Method of coating oxidized inorganic substrates with polyimide
substrates with oxidized surfaces, as e.g. SiO.sub.2 layers on silicon semiconductors and aluminum surfaces, are wetted with an organic silicon compound, for example, .gamma.-aminopropyltriethoxysilane dissolved in an organic solvent such as trichlorotrifluoro ethane. The solvent is then removed in a dry atmosphere. The evaporation step can be carried out by suspending the substrate in volvent vapor over a supply of refluxing solvent while cooling the solvent vapor such that fresh, dry solvent vapor continuously passes along the substrate and absorbs traces of moisture. Subsequently, a coating is applied from a solution of a polyamido carbon acid formed of pyromellitic acid anhydride and an aromatic amino component and the polyamido carbon acid is heated to form an adherent layer of polyimide.
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Type: Grant
Filed: May 19, 1976
Date of Patent: Jan 4, 1977
Assignee: International Business Machines Corporation (Armonk, NY)
Inventors: Friedrich C. Brunner (Sindelfingen), Peter U. Frasch (Boeblingen), Friedrich W. Schwerdt (Boeblingen), Theodor P. Vogtmann (Holzgerlingen)
Application Number: 5/687,965
International Classification: B05D 304; B05D 310;
