With Distilland Treating Devices Patents (Class 202/176)
  • Patent number: 4686009
    Abstract: A vacuum distillation system uses a tower having an open bottom submerged within a tank of solution exposed to atmospheric pressure. The solution within the tower is elevated to barometric level by a high vacuum or low absolute pressure on the tower top. As solution flows through the open bottom and upward, the solution is heated and then cooled to cause degasification and precipitation, and then withdrawn from the tower top. The treated solution is flowed to a vaporization chamber that is subjected to a low absolute pressure. A heater maintains the solution at a selected chamber temperature above the boiling point of water at the selected chamber pressure. The chamber pressure and temperature may be selected as desired to yield the purest water distillate for almost any solution of water and impurities. Water vapor is pumped from the vaporization chamber by a vapor pump to a condenser, where condensation results from increased pressure and decreased temperature.
    Type: Grant
    Filed: October 29, 1985
    Date of Patent: August 11, 1987
    Assignee: James W. Laney
    Inventor: Derald L. McCabe
  • Patent number: 4664751
    Abstract: A de-salinator 10 for brackish- or salt-water has a heat insulating shell 11 closed by end plates 12. A heat exchanger 22 in the bottom of the chamber 13 is heated by engine coolant from a marine engine 27, while a pair of condensor coils 19, connected to manifolds 33, 34, use sea water to cool the fresh water vapour which is drawn off by outlets 21. The engine driven pump 37 which draws the water through the condensor coils 19 operates an eductor 36 which generates a partial vacuum in the chamber 13, drawing off brine from the bottom of the chamber and any excess water in the chamber. The level of water in the chamber 13 is maintained by drawing off a portion of the heated water passing through the condensor tubes 19. The condensate is drawn from the outlets 21 via an eductor 46 which is driven by a suction pump 45 connected to the fresh water tank 47.
    Type: Grant
    Filed: August 5, 1985
    Date of Patent: May 12, 1987
    Assignee: Nautical Services Pty. Ltd.
    Inventor: Ian D. Lloyd
  • Patent number: 4662990
    Abstract: A continuous process and apparatus for drying aqueous solids by evaporation using a fluidizing oil and a surfactant wherein the fluidizing oil and surfactant are recovered and recycled separately or together. The aqueous solids may, or may not, have a heavy, natural oil associated with them.
    Type: Grant
    Filed: October 23, 1985
    Date of Patent: May 5, 1987
    Assignee: Hanover Research Corporation
    Inventor: Anthony J. Bonanno
  • Patent number: 4639293
    Abstract: This invention relates to a solar still wherein the evaporation takes place in partially evacuated tubings which are heated by sunlight. The water to be distilled is supplied from a reservoir vessel which is sealed off after batch loading. The reservoir vessel is elevated above the solar collector. The water is fed into the heater tubings routed through the solar collector by gravity, through an orifice and a heat exchanger-condenser. The steam tubing branches off from the heater tubing in the solar collector vertically, and is routed through the heat exchanger-condenser. At this end, it is connected to a vertical tubing of a sizable length that empties into the distilled water reservoir. The exit end of the heater tubing routed through the solar collector is connected to another vertical tubing of a sizable length that empties into an overflow tank.
    Type: Grant
    Filed: May 6, 1983
    Date of Patent: January 27, 1987
    Inventor: Hyok S. Lew
  • Patent number: 4624747
    Abstract: In the distillation of fresh water from sea water, the sea water is passed ownwardly in a falling film evaporator through a multiplicity of vertical tube evaporator (VTE) stages and multiple stage flash (MSF) evaporators. After the sea water passes through the first VTE stage where it forms a liquid component and a steam component, the liquid component is distributed evenly into the next VTE stage while the steam component enters an adjoining MSF stage. Condensed fresh water flows downwardly from one MSF stage to the next and experiences flash evaporation. The sea water or brine component and the fresh water distillate flow downwardly through the VTE and MSF stages so that the brine component can be removed from the final VTE stage and the fresh water distillate from the final MSF stage.
    Type: Grant
    Filed: October 9, 1985
    Date of Patent: November 25, 1986
    Assignee: D.V.T. Buro fur Anwendung Deutscher Verfahrenstechnik H. Morsy
    Inventor: Gamal el Din Nasser
  • Patent number: 4612090
    Abstract: Water degasification and distillation apparatus having a container for water to be degasified and distilled, a relatively small boiler adjoining said container and having a first conduit extending into the container so that a selected water level in the container will fill said boiler to a selected height, a condenser within the container and immersed in the water contained therein, a second conduit extending from the space above the water in said boiler to the inlet of the condenser, an outlet on the condenser extending through a container wall for discharging degasified and distilled water and heating means in said boiler for heating the water therein.
    Type: Grant
    Filed: April 29, 1983
    Date of Patent: September 16, 1986
    Inventor: John C. Ellis, Jr.
  • Patent number: 4606794
    Abstract: An automated solar still is disclosed which incorporates a system of valves and other controls that halts production when the level of solar insolation is not adequate to support evaporation, admits water for treatment only when the still requires resupply, operates at nominal pressure by gravity flow and flushes out suspended and dissolved contaminants automatically. Production is halted under conditions of inadequate solar insulation by means of a temperature sensitive valve which is exposed to the received sunlight. In one embodiment, heating and evaporation occur directly in a central chamber. In another embodiment heating occurs in external panels and evaporation occurs from trays in an evaporation chamber. With changes in dimensions and proportions the system of controls may be used in solar stills for desalinating sewater.
    Type: Grant
    Filed: January 17, 1985
    Date of Patent: August 19, 1986
    Inventor: Robert L. Wyckoff
  • Patent number: 4601790
    Abstract: Deodorizing and/or physical refining of cocoa butter and cocoa butter substitutes is carried out in accordance with the principle of continuous counter-current falling film stripping steam distillation in at least two different zones, where different flow and current conditions prevail for the liquid film and the vapors, respectively. In the initial zone 10 the vapors pass through trickle passages having a hydraulic equivalent diameter greater than the hydraulic equivalent diameter in the final zone 22.The working pressure in the top of the falling film column 10 is maintained below 2.0 mbar, and in the bottom of the falling film column 22 it is maintained by at most 1.6 mbar in excess of that in the falling film column 10. The accumulation of any significant liquid content in the bottoms of the serially operating zones is avoided. Stripping steam is supplied in an amount of 2 to 10 kg of steam per 100 kg of charged liquid.
    Type: Grant
    Filed: July 18, 1983
    Date of Patent: July 22, 1986
    Inventor: Hermann Stage
  • Patent number: 4601381
    Abstract: Apparatus for monitoring fluid condition in a fluid recovery system for removing water and solid contaminants from a fluid is disclosed. One aspect of the present invention relates to an improved fluid level indicator device for indicating and controlling the fluid level in a vacuum distillation chamber. A second aspect of the invention relates to an improved sight glass used for monitoring the condition of the cleaned fluid. The sight glass is a one-piece unit formed from a homogeneous, substantially transparent material. Both fluid level indicator and sight glass are designed to function individually or in combination in the severe environment and under the diverse operating conditions of the fluid recovery system.
    Type: Grant
    Filed: September 26, 1983
    Date of Patent: July 22, 1986
    Assignee: RPR Filtration Systems, Inc.
    Inventors: August R. Nukala, Arthur Perez, Timothy L. Brumfield
  • Patent number: 4599143
    Abstract: The deodorization and/or physical refining of high-boiling organic edible oils, fats and esters is carried out according to the principle of continuous counter-current falling film stripping steam distillation in an internally imposed temperature field in at least two different zones having different flow conditions for the liquid film and the vapors, respectively, prevailing therein. In the initial zone 10 directly adjacent the liquid charge and ensuring at least two separation stages the vapors flow through trickle passages having a hydraulic equivalent diameter of 73 to 150 mm. If necessary, this initial zone may be subdivided, wherein in the first sub-zone the trickle passages are provided with hydraulic equivalent diameters of 120 to 150 mm and in the second sub-zone the trickle passages are provided with hydraulic equivalent diameters of 73 to 120 mm.
    Type: Grant
    Filed: July 18, 1983
    Date of Patent: July 8, 1986
    Inventor: Hermann Stage
  • Patent number: 4575404
    Abstract: A pure water tank for distillation equipment comprises a casing on a water tank proper and a communicating pipe via which interiors of the casing and tank proper communicate each other. Water in the casing prevents air from entering into the pure water tank through a condenser when generation of steam is halted.
    Type: Grant
    Filed: September 23, 1983
    Date of Patent: March 11, 1986
    Assignee: Yamato Scientific Co., Ltd.
    Inventors: Hideo Goto, Naoki Yoshida
  • Patent number: 4543165
    Abstract: A closed cycle recovery system and apparatus for continuously recovering residual products which have been washed or flushed from tank trucks, tank cars, and other transportation or storage containers while simultaneously separating and recovering the water, solvent or other fluids which are used to wash or flush such tanks and containers in which a mixture of the water, solvent, and other fluids, and the residual product is separated by evaporation of the water, solvent, or other fluids by passing the mixture through a distillation chamber having a series of tube and flat plate heat exchange surfaces so that the individual fluids and product may be purified and separately stored for further use.
    Type: Grant
    Filed: August 1, 1983
    Date of Patent: September 24, 1985
    Assignee: Recovery Technology, Inc.
    Inventor: Joseph A. Capella
  • Patent number: 4534828
    Abstract: An evaporator apparatus (10) and method for converting a contaminated fluid including mostly water and water soluble substances into a vapor and a residue. Apparatus (10) includes a container (11) for retaining the fluid. A heat source (17) is utilized for supplying heat to evaporate the fluid. A flue assembly (18) positioned in the fluid conveys the heat from the heat source (17) through the fluid. A draft mechanism (20) draws off the resulting vapors as they are formed.
    Type: Grant
    Filed: September 30, 1983
    Date of Patent: August 13, 1985
    Assignee: Nordale Incorporated
    Inventors: Dale C. Erickson, Norton J. Erickson
  • Patent number: 4496431
    Abstract: A method of centrifugal evaporation such as may be employed for reclaiming used industrial solvent having water and solid contaminants, including injecting the contaminated solvent into a cyclonic still, heating the contaminated solvent in the still to vaporize the solvent and water content, the solid contaminant being separated and discharged as a wet sludge, conducting the co-mingled solvent and water vapors to a condenser in which the vapors are condensed to liquids, separating the condensed liquids into solvent for reuse and water for disposal, passing the wet sludge into an inclined elongated dryer where the sludge is heated, vaporizing the liquid which is drawn off, the dried solid contaminant being collected for reuse or disposal.
    Type: Grant
    Filed: August 23, 1982
    Date of Patent: January 29, 1985
    Inventor: Leslie L. Fowler
  • Patent number: 4492613
    Abstract: Methanol and cyclohexane are recovered from a condensed methanol-cyclohexane azeotrope by allowing the condensed azeotrope to separate in a vessel into an upper phase rich in cyclohexane and a lower phase rich in methanol, fractionating the upper phase in a first column whereby the methanol-cyclohexane azeotrope is taken off the top and returned to the vessel while cyclohexane is removed from the lower portion of the first column, and fractionating the lower phase in a second column whereby the methanol-cyclohexane azeotrope is taken off the top and returned to the vessel while methanol is removed from the lower portion of the second column.
    Type: Grant
    Filed: August 2, 1982
    Date of Patent: January 8, 1985
    Assignee: The B. F. Goodrich Company
    Inventor: Gerald V. Wootton
  • Patent number: 4488933
    Abstract: Disclosed herein is a process and apparatus for safely distilling relatively small batches of organic compounds such as paint solvents by directly and safely heating the compounds in a vessel having a relatively thick bottom with electrical heating units cast in it and a relatively thick side wall integrally attached to the bottom. The side wall may be integrally attached to the bottom by a weld that penetrates the joint between the side wall and bottom preferably by 100% in order to provide a complete heat transfer from the bottom to the side wall. The vessel is so designed so as to provide a relatively uniform temperature throughout the inner periphery of the vessel thereby avoiding hot spots and insuring that the hottest spot of the inner periphery of the vessel does not exceed the auto ignition temperature of the compound being processed.
    Type: Grant
    Filed: August 27, 1982
    Date of Patent: December 18, 1984
    Assignee: Finish Engineering Company, Inc.
    Inventors: Charles K. Claunch, David Bowes
  • Patent number: 4487659
    Abstract: Solar distillation apparatus is disclosed in which the released heat of condensation of the condensing liquid is recovered in a transparent conduit disposed over the liquid to be distilled. Solar energy passes through the transparent conduit and is received on an undulated plate system over which the liquid to be distilled is conducted. A cooling fluid is circulated through the conduit to absorb heat released by the condensing liquid. In one embodiment, the conduit does not concentrate the solar energy. The conduit is preferably disposed at an angle of up to about 25.degree. with the horizontal so that the system is subjected to minimal pressure. In another embodiment the conduit defines a fluid lens system which concentrates the solar energy on the plate system. Provision is also made to recover heat from the condensate and a concentrate of the liquid to be distilled.
    Type: Grant
    Filed: October 23, 1980
    Date of Patent: December 11, 1984
    Assignee: North American Utility Construction Corp.
    Inventor: Virgil Stark
  • Patent number: 4482431
    Abstract: A distillation apparatus is provided having a first chamber for receiving water to be distilled and which surrounds one end of a second chamber and also contains the condensing tube; liquid from the first chamber passes to a tube located in a second chamber which traverses a path sufficient to heat the water in the tube to a predetermined temperature before exiting through a valve to a liquid/gas separating device; a third chamber receives the liquid from the separation device and is provided with a heater to heat the liquid until it vaporizes whereupon it rises through the second chamber to enter the condenser tube located in the first chamber; the steam entering the condensing tube is cooled by the incoming water and is discharged from the apparatus.
    Type: Grant
    Filed: February 18, 1983
    Date of Patent: November 13, 1984
    Inventor: John L. Voorhees
  • Patent number: 4464227
    Abstract: A charge of distilland (33) is metered into a heated inclined trough (18) within a chamber (10). Vapors of distilland rise to a level (41) which is below the upper level (26) of the trough. The vapors spill over the sides (31 and 32) of the trough and fall to the lower section of the chamber where cooling coils (42) condense the vapors and the resultant distillate flows out an exit conduit (122). Residue materials are moved by a pusher (47) over the end (26) of the trough into a drain chute (51). During the return of the pusher, an air cylinder (103) is operated to lift the pusher from the bottom of the trough.
    Type: Grant
    Filed: September 16, 1982
    Date of Patent: August 7, 1984
    Assignee: AT&T Technologies, Inc.
    Inventor: Darrel R. Colwell
  • Patent number: 4430226
    Abstract: A water treatment cartridge and method for producing ultrapure water is described. The cartridge comprises a container having therein a particulate admixture of activated carbon and mixed bed ion exchange resins. A source of water, preferably pretreated, is passed through the container, preferably following treatment by one or more cartridges containing mixed bed ion exchange resins. The carbon in the admixed cartridge removes residual organic contamination from the water and the resins remove ionic contamination from the carbon, without re-introducing organic material to the water.
    Type: Grant
    Filed: March 9, 1981
    Date of Patent: February 7, 1984
    Assignee: Millipore Corporation
    Inventors: Ramesh S. Hegde, Gary C. Ganzi
  • Patent number: 4427495
    Abstract: Apparatus and a method for upgrading low pressure steam or brine, such as from a geothermal well, to prepare the steam or brine for any one of a number of uses, such as for conversion to pure, high pressure, high temperature steam for driving turbines. The system operates in a degasification phase in which a small amount of superheated steam is applied to the brine to scrub the same to cause the removal of concentrated gases therefrom. The degasified product is then pumped to a high pressure, heated countercurrently, and directed through a demineralized phase to remove the salts and solids in a liquid phase and convert the bulk of the water into pure, high pressure saturated steam. The steam output from the demineralizing phase can then be used to produce useful work, such as driving a turbine. In addition to forming saturated steam from geothermal brine, the system can be used to form pure saturated steam from impure water from any suitable source.
    Type: Grant
    Filed: July 2, 1982
    Date of Patent: January 24, 1984
    Inventor: Kenneth J. Masero
  • Patent number: 4420373
    Abstract: A mechanical energy conversion method and system for the restoration of dissipated heat energy, contained in natural or artificial water bodies at or near ambient temperatures, to industrial process heat, mainly in the form of steam up to 200.degree.-400.degree. C. The sensible heat contained in a water body is concentrated as latent heat in low pressure water vapor which is thermo-compressed by steam ejection to an intermediate pressure level, wherefrom mechanical compression takes over, generating highly superheated output steam. The ejecting steam is not generated in a boiler, but is continuously regenerated by the compressor and routed back for repeated ejection. The compressor is driven by a heat engine whose reject heat is collected and upgraded as well. The output of heat energy is essentially equal to the sun of the heating value of the fuel consumed and the intake of latent heat and amounts thus to substantially more than the heating value of the fuel alone.
    Type: Grant
    Filed: August 3, 1981
    Date of Patent: December 13, 1983
    Inventor: Dan Egosi
  • Patent number: 4420374
    Abstract: Water degasification and distillation apparatus having a container for water to be degasified and distilled, a relatively small boiler adjoining said container and having a first conduit extending into the container so that a selected water level in the container will fill said boiler to a selected height, a condenser within the container and immersed in the water contained therein, a second conduit extending from the space above the water in said boiler to the inlet of the condenser, an outlet on the condenser extending through a container wall for discharging degasified and distilled water and heating means in said boiler for heating the water therein at a rate greater than the capacity of the second conduit to handle the steam generated in the boiler.
    Type: Grant
    Filed: June 3, 1981
    Date of Patent: December 13, 1983
    Inventor: John C. Ellis, Jr.
  • Patent number: 4417951
    Abstract: An apparatus for the distilling and evaporating of sea water so to produce pure fresh water on a large production basis; the apparatus including an evaporator having a baffle system of novel design therein so as to separate evaporated steam from non-evaporated water drops, a duct for conveying the evaporated steam to a condenser and a pure water supply tank; the evaporator being supplied by sea water.
    Type: Grant
    Filed: November 3, 1980
    Date of Patent: November 29, 1983
    Inventors: Jovo Stanisic, George Spector
  • Patent number: 4389226
    Abstract: A flow-promoting device in combination with a heated box tray open at the top in a reaction and degasification column in which a viscous or highly viscous liquid is flowing from an inlet end to an outlet end of the tray and in which a heating tube register is located to be completely covered by the liquid. The tube register includes a plurality of heating tubes spaced from each other, and the flow-promoting device has a bottom heating unit for the box tray positioned outside and along the bottom of the tray, a siphon plate mounted on the tray at a liquid inlet end of the tray and closely in front of the tube register, with the siphon plate having a bottom end extending to the underside of the tube register, and a weir positioned at the liquid outlet end of the box tray. The weir has a top edge extending at least to the topside of the tube register, and the spacing of the weir from the tube register is larger than the spacing of the siphon plate at the inlet end from the tube register.
    Type: Grant
    Filed: October 30, 1981
    Date of Patent: June 21, 1983
    Assignee: Chemische Werke Huls Aktiengesellschaft
    Inventors: Eckhard Moller, Horst-Dieter Bures, Karl-Heinz Magosch, Bernt Kesper, Edgar Muschelknautz, Roland Vogelsgesang
  • Patent number: 4373996
    Abstract: An apparatus for producing fresh water from sea water in which a vertical accumulator utilizes the sensible heat of sea water so as to evaporate said sea water to a temperature above 100.degree. C. under pressure, a heat-exchanger connecting between the upper and lower portions of said accumulator causes a high temperature liquid to effect heat-exchange with sea water to be evaporated, a fresh sea water feed line connected to the lower portion of said accumulator adjusts the pressure within the accumulator and an evaporator receives higher temperature sea water. The accumulator accumulates heat in such a manner that the upper portion of said accumulator holds higher temperature sea water and the lower portion of the accumulator holds lower temperature sea water so that when heat is accumulated, the amount of said higher temperature sea water increases and when heat is radiated, the amount of higher temperature decreases whereby sea water evaporates at all times.
    Type: Grant
    Filed: March 4, 1981
    Date of Patent: February 15, 1983
    Inventor: Saburo Maruko
  • Patent number: 4370236
    Abstract: A hydrocarbon stream containing particulate and water-soluble compound is purified by admixture therewith of an aqueous solution followed by electrostatic precipitation of the aqueous and particulate phases from the hydrocarbon phase. The aqueous phase is separated from the particulate phase and recycled. Preferably, the aqueous phase is fractionated recovering methanol overhead and recycling a portion of the kettle product containing primarily water and not more than 20 volume percent ethylene glycol.
    Type: Grant
    Filed: December 16, 1980
    Date of Patent: January 25, 1983
    Assignee: Phillips Petroleum Company
    Inventor: Robert C. Ferguson
  • Patent number: 4350570
    Abstract: A method of desalinating water resides in evaporating water from an aqueous salt solution upon contact of the latter with air, the water vapor being subsequently retrieved by condensing. The evaporation of water from the aqueous salt solution through contact thereof with the air is conducted by using two air flows, that is, primary and secondary flows. The primary air flow is supplied to a cooling zone, while the secondary air flow and the aqueous salt solution are delivered to an evaporation zone wherein the secondary flow is moistened by the water evaporating from the aqueous salt solution by virture of the psychrometric temperature difference until the moisture content in the secondary air flow is increased, as compared with the initial moisture content therein, by from 3.5 to 116 g/kg. During the course of absorbing the moisture, the secondary air flow acts to cool the primary air flow passing through the cooling zone.
    Type: Grant
    Filed: May 17, 1981
    Date of Patent: September 21, 1982
    Inventors: Valery S. Maisotsenko, Alexandr B. Tsimerman, Mikhail G. Zexer
  • Patent number: 4344826
    Abstract: The waste water output of an RO unit in a distillation system is conveyed to a still's condenser cooling coil to minimize water requirements of the system. A portion of the heated water fron the condenser, in one embodiment, is circulated to the RO unit inlet, where a temperature mixing valve maintains an optimum temperature for the RO inlet water by mixing feed water and condenser output water in the desired proportions.
    Type: Grant
    Filed: June 20, 1980
    Date of Patent: August 17, 1982
    Assignee: Vaponics, Inc.
    Inventor: Verity C. Smith
  • Patent number: 4343683
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: May 7, 1980
    Date of Patent: August 10, 1982
    Inventor: Richard E. Diggs
  • Patent number: 4342624
    Abstract: A liquid containing a solvent to be evaporated is fed to a concentration chamber which is fluidly connected to an evaporation chamber maintained at a reduced pressure. A vapor compression means withdraws solvent vapor from the evaporation chamber, compresses the vapor and forces the compressed vapor to a liquification chamber. Regulator means responsive to the density of the liquid remaining within the concentration chamber will regulate the rate of solvent evaporation to provide a concentrate suitable for recycling.A method of operating the still of this invention utilizes the technique of increasing the compressor capacity until the compressor begins to surge and then reducing the capacity a fixed amount to provide the desired efficiency.
    Type: Grant
    Filed: August 7, 1981
    Date of Patent: August 3, 1982
    Assignee: Eaton Corporation
    Inventors: Richard Chute, Ralph P. Horan
  • Patent number: 4341599
    Abstract: Apparatus usable to heat fluid comprises:(a) a steam vessel having an inlet for water and an outlet for steam,(b) heating means associated with the vessel to heat water received therein and produce steam, and(c) a condenser connected with the vessel outlet to receive steam, the condenser adapted to extend in heat transfer relation with the fluid to heat that fluid in response to condensation of steam in said condenser, the condenser having a condensate outlet, and(d) other means to remove solid particles from the vessel.
    Type: Grant
    Filed: October 24, 1980
    Date of Patent: July 27, 1982
    Inventors: W. Keith R. Watson, Knoxie C. DeLise
  • Patent number: 4339307
    Abstract: The apparatus includes a housing enclosing a boiler in the lower portion and a water-filled condenser in the upper portion with an insulated partition between them. The entry of boiler feed water is controlled by a float valve in the boiler, and steam from the boiler is conveyed through the partition and thus through a condenser coil substantially immersed in the water in the condenser.
    Type: Grant
    Filed: March 20, 1979
    Date of Patent: July 13, 1982
    Inventor: John C. Ellis, Jr.
  • Patent number: 4332643
    Abstract: A method of removing water from a mixture of glycol and water comprises introducing a feed mixture of glycol and water to a distillation column, and collecting a first concentrated glycol-water liquid as still bottoms. The first concentrated liquid is then conveyed to a reboiler where a portion of that liquid is vaporized to form a reboiler vapor and a second concentrated glycol-water liquid. The reboiler vapor is returned to the still for intimate contact with the feed mixture of glycol and water in the distillation column. The second concentrated liquid is then conveyed to a water exhauster at a temperature and pressure such that an equilibrium vapor of said second concentrated liquid, at said conditions, has a glycol/water weight ratio of at least 0.54. At this condition, a portion of the second concentrated glycol-water liquid is vaporized in the water exhauster to form a third concentrated glycol-water liquid and an equilibrium vapor in contact with the third concentrated liquid.
    Type: Grant
    Filed: May 30, 1978
    Date of Patent: June 1, 1982
    Inventor: Laurence S. Reid
  • Patent number: 4323431
    Abstract: A high melting, high boiling organic compound is easily and stably purified by continuously supplying the molten organic compound to a rectification zone under a subatmospheric pressure and continuously distilling off and recovering vapors from the top of the rectification zone, while continuously withdrawing bottoms containing higher boiling impurities and/or involatile impurities than the desired compound from a reboiling zone at the bottom of the rectification zone to the outside of rectification system by means of a barometric leg, without any pretreatment of removing lower boiling impurities therefrom before the rectification, and without disturbing a pressure balance in the rectification system.
    Type: Grant
    Filed: August 4, 1980
    Date of Patent: April 6, 1982
    Assignee: Sumitomo Chemical Company Limited
    Inventors: Masatoshi Takahashi, Norio Kotera, Masatoshi Uegaki, Takashi Miyaoka, Yuzo Maegawa
  • Patent number: 4316774
    Abstract: A urine-water recovery system is described which provides efficient potable water recovery from waste liquids. The design allows use over extended durations such as encountered in space flights. The system has advantages such as low power consumption, compactness, and gravity insensitive operation. The system comprises a vacuum distillation system combining a hollow fiber polysulfone membrane evaporator with a thermoelectric heat pump and condenser. With the system of the present invention, water purified from urine can be produced at a rate of more than 0.5 kg/hr at a total system energy of less than 400 w-hr/kg.
    Type: Grant
    Filed: July 5, 1979
    Date of Patent: February 23, 1982
    Assignee: United Technologies Corporation
    Inventor: Raymond B. Trusch
  • Patent number: 4314891
    Abstract: Reconcentration of moist glycol, which has been used to dry natural gas, by heating the moist glycol with flue gas from a reboiler and by thereafter stripping water from the moist glycol with the dried flue gas or with a hydrocarbon gas by-product of the natural gas being dried.
    Type: Grant
    Filed: November 25, 1980
    Date of Patent: February 9, 1982
    Assignee: Davy International AG
    Inventor: Walter Knobel
  • Patent number: 4309254
    Abstract: A process for the production of alcohol from a fermented feed wherein insoluble organic matter is separated prior to entry into a first distillation column. The insoluble organic matter is dried under pressure to produce dried distillers grain and wherein excess vapor is removed from the drying zone to provide heat to the distillation system. The present process also includes removing excess water vapor from the evaporation zone, obtained from supplemental heating supplied by the overhead from said first distillation column, compressing said water vapor, and recycling it to the distillation columns and the evaporation zone.
    Type: Grant
    Filed: April 17, 1980
    Date of Patent: January 5, 1982
    Assignee: Stone and Webster Eng. Corp.
    Inventors: Rodney A. Dahlstrom, Jacob N. Rubin
  • Patent number: 4279703
    Abstract: The fouling of ammonia stills which results from the clogging, particularly of the lower plates of the stills, with sludge and precipitates is eliminated by use of combined apparatus in which a calcium compound precipitation step followed by a clarification step prior to initiation of actual distillation can be effected.
    Type: Grant
    Filed: December 3, 1979
    Date of Patent: July 21, 1981
    Assignee: Bethlehem Steel Corporation
    Inventors: Daniel Kwasnoski, Charles J. Sterner, Russel J. Horst, Kenneth R. Burcaw
  • Patent number: 4273620
    Abstract: Reconcentration of moist glycol, which has been used to dry natural gas, by heating the moist glycol with flue gas from a reboiler and by thereafter stripping water from the moist glycol with the dried flue gas or with a hydrocarbon gas by-product of the natural gas being dried.
    Type: Grant
    Filed: June 26, 1978
    Date of Patent: June 16, 1981
    Assignee: Davy International AG
    Inventor: Walter Knobel
  • Patent number: 4267021
    Abstract: A single effect solar distillation apparatus of the tilted or inclined floor type is disclosed which absorbs solar energy to evaporate a liquid distilland more efficiently. The present distillation apparatus is especially useful for desalination of sea water and includes a number of structural improvements to utilize the absorbed solar energy in a basically more efficient manner than previous still designs of this type. The distilland is evaporated in the present solar distillation apparatus substantially without turbulence especially at the evaporating surfaces to avoid certain heat transfer losses previously encountered during distillation. This basically novel mode of solar distillation is achieved with a particular relationship between the evaporating and the condensing surfaces in the apparatus which further cooperate with an improved structure where said evaporation takes place.
    Type: Grant
    Filed: February 27, 1978
    Date of Patent: May 12, 1981
    Inventors: Dimitrios M. Speros, Philip C. Speros
  • Patent number: 4261796
    Abstract: There is disclosed a water distiller, primarily for producing water for human consumption which includes a boiler with an electric heater, a fractional distillation tower extending about two or more feet above the boiler, a gas trap at the top of the tower, and a steam conduit exiting from the tower below the gas trap and leading into a condensation tube with a water-cooled jacket. The boiler and tower are of uniform cross-section to facilitate cleaning by running a swab through this tube. An unprocessed water inlet is located in the bottom of the water jacket, and at the top of the water jacket is an exit orifice for preheated input water. A conduit for preheated input water leads to the bottom-most part of the boiler of the distiller. An overflow conduit is provided which is directly opposite the preheated water inlet; the highest point of the overflow conduit serves to automatically regulate the depth and volume of water in the boiler.
    Type: Grant
    Filed: June 12, 1978
    Date of Patent: April 14, 1981
    Inventor: Kenneth D. Lemoine
  • Patent number: 4260461
    Abstract: A vapor compression distillation apparatus and method are provided wherein scaling tendencies are eliminated. The raw feedwater has acid added to it in an amount sufficient to convert the carbonates and/or bicarbonates therein to carbon dioxide. The heated acidified feedwater is then deaerated to remove the carbon dioxide and other non-condensible gases. The deaerated water flows to the evaporator through a line having a valve therein controlled by the liquid level in the deaerator to maintain such level constant even though the tube side of the evaporator is being operated at a pressure less than that of the deaerator. This permits the evaporation to take place under a partial vacuum and at a boiling temperature of less than 212.degree. F. even though the deaerator is operated at atmospheric pressure. Vent steam from the evaporator is added to the deaerator to further preheat the feedwater, and as a sparging or stripping agent to aid in the elimination of carbon dioxide and other non-condensible gases.
    Type: Grant
    Filed: December 21, 1978
    Date of Patent: April 7, 1981
    Inventor: John E. Pottharst, Jr.
  • Patent number: 4252616
    Abstract: A water distillation apparatus having a feed water pre-heater, an evaporator tank, and a storage tank. The storage tank has an upper surface and depending walls, the pre-heater and evaporator tank being on the upper surface, and extending, with the other components, to approximately the same height, all components being within the periphery of the walls. A mixing vessel including a level controlling overflow pipe receives water from the pre-heater, and a short, straight, large diameter conduit connects the mixing vessel and evaporator tank. The mixing vessel contains a valve to drain it and the evaporator tank. The pre-heater comprises two dished elements in facing relation, with a divider plate between them, the elements being joined at their peripheries. A serpentine path is provided in each of the two spaces of the pre-heater, formed by a pair of L-shaped separators extending linearly from one end of the space to a point spaced from the other end.
    Type: Grant
    Filed: March 3, 1978
    Date of Patent: February 24, 1981
    Inventor: Howard Glazer
  • Patent number: 4247371
    Abstract: Water containing dissolved compounds is preheated, and is then pressurized in stages of water pressure, while receiving a quantum of steam. Scale-forming compounds in the water are thermally precipitated, and clarified post-thermal water is formed. This is flash vaporized in stages corresponding to the stages of water pressure, and the flashed vapors are compressed to form each said quantum of steam. Alternately, the flashed vapors themselves comprise each said quantum of steam, by being induced into the water as it flows through an eductor means. Flash-cooled, post-thermal water, substantially devoid of scale-forming compounds, is employed as such, or more generally is evaporated to form fresh water and an end concentrate of dissolved compounds.
    Type: Grant
    Filed: December 20, 1978
    Date of Patent: January 27, 1981
    Inventor: Paul S. Roller
  • Patent number: 4247369
    Abstract: A compact integral apparatus is provided for the continuous distillation of water. The apparatus comprises an upright cylindrical boiling vessel communicating at an upper portion thereof with a vapor condensation tube which leads into a water cooling tube disposed within a reservoir vessel. Water is supplied to said reservoir vessel through a float-controlled valve adapted to maintain a substantially constant amount of water in said reservoir vessel at a height sufficient to immerse said water cooling tube and thereby receive heat therefrom. Water to be distilled flows by gravity from said reservoir vessel to said boiling vessel. The component parts are structurally interconnected to facilitate facile mounting of the apparatus on a support structure.
    Type: Grant
    Filed: June 11, 1979
    Date of Patent: January 27, 1981
    Inventor: Roy E. Bean
  • Patent number: 4239601
    Abstract: There is disclosed a water distiller, primarily for producing water for human consumption which includes a boiler, a distillation tower extending about two or more feet above the boiler, and a steam conduit exiting from near the top of the tower leading into a helically grooved condensation tube with a water-cooled jacket. The boiler and tower are of uniform cross-section to facilitate cleaning. The water jacket has a water inlet located in the bottom and an exit orifice for preheated input water at the top. A conduit from the orifice leads to an evaporator for volatile impurities on top of the tower, and a conduit for preheated input water leads to the bottommost part of the boiler from the evaporator. An overflow conduit with an intermittent siphon is provided connected to the bottom of the boiler; the highest and lowest points of the siphon serve to automatically regulate the maximum and minimum depths of water in the boiler.
    Type: Grant
    Filed: November 27, 1979
    Date of Patent: December 16, 1980
    Inventor: Kenneth D. Lemoine
  • Patent number: 4235680
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: January 12, 1978
    Date of Patent: November 25, 1980
    Inventor: Richard E. Diggs
  • Patent number: 4235677
    Abstract: An apparatus for the continuous production of high-purity water includes a distillation flask, a carboy and a condenser unit, all of borosilicate glass. A respective filter, preferably in the form of a polytetrafluoroethylene sheet, is provided between the ambient atmosphere and the interiors of the flask, the carboy and the condenser unit to remove airborne bacteria and dust particles. An inlet valve is provided for feeding water to be purified into the flask, all water-contacting parts of this valve being of polytetrafluoroethylene. The open parts are interconnected with flexible, polytetrafluoroethylene tubing. A two-way, stopcock allows high-purity water to be removed from the carboy. The flask is provided with a glass overflow trap. In one variant, the water is fed into the flask via members between the trap and the flask.
    Type: Grant
    Filed: February 23, 1978
    Date of Patent: November 25, 1980
    Assignee: The United States of America as represented by the Department of Health, Education and Welfare
    Inventor: Narbik A. Karamian
  • Patent number: 4235679
    Abstract: A solar still into which cold seawater is fed by means of a pipe perforated long its horizontal length. The seawater then flows down an inclined plane through a black wick material placed on top of a double or parallel plate base which serves as a heat exchanger that transfers heat from a working fluid to the seawater. The seawater in turn evaporates while flowing down the wick and the vapor condenses as pure water on the upper inner surface of the still transferring heat back to the working fluid which is being circulated through the upper cover of the still. The vapor condensate is collected as it flows down the inclined upper inner surface and in turn is drawn off; the working fluid is recirculated to continuously heat and then cool the distillate.
    Type: Grant
    Filed: January 15, 1979
    Date of Patent: November 25, 1980
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: Brian E. Swaidan