapor in a low-pH aqueous scrubber.
    Type: Grant
    Filed: July 1, 1996
    Date of Patent: December 8, 1998
    Assignee: Air Liquide Electronics Chemicals & Services, Inc.
    Inventors: Joe G. Hoffman, R. Scot Clark
  • Patent number: 5824122
    Abstract: In a process and an apparatus for purifying flammable gas, in particular low-temperature carbonization gas, the gas is scrubbed and discharged as pure gas and condensate. The condensate is distilled in a distillation unit. Volatile constituents are admixed to the pure gas, so that the calorific value of the latter is increased. The non-volatile constituents are discharged. The non-volatile constituents can be fed to a low-temperature carbonization drum and carbonized therein at low temperature.
    Type: Grant
    Filed: May 27, 1997
    Date of Patent: October 20, 1998
    Assignee: Siemans Aktiengesellschaft
    Inventors: Gerd Baumgartel, Herbert Tratz
  • Patent number: 5817217
    Abstract: The invention relates to a machine for confining a primary fluid by means of a secondary fluid whose boiling temperature is lower than that of the primary fluid. The machine includes, in particular, primary vapor cooling means comprising a heat exchanger (11) for exchanging heat between the primary vapor and the secondary fluid (12), which means are provided with orifices (15) for exhausting the secondary vapor into the inside of the tank (4) so that the hat exchanger ensures that the primary vapor condenses and that the secondary fluid vaporizes, thereby making it possible to obtain thermal self-stabilization inside the tank.
    Type: Grant
    Filed: June 7, 1996
    Date of Patent: October 6, 1998
    Inventor: Jean-Paul Garidel
  • Patent number: 5814192
    Abstract: A vapor compression distillation apparatus includes a vessel for containing a liquid to be distilled and a heat exchanger of the shell and tube type immersed in the liquid. The heat exchanger has top and bottom manifolds and vertical tubes surrounded by a shell. Foraminous vortex-drag induction plates extend across the shell between adjacent rows of tubes for inducing turbulence in the vortices to provide a better heat transfer from vapor passing through the shell to liquid in the tubes. Baffles are provided at selected intervals across the shell, between adjacent rows of tubes to produce a sinuous flow path for the heating medium. Steam injecting sparging tubes extend along the lower manifold of the heat exchanger to inject steam bubbles into the liquid to be evaporated. This produces turbulence in the tubes of the heat exchanger, promotes a better flow through the tubes and scrubs the tube interiors.
    Type: Grant
    Filed: October 3, 1996
    Date of Patent: September 29, 1998
    Assignee: Terra Mannix Inc.
    Inventors: Lee Pittmon, Randy Wasilenko, Brian Fisk
  • Patent number: 5810976
    Abstract: A device for processing water having high concentrations of scale forming compounds and high solids content in a high efficiency vapor compression distillation system wherein a plate-in-frame heat exchanger is submerged in a boiling solution contained in a boiler drum. An impeller in the drum continuously circulates the boiling solution through the heat exchanger at a velocity to prevent suspended solids from accumulating and to inhibit scale formation on the boiling surfaces of the heat exchanger.
    Type: Grant
    Filed: December 23, 1996
    Date of Patent: September 22, 1998
    Assignee: Grand Environmental Corporation
    Inventor: Robert C. Keith
  • Patent number: 5770020
    Abstract: The invention relates to a distillation apparatus (1) which is suitable in particular for the distillation of sea water into fresh water. The apparatus includes a plurality of flat, bag-like elements (3) formed from a thin film material such as plastic film and placed one against the other, the elements serving as heat exchangers between a vaporizing liquid flowing along the exterior surfaces of the element and a condensing vapor directed to the inside of the element, and a compressor (15) for increasing the pressure and temperature of the generated vapor before it is directed to the inside of the elements. The essential idea of the invention is that at the upper end of each bag-like element (3) there is a honeycomb-structured end strip (4) having substantially the width of the element, the strip containing parallel feeding ducts (26) separated from each other by partition walls, the ducts distributing the liquid to be evaporated over the entire width of the element surface.
    Type: Grant
    Filed: November 18, 1996
    Date of Patent: June 23, 1998
    Assignee: Keeran Corporation N.V.
    Inventors: Peter Koistinen, Reijo Rantala
  • Patent number: 5766412
    Abstract: A system is disclosed for reducing the amount of waste water and recovering reusable constituents from a waste stream comprising at least two constituents having different relative volatilities. The system includes a vapor thermocompression evaporator, into which the waste stream is directed, to vaporize one of the constituents within the waste stream without appreciably vaporizing other constituents in the waste stream. The vapor thermocompression evaporator also has a vapor compressor for compressing the vaporized fraction of the first constituent and delivering this compressed vaporized fraction to transfer heat to the waste stream. The system further has a film evaporator in series with the vapor thermocompression evaporator which transfers heat to the stream after it leaves the vapor thermocompression to vaporize substantially all of the first constituent without appreciably vaporizing the second constituent.
    Type: Grant
    Filed: January 13, 1997
    Date of Patent: June 16, 1998
    Assignee: Recovery Technologies Corporation
    Inventor: Jay M. Railey
  • Patent number: 5733417
    Abstract: A regenerating system, for the removal of water and potentially harmful organic constituents from a dehydration fluid used to dehydrate gas. The system includes apparatus for converting all the organic constituents to a gaseous phase; and utilizing the gaseous organic constituents in the separation of the water from the dehydration fluid.
    Type: Grant
    Filed: November 4, 1996
    Date of Patent: March 31, 1998
    Assignee: Gas Research Institute
    Inventor: Adolph J. Foral
  • Patent number: 5732476
    Abstract: The generation of volatiles from liquid or solid materials is enhanced and accelerated by exposure to microwave radiation. Normally the energy transfer is effected preferentially toward the liquid or solid materials over the generated gaseous volatiles. Sufficient energy is provided at a selected rate that enhances the generation of volatiles to effect removal as vapor or to produce a pressurized vapor phase. Flow-through separations from a matrix having a microwave-absorbing liquid component are conducted by exposing to microwave radiation to vaporize this component and processing the vapor either by flowing through a selective permeable membrane, or by enclosing the vapor and matrix in a confined space and flowing matrix through a selected separation medium, and recovering residual matrix. These separations are particularly useful in analysis contexts.
    Type: Grant
    Filed: May 24, 1996
    Date of Patent: March 31, 1998
    Inventor: J.R. Jocelyn Pare
  • Patent number: 5734004
    Abstract: The present invention relates to a distillation process for the purification of carbonic acid diaryl esters.
    Type: Grant
    Filed: January 6, 1997
    Date of Patent: March 31, 1998
    Assignee: Bayer Aktiengesellschaft
    Inventors: Steffen Kuhling, Kaspar Hallenberger, Pieter Ooms, Hans-Josef Buysch, Gunther Jeromin
  • Patent number: 5676801
    Abstract: A radial-inflow large volume-rate low pressure-differential, single-stage compressor comprising 2 periphiral concentric sets of axial blades spaced circumferentially between two supporting rings and further strengthened against bending by intermediate rings if necessary. The outer set of blades rotates to impart energy to the working fluid and the inner set is stationary to recover kinetic energy. Stationary guide surfaces concentric with the blades direct the radially inward flow to axial. A diverging duct recovers further the kinetic energy. The compressor fills the pressure-ratio gap between blowers and turbo-compressors. Its use in desalination instead of the currently used centrifugal compressors, can scale-up the vapor-compression unit-size to more than three fold.
    Type: Grant
    Filed: February 6, 1995
    Date of Patent: October 14, 1997
    Inventor: Yehia El-Sayed
  • Patent number: 5645694
    Abstract: An improved vapor compression distillation process and apparatus are provided having a container with a substantially horizontal longitudinal center axis, two opposing end plates closing each end of the container, a first and second passage area defined within and on opposing ends of the container, each adjacent one of the end plates, a collecting chamber defined within the container between the first and second passage areas, a plurality of generally horizontal tubes spacedly exposed within the collecting chamber generally parallel to the longitudinal axis of the container, each of the tubes having two opposing ends which open into the first and second passage areas respectively, two opposing plates positioned on opposite ends of the horizontal tubes, each plate engaging similar ends of the horizontal tubes, a vapor compressor attached to the container such that the vapor compressor communicates with an upper area of the collecting chamber and communicates with the first passage area, at least one passage fo
    Type: Grant
    Filed: March 31, 1993
    Date of Patent: July 8, 1997
    Assignee: Vacom II, L.P.
    Inventors: James M. Stewart, Bobby D. Morris
  • Patent number: 5645692
    Abstract: A method and apparatus for stabilizing crude oil at the outlet of a well, including at least one separation step wherein the crude oil is pressure distilled in at least one distillation column into at least two cuts, i.e., a C.sub.1-5 hydrocarbon gas cut recovered at the top of the column and a stabilized crude oil cut recovered below the point where the original crude oil was injected into the column. The method advantageously includes at least one decompression step before the separation step.
    Type: Grant
    Filed: June 26, 1995
    Date of Patent: July 8, 1997
    Assignee: Elf Aquitaine Production
    Inventors: Jean-Paul Gourlia, Jacques Tournier Lasserve, Georges Bihn-Cirlot, Jean Vandermeersch
  • Patent number: 5643418
    Abstract: A device for intercepting liquid obtained from a stream of mixed fluids contains an enclosure having an upper opening and a lower opening. The upper opening is connectible to a source of suction while the lower opening is connectible to a source of the mixed fluids. A partition between the openings divides the enclosure into a liquid collecting section which includes the upper opening and a liquid discharging section which includes the lower opening. The partition has a liquid flow passage at the lower end thereof and an orifice at the upper end thereof, and the orifice provides a pressure drop between the two openings. A liquid collecting basin is formed at the bottom of the enclosure, and the lower opening is provided with an overflow for the basin. In operation, the suction source draws a stream of mixed fluids from the mixed fluid source. Liquid is derived from the stream in or above the liquid collecting section and forms a pool in the liquid collecting basin.
    Type: Grant
    Filed: November 14, 1994
    Date of Patent: July 1, 1997
    Inventor: William A. Witschi
  • Patent number: 5632864
    Abstract: A splash shield for the boiler of a distillation type water purification apparatus includes at least two grades of porous media which cooperatively inhibit bubble formation and splashing, thereby preventing transfer of contaminants from the boiler water to the upper, interior surfaces of the boiler and into the distilled, contaminant free water. A first porous media is open cell reticulated foam having relatively large cells. Typically, at least a portion of the open cell foam is disposed above the operating liquid level of the boiler. The second porous media is fabric or screen having pores preferably smaller than about one thousand microns. The screen is disposed above the liquid level of the boiler. The open cell foam inhibits bubble production and breaks down bubbles and the screen intercepts drops and droplets that might otherwise travel to, contact and contaminate the upper boiler chamber surfaces and output to a condenser.
    Type: Grant
    Filed: July 6, 1995
    Date of Patent: May 27, 1997
    Assignee: Kuss Corporation
    Inventor: Brian J. Enneper
  • Patent number: 5630913
    Abstract: A water distillation system (10) includes a boiling chamber (11) and a condensation chamber (12). Water is fed via an inlet pipe (13) to a degassing chamber (15) where volatile gases are removed from the water. The water is evaporated in the boiling chamber (11) and vapour is, in turn, condensed in the condensing chamber (12). Distilled water is collected in a water storage tank (30) and is used, with a pump (28) and entrainment device (27), to provide a substantial vacuum within the system (10).
    Type: Grant
    Filed: March 14, 1995
    Date of Patent: May 20, 1997
    Inventor: Davoud Tajer-Ardebili