Abstract: Described are low ash, low phosphorus motor oils having improved oxidation stability as a result of the addition thereto of synergistic amounts of a dialkyldiphenylamine antioxidant and of a sulfurized polyolefin. The synergism between the two additives compensates for the decreased amounts of phosphorus in the form of zinc dithiophosphate such that the oils retain an SE quality rating.

Abstract: A hydrocarbyl-substituted dihydrouracil represented by the formula: ##STR1## in which R is a hydrocarbyl radical having an average molecular weight ranging from about 150 to 2000 and R' is hydrogen, a hydrocarbyl radical having from 1 to 20 carbon atoms, or an R"--(X--R'").sub.y -- radical in which R" is an alkyl radical having from 1 to 12 carbon atoms, X is oxygen or an --NH-- radical, R'" is a divalent hydrocarbon radical having from 1 to 3 carbon atoms and y is an integer from 1 to 3, a method for preparing said hydrocarbyl-substituted dihydrouracil, and a lubricating oil composition containing same is provided.

Abstract: An antifriction paste containing epoxy resin, molybdenum disulphide, graphite, aluminum, copper, alumosilicate and polyethylenepolyamine, the components being used in the following proportions (in parts by weight):epoxy resin: 40-80molybdenum disulphide: 15-30graphite: 10-15aluminum: 5-10copper: 5-10alumosilicate: 8-15polyethylenepolyamine: 5-10.The antifriction paste may also contain a solvent for the epoxy resin in an amount from 5 to 30 parts by weight. This paste is suitable for both small-and large-size friction assemblies. On the basis of this paste a solid lubricating coating with high antifriction performance is produced. Thus, a coefficient of sliding friction f.sub.fr. at a sliding speed V=0.06 m/s at a load P=10 kgf/cm.sup.2 is 0.2; linear wear rate I.sub.h under the same conditions is 1.0.10.sup.-9, and service life is as high as 500 km.

Abstract: Disclosed are compositions of matter and a method for their manufacture, and lubricating oil compositions containing such compositions. The compositions of matter comprise the reaction product of basic compound comprising overbased metal sulfonate, phenate, or mixtures thereof, with acidic compound comprising organic carboxylic acid, organic carboxylic acid anhydride, phosphoric acid, phosphoric acid ester, thiophosphoric acid ester, or mixtures thereof.

Abstract: A quaternary ammonium succinimide salt composition represented by the formula: ##STR1## in which R is a hydrocarbyl radical having from 25 to 200 carbon atoms, R.sub.1 is a divalent hydrocarbon radical having from 3-10 carbon atoms, R.sub.2 is hydrogen or an alkyl radical having from 1 to 4 carbon atoms, z has a value from 0 to 5 and X is a halide radical is provided, as well as a method of preparation and a lubricating oil composition containing same.

Abstract: The oil-in-water emulsion contains, besides the usual components, xylitol and sorbitol to inhibit water staining. The inhibitor is fully effective even when 1000 parts by weight of the emulsion contain only 1-30 parts by weight each of xylitol and sorbitol.By making this addition of inhibitor the reaction of the water phase with the metal surface freshly created by rolling is to a large degree eliminated and with that also the elimination of the formation of undesirable water stains on the surface of the strip.

Abstract: Engine fuel economy is improved by adding a friction-reducing amount of a N-hydroxymethyl aliphatic hydrocarbyl succinimide to the engine crankcase oil or fuel.

Abstract: Disclosed are molybdenum derivatives of high molecular weight alkenylsuccinimides and lubricant compositions containing such derivatives which impart dispersant, oxidation inhibition, anti-wear and friction-reducing properties to these compositions.

Abstract: A lubricating oil composition containing a blend of sulfurized calcium alkylphenolate having an alkylphenol to calcium metal rate of about 1.0 to 1.4 and a Ca content of 0.5 to 12 wt. % prepared by: (1) reacting at a temperature between 250.degree. and 410.degree. F. an alkylphenol with calcium alkoxyalkoxide to form a first reaction mixture utilizing between about 45 and 90 wt. % of the stoichiometric amount required to convert the alkylphenol to calcium alkylphenolate: (2) contacting the reaction mixture with sulfur at a temperature between about 440.degree. and 460.degree. F. in the presence of between about 13 and 20 wt. % of a lubricating oil based on the step 2 second reaction mixture, (3) contacting the second reaction mixture with calcium alkoxyalkoxide at a temperature between about 400.degree. and 425.degree. F.

Abstract: Amino phenols of the general formula ##STR1## wherein R is a substantially saturated hydrocarbyl substituent having an average of from about 30 to about 750 aliphatic carbon atoms; R' is a substituent selected from the group consisting of lower alkyl, lower alkoxyl, nitro, and halo; and z is 0 or 1, are useful as additives for fuels and lubricants. These amino phenols can be conveniently prepared by nitrating an appropriate hydroxy aromatic compound and reducing the nitro groups to amino groups.

Abstract: Amino phenols of the general formula ##STR1## wherein R is a substantially saturated, hydrocarbon-based group of at least about 30 aliphatic carbon atoms, a, b and c are, for example, each 1, 2 or 3, and Ar is an aromatic moiety such as a benzene nucleus, naphthalene nucleus or linked benzene nuclei, are useful additives for fuels and lubricants. These amino phenols can be conveniently prepared by nitrating an appropriate hydroxy aromatic compound and reducing the nitro groups to amino groups. Typically such amino phenols are formed by nitration and reduction of alkyl phenols having an alkyl or alkenyl group of at least about 50 carbon atoms.

Abstract: Synthetic lubricating oil composition having improved oxidation stability comprising a major portion of an aliphatic ester base oil having lubricating properties, formed by the reaction of pentaerythritol and an organic monocarboxylic acid and containing a phenylnaphthylamine, a dialkyldiphenylamine, a polyhydroxy anthraquinone, a hydrocarbyl phosphate ester and a dialkyldisulfide.

Abstract: A process for recovering and recycling chromium from chromium-iron hydroxide sludge for use in cooling tower make up water and plating solution is disclosed. The process comprises separating chromium from the sludge by selectively oxidizing the trivalent chromium precipitate to soluble hexavalent chromium with a strong oxidizing agent such as chlorine gas, in alkaline medium. The hexavalent chromium ions then enter solution and are thereafter separated from the iron hydroxide precipitate as the sludge is dewatered.

Abstract: The invention provides a process and an apparatus for hydrogenative liquefaction of coal to produce high yields of gasoline fraction and optional yields of diesel and residue fraction, all of superior quality. The coal is slurried and digested in two separate and distinct streams. The parting oil of the first stream is heavy residue fraction derived to a substantial extend from the second stream, mixed with light oil derived partly or wholly from the first stream. The pasting oil of the second stream is middle oil derived from the fractionated discharge of the first stream, any shortfall being made up from the discharge of the second stream. A high degree of flexibility is possible by varying the ratio of coal fed to the respective streams between 3:1 and 1:3, and individual manipulation of the process parameters within each stream in respect of pressure, temperature, catalyst, residence time, pasting oil composition and coal quality.

Abstract: Corrosive wear caused by aminated sulfurized olefins can be reduced by reaction of the aminated sulfurized olefine with a boron compound and formaldehyde.

Abstract: Improved dispersants are prepared by oxidizing an olefin and reacting the oxidized olefin with sulfur or a sulfur-yielding compound and an amine.

Abstract: Processes for the production of aminated sulfurized olefins are improved by performing the reaction in the presence of a tar and charred reaction byproduct reducing amount of an alkali metal or alkaline earth metal compound.

Abstract: Water-soluble polyesters formed by the condensation of polyoxyalkylene glycol with the addition product of a dimer fatty acid and maleic anhydride are found to be particularly useful as lubricants and as viscosity adjusting additives in aqueous hydraulic systems.

Abstract: Metal-working compositions (water-base, oil-base and oil-in-water emulsions) containing triazole and thiadiazole compounds are disclosed. These compositions prolong the working life of metal cutting and grinding tools containing tungsten carbide particles bonded together by nickel or cobalt. The oil-base coolant and lubricant comprises a mineral oil, a triazole or thiadiazole compound, and optionally, an extreme pressure lubricant, fats, rust preventives and mist suppressants. The aqueous base and oil-in-water emulsion metal-working compositions are prepared in the form of a liquid concentrate which subsequently is diluted with water to form the metal-working coolant or lubricant. The concentrate to be diluted and made into an aqueous coolant and lubricant comprises a triazole and thiadiazole compound, boric acid, an amine or mixture of amines, sodium gluconate and an aromatic or paraffinic carboxylic acid.

Abstract: Carboxylic acid terminated diamides and alkali metal, ammonium or amine salts thereof are provided which are derived from the reaction of organic polycarboxylic acids and polyoxyalkylene diamines. The diamides have lubricating properties and are especially useful in aqueous metal working fluids.