Patents Assigned to Axens
  • Patent number: 9295985
    Abstract: A reactor for regenerating catalyst grains comprises a vessel having an oxychlorination zone superimposed over a calcining zone having a line for introducing gas. A chamber, disposed between oxychlorination and calcining zones, comprises an internal space located between two plates which are gas tight and impervious to catalyst grains. A plurality of tubes pass through the chamber to allow catalyst to pass from oxychlorination zone to calcining zone. A plurality of means pass through the chamber to allow calcining gas to pass from calcining zone to oxychlorination zone. At least one oxychlorination gas injection line opens into the internal space of the chamber. Each means for passage of calcining gas comprises at least one orifice communicating with the chamber internal space, and a means for evacuating gas which is permeable to gas and impermeable to catalyst grains.
    Type: Grant
    Filed: July 24, 2013
    Date of Patent: March 29, 2016
    Assignee: AXENS
    Inventors: Xavier Decoodt, Cecile Plais, Frederic Bazer-Bachi
  • Patent number: 9297792
    Abstract: The present invention describes an analysis device and a method associated with this device, said device comprising an analysis cell (8) containing an optrode (10), receiving an input laser signal and sending an output signal to the Raman spectrometer, and said method using two analysis routes: an analysis route 1 connected to the internal circulation current passing from adsorber B to adsorber A, and an analysis route 2 connected to the distilled raffinate originating from distillation column C.
    Type: Grant
    Filed: June 12, 2014
    Date of Patent: March 29, 2016
    Assignee: AXENS
    Inventor: Gerard Hotier
  • Publication number: 20160075955
    Abstract: Process for hydrogenation of aromatic compounds in a feedstock comprising hydrocarbons having at least five carbon atoms, comprising: a) contacting feedstock, a hydrogen gas, and a nickel or platinum hydrogenation catalyst at 100 to 400° C., 0.5 to 8 MPa, and a feedstock flow rate 0.5 to 5 h?1, as to produce a partially-hydrogenated hydrocarbon feedstock and gas; and b) contacting the partially-hydrogenated feedstock, and a nickel or platinum hydrogenation catalyst at 100 and 400° C., a pressure of between 0.5 and 8 MPa, with a flow rate of the partially-hydrogenated feedstock between 0.3 and 8 h?1, a ratio between the volume of hydrogen and the volume of the partially-hydrogenated feedstock between 0.3 and 3 Nm3/m3, and a ratio between the superficial mass flow rate of the partially-hydrogenated feedstock and the superficial mass flow rate of gas (Ul/Ug) at the inlet of the reactor between 50 and 500.
    Type: Application
    Filed: April 10, 2014
    Publication date: March 17, 2016
    Applicant: AXENS
    Inventors: Jean-Christophe CANDELON, Fabienne LE PELTIER, Annick PUCCI
  • Publication number: 20150336023
    Abstract: The present invention relates to a method for recovering heat available at low temperature in a process and its use in order to reduce the energy consumption of the said process. Application of the method to an aromatics complex in which the low-temperature heat is recovered at the head of distillation columns in the form of low-pressure steam and is reused to reboil other distillation columns in which the operating pressure has possibly been lowered.
    Type: Application
    Filed: October 17, 2013
    Publication date: November 26, 2015
    Applicant: AXENS
    Inventors: Alain DUNET, Isabelle PREVOST, Thierry LEFLOUR
  • Publication number: 20150315493
    Abstract: The present invention describes a process for the production of technical white oils or edible or medicinal oils from waste oils originating from industrial use or engine use, said process using a deep hydrotreatment.
    Type: Application
    Filed: December 9, 2014
    Publication date: November 5, 2015
    Applicant: AXENS
    Inventors: Frederic MOREL, Jerome BONNARDOT, Isabelle GUIBARD
  • Publication number: 20150275112
    Abstract: The present invention concerns an integrated process for the production of liquid hydrocarbons starting from a feed containing at least one fraction of biomass and optionally at least one fraction of another feed, said process comprising at least one pre-treatment step, a gasification step, a step for conditioning synthesis gas, a water scrubbing step, a step for eliminating acid gases, a final purification step, and a catalytic Fischer-Tropsch synthesis reaction step.
    Type: Application
    Filed: October 30, 2013
    Publication date: October 1, 2015
    Applicants: IFP ENERGIES NOUVELLES, AXENS, TOTAL RAFFINAGE CHIMIE, SOFIPROTEOL, THYSSENKRUPP UHDE GMBH, BIONEXT
    Inventors: Guillaume Boissonnet, Michael Hecquet, Priscilla Avenier, Laurent Bournay, David Chiche, Jean-Philippe Heraud, Anne Claire Lucquin, Norbert Ullrich, Stéphane Fedou, Julien Rousseau, Raphael Lemaire, Jean-Christophe Viguie
  • Publication number: 20150175906
    Abstract: Method for optimising the production of middle distillate in a refinery, comprising at least one catalytic cracking unit (3) and at least one vacuum distillation unit (2, 4), the optimising operation consisting in: a) recycling (14) at least part of the cut obtained by fractionation of the effluents from catalytic cracking of an atmospheric and/or vacuum residue, distilling at at least 320° C. also called 320° C.+ cut in the feed of the said vacuum distillation unit (4), b) distilling the said cut under vacuum into at least two fractions, a fraction distilling between 320° C. and 550° C. called the HCOSV fraction, and a fraction distilling at at least 550° C. called the SSV fraction, c) sending the HCOSV fraction (18) thereby obtained to at least one of the distillate treatment units, d) and sending the SSV fraction (13) to the feed of the catalytic cracking unit (3), as such or after intermediate upgrading treatment.
    Type: Application
    Filed: December 12, 2012
    Publication date: June 25, 2015
    Applicants: AXENS, TOTAL RAFFINAGE FRANCE
    Inventors: Marc Bories, Michael Echard, Romain Roux
  • Patent number: 9011676
    Abstract: Elimination of mercury contained in a hydrocarbon feed by: a) feed 1 is mixed with a hydrogen stream 14 and a gaseous fraction 13 originating from c), b) mixture 1a contacted with a catalyst to convert mercury compounds to elemental mercury producing an effluent containing elemental mercury 6, c) effluent containing elemental mercury is cooled to between 20° C. and 80° C., then, at 1.5 MPa and 3.5 MPa and between 20° C. and 80° C., separation 10 of said effluent containing the elemental mercury into a gaseous fraction 11 and a liquid fraction 15, at least a part of said gaseous fraction 11 being recycled to step a), d) fractionation 20 of liquid fraction 15 to produce a gaseous phase 42 and a liquid phase 21, and e) contacting at least a part of gaseous phase 42 with a mercury collection material 43.
    Type: Grant
    Filed: February 26, 2013
    Date of Patent: April 21, 2015
    Assignee: AXENS
    Inventors: Jean Christophe Candelon, Annick Pucci, Clotilde Jubin
  • Publication number: 20150065765
    Abstract: A process for purifying a hydrocarbon feed, using a first adsorption unit with first and second adsorption columns respectively filled with first and second adsorbent solids by simultaneously: a) treating the liquid phase hydrocarbon feed in the first adsorption column by contact with the first adsorbent solid to adsorb at least a portion of impurities present and to produce hydrocarbon effluent which is depleted in impurities; b) treating a secondary liquid hydrocarbon feed constituted either by a fraction of the hydrocarbon feed or by a fraction of the hydrocarbon effluent and depleted in impurities to purify the secondary liquid hydrocarbon feed; c) heating the treated secondary liquid hydrocarbon feed from step b); d) regenerating the second adsorbent solid of the second adsorption column which comprises impurities with the secondary hydrocarbon feed heated in step c) to desorb the impurities to produce an effluent with impurities.
    Type: Application
    Filed: March 11, 2013
    Publication date: March 5, 2015
    Applicant: AXENS
    Inventors: Isabelle Villechange, Tom Frising
  • Publication number: 20140368810
    Abstract: The present invention describes an analysis device and a method associated with this device, said device comprising an analysis cell (8) containing an optrode (10), receiving an input laser signal and sending an output signal to the Raman spectrometer, and said method using two analysis routes: an analysis route 1 connected to the internal circulation current passing from adsorber B to adsorber A, and an analysis route 2 connected to the distilled raffinate originating from distillation column C.
    Type: Application
    Filed: June 12, 2014
    Publication date: December 18, 2014
    Applicant: AXENS
    Inventor: Gerard HOTIER
  • Publication number: 20140360919
    Abstract: The invention concerns a fluid distribution device (1) comprising: at least one inlet tube (2) comprising openings (7) and having a first and a second end (3, 4); a cap (5) comprising a principal body (6) with a lenticular shape and with a circular section elongated by a skirt (8) extending in the direction of the second end (4) towards the first end (3) of the inlet tube (2), said cap (5) having an outer surface and an inner surface, the cap being integral with the second end (4) of the tube via the inner surface and the principal body (6) being provided with a plurality of holes (10); and in which the cap (5) comprises at least one deflection means (14) disposed on its outer surface and configured to direct or maintain the gas towards or at the periphery of said cap (5).
    Type: Application
    Filed: June 10, 2014
    Publication date: December 11, 2014
    Applicant: AXENS
    Inventors: Jean Francois LE COZ, Daniel FERRE, Cyril COLLADO
  • Publication number: 20140316173
    Abstract: A process for producing jet fuel comprising the following steps: A.1) separating at least a portion of the C9 to C15 fraction from the product of a hydrocarbon synthesis process; A.2) converting at least a part of the separated C9 to C15 fraction to aromatic hydrocarbons; A.3) obtaining a jet fuel comprising the, optionally further treated, converted separated C9 to C15 fraction of step A.2); B.1) separating at least a portion of the C16+ fraction from the product of a hydrocarbon synthesis process; B.2) reducing the average number of carbon atoms of at least a portion of the separated C16+ fraction; B.3) optionally, separating the C9 to C15 fraction of at least a portion from the product obtained from step B.2); and B.4) adding at least a portion of the C9 to C15 fraction separated in step B.3), if present; or at least a portion of the product of step B.2).
    Type: Application
    Filed: April 16, 2014
    Publication date: October 23, 2014
    Applicants: Sasol Technology (PTY) Ltd., Axens
    Inventors: Ewald Watermeyer De Wet, Pata Clair Williams, Stéphane Fedou, Marielle Gagniere
  • Patent number: 8816147
    Abstract: A process for recovering 1-hexene comprising: a) separating the mixture obtained from the ethylene trimerization reaction into a top fraction comprising ethylene and a bottom fraction, b) separating a portion of the bottom fraction obtained from step a) into a top fraction comprising 1-hexene and 1-butene and a bottom fraction, c) separating a portion of the fraction comprising 1-hexene and 1-butene obtained from step b) into a top fraction principally comprising 1-butene and into a bottom fraction principally comprising 1-hexene, and in said process: a portion of the bottom fraction obtained from step b) is returned to the reaction section and another portion of said bottom fraction obtained from step b) is used in a recirculation loop connecting the reaction section and the column of said step b), said recirculation loop being used to cool the reaction section and to reboil said column of step b).
    Type: Grant
    Filed: July 1, 2013
    Date of Patent: August 26, 2014
    Assignee: Axens
    Inventors: Daniel-Jean Vinel, Jean-Alain Chodorge, Jerome Pigourier, Pierre-Yves Martin, Laurent Bournay
  • Publication number: 20140088332
    Abstract: This invention describes a process for the production of 1,3-butadiene from ethylene implementing a stage for oligomerization of ethylene into n-butenes and into oligomers with 6 carbon atoms and more by homogeneous catalysis, a stage for separation in such a way as to obtain an n-butene-enriched fraction, and then a stage for dehydrogenation of said n-butene-enriched fraction.
    Type: Application
    Filed: September 23, 2013
    Publication date: March 27, 2014
    Applicant: AXENS
    Inventor: Gildas Rolland
  • Patent number: 8673135
    Abstract: The invention described herein relates to a novel process for reducing the carbon dioxide emissions from a coal and/or biomass liquefaction facility by utilizing a steam methane reformer unit in the complex designed to produce additional hydrogen which can be thereafter utilized in the process, as required for the plant fired heaters (including the SMR furnace), and for the production of plant steam. The plant light ends (C1, C2, etc.), which are normally utilized as fuel gas streams are the primary feeds to the SMR Unit along with the tail gas purge from a gasification complex within the facility.
    Type: Grant
    Filed: May 28, 2010
    Date of Patent: March 18, 2014
    Assignee: Axens
    Inventors: James J. Colyar, James B MacArthur, Michael Peluso
  • Publication number: 20140027348
    Abstract: A reactor for regenerating catalyst grains comprises a vessel having an oxychlorination zone superimposed over a calcining zone having a line for introducing gas. A chamber, disposed between oxychlorination and calcining zones, comprises an internal space located between two plates which are gas tight and impervious to catalyst grains. A plurality of tubes pass through the chamber to allow catalyst to pass from oxychlorination zone to calcining zone. A plurality of means pass through the chamber to allow calcining gas to pass from calcining zone to oxychlorination zone. At least one oxychlorination gas injection line opens into the internal space of the chamber. Each means for passage of calcining gas comprises at least one orifice communicating with the chamber internal space, and a means for evacuating gas which is permeable to gas and impermeable to catalyst grains.
    Type: Application
    Filed: July 24, 2013
    Publication date: January 30, 2014
    Applicant: Axens
    Inventors: Xavier DECOODT, Cecile PLAIS, Frederic BAZER-BACHI
  • Publication number: 20140027349
    Abstract: A reactor allowing continuous regeneration of catalyst grains having a chamber with an oxychlorination zone superposed on a calcination zone equipped with a pipe for introducing calcination gas and at least one pipe for injecting oxychlorination gas emptying into the inner space. Each gas passage has a gas evacuation device that is permeable to gas and impermeable to catalyst grains.
    Type: Application
    Filed: July 25, 2013
    Publication date: January 30, 2014
    Applicant: AXENS
    Inventor: Xavier DECOODT
  • Publication number: 20130327682
    Abstract: Method and plant for converting hydrocarbon feedstock comprising a shale oil, comprising a step of decontaminating, a step of hydroconverting in an ebullating bed, a step of fractionating into a light fraction, a naphtha fraction, a gas-oil fraction and a fraction heavier than the gas-oil fraction, the naphtha and gas-oil fractions being hydrotreated, the fraction heavier than the gas-oil fraction being conveyed to the decontaminating step. The method aims to maximize the yield of fuel bases.
    Type: Application
    Filed: December 16, 2011
    Publication date: December 12, 2013
    Applicants: AXENS, TOTAL RAFFINAGE MARKETING
    Inventors: Christophe Halais, Helene Leroy, Frederic Morel, Cecile Plain
  • Publication number: 20130319908
    Abstract: Method and plant for converting hydrocarbon feedstock comprising a shale oil, comprising a step of hydroconverting in an ebullating bed, a fractionation into a light fraction, a naphtha fraction, a gas-oil fraction and a fraction heavier than gas-oil, the naphtha and gas oil fraction being hydrotreated, the fraction heavier than gas oil being hydrocracked, the products of the hydrocracking being sent to the step for hydrotreating. The method aims to maximize the yield of fuel bases.
    Type: Application
    Filed: December 16, 2011
    Publication date: December 5, 2013
    Applicants: AXENS, TOTAL RAFFINAGE MARKETING
    Inventors: Christophe Halais, Héléne Leroy, Frederic Morel, Cecille Plain
  • Publication number: 20130319911
    Abstract: Method for converting hydrocarbon feedstock comprising a shale oil, comprising a step of hydroconverting in an ebullating bed, a step of fractionating by atmospheric distillation into a light fraction, a naphtha fraction, a gas-oil fraction and a fraction heavier than the gas-oil fraction, a step of liquid/liquid extraction of the fraction heavier than the gas-oil fraction, and a dedicated hydrotreating for each of the naphtha and gas-oil fractions. The method aims to maximize the yield of fuel bases.
    Type: Application
    Filed: December 16, 2011
    Publication date: December 5, 2013
    Applicants: AXENS, TOTAL RAFFINAGE MARKETING
    Inventors: Christophe Halais, Helene Leroy, Frederic Morel, Cecile Plain