Abstract: Methods for producing components for use in high temperature systems that include reacting a fluid reactant and a porous preform that has a pore volume and contains a solid oxide reactant that defines a solid volume of the porous preform. The method includes infiltrating the fluid reactant into the porous preform to react with the solid oxide reactant to produce a oxide/metal composite component, during which a displacing metal replaces a displaceable species of the solid oxide reactant to produce at least one solid oxide reaction product that has a reaction product volume that at least partially fills the pore volume. The oxide/metal composite component includes at least one oxide phase and at least one metal phase. The component is exposed to temperatures greater than 500° C. and the at least one oxide phase and the at least one metal phase exhibit thermal expansion values within 50% of one another.
Abstract: The invention relates to a method for preparing synthetic mineral particles with formula (AlyM1-y)2(SixGe1-x)2O5(OH)4, wherein M designates at least one trivalent metal selected from the group made up of gallium and the rare earths, which comprises the following steps: preparing a gel which is a precursor of said synthetic mineral particles by a co-precipitation reaction of at least one salt of metal selected among aluminium and M with at least one silicon source selected from the group made up of potassium metasilicate, sodium metasilicate, potassium metagermanate and sodium metagermanate, the molar ratio of (AlyM1-y) to (SixGe1-x) during the preparation of said precursor gel being equal to 1, at least one base being added during said co-precipitation reaction; and performing a solvothermal treatment of said precursor gel at a temperature of 250° C. to 600° C.
Type:
Grant
Filed:
September 27, 2016
Date of Patent:
June 7, 2022
Assignees:
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE, UNIVERSITE PAUL SABATIER TOULOUSE III
Inventors:
François Martin, Christophe Le Roux, Pierre Micoud, Marie Claverie, Cyril Aymonier
Abstract: A method of manufacturing a part, the method involving providing an apparatus, the apparatus having a metal skin component; a metal HIP can and a hollow space between a portion of the HIP can and a portion of the skin component, the method further involving filling the HIP can with a metal powder; evacuating the HIP can; sealing the evacuated HIP can; and applying a HIP process to the apparatus in a HIP chamber so as to form the part.
Abstract: Provided is a method of manufacturing a machine part having a radial crushing strength of 120 MPa or more, including: a compression molding step of compressing raw material powder including, as a main component, metal powder that is capable of forming an oxide coating and has a pure iron powder content ratio of 95 mass % or more, to thereby obtain a green compact (10) having a predetermined shape; and a coating forming step of causing the metal powder to react with an oxidizing gas while heating the green compact (10) at a temperature lower than a sintering temperature of the metal powder in an oxidizing gas atmosphere, to thereby obtain a reinforced green compact (11) in which the oxide coating (5) is formed between particles of the metal powder.
Abstract: A metal powder for powder metallurgy contains Fe as a principal component, Cr in a proportion of 11.0 mass % or more and 25.0 mass % or less, Ni in a proportion of 8.0 mass % or more and 30.0 mass % or less, Si in a proportion of 0.20 mass % or more and 1.2 mass % or less, C in a proportion of 0.070 mass % or more and 0.40 mass % or less, Mn in a proportion of 0.10 mass % or more and 2.0 mass % or less, P in a proportion of 0.10 mass % or more and 0.50 mass % or less, and at least one of W and Nb in a proportion of 0.20 mass % or more and 3.0 mass % or less in total.
Abstract: A method for producing a powder-metallurgical product, in particular a bearing element or a motor component, is provided. According to the method, a metal powder, typically with a grain size between 2 ?m and 15 ?m, is melt-metallurgically produced and agglomerated into a powder mixture having a grain size smaller than 400 ?m by organic binders and waxes. Subsequently, the agglomerated powder mixture is formed into a green body typically by way of uniaxial pressing and the formed green body thermally debindered. Finally, the debindered green body is sintered typically at temperatures of 1000° C. to 1300° C. and the sintered body reworked into the powder-metallurgical product.
Type:
Grant
Filed:
August 22, 2019
Date of Patent:
May 10, 2022
Assignee:
MAHLE International GmbH
Inventors:
Heiko Heckendorn, Lilia Kurmanaeva, Patrick Sutter, Klaus Wintrich
Abstract: A method and a plant for the production of a powdery starting material, which is provided for the manufacture of rare earth magnets, are disclosed. First of all, at least one magnetic material, which is comminuted into a powdery intermediate product with a possibly increased concentration of impurities, and/or at least one alloy including rare earth metal are provided, which includes a low concentration of impurities.
Abstract: A method of making an alloy includes mechanically alloying aluminum with an alloying element to form an alloy. The method may include a subsequent step of compacting the alloy powder to form an aluminum alloy compact. The alloying element may be chromium (Cr), nickel (Ni), molybdenum (Mo), titanium (Ti), manganese (Mn), vanadium (V), niobium (Nb), or silicon (Si).
Abstract: A method for manufacturing a poppet valve or mushroom valve includes providing a mixture of metal powder and a binder, filling and pressing said mixture in a mold, to obtain a green product, removing the binder from the green product, and thermally sintering the green product to a poppet valve blank, by hot isostatic pressing. A poppet valve is also provided that is manufactured with this method.
Type:
Grant
Filed:
April 27, 2017
Date of Patent:
April 19, 2022
Assignee:
Federal-Mogul Valvetrain GmbH
Inventors:
Andre Mareau, Stefan Kellermann, Antonius Wolking, Oliver Schulze, Andreas Heinek, Guido Bayard, Daniel Eisenring, Olaf Josef, Carsten Struebbe, Wolf-Dieter Streich
Abstract: The present invention discloses a method for manufacturing a thin-walled metal component by three-dimensional (3D) printing and hot gas bulging. The present invention uses 3D printing to obtain a complex thin-walled preform, which reduces a deformation during subsequent hot gas bulging. The present invention avoids local bulging thinning and cracking, undercuts at the parting during die closing, and wrinkles due to the uneven distribution of cross-sectional materials, etc. The present invention obtains a high accuracy in the form and dimension through hot gas bulging. After a desired shape is obtained by hot gas bulging, a die is closed to keep the component under high temperature and high pressure for a period of time, so that a grain and a phase of the material are transformed to form a desired microstructure.
Type:
Grant
Filed:
April 30, 2020
Date of Patent:
April 5, 2022
Assignee:
Dalian University of Technology
Inventors:
Zhubin He, Yi Xu, Jiangkai Liang, Wei Du, Peng Lin
Abstract: A system is provided, comprising a two-sided adapter, made of a Ni-based alloy, that is connected at each of the two sides with a different type of metal, e.g. steel, and wherein the connection of the different types of metal, e.g. steel with the adapter is characterized in that it is achieved at least in part by use of friction welding. A method for linking different types of metal, e.g. steel by using a two-sided adapter as an intermediate, wherein at least one of the adapter-metal (e.g. steel) connections is made by means of friction welding, is also provided.
Abstract: A film-shaped fired material of the present invention is a film-shaped fired material 1 which contains sinterable metal particles 10 and a binder component 20, in which a time (A1) after the start of a temperature increase, at which a negative gradient is the highest, in a thermogravimetric curve (TG curve) measured from 40° C. to 600° C. at a temperature-rising-rate of 10° C./min in an air atmosphere and a maximum peak time (B1) in a time range of 0 seconds to 2160 seconds after the start of a temperature increase in a differential thermal analysis curve (DTA curve) measured from 40° C. to 600° C. at a temperature-rising-rate of 10° C./min in an air atmosphere using alumina particles as a reference sample satisfy a relationship of “A1<B1<A1+200 seconds” and a relationship of “A1<2000 seconds”.
Abstract: Provided are a boron-nitride nanoplatelet(s) (BNNP)/metal nanocomposite powder and a preparing method thereof, the BNNP/metal nanocomposite powder including a base metal and BNNP dispersed in the base metal and configured to serve as a reinforcement of the base metal, wherein the BNNP are interposed between metal particles of the base metal in the form of a thin film of a plurality of layers and combined with the metal particles, and an amount of the BNNP in the base metal is greater than 0 vol % and less than 90 vol %.
Type:
Grant
Filed:
January 23, 2019
Date of Patent:
March 29, 2022
Assignee:
Korea Advanced Institute of Science and Technology
Inventors:
Soon Hyung Hong, Sung Chan Yoo, Jun Ho Lee, Hee Su Byeon
Abstract: Intended is to provide an aluminum alloy for die casting having a high strength as well as capable of achieving excellent elongation properties and a functional component using the aluminum alloy. The aluminum alloy comprises, by mass, 6 to 9% of Si, 0.30 to 0.60% of Mg, 0.30 to 0.60% of Cu, 0.25% or less of Fe, 0.60% or less of Mn, 0.2% or less of Ti, 200 ppm or less of Sr, and 5 ppm or less of P, with the balance being Al and inevitable impurities, and wherein Sr(ppm)?4.2×P(ppm)?50.
Abstract: A non-limiting embodiment of a titanium alloy comprises, in weight percentages based on total alloy weight: 5.5 to 6.5 aluminum; 1.5 to 2.5 tin; 1.3 to 2.3 molybdenum; 0.1 to 10.0 zirconium; 0.01 to 0.30 silicon; 0.1 to 2.0 germanium; titanium; and impurities. A non-limiting embodiment of the titanium alloy comprises a zirconium-silicon-germanium intermetallic precipitate, and exhibits a steady-state creep rate less than 8×10?4 (24 hrs)?1 at a temperature of at least 890° F. under a load of 52 ksi.
Type:
Grant
Filed:
August 28, 2018
Date of Patent:
March 8, 2022
Assignee:
ATI PROPERTIES LLC
Inventors:
John V. Mantione, David J. Bryan, Matias Garcia-Avila
Abstract: Manufacturing hard-metal pressed articles includes providing a multi-part die comprising a plurality of lateral mold parts defining lateral surfaces of a cavity for the article. At least one of the plurality of lateral mold parts defines a portion of an upper side of the cavity. The lateral mold parts and at least two lateral punch parts are fed. At least two of the plurality of lateral mold parts are provided with a guide recess for one of the at least two lateral punch parts. A filling unit feeds an opening of the cavity which is filled with a hard-metal powder. At least one upper mold part is fed, which defines a portion of the upper side of the cavity. The lateral mold parts and the upper mold part are held to form the cavity. The powder is compressed with at least two lateral punch parts and the part demolded.
Abstract: The present invention relates to a hot stamped component, a precoated steel sheet used for hot stamping, and a hot stamping process. The hot stamped component of the present invention is provided with a coating of aluminium or an aluminium alloy on at least one surface of the base steel, the coating is produced by interdiffusion between the base steel and a precoating of aluminium or aluminium alloy, and the coating has a thickness of 6 to 26 ?m.
Abstract: Methods for manufacturing components that include casting a first melt to produce an ingot, remelting the ingot to form a second melt, forming a powder from the second melt using an atomization process, and fabricating a component utilizing the powder in an additive manufacturing process. The ingot and the powder include an aluminum matrix that contains dispersions of TiB2 particles and Al3Ti particles and the component is a metal matrix composite having an aluminum matrix that contains dispersions of TiB2 particles and Al3Ti particles. Optionally, the metal matrix composite may include particles of an intermetallic compound of aluminum and at least one alloying element.
Abstract: The present invention provides a solder alloy, a solder paste, a solder ball, a resin flux-cored solder and a solder joint, both of which has the low-melting point to suppress the occurrence of the fusion failure, improves the ductility and the shear strength, and has excellent heat-cycle resistance. The solder alloy comprises an alloy composition composed of 35 to 68 mass % of Bi, 0.1 to 2.0 mass % of Sb, 0.01 to 0.10 mass % of Ni, and a balance of Sn. The alloy composition may contain at least one of Co, Ti, Al and Mn in total amount of 0.1 mass % or less. The solder alloy may be suitably used for a solder paste, a solder ball, a resin flux-cored solder and a solder joint.
Abstract: Fine metal particles of any one of Ag, Cu or Zn having a dispersing agent that is coordinated on the surfaces thereof, the dispersing agent having an acid value and an amine value which are both in a range of 0 to 20 mgKOH/g (wherein when either the acid value or the amine value is 0, the other one is not 0), and a dispersion solution in which the fine metal particles are dispersed. The fine metal particles and the dispersion solution containing the fine metal particles can be diluted with various kinds of solvents of either the water type or the organic type, and feature excellent dispersion property even after having been diluted.