Patents Examined by Francis C Campanell
  • Patent number: 9550799
    Abstract: A process is provided for preparing a salt of a hydroxy-substituted ester of phosphoric acid, comprising: (a) reacting a phosphate diester with an alkylene oxide, (b) reacting the product mixture of step (a) with a phosphating agent; and (c) reacting the product mixture of step (b) with an amine; wherein the phosphate diester is reacted with the alkylene oxide of step (a) in the substantial absence of a phosphate monoester. The product is useful as an antiwear agent.
    Type: Grant
    Filed: August 23, 2011
    Date of Patent: January 24, 2017
    Assignee: The Lubrizol Corporation
    Inventors: Daniel J. Knapton, Troy A. Conant
  • Patent number: 9534182
    Abstract: A method of producing industrial corn base oil from a raw corn oil byproduct of a corn ethanol production process. The raw corn oil byproduct of the corn ethanol production process is first washed to separate water-soluble products from raw corn oil, then the free fatty acid in the resulting corn oil is neutralized using potassium hydroxide, and a polymeric quaternary biocide is added in a demulsification step, followed by vacuum dehydration of the demulsified corn oil, degumming of the dehydrated corn oil using citric acid, removal of red color from the oil, and final polishing.
    Type: Grant
    Filed: December 18, 2013
    Date of Patent: January 3, 2017
    Assignee: LiquiTech, LLC
    Inventor: Alan Ballard
  • Patent number: 9528069
    Abstract: The disclosed invention relates to lubricant or functional fluid compositions containing viscosity index improvers in the form of self-healing polymers. The polymers may comprise one or more cleavable linkages, such as one or more disulfide bonds and/or one or more diene/dienophile linkages, to permit the polymer to reform if cleaved during use.
    Type: Grant
    Filed: January 9, 2012
    Date of Patent: December 27, 2016
    Assignee: The Lubrizol Corporation
    Inventors: David Price, William R. S. Barton
  • Patent number: 9512377
    Abstract: The process basically comprises: dissolving a lamellar disulphide, as a source of the solid lubricant, in an aqueous solvent, forming a first aqueous solution; dissolving a reducing agent, as hydroxylamine, sodium hypophosphite or sodium borohydride, in an aqueous solvent, forming a second aqueous solution; mixing the first and second aqueous solutions, forming a third aqueous solution; neutralizing the pH of the third aqueous solution; dissolving a sulphur source, in an aqueous solvent, forming a fourth aqueous solution; mixing the third and fourth aqueous solutions, forming a fifth aqueous solution, which is contained and heated in an autoclave; cooling the fifth aqueous solution to the room temperature; and removing, from the autoclave, the nanoparticles in powder form.
    Type: Grant
    Filed: July 12, 2012
    Date of Patent: December 6, 2016
    Assignees: Whirlpool S.A., Universidade Federal De Santa Catarina
    Inventors: Roberto Binder, Fernando Withers Torres, Valderes Drago, Cristian Bernardi, Aloisio Nelmo Klein, Cristiano Binder, Andre Messias Teixeira
  • Patent number: 9512381
    Abstract: The invention relates to novel lubricity enhancing additives, to a method for producing the same, and to the use thereof.
    Type: Grant
    Filed: May 3, 2010
    Date of Patent: December 6, 2016
    Assignee: Rhein Chemie Rheinau GmbH
    Inventors: David Larem, Sandra Horstmann, Steffen Sandhöfner
  • Patent number: 9506008
    Abstract: A method for improving fuel efficiency and reducing frictional properties, while maintaining or improving deposit control, in an engine lubricated with a lubricating oil by using as the lubricating oil a formulated oil. The formulated oil has a composition including a lubricating oil base stock as a major component, and a combination of (i) a friction modifier mixture and (ii) a detergent, as a minor component. Fuel efficiency and friction reduction properties are improved and deposit control is maintained or improved as compared to friction reduction properties and deposit control achieved using a lubricating engine oil containing a minor component other than the combination of the friction modifier mixture and detergent. A lubricating engine oil having a composition including a lubricating oil base stock as a major component, and a combination of (i) a friction modifier mixture and (ii) a detergent, as a minor component.
    Type: Grant
    Filed: March 19, 2014
    Date of Patent: November 29, 2016
    Assignee: ExxonMobil Research and Engineering Company
    Inventors: Dennis A. Gaal, Erik Herz, Mrugesh Nilesh Patel, Douglas Edward Deckman, Smruti A. Dance
  • Patent number: 9487729
    Abstract: Provided are lubricant compositions and hydrocarbon fluids including one or more lubricant base stocks and an effective amount of one more zero SAP antiwear additives and/or corrosion inhibitor additives, wherein the one more antiwear and/or corrosion inhibitor additives include one or more functionalized polyolefins having one or more pyridazine moieties. Such compositions exhibit improved anti-wear, friction reduction and anti-corrosion properties.
    Type: Grant
    Filed: October 22, 2013
    Date of Patent: November 8, 2016
    Assignee: ExxonMobil Chemical Patents Inc.
    Inventors: Tabassumul Haque, Andy Haishung Tsou, Peter W. Jacobs, Rahul Ravindra Kulkarni, Donna Jean Crowther
  • Patent number: 9458406
    Abstract: An overbased calcium sulfonate grease composition comprising a reduced amount of overbased calcium sulfonate, calcium hydroxyapatite, base oil, one or more converting agents, and one or more complexing acids if a complex grease is desired. The calcium sulfonate grease composition improves thickener yield and expected high temperature utility as demonstrated by dropping point. A method of making the composition comprising the steps of mixing the calcium sulfonate and base oil, adding the calcium carbonate either before or after conversion, adding one or more converting agents, and adding one or more complexing acids. All or a portion of one or more of the complexing acids may be added with or prior to the one or more converting agents.
    Type: Grant
    Filed: October 31, 2012
    Date of Patent: October 4, 2016
    Assignee: NCH Corporation
    Inventor: J. Andrew Waynick
  • Patent number: 9441181
    Abstract: A friction modifying lubricant additive is provided comprising a base oil, colloidal nanocarbon particles, and a fluorine containing oligomeric dispersant. The fluorine containing oligomeric dispersant includes an anchoring group, a lipophilic hydrocarbon group, and a fluorinated oleophobic group. Further, a friction modifying lubricant additive is provided comprising a base oil, colloidal nanocarbon particles, a fluorine containing oligomeric dispersant, and at least one component selected from the group consisting of an antifriction component, an antiwear component, and an extreme pressure component. In another aspect, a method of manufacturing a lubricant additive is provided, the method comprising the step of mixing together a fluorine containing oligomeric dispersant, a dispersion of colloidal nanocarbon particles in a first base oil, and a second base oil.
    Type: Grant
    Filed: July 23, 2010
    Date of Patent: September 13, 2016
    Assignee: INTERNATIONAL TECHNOLOGY CENTER
    Inventors: Michail Grigorievich Ivanov, Leonid Evgenievich Deev, Olga Aleksandrova Shenderova
  • Patent number: 9404062
    Abstract: The invention provides a lubricating oil composition comprising a lubricating base oil with a kinematic viscosity at 100° C. of 1-10 mm2/s, a % Cp; of 70 or greater and a % CA of no greater than 2 and a viscosity index improver having a weight-average molecular weight of 100,000 or greater and a ratio of weight-average molecular weight to PSSI of 1.0×104 or greater, at 0.1-50% by mass based on the total amount of the composition, and having a kinematic viscosity at 100° C. of 9.0-12.5 mm2/s and a HTHS viscosity at 150° C. of 2.8 mPa·s or greater. It further provides a lubricating oil composition comprising a lubricating base oil with a kinematic viscosity at 100° C. of 1-6 mm2/s, a % Cp of 70 or greater and a % CA of no greater than 2, a hydrocarbon-based viscosity index improver with a PSSI of no greater than 20, and a poly(meth)acrylate-based viscosity index improver.
    Type: Grant
    Filed: May 11, 2010
    Date of Patent: August 2, 2016
    Assignee: JX NIPPON OIL & ENERGY CORPORATION
    Inventors: Akira Yaguchi, Shigeki Matsui, Teppei Tsujimoto
  • Patent number: 9394501
    Abstract: Provided herein are grease compositions comprising at least one estolide compound of formula: in which n is an integer equal to or greater than 0; m is an integer equal to or greater than 2; R1, independently for each occurrence, is selected from optionally substituted alkyl that is saturated or unsaturated, and branched or unbranched; R2 is selected from hydrogen and optionally substituted alkyl that is saturated or unsaturated, and branched or unbranched; and R3 and R4, independently for each occurrence, are selected from optionally substituted alkyl that is saturated or unsaturated, and branched or unbranched. Also provided are methods of making estolide-based grease products.
    Type: Grant
    Filed: February 6, 2012
    Date of Patent: July 19, 2016
    Assignee: Biosynthetic Technologies, LLC
    Inventors: Jeremy Forest, Jakob Bredsguard
  • Patent number: 9388362
    Abstract: A lubricating oil additive composition comprising the reaction product of an (a) an alkylated aromatic ether alcohol, (b) a source of boron, and (c) a hydrocarbyl polyol, having at least two hydroxyl groups.
    Type: Grant
    Filed: October 30, 2012
    Date of Patent: July 12, 2016
    Assignee: Chevron Oronite Company LLC
    Inventor: Yat Fan Suen
  • Patent number: 9371499
    Abstract: A lubricating oil additive composition comprising the reaction product of a (a) nitrogen-containing reactant, wherein the nitrogen-containing reactant comprises an alkyl alkanolamide, an alkyl alkoxylated alkanolamide, an alkyl alkanolamine, an alkyl alkoxylated alkanolamine or mixtures thereof, and wherein the nitrogen-containing reactant contains less than 10 mass percent of glycerol alkyl ester; (b) a source of boron; and (c) a hydrocarbyl polyol, having at least three hydroxyl groups.
    Type: Grant
    Filed: October 30, 2012
    Date of Patent: June 21, 2016
    Assignee: Chevron Oronite Company LLC
    Inventors: Yat Fan Suen, Francois Simard, Rachel M. Knight, John K. Ward
  • Patent number: 9365789
    Abstract: The invention provides a dialkyl ether represented by the following formula (1): (wherein each of R1 and R2 represents a C1 to C20 alkyl group, and n is an integer of 1 to 20), and a lubricating base oil and a lubricating oil composition containing the dialkyl ether. The lubricating base oil and the lubricating oil composition exhibit low viscosity, excellent viscosity-temperature characteristics, and high fluidity at low temperature.
    Type: Grant
    Filed: December 20, 2013
    Date of Patent: June 14, 2016
    Assignee: IDEMITSU KOSAN CO., LTD.
    Inventors: Yukio Yoshida, Miki Monoi
  • Patent number: 9347018
    Abstract: A lubricating oil composition for automatic transmission including (A) a lubricant base oil having a kinematic viscosity at 100° C. of from 1.5 to 20 mm2/s, (B) a polymethacrylate based viscosity index improver, and (C) a sulfur based compound having an acid value of not more than 1.0 mg-KOH/g and represented by the following general formula (1): S—(CH2CH2COOR)2??(1) (in the formula, R represents a hydrocarbon group having from 8 to 30 carbon atoms), which has a high transmission torque capacity and satisfactory gear change shock characteristics and attains excellent fuel efficiency, is provided. Also, a lubricating oil composition for automatic transmission which is a lubricating oil having a low viscosity and a high viscosity index and which, despite this, not only has excellent shear stability and fatigue resistance (durability) but has a high transmission torque capacity and satisfactory gear change shock characteristics and attains excellent fuel efficiency, is provided.
    Type: Grant
    Filed: January 28, 2010
    Date of Patent: May 24, 2016
    Assignee: IDEMITSU KOSAN CO., LTD.
    Inventor: Keiichi Narita
  • Patent number: 9309482
    Abstract: A universal synthetic water displacement multi-purpose penetrating lubricant with the capacity to protect metal surfaces against corrosion, with galvanic and electrolysis protection, while providing excellent lubrication properties. The lubricant actively penetrates the crystalline surface of the metal while exhibiting extreme pressure lubrication, non-migrating with lasting protection. The lubricant exhibits dielectric strength of over 14,000 volts, at the same time cleaning electrical contacts while reducing resistance and associated heat. A preferred embodiment comprises polymerized alpha-olefins, K-1 kerosene, and at least one base oil selected from the base oil group consisting of Hydroisomerized high base oils and HT severe hydro-cracked base oils. Various combinations of other optional ingredients are also disclosed.
    Type: Grant
    Filed: September 20, 2011
    Date of Patent: April 12, 2016
    Assignee: Bestline International Research, Inc.
    Inventor: Ronald J. Sloan
  • Patent number: 9309480
    Abstract: The disclosed invention relates to a multigrade lubricant composition which can be used for numerous lubricant applications, but is particularly useful for lubricating a diesel engine. The lubricant composition comprises an oil of lubricating viscosity, a detergent, a dispersant, a viscosity index improver, and a combination of anti-foam agents. The lubricant composition may be used for providing enhanced fuel economy and avoiding air entrainment problems when used in lubricating diesel engines.
    Type: Grant
    Filed: January 26, 2012
    Date of Patent: April 12, 2016
    Assignee: The Lubrizol Corporation
    Inventors: John G. Loop, William D. Abraham
  • Patent number: 9309478
    Abstract: The invention relates to a lubricating composition comprising (a) at least 0.05 wt % of a non-aromatic metal carboxylate, wherein the metal carboxylate is derived from a branched carboxylic acid, and (b) an oil of lubricating viscosity. The invention further provides for the use of the lubricating composition for lubricating a limited slip differential.
    Type: Grant
    Filed: October 21, 2009
    Date of Patent: April 12, 2016
    Assignee: The Lubrizol Corporation
    Inventors: Stuart L. Bartley, Mark R. Baker
  • Patent number: 9309481
    Abstract: A lubricant oil composition which is excellent in deposition resistance, corrosion resistance and wear resistance, despite its low phosphorus content and low sulfuric acid ash content, is provided by using a succinimide compound in combination with at least one selected from specific sulfur-containing compounds, specific heterocyclic compounds and reaction products thereof.
    Type: Grant
    Filed: March 10, 2011
    Date of Patent: April 12, 2016
    Assignee: IDEMITSU KOSAN CO., LTD.
    Inventors: Hideki Kamano, Masashi Kaji
  • Patent number: 9296972
    Abstract: A wear and/or friction reducing additive for a lubricating fluid in which the additive is a combination of a moderately hydrophilic single-phase compound and an anti-wear and/or anti-friction aqueous salt solution. The aqueous salt solution produces a coating on boundary layer surfaces. The lubricating fluid can be an emulsion-free hydrophobic oil, hydraulic fluid, antifreeze, or water. Preferably, the moderately hydrophilic single-phase compound is sulfonated castor oil and the aqueous salt solution additionally contains boric acid and zinc oxide. The emulsions produced by the aqueous salt solutions, the moderately hydrophilic single-phase compounds, or the combination thereof provide targeted boundary layer organizers that significantly enhance the anti-wear and/or anti-friction properties of the base lubricant by decreasing wear and/or friction of sliding and/or rolling surfaces at boundary layers.
    Type: Grant
    Filed: March 7, 2013
    Date of Patent: March 29, 2016
    Assignee: The United States of America as Represented by the Administrator of the National Aeronautics and Space Administration
    Inventors: Robert Chaffee Richmond, Harry F. Schramm, Jr., Francis G. Defalco