Abstract: A working electrode for cyclic voltammetry experiments and the like provides an electrode carrier releasably attaching to replaceable tips each holding a solid working electrode material that may be polished for receipt of a reactant material and which electrically connects to an electrode in the electrode carrier when the tip and carrier are connected.
Abstract: An electrochemical gas sensor includes an electrolyte including at least one ionic liquid which includes an additive portion including at least one organic additive, at least one organometallic additive or at least one inorganic additive.
Abstract: An aryl-alkyl (R—Ar) hydrocarbon is prepared by an electrosynthesis process in an electrolytic cell having an alkali ion conductive membrane positioned between an anolyte compartment configured with an anode and a catholyte compartment configured with a cathode. An anolyte solution containing an alkali metal salt of an alkyl carboxylic acid and an aryl compound is introduced into the anolyte compartment. The aryl compound may include an alkali metal salt of an aryl carboxylic acid, an arene (aromatic) hydrocarbon, or an aryl alkali metal adduct (Ar?M+). The anolyte solution undergoes electrolytic decarboxylation to form an alkyl radical. The alkyl radical reacts with the aryl compound to produce the aryl-alkyl hydrocarbon.
Type:
Grant
Filed:
April 22, 2011
Date of Patent:
June 9, 2015
Assignee:
CERAMATEC, INC.
Inventors:
Sai Bhavaraju, Mukund Karanjikar, Pallavi Chitta
Abstract: This invention relates to a sacrificial anode, comprising: a first layer of a first material; and, a second layer of a second material which is electrically connected to the first layer, wherein the first material is more anodic with respect to a galvanic series than the second material. The invention also relates to a body including the sacrificial anode.
Abstract: An analysis device is disclosed which includes an electron detection medium to obtain information needed for analyzing an analyte in correlation with an electron transfer level, and a reagent part which is disposed on the electron detection medium and includes an electron transporting substance to transport electrons between the analyte and the electron detection medium, the electron transporting substance including a water-soluble aromatic heterocycle compound, and being free of a metal complex. An analysis method using the analysis device is also disclosed.
Abstract: Electrode configurations for electric-field enhanced performance in catalysis and solid-state devices involving gases are provided. According to an embodiment, electric-field electrodes can be incorporated in devices such as gas sensors and fuel cells to shape an electric field provided with respect to sensing electrodes for the gas sensors and surfaces of the fuel cells. The shaped electric fields can alter surface dynamics, system thermodynamics, reaction kinetics, and adsorption/desorption processes. In one embodiment, ring-shaped electric-field electrodes can be provided around sensing electrodes of a planar gas sensor.
Type:
Grant
Filed:
December 12, 2008
Date of Patent:
May 19, 2015
Assignee:
University of Florida Research Foundation, Inc.
Inventors:
Bryan M. Blackburn, Eric D. Wachsman, Frederick Martin Van Assche, IV
Abstract: An electrochemical test sensor for detecting the concentration of an analyte in a fluid sample. The electrochemical test sensor includes a housing that has a first end and a second opposing end. The housing includes an opening at the first end to receive a fluid test sample. An electrode assembly includes a substrate, a working electrode, a counter electrode and a reagent. The substrate has a first surface and an opposing second surface. The working electrode is disposed on the first surface of the substrate, and the counter electrode is disposed on the second surface of the substrate. The electrode assembly is positioned within the housing to define a reaction channel. The electrochemical test sensor may be used with a removable lancet mechanism or integrated within a lancet mechanism to form one integral unit.
Abstract: The method for detection of cyanide in water is a method for the detection of a highly toxic pollutant, cyanide, in water using ZnO2 nanoparticles synthesized locally by an elegant Pulsed Laser Ablation technique. ZnO2 nanoparticles having a median size of 4 nm are synthesized from pure zinc metal target under UV laser irradiation in a 1-10% H2O2 environment in deionized water. The synthesized ZnO2 nanoparticles are suspended in dimethyl formamide in the presence of Nafion, and then ultrasonicated to create a homogenous suspension, which is used to prepare a thin film of ZnO2 nanoparticles on a metal electrode. The electrode is used for cyanide detection.
Type:
Grant
Filed:
March 14, 2013
Date of Patent:
May 19, 2015
Assignee:
KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
Inventors:
Mohammed Ashraf Gondal, Qasem Ahmed Qasem Drmosh, Z. H. Yamani, Tawfik Abdo Saleh
Abstract: A sensor system, device, and methods for determining the concentration of an analyte in a sample is described. Input signals including multiple duty cycles of sequential excitation pulses and relaxations are input to the sample. One or more signals output from the sample within 300 ms of the input of an excitation pulse may be correlated with the analyte concentration of the sample to improve the accuracy and/or precision of the analysis. Determining the analyte concentration of the sample from these rapidly measured output values may reduce analysis errors arising from the hematocrit effect, mediator background, and other error sources.
Abstract: A sensor cartridge for supplying a sensor is used. The sensor cartridge includes a casing within which the plurality of sensors can be arranged, and that allows a sample to be introduced to a sensor located at a preset location, and a connection structure. The connection structure electrically connects an external device and a sensor electrode of the sensor located at the preset location. The casing is formed so as to be held by the external device when the external device and the sensor electrode of the sensor are electrically connected via the connection structure.
Abstract: For use for a circuit board where a through hole and a blind via hole co-exist, an electrolytic copper plating bath in which the covering power for the through hole and the plugging performance for the blind via hole are sufficient, and an electroplating method that uses the electrolytic copper plating bath, are disclosed. The electrolytic copper plating bath is mainly composed of a water-soluble copper salt, sulfuric acid and chloride ions. A polyamide polyamine, obtained on processing by heating of an epichlorohydrin modified product of a polycondensation product of diethylene triamine, adipic acid and ?-caprolactam, is contained in the bath as a leveler.
Type:
Grant
Filed:
July 21, 2010
Date of Patent:
May 12, 2015
Assignee:
C. Uyemura & Co., Ltd
Inventors:
Toshihisa Isono, Naoyuki Omura, Koji Shimizu, Shinji Tachibana
Abstract: A method of manufacturing an electrode includes: providing a metal foil; depositing titanium metal on the metal foil; masking the titanium metal surface to control the density of sites where anodization will occur; and anodizing the Ti/metal foil so as to produce a nano-porous titania dielectric on the surface of the anode. The process may be on only one surface of the metal foil or on both sides simultaneously. The metal foil may be an aluminum foil. The porous titania dielectric may comprise titania nanotubes. An electrode structure may be fabricated using a linear process tool for reel-to-reel processing of a metal foil, the tool may include: a titanium deposition station for depositing a uniform thin film of titanium on the surface of the metal foil; a masking station for modifying the titanium surface to control the density of sites where anodization will occur; and an anodization station for transforming the Ti thin film into a porous titania dielectric film.
Abstract: A method for electroplating titanium alloy coating into plastic and carbon foam comprises the steps of activating the given specimen, deposition of electroless nickel and electroplating process of titanium alloy to the surface of the specimen. The electroplating process of electroplating titanium alloy coating includes a direct current method and a pulse plating method. The direct current method characterized by lager sized grains and the pulse plating method characterized by smaller sized grains. The advantages of proposed electroplating processes are: a) low cost, b) very broad applications and c) relatively low number of the process steps. Unique combination of physical, mechanical and chemical properties makes the electroplating methods of titanium coating an attractive technology for medicine, biotechnology, sports, defense, aeronautic, and auto industries.
Type:
Grant
Filed:
February 3, 2012
Date of Patent:
May 5, 2015
Assignee:
Crista Chemical Company LLC
Inventors:
Margaret E Parker, Piotr Cieplak, Barbara Gorecka
Abstract: Systems and methods for reducing overhang on electroplated surfaces of printed circuit boards are described. One such method includes applying a first resist layer on a substrate having a first copper layer, applying a first image to the first resist layer, developing the first resist layer in accordance with the first image, applying a second copper layer on the first copper layer, electroplating a first metallic layer on the second copper layer, removing the first resist layer, etching a portion of the first copper layer, removing the first metallic layer, depositing a third copper layer on a surface of the assembly, applying a second resist layer on the third copper layer, applying a second image to the second resist layer, developing the second resist layer in accordance with the second image, electroplating a preselected metal layer on the third copper layer, removing the second resist layer, and etching a portion of the third copper layer.
Type:
Grant
Filed:
June 16, 2011
Date of Patent:
April 28, 2015
Assignee:
Viasystems Technologies Corp. L.L.C.
Inventors:
Rajwant S. Sidhu, Ruben A. Zepeda, Carlos A. Lopez
Abstract: An electroplating system and components thereof facilitate an efficient electroplating process which in part reduces or eliminates the number of clips used on electroplating racks. Some electroplating racks may use skewers on which multiple plastic pieces are typically mounted. The plastic pieces may also be configured to be joined to form an assembly which is mounted on an electroplating rack. The configurations help reduce the time spent loading and unloading pieces on the racks.
Abstract: The present invention relates to a sampling plate. In particular the invention relates to a sampling plate for measuring certain selected properties of a liquid sample, such as the glucose levels in a blood sample. Sampling plates of the present invention have a sample zone (20) for receiving a liquid sample and an overflow reservoir (26) linked to the sample zone (20) via an overflow channel (26a), so that excess blood sample can be redirected away from the sample zone (20) and contained.
Abstract: An electronic device includes a substrate and a plurality of sensors. Each sensor is disposed in a well over the substrate and includes a working electrode, an inner filling solution disposed thereover, and an ion-selective membrane. The working electrode is in contact with the substrate and the ion-selective membrane is disposed over the inner filling solution and substantially seals the well.
Type:
Grant
Filed:
August 14, 2009
Date of Patent:
April 21, 2015
Assignee:
The Charles Stark Draper Laboratory, Inc.
Inventors:
James A. Bickford, John R. Williams, Daniel I. Harjes, Andrew Reiter
Abstract: Communications systems are provided for use with an impressed current cathodic protection (ICCP) system having single or multiple ICCP components. A pipeline may be provided by connecting multiple pipeline sections together as an integrated pipeline where each section has an associated ICCP system. A communications signal comprising an AC signal is impressed on the pipeline and received by receivers associated with power supplies associated with each ICCP system. Upon reception of the AC signal, a controllable switch is operated within the power supplies to synchronously disconnect them from their power source and thereby enable accurate testing of the ICCP system.
Abstract: A method of protecting a metal section in concrete. The method comprises the steps of providing a sacrificial anode and embedding the sacrificial anode in a porous matrix in the cavity; providing a source of DC power with positive and negative connections and electrically connecting one of the connections of the source of DC power to the metal section to be protected; electrically connecting the a sacrificial anode in series with the other connection of the source of DC power and spacing the source of DC power from the cavity and the connections to the source of DC power which comprise at least one of wires and cables; and driving an anode current density from the sacrificial anode in excess of 500 mA/m2. An apparatus of protecting a metal section in concrete is also disclosed.
Type:
Grant
Filed:
June 29, 2012
Date of Patent:
April 7, 2015
Inventors:
Gareth Kevin Glass, Adrian Charles Roberts, Nigel Davison