Abstract: The concentrate holding lower portion of a sample and concentrate holding vessel has a jacket for shielding such concentrate holding portion from heat sufficient to volatilize appreciable solvent therefrom when the vessel is subjected to sufficient heat for effecting evaporative concentration of solution in such vessel.

Abstract: A liquid evaporator includes an air-tight outer container containing liquid therein, the liquid container having support legs adjacent the bottom surface thereof; an inner container mounted on the legs for partitioning the interior space of the outer container, the inner container having a wall made of insulating material; and a heater fixed to an upper portion of the outer container and positioned inside the inner container. The liquid evaporator may be combined with a deodorizing device for forming a urine treating device, wherein the urine treating device includes a deodorizing housing having an upper portion provided with a secondary heater therein, a catalyst surrounding the secondary heater, a blower provided outside the housing, and a diffusion pipe provided at the upper portion of the housing.

Abstract: A coolant recycling apparatus has a boiler and condenser for distilling a glycol and water from a used coolant. The glycol and water are recombined in a mixing tank to form a mixture having a desired ratio of water to glycol, and an inhibitor is added to the mixture to obtain a fresh coolant mixture ready for use in an engine cooling system. Contaminants in the used coolant are concentrated to form a sludge.

Abstract: A process for the separation of multicomponent systems containing intermediate boiling substances in separating separating columns with side discharge, the temperatures T.sub.u and T.sub.o above and below the side discharge are measured on the column or inside the column and the temperature difference T.sub.u -T.sub.o is used for controlling the side discharge. The control is carried out by constantly controlling one of the two temperatures T.sub.u or T.sub.o by the output of the evaporator or the discharge from the sump or the reflux or the removal of distillate or the reflux ratio.

Abstract: An apparatus for evaporative concentration of a liquid sample comprises a housing including an upper chamber and a lower chamber, a concentrator flask, a reflex tube and a vortex tube. The concentrator flask includes an upper solution vessel section and a lower cold finger section, and the flask is arranged within the housing with the solution vessel section positioned in the upper chamber and the cold finger section positioned in the lower chamber. The reflex tube is arranged at the upper end of the concentrator flask. The vortex tube has a cold air outlet connected with an inlet to the lower chamber of the housing and a hot air outlet connected with an inlet to the upper chamber of the housing. The apparatus is employed to concentrate a liquid sample contained in the concentrator flask with the temperatures of the cold and hot air from the vortex tube being sufficient to induce the evaporative separation of samples.

Abstract: A method and apparatus are disclosed wherein a standpipe mounted in an accumulator outside the operating zone of a distillation column is used in conjunction with a liquid level controller to measure condensate collected in the accumulator and to change the amount of energy provided to the distillation column in response to changes in the level of condensate collected in the accumulator.

Abstract: A water distilling apparatus (10) which includes vertically stacked components, i.e. an uppermost water storage tank (12), an intermediate boiling tank (14) and a lowermost condensing unit (16). Stacking of the distiller components creates a space efficient design with ready access to the respective components. The preferred apparatus (10) is also equipped with a small, dedicated water conditioning unit (20) situated between the main solenoid water valve (94) and the inlet of the boiling tank (14).

Abstract: A liquid evaporator includes an air-tight outer container containing liquid therein, the liquid container having support legs adjacent the bottom surface thereof; an inner container mounted on the legs for partitioning the interior space of the outer container, the inner container having a wall made of insulating material; and a heater fixed to an upper portion of the outer container and positioned inside the inner container. The liquid evaporator may be combined with a deodorizing device for forming a urine treating device, wherein the urine treating device includes a deodorizing housing having an upper portion provided with a secondary heater therein, a catalyst surrounding the secondary heater, a blower provided outside the housing, and a diffusion pipe provided at the upper portion of the housing.

Abstract: An improved method of and apparatus rendering water-based fluid waste stream evaporation operations environmentally and otherwise safe, involving separately and independently existing the hot gas stream produced by fuel combustion and the vaporized fluid-air exhaust stream resulting from heat-vaporizing of the fluid, independently directing the streams in opposite directions toward one another and to a common region, and applying fan suction immediately at said region to exert the sole control of withdrawing the streams simultaneously.

Abstract: A packed column with temperature sensors to measure the temperature profile longitudinally and transversely of the column without the temperature profile or flow conditions being affected by the measuring arrangement. The temperature measuring leads (10) are introduced into the upper part of a column section (1) through a single tube (12) and, are routed to the desired measuring points (8) through the peripheral zone between the packing (9) and the column wall (2).

Abstract: A water distiller for vaporizing and condensing water. The distiller is provided with a container for holding the water to be distilled and a water level regulator for maintaining the water in the container at a desired level. A heating element is provided that is positioned just below the desired water level and spaced from the sides of the container. A cover is positioned atop the container for sealing the container and for suspending the heating element into the water. A condenser on top of the cover condenses vapor produced by the heating element. The distiller may be equipped with a sensor for sensing the temperature of the air above water level in the container and a shut off switch for removing power from the heating element responsive to a high temperature reading in the sensor.

Abstract: A method and apparatus for automatically and sequentially distilling batches of water having substantially equal volumes in a plurality of distillation cycles, one batch in each cycle. During each cycle, water is admitted to a boiler tank for a fixed interval of time to form a batch in the tank. The batch of water in the tank is then vigorously boiled while venting the tank through a pipe to the atmosphere. The vigorous boiling is terminated when the temperature within the vent pipe reaches the boiling point of pure water. Upon termination of the vigorous boiling phase, a gentle boiling phase is initiated, the vent pipe is closed, and vapor in the tank is admitted to a condenser. The condenser condenses the vapor to obtain distilled water which is collected in a collection device. The gentle boiling phase continues until the level of water in the tank recedes to the level of a heater in the tank.

Abstract: Apparatus and methods for determining the Reid Vapor Pressure of either an overhead, side draw or bottoms product stream of a fractionating column used for fractionating a multi-component hydrocarbon feed stream into an overhead product stream, a side draw product stream and a bottoms product stream are provided. The Reid Vapor Pressure of the particular product stream is determined in response to the temperature of the product stream, the vapor pressure of the product stream, the rate of flow of the bottoms product stream, the rate of flow of the overhead product stream, and/or the rate of flow of the side draw product stream without further analyses thereof. The Reid Vapor Pressure indication is used to maintain the actual Reid Vapor Pressure of the particular product stream substantially equal to the desired Reid Vapor Pressure of the particular product stream and to thereby control the quality of the desired product stream.

Abstract: A potable water dispenser includes a first reservoir for storing raw water, a second reservoir for storing boiled hot water, and a third reservoir for storing boiled warm water. The second reservoir is surrounded by the raw water in the first reservoir so as to effect a heat exchange therebetween. A condenser is disposed on the top end of the second reservoir. A heating device is interposed between the first and second reservoirs so as to vaporize the raw water from the first reservoir. Then, the vapor flows into the condenser so as to form boiled hot water which falls into the second reservoir. The boiled hot water will flow from the second reserovir into the third reservoir through a water duct so as to form boiled warm water. Two water tap units are respectively communicated with the second and third reservoirs so as to supply hot and warm water.

Abstract: An apparatus for supplying both hot water and distilled water includes a water distillation unit having a steam generator, a condenser connected with the steam generator for converting steam into distilled water and a holding tank for receiving distilled water from the condenser. The condenser is in heat transfer relation to the interior of a water heater tank. Water level monitors are provided for monitoring the level of water in the steam generator and the holding tank and temperature sensors sense the temperature of water in the steam generator and water heater tank. When the level of water in the holding tank is above a predetermined value, the steam generator is de-energized and feed water is admitted to the steam generator to dilute the contents to a safe temperature before the contents are discharged to drain.

Abstract: In a fractional distillation tower which is divided into a plurality of sections by total drawoff trays, and wherein at least one fraction is withdrawn from each section. The cut point temperature between fractions is determined based on the partial pressure and temperature of the vapor in the upper portion of a section. The thus determined cut point temperature may be compared to a set point with the results of the comparison being utilized to maintain the actual cut point temperature between fractions substantially equal to the desired cut point temperature.

Abstract: Apparatus and methods for determining the Reid Vapor Pressure of a bottoms product stream of a fractionating column used for fractionating a multi-component hydrocarbon feed stream into an overhead product stream and a bottoms product stream are provided. The Reid Vapor Pressure of the bottoms product stream is determined in response to the temperature of the bottoms product stream, the vapor pressure of the bottoms product stream, the rate of flow of the bottoms product stream and the rate of flow of the overhead product stream, without an analysis of the particular product stream. The Reid Vapor Pressure indication is used to maintain the actual Reid Vapor Pressure of the bottoms product system substantially equal to the desired Reid Vapor Pressure of the bottoms product stream and to thereby control the quality of the bottoms and other product streams.

Abstract: A steam distillation apparatus is provided which has a column body, a head connected to one end of the column body which has a diameter larger than the column body, a sump connected to the other end of the column body and contact elements disposed within the column body which are positioned and arranged to avoid formation of preferential pathways for the steam passing through the column body while providing for ready flow of the material being steam distilled through the column body. The connection of the head and column body may be frustoconical in shape such that its diameter diminishes from a diameter corresponding with that of the head at its connection with the head to a diameter corresponding with that of the column body at its connection with the column body. A collar is positioned at the connection of the neck and column body and extends into the head to define an annular space between the neck and collar.

Abstract: In an absorption process utilizing a feed gas compressor, the absorption pressure is maximized within the constraints of the system by a computer controller that automatically increases the pressure until a constraint for compressor speed or absorption pressure is encountered. The control action coordinately manipulates compressor speed and the absorption pressure in response to the actual compressor suction pressure to achieve the desired result.

Abstract: In a fractional distillation process, the operation of a reflux pump in the process is enhanced by providing that liquid discharged from the reflux pump is returned directly to the reflux pump suction during the periods when the liquid reflux supply from the fractional distillation process is not sufficient to keep the reflux pump in constant operation.

Abstract: A computer control system for automatically optimizing the temperature of the feed supplied to a distillation column from a fuel fired preheat furnace, wherein the furnace temperature is manipulated in response to a measured ratio of distillate flow (D) from the tower to fuel flow (F) to the furnace. The D/F ratio is maximized by periodically comparing the present value of D/F to the previous value and incrementally increasing the furnace temperature as long as the D/F ratio increases. When no change is detected or the D/F ratio starts to decrease the furnace temperature is incrementally decreased until the D/F ratio again increases and reverses the control action once more.

Abstract: Method and apparatus for disposing of waste rinse water used in photographic processes in which the waste rinse water is heated in a dissolution tank to be reduced to a slurry which is accumulated and stored in drums for later processing. The apparatus is compact consisting of separate tanks for the different rinse water, a holding tank to collect the contaminated rinse water and a separate dissolution tank. There is no discharge of any liquid waste products into the environment.

Abstract: Process and apparatus for the preliminary determination of the efficiency of the trays of distillation and/or absorption columns in order to establish the actual tray number of the columns, as well as for those columns the tray number of which was determined thereby. Each column section of different geometry or load is loaded with a set of trays (12) with air water system consisting at least of two trays having identical geometry (13,13a) and one air distributor (14). On the basis of the recognition that each set of trays (12) may be regarded as a cascade consisting of mixers which include series-connected mixers formed from the trays (13,13a), the liquid content of which is mixed by ascending vapor, or gas, in this case by air.

Abstract: A feedforward control system for a multiple-effect evaporator is provided wherein control is based on maintaining desired values for inferential variables of concentration and boiling point rise for a solution of a solid inorganic substance.

Abstract: A process for controlling a distillation column in which feed liquid supplied thereto is heated by heating steam comprises the steps of: controlling the steam flow rate so that the steam flow rate is increased in response to the difference between the temperature measured at the bottom of a calculated column and the temperature of boiling point of the feed liquid until the former temperature exceeds the latter temperature when the former is not higher than the latter; controlling the steam flow rate so that the temperature around an intermediate tray falls within a first predetermined temperature range when the temperature measured at the bottom of the column exceeds the calculated temperature of the boiling point of the feed liquid; controlling the steam flow rate so that a reflux ratio is adjusted to within a predetermined reflux ratio range when the temperature around the intermediate tray falls in the predetermined temperature range; and controlling the steam flow rate so that the reflux ratio is maintain

Abstract: The temperature of a crude oil provided from a crude oil preheat furnace to a crude tower is substantially minimized by controlling such temperature so as to maintain a desired minimum overflash flow in the crude tower. Also, the temperature of each of the individual coils in the preheat furnace are balanced with respect to each other. Such minimization and balancing results in substantially optimal utilization of the fuel provided to the preheat furnace which results in considerable economic savings with respect to the operation of the preheat furnace.

Abstract: A measurement of the pressure in a fractional distillation column is utilized to bias the desired external reflux flow rate which is determined by some conventional method. The bias is applied only when a pressure limitation is exceeded and the external reflux flow rate is reduced as a result of the bias which results in a reduction of column pressure.

Abstract: The Reid Vapor Pressure of a hydrocarbon mixture consisting essentially of hydrocarbons selected from the same series is determined based on the actual temperature and vapor pressure of the hydrocarbon mixture. The thus determined Reid Vapor Pressure may be compared to a set point for the Reid Vapor Pressure with the results of the comparison being utilized to maintain the actual Reid Vapor Pressure substantially equal to the desired Reid Vapor Pressure.

Abstract: A vapor distillation system sprays a mixture of liquids to be distilled into an evacuated vaporizer chamber. The low boiling point components of the mixture will be vaporized while the remainder of the mixture will collect at the bottom of the vaporizer chamber. The collected liquid is recirculated and heated. The recirculating liquid is discharged, and fresh mixture is introduced, as a function of the sensed temperature of the recirculating liquid. The vapor is transferred to a condenser chamber having a water spray head so that the chilled spray condenses the vapor. Both the condenser chamber and the vaporizer chamber have fluid level control systems.

Abstract: A desired separation between sidedraw product streams withdrawn from a fractional distillation column is maintained by controlling the flow rate of the external reflux associated with a particular sidedraw product stream in response to the output signal from a temperature controller which is reset by an internal reflux controller. Such cascade control improves the stability of a fractionation process and provides for good control of the separation between sidedraw product streams.

Abstract: In a fractional distillation process in which it is desired to maintain a desired ASTM end point temperature of the overhead liquid product withdrawn from the fractional distillation process, changes in the slope of the equilibrium flash vaporization boiling point line are utilized to determine the actual slope of the ASTM boiling point curve at any particular time. The actual ASTM end point temperature for the overhead liquid product is derived based on the actual slope of the ASTM boiling point curve thus determined. The actual ASTM end point temperature is utilized to control the fractional distillation process so as to maintain a desired ASTM end point temperature for the overhead liquid product withdrawn from the fractional distillation process.

Abstract: In a fractional distillation process in which a sidedraw product stream is withdrawn from the fractional distillation column, the flow rate of the overhead product stream is controlled so as to increase the flow of the upper external reflux so as to drop as much as possible of the overhead product into the sidedraw product stream. However, valve position control is utilized to override the control of the flow of the overhead product stream, which is being controlled so as to substantially maximize the flow of the sidedraw product stream, if the valve controlling the flow of the upper external reflux approaches fully open such that control of the liquid level in the overhead accumulator associated with the fractional distillation process is not lost.

Abstract: In a fractional distillation process in which it is desired to maintain a desired ASTM end point temperature of the overhead liquid product withdrawn from the fractional distillation process, changes in the heat removed by the fractional distillation process per unit of the feed are utilized to determine the equilibrium flash vaporization initial point and the equilibrium flash vaporization end point temperature for the overhead liquid product. The initial point temperature and end point temperature are then utilized to determine the actual slope of the equilibrium flash vaporization boiling point line. Changes in the slope of the equilibrium flash vaporization boiling point line are utilized to determine the actual slope of the ASTM boiling point curve at any particular time. The actual ASTM end point temperature for the overhead liquid product is derived based on the actual slope of the ASTM boiling point curve thus determined.

Abstract: Process and apparatus are provided for the recovery of low, medium and high boiling components from feed streams containing same wherein reboiler fouling, gumming and the like are minimized, via the control of fractionator reboiler temperatures.

Abstract: In a fractional distillation process in which it is desired to maintain a desired overhead product composition and bottoms product composition, a set point for the flow rate of the external reflux to the fractional distillation column is increased or decreased by an incremental amount or is left constant based on whether the concentration by the heavy key component in the overhead product stream and the concentration of the light key component in the bottoms product stream are above a high limit, below a low limit, between the high limit and low limit or some combination thereof and also based on the relationship between a set point for the flow rate of the external reflux and a high limit for the flow rate of the external reflux. At the same time, a temperature set point for the fractional distillation column is increased or decreased by an incremental amount or is left constant depending on the same factors.

Abstract: A vapor compression distillation system for distillation of any two-component liquid mixture where separation of the more volatile from the less volatile component is required. This system achieves a very high efficiency through the use of vapor compression in conjunction with three heat exchangers: a reboiler which condenses the hot vapors compressed by a vapor pump and uses the heat given up by the condensing vapor to boil bottoms liquid to produce vapor within the stripper, a distillate heat exchanger which recovers heat from the distillate stream, and a bottoms heat exchanger which recovers heat from the outgoing bottoms effluent. This particular component configuration and process results in an exceptionally stable and reliable operation requiring the continuous control of only one parameter, reboiler temperature, while fixing all other process variables.

Abstract: In a fractional distillation process in which it is desired to maintain a desired overhead product composition and bottoms product composition, a set point for the flow rate of the external reflux to the fractional distillation column is increased or decreased by an incremental amount or is left constant based on whether the concentration of the heavy key component in the overhead product stream and the concentration of the light key component in the bottoms product stream are above a high limit, below a low limit, between the high limit and low limit or some combination thereof. At the same time, a temperature set point for the fractional distillation column is increased or decreased by an incremental amount or is left constant depending on the same factors. Use of these set points for process control provides control of the overhead product composition and bottoms product composition without the use of analysis controllers.

Abstract: In a fractional distillation process in which a pump around stream is utilized to control heat removal from an upper portion of the fractional distillation column and in which the pump around stream is utilized to preheat the feed stream flowing to the fractional distillation column, control signals derived from an analysis of the overhead product stream from the fractional distillation column are utilized to substantially maximize the flow rate of the pump around stream. This results in a maximum preheating of the feed stream flowing to the fractional distillation column which improves the energy efficiency of the fractional distillation process. Also, a desired overhead product specification is maintained.

Abstract: Control of multiple distillation columns for producing anhydrous alcohol suitable for blending with gasoline to produce gasohol. The distillation process involves production of a first-stage distillate containing a predetermined amount of water, followed by azeotropic distillation in the presence of a hydrocarbon entrainer to strip the distillate of its water content, leaving anhydrous alcohol as a bottom product. Tight controls are present during first-stage distillate production to hold its proof at an optimum value derived at through material balance calculations to minimize energy consumption for the overall system. Control over the dehydrating stage is accomplished by a combination of ratio control to regulate and maintain the proper proportion of the entrainer and temperature control to regulate within the column the actual inventory of entrainer.

Abstract: The heat to a feed in a distillation operation is controlled in response to the amount of liquid in a liquid condensate collection means.

Abstract: A process and apparatus are provided controlling the heat input of an extractive distillation column. The bottom of the column is heated with a major stream of thermal energy which is either slowly varying in time or controlled by the amount of starting material mixture and with a minor stream of thermal energy which is controlled by sensing the thermodynamic state in the upper half of the column during the process. The major stream can provide about 90 percent and the minor stream about 10 percent of the heat fed to the column. The minor stream can be controlled by the temperature at one point in the upper half of the column, by the temperature difference at two points in the upper half of the column or by gas chromatographic analysis of the extract material concentration near the top of the column. The process allows one to keep a low concentration of the extract material in the raffinate.

Abstract: In an alkylation process in which an acid regenerator is utilized to separate an acid catalyst from acid soluble oil contained in a spent acid catalyst stream, the heat input to the acid regenerator is manipulated based on the feed flow rate of the spent acid catalyst stream so as to maintain a substantially constant heat input per pound of feed flowing to the acid regenerator and the liquid level in the acid regenerator is manipulated so as to maintain the acid catalyst and acid soluble oil interface in the acid regenerator at a desired level. Such manipulation of the heat input to and the liquid level in the acid regenerator results in a substantially optimum separation of acid catalyst from acid soluble oil.

Abstract: In a fractional distillation process in which first (light key) and second (heavy key) components contained in a feed stream are separated with the major portion of the light key component being removed in an overhead product stream and the major portion of the heavy key component being removed in a bottoms product stream, a signal which is responsive to the concentration of the light key component in the bottoms product stream is summed with a signal which is responsive to the concentration of the heavy key component in the overhead product stream to derive a signal which is utilized to manipulate the flow rate of the external reflux (sigma control). Also, the difference between a signal which is responsive to the concentration of the light key component in the bottoms product stream and a signal which is responsive to the concentration of the heavy key component in the overhead product stream is utilized to control the flow rate of the bottoms product stream (delta control).

Abstract: Normal butane withdrawn from the main fractionator in an acid alkylation process is recycled to the main fractionator as required to insure that the actual alkylate to normal butane ratio in the alkylate product withdrawn from the main fractionator does not go below a desired ratio. Maintenance of the actual ratio at or above the desired ratio substantially minimizes the concentration of isobutane in the alkylate product stream.

Abstract: A vapor generating and recovery apparatus for vaporizing a liquid and condensing the vapor including at least one chamber in which vapor is generated from the liquid and recovering the vapor in liquid form, the vapor generating portion of the chamber being in heat emitting relation with a heat emitting means and the vapor recovery portion of the chamber being in heat absorbing relation with a heat absorbing means. A preferred system for providing heating and cooling to the vapor generating and recovery apparatus is a refrigerant system which includes at least one refrigerant condensing coil (heat emitting means) and at least one refrigerant evaporating coil (heat absorbing means) in heat transfer relationship with the vapor generating portion and vapor recovery portion, respectively, of the chamber, and two refrigerant heat exchanger means, one being downstream and one being upstream of the heat emitting means for removing excess heat from the refrigerant system.

Abstract: In a fractional distillation process in which the designation of the primary product stream changes, the desired composition of the primary product stream and a secondary product stream are maintained without losing automatic control of the process for an extended period of time while the controllers controlling the process are retuned for the new operating conditions. Two sets of tuning constants are available to each controller and these tuning constants are automatically switched as required by the designation of the primary product stream.

Abstract: A continuous trickle-down distillation unit for producing hydrated alcohol having a compact, elongated distillation tube through which a fluid mixture including alcohol as one of its constituents passes. Within the distillation tube only the alcohol-predominant portion of the fluid mixture is vaporized while the remaining constituents of the fluid mixture are removed. The vaporized alcohol-predominant portion is condensed within a chamber which communicates with the distillation tube and is removed therefrom by a collection plate which extends partially into the chamber.

Abstract: A desired cloud point temperature for a side draw product stream from a fractional distillation column is maintained at a desired level by comparing a calculated actual cloud point temperature, which is updated periodically by a cloud point measurement, to a desired cloud point temperature with results of the comparison being utilized to control the flow rate of the side draw product stream so as to maintain the actual cloud point temperature of the side draw product stream substantially equal to the desired cloud point temperature. Use of the calculated cloud point temperature provides a means by which continuous control of the actual cloud point temperature of the side draw product stream can be maintained.

Abstract: An apparatus and method for producing alcohol fuel in an efficient and continuous manner are provided. The apparatus and method utilize otherwise lost heat to reduce the amount of heat required to convert feed stock into alcohol fuel. The apparatus and method utilize the supply of feed stock from a hopper through an auger to a cooker vessel, and then in turn to enzyme and fermenting tanks or vessels, which in turn discharge fermented mash to a strainer for separation of the alcohol beer from the mash. The beer is then discharged to a level controlled beer tank which regulates a residue valve controlling the amount of residue liquid returned to the apparatus and maintained under process. From the beer tank, the flow of the beer is regulated by passage through a non-clogging control valve into a reflux column.

Abstract: A batch distillation operation is automatically controlled from a start-up mode to a shut-down mode.