Abstract: A fractional distillation process, in which the flow rate of the external reflux is utilized to control the bottoms product composition, is controlled so as to maintain a desired bottoms product composition to the extent that maintaining the desired bottoms product composition does not cause a process constraint to be violated. A plurality of actual process conditions are compared to process constraints for those process conditions to determine if the flow rate of the external reflux should remain the same, be increased by an incremental amount or be decreased by an incremental amount. The order of the comparison of process constraints to actual process conditions is such that the most important comparison will control the external reflux flow rate if that comparison indicates that a process constraint has been violated.

Abstract: In a fractional distillation process in which a compressor is used to supply heat to the fractional distillation process, a plurality of signals representative of a plurality of speeds of the compressor, required to prevent various process constraints from being violated or maintain various desired process operating conditions respectively, are compared. The signal representative of the highest compressor speed is utilized to control the compressor. In this manner, the compressor is run at the minimum speed required to satisfy the various process constraints and maintain the desired process operating conditions.

Abstract: In a process in which liquid flows to a vessel and is then withdrawn from the vessel, method and apparatus is provided for implementing nonlinear liquid level control by providing a variable set point to a conventional level controller. The variable set point is a nonlinear function of the actual liquid level in the vessel. The variable set point enables the vessel to absorb disturbances in the flow rate of the liquid flowing to the vessel while the actual liquid level in the vessel remains between a desired high and low limit thus providing a smooth flow of liquid from the vessel.

Abstract: In a fractional distillation process in which a heating fluid and waste heat stream are utilized to supply heat to a fractional distillation column and in which the heat supplied from the waste heat stream is not controllable, control of the liquid level in the fractional distillation column is accomplished by manipulating the flow rate of the heating fluid so as to maintain a desired liquid level until such time as the flow rate of the heating fluid becomes zero at which time the flow rate of the external reflux to the fractional distillation column is manipulated to maintain a desired liquid level in the fractional distillation column. A switching of control of the liquid level provides a means by which an uncontrollable heat input may be provided to the fractional distillation column without losing control of the liquid level in the fractional distillation column.

Abstract: An alcohol still having a boiler with a valve for maintaining the amount of liquor constant. The boiler mounts a distilling column having a temperature controlled inlet for liquor to be distilled which assists in maintaining the operation at a constant optimum operating temperature.

Abstract: Apparatus for preparation and distillation of low-alcohol-content, fermentation products into high-alcohol-content, fuel-grade product using solar energy to carry out the fermentation and distillation. The apparatus includes a solar collector with reflectors, fermenting tanks, a distillation column, and temperature controls. The working fluid for the solar collector is isolated from the fluid being distilled.

Abstract: In a fractional distillation column in which at least a first component and a second component are at least partially separated with the first component being removed principally as an overhead product and the second component being removed principally as a bottoms product and in which the heat supplied to the fractional distillation column is used as the primary control for the overhead product composition with the flow rate of external reflux to the fractional distillation column being used to control the bottoms product composition, a comparison of the actual concentration of the second component in the overhead product to the desired concentration is utilized to bias the control signal which is utilized to manipulate the flow rate of the external reflux to the fractional distillation column.

Abstract: Flow of lean oil to an absorption section of an absorber is controlled responsive to pressure drop at least a portion of said absorption section. Flow of lean oil can be maximized, short of flooding, responsive to said pressure differential. Apparatus is also described.

Abstract: Control of multiple distillation columns for producing anhydrous alcohol suitable for blending with gasoline to produce gasohol. The distillation process involves production of a first-stage distillate containing a predetermined amount of water, followed by azeotropic distillation in the presence of a hydrocarbon entrainer to strip the distillate of its water content, leaving anhydrous alcohol as a bottom product. Tight controls are present during first-stage distillate production to hold its proof at an optimum value derived at through material balance calculations to minimize energy consumption for the overall system. Control over the dehydrating stage is accomplished by a combination of ratio control to regulate and maintain the proper proportion of the entrainer and temperature control to regulate within the column the actual inventory of entrainer.

Abstract: A control system for distillation column with a sidedraw line is provided wherein a prediction on the influence by changes in the feed stream with respect to the sidedraw composition is made.

Abstract: In a fractional distillation column, a desired ratio between the flow rate of a side draw product stream and the internal reflux flow rate at the particular tray from which a side draw stream is withdrawn from the fractional distillation column is maintained by manipulating the flow rate of the center reflux stream so as to maintain the desired ratio between the internal reflux flow rate and a side draw product stream flow rate at the particular tray from which the side draw stream is withdrawn from the fractional distillation column. Control of the ratio between the flow rate of a side draw product stream and the internal reflux flow rate results in an improved side draw product stream purity.

Abstract: In a fractional distillation process in which the designation of the primary product stream changes, the desired composition of the primary product stream and a secondary product stream are maintained without loosing automatic control of the process for an extended period of time while the controllers controlling the process are retuned for the new operating conditions. Two sets of tuning constants are available to each controller and these tuning constants are automatically switched as required by the designation of the primary product stream.

Abstract: In a fractionation distillation process in which a pump around stream and an external reflux are utilized to control heat removal from an upper portion of the fractional distillation column and in which the pump around stream is utilized to preheat the feed stream flowing to the fractional distillation, the flow rate of the pump around stream is manipulated so as to substantially maximize the flow rate of the pump around stream while maintaining a desired heat removal from the fractional distillation column. Priority control of the pump around stream and external reflux result in a maximum preheating of the feed stream flowing to the fractional distillation column which improves the energy efficiency of the fractional distillation process.

Abstract: This invention relates to an improved apparatus and process for controlling heat input to a fractionation tower so that a proper energy balance is maintained. The apparatus and method for controlling a fractionation tower and process wherein feed and heat flow into the tower and feed is distilled and separated into distillate and bottoms, said distillate flowing from the tower through an overhead line into a condenser where it is allowed to condense before it is drawn off as product with a portion of this product being returned to the tower as reflux, and said bottoms being allowed to at least partially collect in the tower thereby establishing a liquid level which is allowed to fluctuate within predetermined limits, which method comprises generating and using the signal:Q.sub.I =Kp(K.sub.R +K.sub.D -K.sub.F)whereQ.sub.I is the heat required by the fractionation tower;Kp is the pressure controller output signal;K.sub.R is the reflux flow rate signal;K.sub.D is the distillate flow rate signal;K.sub.

Abstract: A mixture of xylenol, water, alcohol and other substances is put into an evaporator tank which is adjusted to a pressure and temperature to evaporate the water and alcohol. The water and alcohol vapors flow through an expansion chamber into a condenser and the condensate flows back through a distributor and a control valve into a collector tank. Through a two-stage control dial a second temperature and pressure is imposed upon the evaporator tank to evaporate the xylenol which is similarly condensed and the condensate flows back through the distributor which control valve has been actuated to direct the xylenol into a second collector tank. A second evaporator is connected through a selectively operable shut-off valve to the expansion chamber. The second evaporator tank is provided with an inlet funnel which can be heated to melt solid paraffin therein. A filter is within this funnel to filter out solid foreign matter.

Abstract: A non-linear level controller is provided in which the proportional term is a function of the actual liquid level in a vessel compared to the actual liquid level in the vessel at a previous time. The integral term is a function of the actual liquid level in the vessel compared to a set point which is representative of the desired liquid level in the vessel. Both the proportional term and the integral term are modified by a variable gain factor which is a non-linear function of the liquid level being controlled. The proportional term and integral term are combined to provide the controller output which is utilized to manipulate a flow of liquid from the vessel in which the liquid level is being controlled.

Abstract: A draw rate signal generator for an atmospheric crude distillation unit receiving crude oil and providing streams 1 through 5 and a reduced crude oil includes flow rate sensors sensing the flow rates of the crude oil and of streams 1 through 4 and providing corresponding signals. Analyzers sample the crude oil and provide signals corresponding to the 35% point temperature, the API gravity and the vapor pressure of the crude oil. End point analyzers sample streams Nos. 1 and 3 and provide signals representative of the end point temperatures of streams Nos. 1 and 3, respectively. 50% point analyzers sample streams 2, 3 and 4 and provide signals corresponding to the 50% point temperatures of streams Nos. 2, 3 and 4, respectively. A circuit connected to the sensors, to the crude analyzers, to the end point analyzers and to the 50% analyzers provide signals corresponding to the draw rates for streams Nos. 1 through 5 in accordance with signals from the sensors and analyzers.

Abstract: An azeotropic column has staged processing, separate dehydration load control, and integral flash desolventizing for greater capacity, efficiency, and control of conditions in a plural stacked fluidized bed column.

Abstract: The invention provides apparatus and a process for removing mercury from solid waste material. The solid waste material is placed in a vacuum chamber. The chamber is heated above the vaporization temperature of mercury. A vacuum condition is formed and then, while the temperature is maintained above the vaporization temperature of mercury, an inert gas is placed in the vacuum chamber. During this heating period, the pressure in the vacuum chamber is periodically varied from a maximum to a minimum. The apparatus utilized is a vacuum chamber, a vacuum pump, and a pipe that contains a mercury condenser. The pipe also functions through a side inlet as a means for introducing the inert gas into the vacuum chamber, while the vacuum pump is closed off. A control unit for controlling the alternate periods of mercury vapor withdrawal and inert gas introduction into the vacuum chamber is provided.

Abstract: A control system for a multiple feed fractional distillation column is disclosed in which the flow rate signals of the multiple feed streams are delayed and combined for use in feedforward predictive control of the upper reflux flow, intermediate reflux flow and/or reboiler fluid flow to the fractional distillation column. Temperature measurements of the upper vapor stream, the upper reflux stream, the intermediate vapor stream and the intermediate reflux stream as well as analysis of a product stream can be utilized to provide feedback control of the fractional distillation column.

Abstract: A control system for a fractional distillation column in which a pumparound stream is used to remove heat from the fractional distillation column is disclosed. A combination of feedforward and feedback control is utilized to control the heat removal by the pumparound stream in such a manner that smoother operation of the fractional distillation column will be accomplished and a closer approach to required product specifications will be approached.

Abstract: In a fractionation process in which at least two fractional distillation columns are cascaded in series, the vapor from the overhead accumulator associated with the first fractional distillation column in the series is provided to a feed tank for the second fractional distillation column in the series. The flow of the vapor from the overhead accumulator associated with the first fractional distillation column in the series is controlled by means of a control valve. An interactive control system is utilized to maintain the pressure in the overhead accumulator associated with the first fractional distillation column within safe operating limits, maintain the control valve at a substantially fully open position so as to minimize the pressure drop across the control valve controlling the flow of vapor from the overhead accumulator associated with the first fractional distillation column, and maintain the pressure in the feed tank to the second fractional distillation column at a desired value.

Abstract: A control system for a fractional distillation column, where the feed to the fractional distillation column is supplied from at least one separator, is disclosed in which overloading of the fractional distillation column is prevented by monitoring a control parameter associated with the fractional distillation column which indicates that the fractional distillation column is being overloaded. The flow of the feed from the at least one separator is manipulated to maintain the control parameter which indicates that the fractional distillation column is being overloaded within desired limits. The feed to the at least one separator is manipulated to maintain the liquid level in the at least one separator within desired limits.

Abstract: A control system is provided for a fractional distillation column where at least a portion of the overhead vapor stream from the fractional distillation column is utilized in a refrigeration and heating system for a process with which the fractional distillation column is associated. The liquid level is an overhead accumulator associated with the fractional distillation column is maintained at a level sufficient to insure that a sufficient supply of the overhead vapor stream from the fractional distillation column is available to supply the refrigeration and heating needs of the process with which the fractional distillation column is associated.

Abstract: Method and apparatus are disclosed for the automatic adjustment of the fractionation column pressure in a fractionator system which employs total condensation of overhead vapor and a liquid full reflux accumulator to thus float the column pressure above minimum column pressure. The set point of a pressure controller, which manipulates the overhead product control valve to adjust column pressure, is automatically adjusted in response to a desired offset of condensate subcooling from the overhead bubble point temperature which is repeatedly automatically calculated in response to analysis of the overhead product composition and pressure. Appropriate limits and overrides are also disclosed to prevent sudden changes in column pressure which might upset system operation.

Abstract: A process, apparatus and control system for the fractionation of a hydrocarbon feed stream containing relatively nonvolatile impurities. A sidecut liquid stream which is substantially free of the impurities is withdrawn below the feed point. The liquid derived from the feed stream is confined to a first lateral half of the fractionation column to prevent the transfer of the nonvolatile impurities to the second lateral half from which the sidecut is removed. Liquid descending from above the feed point is collected and distributed between the two lateral halves of the column in response to temperature measurements taken in the two halves to thereby equalize liquid flow rates in the two halves. The flow of vapor between the two halves is not obstructed.

Abstract: Method and apparatus are disclosed for the automatic adjustment of the fractionation column pressure in a fractionator system which employs total condensation of overhead vapor and a liquid full reflux accumulator to thus float the column pressure above minimum column pressure. The set point of a condensder fan pitch controller, which manipulates the blade pitch of the condenser fan, is automatically adjusted in response to a desired offset of condensate subcooling from the overhead bubble point temperature which is repeatedly automatically calculated in response to analysis of the overhead product composition and pressure. The set point of a pressure controller, which manipulates the overhead product control valve to adjust column pressure, is automatically adjusted in response to a fan pitch signal from the condenser fan pitch controller and a desired fan pitch set point. Appropriate limits and overrides are also disclosed to prevent sudden changes in column pressure which might upset system operation.

Abstract: A control system for a fractionation column which separates a feed into a heavy bottoms product, which is used as fuel for a plant, and into a light overhead product, which is used in a process, is disclosed. The fractionation column is controlled in such a manner that sufficient bottoms product is supplied to meet the plant fuel requirements while maintaining a desired distillation temperature for the overhead product. The flow rate of fuel oil to the reboiler furnace associated with the fractionation column and the flow rate of the external reflux to the fractionation column are controlled in such a manner that the objectives of supplying sufficient bottoms product to meet plant fuel requirements and supplying an overhead product having a desired distillation temperature are met while still minimizing the external reflux flow rate and the flow rate of the fuel oil to the reboiler furnace to increase fuel economy.

Abstract: A direct contact condenser of a distillation system has a condenser vessel comprising a vapor space with a vapor inlet, a condensate pump, with the liquids' level defining the top of the sump and the bottom of the vapor space. The thermal efficiency of the system is improved wherein the heat of condensation is concentrated in one of two coolant effluent lines while the other coolant line removes unheated excess liquid coolant. This is accomplished with the use of two temperature sensors at spaced vertical locations of the sump and a liquid level control together regulating the opening and closing of respective valves in respective influent and effluent lines of the sump.

Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.

Abstract: The flow rate of feed material containing a constituent to be absorbed and the flow rate of the absorption medium entering an absorption zone are controlled in response to the content and flow rate of feed material entering the absorption zone and the amount of a desired bottoms constituent in the overhead stream of the absorption zone so that the efficiency of the absorption process is optimized. Under circumstances necessitating maximum production from the absorption zone and its associated stripping zone, the absorption medium flow rate is maintained at a maximum value and the feed flow rate is controlled in response to feed composition and flow as well as the concentration of desired bottom product in the overhead stream. The output of the absorption unit is stabilized by alteration of the flow control apparatus associated with the output stream of the stripping zone in order to alter the amount of control over the output flow.

Abstract: A home water distiller which provides for an efficient distillation process wherein the inlet water supply is controlled as a function of the temperature of the output of the distiller, and which inlet water is preheated by introducing it into a chamber surrounding the condensor coils. After preheating, the water flows into the boiling chamber. The unit is provided with a flowthrough or constant-flush drainage system to keep mineral buildup to a minimum, and to provide for automatic control of the input water.

Abstract: An electronic system for automatically controlling the operation of a desalination system, and particularly such systems utilizing waste heat from internal combustion engines. The automatic control system is responsive to physical parameters within the desalinator and is particularly useful during warm-up and cooling periods at the beginning and end of use of such a desalination system for minimizing wear on system components and for maximizing the operational life of the system.

Abstract: Control of a fractionation column is accomplished by manipulating the flow rate of the external reflux in response to a calculation of the internal reflux flow rate to maintain the actual flow rate of the internal reflux at a substantially constant, desired value. An improved method for calculating the internal reflux flow rate when the heats of vaporization of the external and internal reflux are different utilizes a constant, representative of the heat of vaporization of the external reflux divided by the heat of vaporization of the internal reflux, to obtain an accurate calculation of the internal reflux flow rate. Greater accuracy in the calculation yields improved control of the fractionation column. Alternatively, the constant, representative of the heat of vaporization of the external reflux divided by the heat of vaporization of the internal reflux, may be utilized to calculate the required flow rate of the external reflux necessary to maintain some desired internal reflux flow rate.

Abstract: A vapor generating and recovering apparatus including vapor condenser control means wherein one component is separated from a second component of a liquid solution by vaporization and then recovered by condensing including at least one chamber for vaporizing the first component from the liquid solution and a second chamber for recovering the vapor, the vapor generating chamber being in heat emitting relation with a heat emitting means and the vapor recovering chamber being in heat abosrbing relation with a heat absorbing means, the heat absorbing means including a temperature sensing device at a preselected position within the second chamber to control the vapor level of the vaporized component, the sensing device actuating a cooling fluid which is included within the heat absorbing means whereby the vapor level in the apparatus is controlled by the temperature sensing device in combination with the heat absorbing control means.

Abstract: A method for controlling the production of pitch and the like is disclosed comprising simultaneously measuring the viscosity and temperature of the pitch material from the production unit, comparing the measured value with a predetermined correlation of the viscosity and temperature for the pitch, and adjusting the parameters of the production operation in response to the comparison. An apparatus for carrying out the method is also disclosed comprising a means for withdrawing and returning a sample of the pitch material from the still, a chamber for holding the sample of the pitch material, the chamber having a means for heating and cooling the sample, a temperature sensing device and a viscosity measuring device located in the chamber, and a means for recording the temperature and viscosity values.

Abstract: A pressure control system and method for utilization in a process for effecting the alkylation of an aromatic hydrocarbon with a normally gaseous olefinic feed stream. The system is intended to control the pressure within a fractional distillation column which initially recovers the alkylaromatic product from unreacted aromatic hydrocarbons and a minor quantity of normally gaseous paraffinic contaminants contained in the olefinic feed stream. The system is especially advantageous in the boron trifluoride-catalyzed alkylation of benzene with ethylene, the latter containing minor quantities of ethane which must necessarily be vented, or removed from the system.

Abstract: The environment of the invention comprises work degreasing apparatus wherein a tank contains liquid solvent to be vaporized by a heater for degreasing contact with work introduced into the tank, the vapor being subject to condensation, there also being a tank cover having open and closed positions. The inventive improvement comprises means responsive to closing of the cover to control the heater to reduce heat transfer to the liquid solvent, and also responsive to opening of the cover to control the heater to increase heat transfer to the liquid solvent.

Abstract: A method and apparatus for high volume distillation of impure liquid comprises evaporating the impure liquid in an evaporator to form a vapor at a temperature above the freezing point and at or below the boiling point of said liquid at atmospheric pressure and at a pressure corresponding to the evaporation temperature under saturated conditions; compressing said vapor adiabatically; admixing in a mixing chamber the compressed vapor under substantially isobaric conditions directly with hot gases having a temperature sufficiently greater than the temperature of the compressed vapor that the resulting vapor-gas mixture temperature is greater than the temperature of the compressed vapor prior to the mixing; passing the vapor-gas mixture through an expansion engine to motivate the engine and to produce shaft energy, whereby the vapor-gas mixture adiabatically expands and cools; compressing the expanded vapor-gas mixture adiabatically in an independently powered compressor to a predetermined pressure corresponding

Abstract: A method and apparatus for controlling the operation of a distillation column which utilizes cost factors to achieve the best economical production of a product within acceptable purity limits while maintaining the column at maximum operating capacity. The control is based on a series of priorities in which each of the following control signals is selectively used in turn to modify the control the heat-input to the column; cost factors applying to the column, cost factors applying to the several columns in the system, the purity of the product, the operating pressure limit of the column and, for lighter products, the rate of fluid velocity through the column. For heavier products, the rate of fluid velocity through the column is used independently of the heat-input control to restrict the flow of overhead product to the condenser to increase the back pressure on the column.

Abstract: Heat balance of a fractionation column is controlled and maintained by obtaining three differential temperatures between selected temperature-sensing points along the height of the column. A signal representing one of the delta-T's is employed in regulating the quantity of reflux returned to the rectification zone. The remaining two delta-T's are conjunctively utilized to regulate the enthalpy (heat-input content) of the reboiled liquid bottoms stream being returned to the reboiler section of the column. With respect to the latter, a selected one of the two delta-T signals is multiplied by a multiplier representing the ratio of the number of trays between the temperature sensing points supplying the non-selected delta-T signal to the number of trays between the temperature sensing points supplying the selected delta-T signal.

Abstract: Control of a fractionation column is maintained by obtaining two differential temperatures between pairs of selected temperature-sensing points along the height of the column. One pair of temperature sensors is vertically-spaced above the feed tray, while the second pair is below the feed tray. Signals representing the sensed and measured delta-T's are employed in conjunction with a signal representing the flow rate of the feed stream in regulating the quantity of reflux to the rectification zone and in maintaining the required reflux to feed ratio.

Abstract: Heat balance of a fractionation column is controlled and maintained by obtaining three differential temperatures between selected temperature-sensing points along the height of the column. Signals representing the three delta-T's are employed in regulating the quantity of reflux to the rectification zone and the enthalpy (heat-input content) of the reboiled liquid bottoms stream. With respect to the latter, two delta-T's, obtained below the feed locus are used. One of these is considered in conjunction with the third delta-T, obtained above the feed tray, and an additional signal representing the flow rate of the feed stream, to regulate the quantity of reflux.

Abstract: Heat balance of a fractionation column is maintained through the utilization of differential temperature sensors located at selected points in the height of the column. Signals representative of three delta-T's are employed in regulating the quantity of reflux to the rectification zone and the enthalpy (heat-input content) of the reboiled liquid bottoms stream. With respect to the former, two differential-temperature signals are used; these result from four temperature sensors vertically-spaced along virtually the entire height of the fractionation column.

Abstract: Equipment is provided having a distillation tank with a heater and a vapor offtake, with a condenser receiving the offtake vapor and delivering liquid condensate. A control system provides safety features including pressure and temperature responsive devices operative to shut off the heater and further including means for shut off of the heater when the tank is being filled. Still further provision is made for shutting off the heater under the influence of a float valve associated with the condensate discharge line and operative to shut off the heater under the influence of rise in level of condensate in the receiving vessel.

Abstract: A control method and system for regulating the heat input to the reboiler section of a distillation column having attendant thereto a first external heat-recovery reboiler. Flow-measuring means, disposed within a substantially liquid-free environment, produces a signal which is representative of the quantity of vapor flowing from the reboiler section upwardly into the fractionation section of the column. This signal is transmitted to heat-varying means whereby the heat input to a second external reboiler heater is regulated in response to the quantity of vapor flow.

Abstract: A vapor generating and recovering apparatus for separating one component from a second component of a liquid solution and recovering the first component including at least one chamber for generating vapor from the liquid solution and recovering the vapor in a liquid form, the vapor generating portion of the chamber being in heat emitting relation with a heat emitting means and the vapor recovering portion chamber being in heat absorbing relation with a heat absorbing means. A preferred system for providing heat to the vapor generating portion of the chamber and removing heat from the vapor recovering portion of the chamber is a refrigerating system which includes condensing coils and evaporating coils in heat transfer relation with the vapor generating and vapor recovery chamber.

Abstract: A method for regulating, or controlling heat input to the reboiler section of a fractionation column. Flow-measuring means, disposed in a substantially liquid-free environment within the confines of the reboiler section, produces a signal which is representative of the quantity of vapor flowing from the reboiler section upwardly into the fractionation section. This signal is transmitted to heat-varying means, whereby fuel input to an external reboiler heater is regulated in response to the quantity of vapor flow.

Abstract: A vapor generating and recovering apparatus for separating one component from a second component of a liquid solution and recovering the first component including at least one chamber for generating vapor from the liquid solution and recovering the vapor in a liquid form, the vapor generating portion of the chamber being in heat emitting relation with a heat emitting means and the vapor recovering portion chamber being in heat absorbing relation with a heat absorbing means. A preferred system for providing heat to the vapor generating portion of the chamber and removing heat from the vapor recovering portion of the chamber is a refrigerating system which includes condensing coils and evaporating coils in heat transfer relation with the vapor generating and vapor recovery chamber.

Abstract: Automatic regulation system for a distillation unit including a charging vessel, provided with heating means, surmounted by a distillation column overtopped by a condenser, a withdrawing system and recovery tanks, said system comprising an intermediate tank between the withdrawing system and the recovery tanks, means for controlling the liquid level in said intermediate tank and the discharge of liquid therefrom into the recovery tanks, valve means for applying at will a reduced pressure or the atmospheric pressure to the distillation unit and the intermediate tank and means for changing the recovery tanks in synchronization with the actuation of said valve means.