Abstract: The invention relates to a method for preparing natural fibre-based composite materials containing natural binders and powdery proteins, comprising the following steps; adding a powdery protein adhesive binder to natural fibres having a moisture content of 1 15%; mixing the natural fibres together with the powdery protein adhesive; adjusting the moisture content of the composition to 6 24% w/w; and submitting the mixture to a heat pressure treatment to form the natural fibre-based material.
Type:
Grant
Filed:
January 21, 2002
Date of Patent:
June 17, 2008
Assignees:
Tate & Lyle Europe, ENSAM
Inventors:
Stephane Guilbert, Andreas Redl, Marie-Helene Morel
Abstract: Method for the preparation of gliadin- and glutenin-rich fractions from gluten in an aqueous medium and in the presence of an acid, wherein the gluten are dispersed continuously or not in water up to a dry substance varying between 5 and 30%, by which the pH of the dispersion is monitored between 4.4 and 4.8 and the gluten-water mixture is submitted to shearing actions, through which the dispersion, continuously or not, can be fractionated in gliadin- and glutenin-rich fractions, by which a single gliadin-rich fraction with a gliadin/glutenin ratio of at least 2.5 is obtained, and a single glutenin-rich fraction with a gliadin/glutenin ratio of less than 0.8 is obtained.
Abstract: Yeast strains transformed with at least one copy of a gene coding for lactic dehydrogenase (LDH) and further modified for the production of lactic acid with high yield and productivities, are described.
Type:
Grant
Filed:
December 27, 2005
Date of Patent:
February 5, 2008
Assignee:
Tate & Lyle Ingredients Americas, Inc.
Inventors:
Danilo Porro, Michele Bianchi, Bianca Maria Ranzi, Laura Frontali, Marina Vai, Aaron Adrian Winkler, Lilia Alberghina
Abstract: We report herein a composition comprising tricalcium citrate, wherein the tricalcium citrate has an X-ray powder diffraction pattern comprising peaks at 2-theta (2?) values of about 8.236, about 16.02, about 17.97, about 19.75, about 21.42, about 25.74, and about 28.65. This tricalcium citrate is produced at high temperatures in a low-water environment. This composition is highly soluble (more than about 200 mg per 8 fluid ounces) in potable aqueous solutions (beverages), and can be used to fortify beverages (such as fruit juices) or foods with calcium at higher doses than seen when using previously-known compositions of tricalcium citrate.
Type:
Grant
Filed:
June 8, 2004
Date of Patent:
January 29, 2008
Assignee:
Tate & Lyle Ingredients Americas, Inc.
Inventors:
Alexandria L. Bailey, Warren L. Nehmer, Roy O. Elmore
Abstract: A process for producing alpha-amylase resistant starch comprises extruding a feed starch at a temperature in the range of about 60-220° C., thereby producing a product alpha-amylase resistant starch. The feed starch can be in the form of an aqueous slurry or paste that has a dry solids concentration of at least about 50% by weight. The process optionally can include the additional step of heating the product starch to a temperature of at least about 90° C. in the presence of moisture, to increase further the alpha-amylase resistance of the product.
Type:
Grant
Filed:
June 3, 2005
Date of Patent:
October 2, 2007
Assignee:
Tate and Lyle Ingredients Americas, Inc.
Inventors:
Warren L. Nehmer, Geoffrey A. R. Nobes, Walter C. Yackel
Abstract: The invention is directed to a chewing gum, including a gum base and at least one other conventional chewing gum component, said chewing gum including as gum base at least one branched polymer mainly based on biodegradable and/or hydrolyzable ester groups.
Abstract: A process for producing an enzyme-resistant starch uses an aqueous feed composition that comprises (i) starch that contains at least about 50% by weight amylose, (ii) water, and (iii) alcohol. The concentration of starch in the feed composition is between about 5% and about 50% by weight, and the pH of the feed composition is between about 3.5 and about 6.5. In a first heating step, the feed composition is heated to a temperature between about 130–170° C. for about 0.1–3.0 hours. The feed composition is cooled to a temperature between about 4–70° C. for about 0.1–6.0 hours. In a second heating step, the feed composition is heated to a temperature between about 110–150° C. for about 0.1–10.0 hours. The starch is separated from the majority of the water and alcohol and is dried.
Type:
Grant
Filed:
October 8, 2004
Date of Patent:
March 13, 2007
Assignee:
Tate & Lyle Ingredients Americas, Inc.
Inventors:
Ethel D. Stanley, legal representative, Patricia A. Richmond, Walter C. Yackel, Donald W. Harris, Thomas A. Eilers, Eric A. Marion, Keith D. Stanley, deceased
Abstract: The invention relates first of all to a process for preparing alkali- and heat-stable sugar alcohol compositions which exhibits an optical density lower than or equal to 0.100 in an S-test, in which a sugar alcohol composition is treated with a strong base anion exchange resin in the hydroxide form, at a temperature between 30° C. and 100° C. Second of all, the invention relates to a sorbitol composition.
Abstract: The invention relates to a method for preparing alkali and heat stable polyols, whereby sugar alcohols are treated with reagents to obtain stabilized sugar alcohol syrups and the stabilized alcohol syrup is subjected to a purification step by passing the stabilized sugar alcohol syrup over at least one ion-exchanger resin, and the stabilized sugar alcohol syrup being purified by a double passage over a cationic anionic ion-exchanger configuration (CACA), comprising at least a first weak acidic cationic ion-exchanger resin and a second strong, medium or weak basic anionic ion-exchanger resin.
Abstract: The invention relates to a method for preparing a high dry substance Stein Hall adhesive, comprising the steps of preparing a carrier portion by gelatinising at least a part of the total starch in the adhesive in an alkaline medium, diluting the carrier portion with a volume of water, and adding the remaining secundary starch in which a first step said carrier portion is prepared, in a second step the carrier portion is diluted with a volume of water, followed by the addition of at least a portion of the secundary starch, and in a third step the remaining alkali is added in a diluted form together with the secundary starch. The addition of the remaining secundary starch and alkali is preferably performed stepwise.
Abstract: Disclosed herein are processes for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The weight ratio in the first phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant. The first phase can be removed from the separated second phase in order to recover the 1,3-propanediol.
Type:
Grant
Filed:
May 6, 2003
Date of Patent:
June 6, 2006
Assignee:
Tate & Lyle Ingredidents Americas, Inc.
Inventors:
Avraham M. Baniel, Robert P. Jansen, Asher Vitner, Anthony Baiada
Abstract: The present invention relates to novel extractive methods for purifying sucralose. The present invention also relates to compositions comprising the sucralose preparations made by the methods of the present invention.
Type:
Grant
Filed:
March 8, 2002
Date of Patent:
May 23, 2006
Assignee:
Tate & Lyle Public Limited Company
Inventors:
Steven J. Catani, Nicholas M. Vernon, David Saul Neiditch, James Edwin Wiley, Jr., Edward Micinski
Abstract: Yeast strains transformed with at least one copy of a gene coding for lactic dehydrogenase (LDH) and further modified for the production of lactic acid with high yield and productivities, are described.
Type:
Grant
Filed:
February 6, 2002
Date of Patent:
May 23, 2006
Assignee:
Tate & Lyle Ingredients Americas, Inc.
Inventors:
Danilo Porro, Michele Bianchi, Bianca Maria Ranzi, Laura Frontali, Marina Vai, Aaron Adrian Winkler, Lilia Alberghina
Abstract: The invention refers to the production of recombinant gene products from cultures of the yeast Zygosaccharomyces bailii strains transformed with expression vectors bearing the gene coding for said proteins.
Abstract: Processes are disclosed for the purification and recovery of polysaccharide gums from an aqueous solution, particularly xanthan gum from a fermentation broth. An aqueous solution of at least one polysaccharide gum is mixed with a non-solvent stream comprising water and a subprecipitant level of a non-solvent of the polysaccharide gum. The mixture is concentrated to increase the polysaccharide gum concentration, and optionally undergoes a heat treatment. Additional non-solvent is added to the concentrated mixture to precipitate the polysaccharide gum. The precipitated gum is dried after being separated from the liquid component of the mixture. The removed liquid component can be recycled to the earlier step in the process in which the polysaccharide gum solution is mixed with the non-solvent stream.
Abstract: The present invention provides a meltable sucralose and acesulfame-k sweetener. This sweetener may be incorporated in a wide variety of reduced calorie food products such as cooked and hard candies, microwaveable food products, glazed food products, deep fried food products and as a substitute for sugar in applications that require melt sugar.
Abstract: This invention relates to processes for purifying sucralose by the use of an initial non-crystallization purification procedure followed by three or more sequential crystallization steps and recycle of the mother liquor remaining from each crystallization step to the feed of another crystallization or purification step. This invention also relates to sucralose compositions as well as compositions comprising the sucralose compositions of the present invention. These compositions may be highly pure and have a superior taste profile.
Type:
Grant
Filed:
March 8, 2002
Date of Patent:
February 14, 2006
Assignee:
Tate & Lyle Public Limited Company
Inventors:
Steven J. Catani, James E. Wiley, Nicholas M. Vernon, Carolyn M. Merkel, Edward Micinski
Abstract: Disclosed herein are methods for the recovery of at least one of an organic acid or an organic acid amide, such as a heat stable lactic acid or lactamide, from a feed stream which contains the organic acid and/or organic acid amide. The feed stream is mixed with at least one azeotroping agent. The azeotroping agent is a hydrocarbon capable of forming at least one heteroazeotrope with the organic acid or the organic acid amide in the feed stream. The mixture of the feed stream and the azeotroping agent is heated to produce a vapor stream. The heteroazeotrope is a component of that vapor stream. The vapor stream can be heated further to separate components or it can be condensed into a liquid stream. The liquid stream is capable of being separated into a first phase and a second phase. The first phase contains the highest concentration of the organic acid and/or the organic acid amide and the azeotroping agent is part of the second phase.
Type:
Grant
Filed:
March 15, 2001
Date of Patent:
January 3, 2006
Assignee:
Tate & Lyle Ingredients Americas, Inc.
Inventors:
Michael Charles Milner Cockrem, Istvan Kovacs
Abstract: A crystalline form of sucralose, and a method of making it. The method involves continuously crystallizing sucralose from an aqueous solution by a process providing continuous removal and recirculation of the vessel contents, and providing a long residence time for sucralose in the system. The crystals thus formed are of a relatively low length/diameter ratio, have an unsymmetrical shape, and exhibit good stability. The larger crystals in particular are tapered as compared to the rod-like larger crystals in prior art product.
Type:
Grant
Filed:
April 30, 2003
Date of Patent:
September 13, 2005
Assignee:
Tate & Lyle Public Limited Company
Inventors:
Steven J. Catani, Carolyn M. Merkel, Nicholas M. Vernon
Abstract: There is described a process for the synthesis of a sucrose-6-ester comprising: (a) reacting a mixture comprising sucrose and a polar aprotic solvent with an organotin-based acylation promoter, while adding a solvent capable of removing water by co-distillation, and removing water by co-distillation, to afford a first reaction mixture which is substantially free from water, followed by (b) adding a carboxylic anhydride to said first reaction mixture to afford a second reaction mixture, and maintaining said second reaction mixture at a temperature and for a period of time sufficient to produce a sucrose-6-ester, characterised in that step (a) is performed at a temperature of from 85 to 125° C. and at a pressure of from 20 to 80 kPa. In the most preferred embodiment, the polar aprotic solvent is DMF, the solvent capable of removing water by co-distillation is cyclohexane, the organotion-based acylation promoter is a 1,3-diacyloxy-1,1,3,3-tetrabutyldistannoxane, and step (a) is performed at approximately 97° C.