Automatic Temperature And/or Pressure Control Patents (Class 202/160)
-
Patent number: 8206557Abstract: In one embodiment, an apparatus includes a housing that has at least an inlet and an outlet. The housing is configured to receive a volume of fluid via the inlet. The volume of fluid is in a substantially liquid state and at least a portion of the volume of fluid includes a dissolved impurity. The apparatus also includes a heat-transfer element coupled to an interior volume of the housing. The heat-transfer element includes a surface, at least a portion of which is disposed at an angle with respect to a horizontal plane. The volume of fluid includes a surface parallel to the horizontal plane. The apparatus further includes a compression component configured to compress at least a portion of fluid boiled from the volume of fluid.Type: GrantFiled: November 7, 2007Date of Patent: June 26, 2012Assignee: Hydrologic Industries, Inc.Inventors: Francis P. Burke, Kenneth J. Horne, David B. Taylor, Stephen R. Topaz
-
Patent number: 8202401Abstract: In one embodiment, a method includes moving a first volume of fluid from a region above a heat-transfer element to a region below the heat-transfer element after the first volume of fluid is boiled from a second volume of fluid within the region above the heat-transfer element. The first volume of fluid including an impurity concentration lower than an impurity concentration of the second volume of fluid. The region below the heat-transfer element has a temperature higher than a temperature of the region above the heat-transfer element. The method also includes transferring latent heat from the first volume of fluid to a third volume of fluid on a top surface of the heat transfer element. The latent heat is released when the first volume of fluid condenses.Type: GrantFiled: November 7, 2007Date of Patent: June 19, 2012Assignee: Hydrologic Industries, Inc.Inventors: David B. Taylor, Stephen R. Topaz
-
Patent number: 8192588Abstract: Water is removed from oily water produced during operation of a separation column by withdrawing the oily water from the column during separation into an external separator where the oily water is separated into a water phase and an oily phase. The oily phase is then heated to a temperature effective to produce a density differential that drives the oily phase back into the operating column.Type: GrantFiled: August 28, 2008Date of Patent: June 5, 2012Assignee: Fluor Technologies CorporationInventor: John Mak
-
Patent number: 8177936Abstract: Evaporation of calciferous water is performed by an evaporator using electrical heating. An injection nozzle is connected to a spray hose arranged in an upper third of the evaporator, immediately above a thermostat that is disposed on the bottom side of the evaporator. A distance between the injection nozzle and the thermostat is less than 15 mm. A steam hose is connected to the evaporator via a steam connector. The steam connector has an inside diameter of at least 5 mm. The steam hose leads to a collector situated at an angle of inclination of 5° to 10°.Type: GrantFiled: May 5, 2009Date of Patent: May 15, 2012Inventor: Dietmar Berghaenel
-
Publication number: 20110308930Abstract: Provided is a dividing wall distillation column. The dividing wall distillation column includes a main column having a dividing wall. The main column includes a pressure equalization unit for pressure equalization between a preliminary divisional section and a main divisional section which are divided by the dividing wall. The dividing wall distillation column has an effect of enabling easier operations due to the uniform pressure drop between the two divisional sections divided by the dividing wall.Type: ApplicationFiled: February 12, 2010Publication date: December 22, 2011Applicant: LG CHEM, LTD.Inventors: Sung Kyu Lee, Joon Ho Shin, Jong Ku Lee
-
Publication number: 20110284361Abstract: The present invention provides fractional condensation apparatuses, systems and methods that can recover volatile products from highly diluted liquid and vapor feed mixtures with high purity and recovery yield, both in batch and continuous distillation, while being also designed to achieve low-cost and efficient recovery processes. Single apparatuses and columns can be connected to each other to expand or shrink the column length for desired separation. The apparatuses, systems and methods can be applied to separate mixtures with both narrow and wide boiling point ranges.Type: ApplicationFiled: August 5, 2011Publication date: November 24, 2011Applicant: Joule Unlimited Technologies, Inc.Inventors: Yizu Zhu, Johan van Walsem
-
Patent number: 8034217Abstract: A liquid condensation system heats a liquid raw material under a decompressed circumstance and evaporates a volatile component from a liquid surface to condense the liquid raw material. Therefore, the liquid condensation system includes: liquid condensers, each of which condenses the liquid raw material; a vacuum pump that is in communication with the liquid condensers; and a warm water circulation system as a heating source that heats the liquid raw material in the liquid condensers. The volatile component evaporated in the liquid condensers is led to the outside of the liquid condensers through vapor lines. The condensed liquid that is not evaporated in the liquid condensers is led to the outside of the liquid condensers through condensed-liquid lines. Condensed-liquid-line adjusting valves are interposed on the condensed-liquid lines, and heaters are attached to the condensed-liquid lines. A control unit controls the heaters and the condensed-liquid-line adjusting valves.Type: GrantFiled: February 7, 2008Date of Patent: October 11, 2011Assignee: Hitachi Plant Technologies, Ltd.Inventors: Yuzuru Ito, Yoshishige Endo, Hidekazu Tsudome, Fumiaki Numajiri
-
Patent number: 8029675Abstract: In a membrane distillation process in which a liquid to be concentrated is separated from a vapor space (11) by a vapor-permeable liquid- or water-tight membrane or membrane wall (13), to set the absolute pressure of the liquid to be concentrated a reduced pressure is imparted to this which lowers the absolute pressure of the liquid to be concentrated. A corresponding membrane distillation device is also specified.Type: GrantFiled: November 9, 2006Date of Patent: October 4, 2011Inventor: Wolfgang Heinzl
-
Patent number: 7955476Abstract: A multiple application recycling and purification device has a coaxial core that is horizontally oriented, non-rotating, cylindrical distillation chamber. The enhanced, completely coaxial configuration continuously cleans the entire distillation chamber and spreads a thin film of liquid to enhance distillation and positively aid in the removal of remaining contaminants. Through a timed and positioned valve, the device removes and purges lower-temperature contaminants. Timed valves and sensors control all phases of the distillation to provide a coaxially integrated, stand-alone, adaptable, scalable and maintenance free distillation unit that self-monitors, self-cleans and economically functions to produce the pure distilled liquid, e.g., water. This device can be modified to purify any numerous array of liquids and can be scaled to produce any amount of purified liquids for either household, commercial, or industrial applications.Type: GrantFiled: January 18, 2007Date of Patent: June 7, 2011Assignee: Mansur CorporationInventor: Pierre G. Mansur
-
Patent number: 7931782Abstract: A method of recovering a liquid medium from a mixture containing the liquid medium, the method including: (a) blowing a first gas into the mixture containing the liquid medium to vaporize the liquid medium, in a first vaporizing means, thereby to form a second gas containing which is a mixture of the first gas and vaporized liquid medium; (b) continuously dropwise feeding the mixture containing the liquid medium into a second vaporizing means and counter-flowingly contacting the mixture containing the liquid medium, with the second gas to vaporize additional liquid medium to form a third gas which is a mixture of the second gas and additional vaporized liquid medium; and (c) feeding the third gas into a condensing means to condense the vaporized liquid medium into a liquid and separate the first gas, which is then blown into the first vaporizing means in step (a).Type: GrantFiled: March 26, 2004Date of Patent: April 26, 2011Assignee: The Institute of Creative Chemistry Co., Ltd.Inventors: Sigeru Torii, Kouichi Miki
-
Patent number: 7909966Abstract: The invention disclosed relates to catalytic distillation column internals providing improved liquid reaction mixture and catalyst contacting for simultaneous catalytic reaction and separation of the reaction mixture. The invention is an improved catalytic distillation apparatus providing optimum balance of catalytic reaction and mass transfer steps, wherein distribution, mixing and feeding of liquid reaction mixture to the reaction zone and distillation section are better controlled and more uniformly applied. At least one catalyst bed is situated in at least one receiving pan of a distillation tray so that the tray performs the functions of both of the reaction section and the distillation section of the catalytic distillation column simultaneously within a stage.Type: GrantFiled: November 2, 2005Date of Patent: March 22, 2011Assignees: AMT International, Inc., CPC Corporation, TaiwanInventors: Kuang-Yeu Wu, Pai-Yu Polly Chiang, Tzong-Bin Lin, Hung-Chung Shen, Karl T. Chuang
-
Publication number: 20110048922Abstract: Methods and apparatuses for extractive distillation using internal addition of steam to an extractive distillation column from a reboiler are described herein. The apparatuses include an extractive distillation column, a reboiler (for example, a kettle reboiler) coupled to the extractive distillation column, and a steam input line. The steam input line is coupled to an internal steam sparger device of the reboiler. Methods utilizing the apparatuses to perform extractive distillation of a hydrocarbon feed stream are also described herein.Type: ApplicationFiled: February 17, 2010Publication date: March 3, 2011Inventors: Mircea Cretoiu, Andrei Cimpeanu
-
Patent number: 7820015Abstract: A device for recording the boiling curve of liquids, in particular petroleum products, made of a distillation apparatus which includes a distillation column and a condenser, a sample dish connected to the distillation apparatus and a pump connected to the sample dish to fill the sample dish, wherein the filling means and the condenser are made of well heat-conducting material and the filling means and the condenser are connected to a temperature controller.Type: GrantFiled: June 26, 2008Date of Patent: October 26, 2010Assignee: Grabner Instruments Messtechnik Nfg. Gesellschaft m.b.H. & Co. KG.Inventors: Matthias Burian, Roland Aschauer
-
Patent number: 7811420Abstract: A method of and apparatus is disclosed for water desalination including steps of transferring water vapor from salt-water in a vaporization zone 7, via a water vapor transfer zone 12, to a condensation zone 11, and condensing the water vapor into fresh-water. The water vapor transfer zone 12 is maintained substantially free of any gas other than water vapor. Heat is supplied to the vaporization zone 7 and extracted from the condensation zone 11, at relative rates such that there is a net transfer of water from the vaporization zone to the condensation zone. Also disclosed is a method of and apparatus for degassing salt water using at least two degassing chambers 17A, 17B each provided with a valved vent 47 and a valved inlet 21,29,90,91, with a valved pipe circuit 17a, 72-82,85-87, having a pump 71.Type: GrantFiled: August 21, 2006Date of Patent: October 12, 2010Inventor: Sven Olof Sonander
-
Patent number: 7713386Abstract: The apparatus includes an alkylation unit connected to a first benzene recycle conduit, a feed conduit and an alkylation effluent conduit; a transalkylation unit connected to an polyalkylbenzene recycle conduit, a second benzene recycle conduit, and a transalkylation effluent conduit. A dividing wall distillation column is in fluid communication with the transalkylation effluent conduit, the alkylation effluent conduit, a product stream, a bottoms stream conduit and first and second benzene recycle conduits. A polyalkylbenzene fractionation column is connected to the bottoms stream conduit, the polyalkylbenzene recycle conduit and a heavy component conduit.Type: GrantFiled: May 23, 2007Date of Patent: May 11, 2010Assignee: UOP LLCInventors: Michael A. Schultz, Steven P. Lankton, Constante P. Tagamolila
-
Patent number: 7691239Abstract: A differential vapor pressure (DYP) cell is disposed in a divided wall column that receives a feed comprising a first, second, and third component. A separation section on the feed side of the divided wall column separates the feed in a vapor comprising the first and second component, and a liquid comprising the second and third component. The DYP cell is disposed in the divided wall column at a level below the point where the feed enters the column, and the DYP cell measures the concentration of the first component.Type: GrantFiled: December 4, 2002Date of Patent: April 6, 2010Assignee: Fluor Technologies CorporationInventors: Henry Kister, Walt Stupin
-
Patent number: 7678235Abstract: Embodiments of the invention provide systems and methods for water purification. The systems have a preheater, a degasser, an evaporation chamber, a demister, and a control system, wherein the control system permits operation of the purification system through repeated cycles without requiring user intervention or cleaning. The system is capable of removing, from a contaminated water sample, a plurality of contaminant types including: microbiological contaminants, radiological contaminants, metals, salts, volatile organics, and non-volatile organics.Type: GrantFiled: October 19, 2005Date of Patent: March 16, 2010Assignee: Sylvan Source, Inc.Inventors: Richard J. Deep, Eugene Thiers, Douglas Michael Thom
-
Patent number: 7641772Abstract: A distillation unit (10) employs a fluid circuit (FIG. 8) in which a counterflow heat exchanger (102, 104, 106, 108, 110) transfers heat from condensate and concentrate to feed liquid to be distilled. The pumping system (100, 238) that drives fluid through the circuit is arranged to keep the pressure in the counterflow heat exchanger's condensate higher than that in its feed-liquid passage. This tends to discourage the contamination that could otherwise occur in the concentrate if the fluid isolation ordinarily maintained between those passages is compromised.Type: GrantFiled: January 20, 2005Date of Patent: January 5, 2010Assignee: Zanaqua Technologies, Inc.Inventor: William H. Zebuhr
-
Patent number: 7628893Abstract: A method and an apparatus is provided for the separation of liquid-liquid and liquid-solids compositions by flash evaporation in a heated vacuum chamber. The compositions are injected through an atomizing spray nozzle having a spray cone downward of about 30 to 150 degrees. The compositions are preheated and injected under pressure into the preheated vacuum evaporation chamber. The vaporized liquid that is formed is collected in a condenser which draws the vapors by vacuum or pressure differential. Any solids are collected at the bottom of the vacuum chamber as semi-dry or dry solids.Type: GrantFiled: August 1, 2005Date of Patent: December 8, 2009Assignees: Pure Energy Technology Co, PPT Research Inc.Inventors: David William Bonser, Irl E. Ward, Alan R. Duly
-
Patent number: 7597784Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.Type: GrantFiled: November 13, 2003Date of Patent: October 6, 2009Assignee: DEKA Products Limited PartnershipInventors: David F. Bednarek, Jason A. Demers, Timothy P. Duggan, James L. Jackson, Scott A. Leonard, David W. McGill, Kingston Owens
-
Patent number: 7588666Abstract: The invention relates to a compact rectifying unit for separation of mixed fluids using for heat transfer purpose a fluid heat carrier and its vapours on one of the sides of heat and mass exchanging walls. In order to increase the efficiency of the heat and mass exchange process, the heat and mass exchange tubes of the rectifying part and/or of the evaporator part have means to provide irregular/varying amounts of heat transfer between the inside and the outside of tube wall along the height of the heat and mass exchange tubes. This allows for a reduction in the rectification column height by 3-10 times.Type: GrantFiled: March 20, 2002Date of Patent: September 15, 2009Inventors: Albert Faritovich Saifutdinov, Oleg Yegorovich Beketov, Viktor Seliverstovich Ladoshkin, Guennadi Anatolievich Nesterov, Anatoly Semenovich Tlousty, Guennady Ivanovich Ivanov
-
Publication number: 20090205945Abstract: Processes and apparatus for the alkylation of benzene with mono-olefin aliphatic compound in at least two reaction zones in the presence of solid alkylation catalyst use a crude distillation of the reaction effluent passing between reaction zones to remove a substantial portion of the alkylbenzene. The processes reduce the amount of heavies generated in an economically attractive manner.Type: ApplicationFiled: January 25, 2005Publication date: August 20, 2009Inventors: Stephen W. Sohn, Bryan K. Glover, Andrea G. Bozzano
-
Publication number: 20090139852Abstract: A process and an apparatus for the separation of a feed by distillation into a low-boiler (A), a medium-boiler (B) and a high-boiler fraction (C). Separation takes place in one or more dividing-wall columns, in which a dividing wall is arranged in the longitudinal direction of the column to thereby form an upper, common column region, a lower, common column region, a feed part with rectifying section and stripping section, and a withdrawal region with rectifying section and stripping section. The feed of the C5+ cut is in the central region of the feed part. The high-boiler fraction (C) is discharged from the bottom of the column, the low-boiler fraction (A) is discharged via the top of the column, and the medium-boiler fraction (B) is discharged from the central region of the withdrawal part. A first heat source is provided for heating the lower column region.Type: ApplicationFiled: December 4, 2007Publication date: June 4, 2009Inventors: Marco L. VanNuland, Joseph M. Cheben, Ronald L. DeMartino, John R. Porter
-
Patent number: 7531065Abstract: A fluid distillation apparatus includes at least one each of a fluid inlet port Through which the fluid to be distilled is transferred from a container containing the fluid to be distilled to distillation chamber, a fluid outlet port through which the distilled fluid is transferred to a container to hold the distilled fluid, an air supply port to which compressed air supply is to be connected, a power cord through which the electric power is supplied, preferably an outlet through which air pressure for fluid agitation is supplied to said container containing the fluid to be distilled, and preferably art outlet through which air pressure is supplied to a pump means for transferring the distilled fluid from the receiving container to the duty fluid container. The apparatus includes a debris draining system for automatically draining debris from said distillation tank.Type: GrantFiled: October 18, 2002Date of Patent: May 12, 2009Assignee: Uni-Ram CorporationInventor: Soichiro Yamamoto
-
Patent number: 7503997Abstract: A centrifugal evaporator includes a chamber in which sample containers are carried and rotated by a rotor and are pivotally mounted so as to swing up to a substantially horizontal orientation as the rotor rotates. The evaporator includes an infra-red source to direct infra-red radiation towards the rotor and the sample containers carried thereon, to heat at least the latter and any sample material therein. A non-contact temperature sensing infra-red pyrometer having a sensor with a defined field of view is mounted in the chamber, such that while the rotor as such is substantially out of its field of view, each sample container at least partly occupies the pyrometer field of view for a part of each rotation of the rotor. The positions of the infra-red source and the pyrometer components are selected so that the radiation from the infra-red source does not impinge on the pyrometer sensor.Type: GrantFiled: October 29, 2003Date of Patent: March 17, 2009Assignee: Genevac Ltd.Inventors: Roger Lee-Smith, Richard Smith, Duncan Guthrie
-
Publication number: 20090057128Abstract: An improved process for separation of liquid mixtures involves vapor stripping followed by mechanical compression of the vapor which is then exposed to a permeation membrane for separation of the compressed vapor.Type: ApplicationFiled: August 30, 2007Publication date: March 5, 2009Inventors: Leland Vane, Franklin R. Alvarez
-
Publication number: 20090000939Abstract: In a membrane distillation process in which a liquid to be concentrated is separated from a vapour space (11) by a vapour-permeable liquid- or water-tight membrane or membrane wall (13), to set the absolute pressure of the liquid to be concentrated a reduced pressure is imparted to this which lowers the absolute pressure of the liquid to be concentrated. A corresponding membrane distillation device is also specified.Type: ApplicationFiled: November 9, 2006Publication date: January 1, 2009Inventor: Wolfgang Heinzl
-
Patent number: 7465376Abstract: The invention provides for the removal of impurities from treatment fluid including a base liquid and a variety of impurities contained in the base liquid by conveying the treatment fluid to at least one preheating separating device, including a preheating heat exchanger and a separator unit, before the admixture of a carrier gas to the treatment fluid. The treatment fluid is preheated by the preheating heat exchanger to a temperature below the boiling temperature of a base liquid so that the liquid impurities with lower boiling temperatures than the base liquid are evaporated and expelled thermally, whereby the evaporated and expelled impurities are separated in the separator unit of the preheating separator device. The treatment fluid is then evaporated and separated from impurities having a higher boiling point than the base liquid.Type: GrantFiled: February 9, 2002Date of Patent: December 16, 2008Inventors: Joachim Neubert, Karl-Ferdinand Staab
-
Patent number: 7465375Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.Type: GrantFiled: November 13, 2003Date of Patent: December 16, 2008Assignee: DEKA Products Limited PartnershipInventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
-
Publication number: 20080289947Abstract: A vacuum still for the distillation of grape products has a boiler to heat grape products to a temperature at which nutriments have no or minimal damage, the vapors from the vapor space of the boiler passing through three condensers in series. A vacuum is applied through the condensers in series to the vapor space of the boiler, the concentrated grape product in the boiler being processed into a food product containing the nutriments and vitamins contained in the grape product.Type: ApplicationFiled: January 14, 2008Publication date: November 27, 2008Applicant: BARROSA GRAPE PRODUCTS PTY LTDInventor: Hermann Thumm
-
Publication number: 20080277260Abstract: A tray valve assembly for a process column of a type wherein a first, heavier fluid flows downwardly from a downcomer onto a tray and thereacross in a first direction through which a second, lighter fluid flows upwardly therethrough for interaction and mass transfer with the heavier fluid before passing therefrom. A plurality of valves disposed across a surface of the tray and mounted above a plurality of apertures on the surface of the tray, each valve of the plurality of valves comprising a top surface and at least one securement leg. A first securement leg of is adapted to intercept the heavier fluid flow in the first direction forming a diverting baffle for engaging the heavier fluid flow across the tray. Each valve includes at least one aperture to facilitate the lighter fluid flow therefrom and further comprising a first aperture in the first securement leg.Type: ApplicationFiled: April 25, 2008Publication date: November 13, 2008Inventors: Michael J. Binkley, Casey Bowles
-
Patent number: 7435317Abstract: An improved distillation of water. involves distilling significant quantities of water at temperatures well below the boiling point. During distillation, a compound is taken from a liquid-phase to a gas-phase and then condensed to the liquid-phase again to get a pure liquid. The present invention uses water sprayed (105) and absorbed onto a solid surface such as micro-powder (104) made from wood as a starting material. Absorbing water onto such a surface results in rapid evaporation with a relatively low temperature gradient when the water and particles are agitated. The present invention could be characterized as solid-phase distillation.Type: GrantFiled: March 29, 2001Date of Patent: October 14, 2008Assignee: Biomass Conversions, L.L.C.Inventor: Seiji Hata
-
Patent number: 7431805Abstract: A method, system, and apparatuses for simultaneous heat and mass transfer utilizing a carrier-gas at various absolute pressures are described. A method may include: thermally coupling at least two continuous contacting apparatuses together; varying the pressure between the at least two continuous contacting apparatuses; allowing heat removed from the first continuous contacting apparatus to be the heat delivered to the second continuous contacting apparatus. A system may include: at least two continuous contacting apparatuses thermally coupled together and operating at different absolute pressures. A continuous contacting apparatus may include: an evaporation chamber and a dew-formation chamber both operating at an absolute pressure in a vacuum range. A continuous contacting vapor recompression apparatus may include: an evaporation chamber operating at a first absolute pressure; and a dew-formation chamber operating at a second absolute pressure higher than the first absolute pressure.Type: GrantFiled: December 3, 2004Date of Patent: October 7, 2008Assignee: Arizona Board of RegentsInventor: James R. Beckman
-
Patent number: 7429312Abstract: The present group of inventions relates to processing of multi-component liquid mixtures (MCLM) employing reforming process, preferably for vacuum distillation of hydrocarbon mixtures and in petroleum refining and chemical industries. The inventions include the method for processing of multi-component liquid mixtures. The method of MCLM separation includes pressure feeding of a hydrocarbon liquid mixture to an a liquid-gas jet device nozzle which discharges to a vacuum chamber of liquid-gas jet device. A counter pressure jointly with the liquid-gas jet device forms a pressure surge in the vacuum chamber. The counter pressure is 0.4 to 0.7 of the magnitude of the feed pressure generated by the pump. The plant for MCLM processing includes a feed pump, a head delivery main, a discharge main, control instrumentation and a vacuum-generating device including a vacuum chamber, a liquid-gas jet device with a nozzle in the front end wall of the vacuum chamber.Type: GrantFiled: December 27, 2002Date of Patent: September 30, 2008Assignee: Energy Savings Technologies Financial Industrial Group LLCInventors: Yuriy Pavlovich Skakunov, Chamil Khakimovich Iskhakov, Sergey Vladimirovich Tishkin
-
Patent number: 7416642Abstract: A system for cooling a heated juice by partial low-pressure evaporation, the system includes a vat with at least two compartments that are connected to each other through a variably positioned shutter element, where the juice is subjected to decreasing pressure reductions within the vat and the movement of the variably positioned shutter element creates a pulsed effect that removes solid particles contained in the juice.Type: GrantFiled: May 29, 2002Date of Patent: August 26, 2008Assignee: Centre National de la Recherche Scientific (CNRS)Inventors: Jean-Pierre Nadeau, Dominique Cadiot, Patrick Sebastian, David Callede
-
Publication number: 20080128262Abstract: A separation system for a methyl acetate hydrolysis is provided. The separation system comprises a reactive distillation system, a reflux system, a first separation system and a second separation. The reactive distillation system allows the hydrolysis of a methyl acetate solution to generate a first mixture and a second mixture. The reflux system is packed with a heterogeneous catalyst and coupled to the reactive distillation system, which refluxes the first mixture to the reactive distillation system. The first separation system is coupled to the reactive distillation system, which directs the second mixture thereinto so as to isolate an acetic acid and a third mixture therefrom. The second separation system is coupled to the first separation system, which directs the third mixture thereintio so as to separate a methanol therefrom. The methyl acetate feeding system is coupled to, one of the reactive distillation system and the reflux system, which feeds the methyl acetate solution thereinto.Type: ApplicationFiled: January 30, 2007Publication date: June 5, 2008Applicant: National Taiwan UniversityInventors: Hsiao-Ping Huang, Cheng-Ching Yu, Ming-Jer Lee, Yu-De Lin, Jian-Kai Cheng
-
Patent number: 7368038Abstract: An anti-pressure system for a vessel which is subject to internal pressure created by heating or boiling of its contents, the system including first and second spaced-apart outlets for vapor to exit the vessel, each outlet having a first side communicating with the vessel interior and a second side communicating with the vessel exterior. The invention provides a reliable method of protecting a normally un-pressurized vessel, such as an autoclave, distillation vessel, boiler or the like, from dangerous pressure build-up, resulting from its vapor outlet being blocked, regardless of what other pressure release devices, if any, may be present on the vessel.Type: GrantFiled: August 23, 2001Date of Patent: May 6, 2008Assignee: Chem-Champ (Barbados) Inc.Inventor: Dennis William Mount
-
Patent number: 7288169Abstract: A distillation apparatus for subjecting a crude readily polymerizable compound to distillation under vacuum conditions to purify the same includes a distillation column and a vacuum generator, an exhaust gas conduit of the vacuum generator being connected to a connecting conduit therebetween through a pressure control valve. The purification method includes using the disclosed distillation apparatus and controlling the action of the pressure control valve based on a pressure of the distillation column, thereby controlling the amount of the exhaust gas to be introduced to control the pressure of the distillation column.Type: GrantFiled: February 20, 2004Date of Patent: October 30, 2007Assignee: Mitsubishi Chemical CorporationInventors: Shuhei Yada, Yasushi Ogawa, Yoshiro Suzuki, Kenji Takasaki, Kiyoshi Takahashi
-
Patent number: 7267746Abstract: A control apparatus and control method for controlling the separation in a dividing wall distillation column of at least two feeds into at least three products is disclosed. The apparatus uses a temperature measuring device to measure the temperature of fluid in the column, a controller, and a means for adjusting the temperature of fluid in the column. The temperature measuring device may be on either side of the dividing wall or above or below the dividing wall, and more than one such device may be used. The apparatus and method may be used in the production of alkylaromatic hydrocarbons by alkylating aromatic hydrocarbons with olefinic hydrocarbons.Type: GrantFiled: August 27, 2003Date of Patent: September 11, 2007Assignee: UOP LLCInventors: James W. Harris, Steven P. Rosenblum, Michael A. Schultz, Dennis E. O'Brien, Douglas G. Stewart
-
Patent number: 7258765Abstract: Vaporization chambers (distillation “pots”) are disclosed in which the liquid contained in such a pot is heated and circulated to establish thermal uniformity of the liquid and to route the circulated liquid past a thermally conductive member that contacts the liquid. The thermally conductive member extends from a location on a wall of the pot in a portion of the pot that holds the liquid as the liquid is being heated in the pot and conducts thermal energy directly from the liquid to a location outside the pot corresponding to the location on the wall. The pot desirably is divided into an upper portion and lower portion, wherein the liquid circulates from the lower portion to the upper portion and from the upper portion to the lower portion during heating. During this circulation, bubbles formed in the liquid can be routed into the upper portion in a manner resulting in fracture of the bubbles and recovery of liquid entrained in the bubbles, thereby preventing foam accumulation in the pot.Type: GrantFiled: November 12, 2003Date of Patent: August 21, 2007Assignee: Drawform, Inc.Inventor: Robert D. Westcott
-
Publication number: 20070170049Abstract: A multiple application recycling and purification device has a coaxial core that is horizontally oriented, non-rotating, cylindrical distillation chamber. The enhanced, completely coaxial configuration continuously cleans the entire distillation chamber and spreads a thin film of liquid to enhance distillation and positively aid in the removal of remaining contaminants. Through a timed and positioned valve, the device removes and purges lower-temperature contaminants. Timed valves and sensors control all phases of the distillation to provide a coaxially integrated, stand-alone, adaptable, scalable and maintenance free distillation unit that self-monitors, self-cleans and economically functions to produce the pure distilled liquid, e.g., water. This device can be modified to purify any numerous array of liquids and can be scaled to produce any amount of purified liquids for either household, commercial, or industrial applications.Type: ApplicationFiled: January 18, 2007Publication date: July 26, 2007Inventor: Pierre G. Mansur
-
Patent number: 7232504Abstract: A distilling apparatus and method use a two step distillation and purification process for processing a waste liquid, such as an impure sulfuric acid solution, to form a highly concentrated sulfuric acid solution. First, the waste liquid is stored in a concentrating column, where it is heated. A condenser, which uses the waste liquid as a cooling medium, condenses the vapor generated by the heater. The condensed vapor is passed through a filter, which separates impurities out of the waste liquid, prior to feeding the waste liquid back into the concentrating column. Water is then removed from the waste liquid via a distilling process. The resulting concentrated liquid is then fed to a purifying column, where it is again heated, to remove residue, and condensed, resulting in a highly pure waste liquid.Type: GrantFiled: November 22, 2002Date of Patent: June 19, 2007Assignee: Fujitsu LimitedInventors: Hiroshi Osuda, Toru Matoba, Daisuke Adachi, Masataka Fukuizumi
-
Patent number: 7208079Abstract: A process for the treatment of waste oil comprises the steps of (a) supplying a stream of the waste oil to a dehydrator to dehydrate the waste oil and obtain a stream of dehydrated waste oil; (b) supplying the stream of dehydrated waste oil to a fractionated distillation column having a lower tray, an upper tray and a middle tray therebetween, wherein the lower tray is operated at a temperature of 370 to 390° C. under a sub-atmospheric pressure of 50 to 100 mmHg, the middle tray is operated at a temperature of 265 to 280° C. under a sub-atmospheric pressure of 35 to 45 mmHg and the upper tray is operated at a temperature of 100 to 110° C. under a sub-atmospheric pressure of 30 to 40 mmHg; (c) withdrawing from the distillation column a bottom product comprising a bituminous material; (d) withdrawing a first side stream from the distillation column between the first and second trays, the first side stream comprising a heavy oil having a viscosity of 130 to 180 cSt at 40° C.Type: GrantFiled: March 3, 2003Date of Patent: April 24, 2007Inventor: Nouredine Fakhri
-
Patent number: 7037411Abstract: In an apparatus capable of distilling and refining an easily polymerizable substance, piping is performed so that when a strainer in action is switched to a backup strainer, the strainer can be switched after removing air in the backup strainer to replace air in the backup strainer with a discharge liquid of a pump. According to the apparatus, switching the strainers installed on an upstream side of the pump for extracting a liquid of a vacuum distillation column, which distills and refines the easily polymerizable substance, can be performed with no trouble during operation of the distillation column. When the apparatus includes a device for measuring a differential pressure between an upstream side and a downstream side of the strainer in action, two or more strainers installed in parallel can be switched at proper times and the easily polymerizable substance can be produced efficiently.Type: GrantFiled: June 21, 2004Date of Patent: May 2, 2006Assignee: Mitsubishi Chemical CorporationInventors: Shuhei Yada, Yasushi Ogawa, Hirochika Hosaka, Yoshiro Suzuki, Mitsuo Nakamura
-
Patent number: 7001490Abstract: Crude ammonia is separated into a low boiler fraction, a high boiler fraction and an intermediate-boiling pure fraction by continuous fractional distillation in a distillation apparatus configured either as a dividing wall column or as a system of thermally coupled distillation columns. In the process of the present invention, the low boiler fraction is taken off at the top of the distillation apparatus. The intermediate-boiling pure fraction is obtained at a side offtake which is preferably provided with droplet precipitators. In addition, the gas loading of the distillation column is restricted so that the operating pressure is in the range from 2 to 30 bar and the F factor does not exceed 2.0 Pa0.5.Type: GrantFiled: January 24, 2001Date of Patent: February 21, 2006Assignee: BASF AktiengesellschaftInventors: Karl-Heinz Wostbrock, Gerd Kaibel, Christian Tragut, Gabriele Anken
-
Patent number: 6936140Abstract: A distillation system is provided for recovering water from sea water and other polluted water source. The system has a heat engine embodying Carnot cycle and a Rankine cycle formed by heat exchangers, flash evaporator and condenser. Burnt gases from the engine such as a jet engine no longer fit for flying are directed into a duct where the exchangers are located. Sea water is pumped into the heat exchanger for preheating by residue heat in the duct and then into the exchanger for further heating. A recirculating pump raises water pressure in the exchanger for increasing boiling point to about 165° C. The heated water is fed into the evaporator where it changes into vapour and condensed into water by the condenser. The jet air stream is used to create Venturi effect for maintaining sub-atmospheric pressure in the evaporator. Any solid left in the evaporator is removed by a transfer mechanism.Type: GrantFiled: February 2, 2001Date of Patent: August 30, 2005Assignee: Aqua Dyne, Inc.Inventors: Gregory Mark Paxton, Patrick Joseph Glynn
-
Patent number: 6911120Abstract: The present invention is a distillation system with individual fractionator tray temperature control, with the use of either a heating element or a cooling element, and in some preferred embodiments, the use of both a heating element and a cooling element in a plurality of fractionator trays. There is at least, and typically more than one distillation column having a plurality of fractionation trays, and having feed input, liquid removal, and vapor removal with the plurality of trays including at least one of a heating element and a cooling element. Controls are included for separate control of each of the heating element(s) and/or said cooling element(s). These controls may be regulated by a programmable microprocessor, and feedback from temperature sensors may be employed to provide discrete tray-by-tray temperature controls.Type: GrantFiled: August 1, 2001Date of Patent: June 28, 2005Inventor: Li Young
-
Patent number: 6911119Abstract: This invention relates to a simple, convenient, portable mini-distillation apparatus for the production of essential oils and hydrosols, said apparatus is useful to distill essential oils and hydrosols such as rose water, ajowain water from fresh and dried plant material like leaves, flowers, roots and rhizomes by water distillation, water and steam distillations and as an optional, steam distillation can also be perform at atmospheric pressure as well as slightly higher and lower than atmospheric pressure, said apparatus can be heated on brick-clay furnace with small agro-waste, LPG cooking gas, electrically heated stove or kerosene/diesel burner etc. and requires minimum attention during handling; since the apparatus is made of stainless steel and glass, the essential oil distilled is of better quality.Type: GrantFiled: March 23, 2001Date of Patent: June 28, 2005Assignee: Council of Scientific & Industrial ResearchInventors: Garikapati D. Kiran Babu, Paramvir Singh Ahuja, Vijay Kumar Kaul, Virendra Singh
-
Patent number: 6887344Abstract: A compact, self-contained apparatus for treating wastewater containing as impurities and pollutants various non-volatile (at water boiling points) fluids such as greases, oils and soaps, a vessel for collecting the wastewater, a heating chamber including electric heating elements and a heat transfer liquid such as mineral oil to heat the wastewater admixture to boil off the water and to reduce the volume of liquid for disposal, and a wastewater supply tank positioned under the apparatus. The apparatus may further include a disposable liner to isolate the wastewater from the vessel itself and facilitate rapid and clean removal and disposal of waste material after evaporation of the water, and thermally-activated sensors to maintain a desired temperature differential between the heating elements and the heat transfer liquid contained in the apparatus.Type: GrantFiled: August 2, 2000Date of Patent: May 3, 2005Inventor: Raymond E. VanKouwenberg
-
Publication number: 20040222077Abstract: In a distillation apparatus, a production process and a purification method of readily polymerizable compounds, a problem of the invention is to solve a serious plugging problem in a large-sized distillation column as in the commercial equipment and to provide an apparatus and a method for distilling and purifying a readily polymerizable compound stably over a long period of time.Type: ApplicationFiled: February 20, 2004Publication date: November 11, 2004Applicant: MITSUBISHI CHEMICAL CORPORATIONInventors: Shuhei Yada, Yasushi Ogawa, Yoshiro Suzuki, Kenji Takasaki, Kiyoshi Takahashi