Vacuum Patents (Class 202/205)
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Patent number: 8444830Abstract: A desalination process including heating brine in a preheating chamber and transferring the brine to a rotary kiln to be sprayed against the wall structure of the rotary kiln to boil to steam and a residue of salt/impurities, the exiting steam being pressurized in a compressor and passed to an externally powered heater to be heated and then fed to a hollow wall structure of the rotating kiln in which the steam condenses to pure water to be transferred to the preheating chamber to preheat the incoming brine, the rotating kiln being arranged to rotate past a scraper to remove salt/impurities from the wall structure for collection at the base of the kiln.Type: GrantFiled: June 17, 2008Date of Patent: May 21, 2013Inventor: Garth Davey
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Patent number: 8361277Abstract: An evaporator is provided for evaporation of liquid from a solution or liquid mixtures, together with methods of operation of the evaporator. The evaporator comprises a chamber (1); a liquid reservoir (3) for holding a heat transfer liquid exposed to the interior of the chamber; a support (6) for supporting a container (8) in the chamber, such that the liquid sample in the container is exposed to a fluid path (15) for connection to a condenser (16), the fluid path being separated from the chamber interior, and at least a portion of the container is closely thermally coupled to the chamber interior; and means (4) for heating the heat transfer liquid in the reservoir to create heat transfer liquid vapor, which in use condenses and releases latent heat of vaporization to the liquid sample in the container. As the temperature of the sample is dependent on the saturated vapor temperature of the liquid in the reservoir, the temperature of the samples is reliably limited, thereby avoiding overheating.Type: GrantFiled: March 14, 2007Date of Patent: January 29, 2013Assignee: Genevac LimitedInventor: Donald Roger Lee-Smith
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Patent number: 8343316Abstract: A vacuum dehydrator for processing an oil containing entrained contaminants such as water, air, and particulates comprises a tower enclosing upper and lower chambers. A random packing is contained in the upper chamber. The oil is preheated to a temperature above the boiling point of water and is introduced into the upper chamber for downward flow through the random packing into the lower chamber. Entrained air and water is retained as water vapor in the upper chamber, and particulates are retained in the random packing. Heated ambient air is introduced into the lower chamber for upward flow through the random packing into the upper chamber, and the upper chamber is cooled to condense the water vapor. Oil and condensed water are pumped respectively from the lower and upper chambers.Type: GrantFiled: November 10, 2009Date of Patent: January 1, 2013Assignee: Siemens Industry, Inc.Inventors: Mortimer Daniel Williams, John G. Donnelly, Eric M. Laliberte, J. Rafael Lazo, Juan Alejandro Segrelles Sacristan, Anselmo Garcia Gracia
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Patent number: 8337672Abstract: The invention relates to the oil processing industry and can be used for producing vacuum in a vacuum petroleum distillation column. The inventive method involves pumping out a vapor-gas medium from the column by of a gas-gas ejector in such a way that a vapor-gas mixture is formed at the entry thereof and supplying said mixture to a condenser for producing a gas mixture and a vapor phase condensate. The gas mixture is supplied from the condenser to a liquid-gas jet apparatus and the condensate is delivered to an additional separator. A hydrocarbon-containing condensate is removed from the additional separator for the intended use thereof and a water-containing condensate is fed to a steam generator for producing steam by supplying heat of a hot distillate evacuated from the vacuum column. The thus obtained steam is used in the gas-gas ejector as a high-pressure gas.Type: GrantFiled: November 6, 2008Date of Patent: December 25, 2012Inventor: Valery Grigorievich Tsegelsky
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Patent number: 8308913Abstract: Disclosed is an apparatus for recovering an acrylic acid from a mixture containing acrylic acid, acrylic acid dimer and impurities with high boiling point, including: an acrylic acid recovering device that comprises an acrylic acid distillation unit being present within an acrylic acid dimer pyrolysis tank, and is operated under reduced pressure; a separation column for removing impurities with high boiling point from the mixture which is introduced into the acrylic acid recovering device; and a line for introducing the mixture into the acrylic acid recovering device.Type: GrantFiled: September 23, 2009Date of Patent: November 13, 2012Assignee: LG Chem, Ltd.Inventors: Seong Pil Kang, Seok Kwan Choi, Kyoung Su Ha, Jun Seok Ko, Boo Gon Woo, Young Bae Kim
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Patent number: 8226799Abstract: An embodiment of a distillation system is disclosed having an influent column with an influent column first end and an influent column second end and having therein, a gas deflector. The influent column may contain at least an influent liquid and vapor from the influent liquid. The influent column first end may be in fluid communication with an influent liquid source. A distillation system is disclosed as having at least one effluent column having an effluent column first end and an effluent column second end and further comprising a condensation chamber adjacent the effluent second end. The effluent column may be positioned within the influent column and may contain at least an effluent liquid and vapor. A primary vacuum source may be in fluid communication with an influent column and positioned at an influent second end. A blower may be provided and connected to the condensation chamber. The influent column may have at least one vertically positioned influent conduit.Type: GrantFiled: June 11, 2009Date of Patent: July 24, 2012Inventor: Anthony D. Young
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Patent number: 8206557Abstract: In one embodiment, an apparatus includes a housing that has at least an inlet and an outlet. The housing is configured to receive a volume of fluid via the inlet. The volume of fluid is in a substantially liquid state and at least a portion of the volume of fluid includes a dissolved impurity. The apparatus also includes a heat-transfer element coupled to an interior volume of the housing. The heat-transfer element includes a surface, at least a portion of which is disposed at an angle with respect to a horizontal plane. The volume of fluid includes a surface parallel to the horizontal plane. The apparatus further includes a compression component configured to compress at least a portion of fluid boiled from the volume of fluid.Type: GrantFiled: November 7, 2007Date of Patent: June 26, 2012Assignee: Hydrologic Industries, Inc.Inventors: Francis P. Burke, Kenneth J. Horne, David B. Taylor, Stephen R. Topaz
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Patent number: 8206558Abstract: A processing apparatus (1) for the processing of process or industrial wastewaters is provided. The processing apparatus (1) has an evaporator (4) in which a tube bundle heat exchanger is provided, whose pure distillate side is connected to a separating apparatus for separating the distillate from floating organic phase or similar free liquid constituents. This separating apparatus is intended to collect the floating organic phase from the condensate, in order that this phase can be sucked back into the evaporator (4). In addition, the vapor mixture is conducted from the separating apparatus (8) to a recuperator (3) and cooled to such an extent that the water, the volatile solvents and the organic material dissolved in the vapor can be condensed and discharged separately or can be sucked back into the evaporator (4). This allows significantly better distillate qualities to be achieved.Type: GrantFiled: February 3, 2007Date of Patent: June 26, 2012Assignee: H20 GmbHInventors: Matthias Fickenscher, Daniel Ladenberger
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Patent number: 8202402Abstract: The present invention relates to systems and related methods of water purification by distillation that will operate in a self-contained mode using a passive heat source, such as, without limitation, solar heat, air conditioning waste heat, or waste heat from the exhaust or cooling systems of an internal combustion engine, which may be used to desalinate sea water, saline water, or saline water containing contaminants. The present invention may also be used to distil sewage water, creek water, swamp water or water containing contaminants or used to cleanse or purify water contaminated with mud, chemicals, minerals, or bacteria in a local environment.Type: GrantFiled: November 29, 2006Date of Patent: June 19, 2012Assignee: Hse Hittt Solar Enerji Anonim SirkertiInventor: Rahmi Oguz Capan
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Patent number: 8202401Abstract: In one embodiment, a method includes moving a first volume of fluid from a region above a heat-transfer element to a region below the heat-transfer element after the first volume of fluid is boiled from a second volume of fluid within the region above the heat-transfer element. The first volume of fluid including an impurity concentration lower than an impurity concentration of the second volume of fluid. The region below the heat-transfer element has a temperature higher than a temperature of the region above the heat-transfer element. The method also includes transferring latent heat from the first volume of fluid to a third volume of fluid on a top surface of the heat transfer element. The latent heat is released when the first volume of fluid condenses.Type: GrantFiled: November 7, 2007Date of Patent: June 19, 2012Assignee: Hydrologic Industries, Inc.Inventors: David B. Taylor, Stephen R. Topaz
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Patent number: 8202403Abstract: A distillation tower for use in a petrochemical or petroleum operation effects liquid and vapor separation by using centrifugal force applied to the feed introduced into a ring from a tangential inlet. The feed is separated into a liquid component that flows into the bottoms section of the tower and a vapor component that flows upwardly through the core of the ring to a wash zone in the tower. De-entrainment devices are provided in the core so that the vapor swirling upwardly impacts the devices and any remaining entrained liquid is separated from the vapor. As a result, overflash with decreased resid can be collected from the wash zone and used as feed suitable for a fluid catalytic cracking operation, for example.Type: GrantFiled: February 19, 2008Date of Patent: June 19, 2012Assignee: ExxonMobil Research & Engineering CompanyInventors: Theodore Sideropoulos, Arun K. Sharma
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Publication number: 20120085634Abstract: Described herein is a solution for use in cleaning articles comprising, a dry cleaning agent, wherein the dry cleaning agent comprises a siloxane solvent, a hydrocarbon solvent or a combination thereof, and an enhancer, which raises a KBV value of the solution. The enhancer can be soluble in the dry cleaning agent and water. Also described herein is a dry cleaning system that utilizes the solution, as well as a purification system for purifying the solution.Type: ApplicationFiled: October 7, 2011Publication date: April 12, 2012Applicant: GREENEARTH CLEANING, LLCInventors: James E. Douglas, Wolf-dieter R. Berndt
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Patent number: 8137504Abstract: A system and method for preparation of meat flavorants, and flavorants, having increased flavor and aromatic intensity and which more closely resemble the natural flavor and aroma of cooked meat. Preheated edible, food grade oils and fats are exposed to temperatures between 290° C. and 475° C. under vacuum, in the presence of oxygen. The developing flavor vapors are immediately and completely removed from the heated oils and fats. The mixture of air-purge/flavor-vapor is immediately carried away from the heat transfer surface of the edible oil or fat. An evaporator, preferably a spinning disc, spinning band or thin film evaporator, without a condenser is used as process equipment. The air-purged flavor-vapors are diffused and absorbed in an absorption device into suitable food-grade liquids.Type: GrantFiled: July 28, 2011Date of Patent: March 20, 2012Assignee: Flavor & Food Ingredients, Inc.Inventors: Jurgen D. Scheide, John M. Stefanicha
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Patent number: 8092646Abstract: A vaporization apparatus and related vaporization method is provided that relies on thermocapillary convection. The apparatus of a thermocapillary evaporator has three sections: an evaporation section, a displacement section, and a storage system for storing the liquid to be evaporated. The evaporation section is operable to distribute thermal energy substantially along the entire liquid-gas interface. The method of the present invention includes providing a thermocapillary evaporator. Advantageously, the present invention provides substantial evaporation from relatively low temperature heat sources, compared to conventional evaporators.Type: GrantFiled: August 31, 2006Date of Patent: January 10, 2012Inventor: Ward Charles Albert
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Patent number: 8080138Abstract: This invention describes a low temperature, self-sustainable desalination process operated under natural vacuum conditions created and maintained by barometric pressure head.Type: GrantFiled: December 12, 2007Date of Patent: December 20, 2011Assignee: Arrowhead Center, Inc.Inventors: Nagamany Nirmalakhandan, Veera Gnaneswar Gude
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Patent number: 8034214Abstract: A reciprocating film type evaporator for solvents and other chemicals which eliminates the need for a large powerful motor, and other associated equipment such as rotary gaskets, by using reciprocation, versus 360 degree rotation.Type: GrantFiled: April 12, 2007Date of Patent: October 11, 2011Assignee: Tracera LLCInventors: Collin McKinney, Rob Musser
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Patent number: 8034217Abstract: A liquid condensation system heats a liquid raw material under a decompressed circumstance and evaporates a volatile component from a liquid surface to condense the liquid raw material. Therefore, the liquid condensation system includes: liquid condensers, each of which condenses the liquid raw material; a vacuum pump that is in communication with the liquid condensers; and a warm water circulation system as a heating source that heats the liquid raw material in the liquid condensers. The volatile component evaporated in the liquid condensers is led to the outside of the liquid condensers through vapor lines. The condensed liquid that is not evaporated in the liquid condensers is led to the outside of the liquid condensers through condensed-liquid lines. Condensed-liquid-line adjusting valves are interposed on the condensed-liquid lines, and heaters are attached to the condensed-liquid lines. A control unit controls the heaters and the condensed-liquid-line adjusting valves.Type: GrantFiled: February 7, 2008Date of Patent: October 11, 2011Assignee: Hitachi Plant Technologies, Ltd.Inventors: Yuzuru Ito, Yoshishige Endo, Hidekazu Tsudome, Fumiaki Numajiri
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Patent number: 8021519Abstract: A system for distilling sea or brackish water includes a feed water arrangement for supplying feed water from a feed water source to one or more flashing stages. Each flashing stage has a water flash evaporator for vaporizing at least part of the water therein, and a condenser for receiving the vapour and converting at least a part of the vapour into distilled water. A heat storage arrangement provided with a heat generating source for storing heat energy is used to heat a fluid medium flowing through it. A heat exchange arrangement receives the hot fluid medium and transfers heat to a stream of vapour flowing under pressure from each flashing stage. The vapour leaving the heat exchange arrangement being at a raised temperature is arranged to be condensed into water at the condenser and to transfer some of its latent heat to the evaporator.Type: GrantFiled: September 14, 2005Date of Patent: September 20, 2011Inventor: Gregory Mark Paxton
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Patent number: 7998317Abstract: A glycerol preparation method for preparation of medical grade glycerol from a by-product of a bio-diesel process includes a first stage phosphoric acid chemical reaction process and a posterior by-product centrifugal separation process to have the phosphoric acid chemical reaction by-product be separated into free fatty acid, potassium phosphoric acid, and a crude glycerol and methanol mixture. The crude glycerol and methanol mixture is further processed through a first step of thin film evaporation process where methanol is reclaimed, a second step of thin film evaporation process where the mixture is dehydrated, a third step of molecular distillation process where an industrial grade glycerol of purity over 95% is extracted, and a fourth step of molecular distillation process where a medical grade glycerol of purity in exceed of 99.75% that meets USP/BP standards is extracted.Type: GrantFiled: September 5, 2008Date of Patent: August 16, 2011Inventor: Wei Ming Chang
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Patent number: 7988819Abstract: A system and method for preparation of meat flavorants, and flavorants, having increased flavor and aromatic intensity and which more closely resemble the natural flavor and aroma of cooked meat. Preheated edible, food grade oils and fats are exposed to temperatures between 290° C. and 475° C. under vacuum, in the presence of oxygen. The developing flavor vapors are immediately and completely removed from the heated oils and fats. The mixture of air-purge/flavor-vapor is immediately carried away from the heat transfer surface of the edible oil or fat. An evaporator, preferably a spinning disc, spinning band or thin film evaporator, without a condenser is used as process equipment. The air-purged flavor-vapors are diffused and absorbed in an absorption device into suitable food-grade liquids.Type: GrantFiled: January 30, 2008Date of Patent: August 2, 2011Assignee: Flavor & Food Ingredients, Inc.Inventors: Jurgen D. Scheide, John M. Stefanicha
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Patent number: 7981253Abstract: An improved de-entrainment device for use in distillation towers, especially vacuum distillation towers used for fractionating petroleum atmospheric resids is in the form of a baffle which is to be located in the portion of the tower below the feed zone and at the top of the flash zone. The baffle is in the form of an apertured plate above the stripping zone and in its preferred form comprises number of radial fins or blades, resembling a static fan with openings between the fins to permit vapors from the lower portions of the tower to pass upwards through the baffle with a minimal pressure drop. The fins of the baffle are preferably oriented at an angle between 30° and 60° away from the incoming feed so that the incoming feed stream skims over the top edges of the fins.Type: GrantFiled: January 26, 2007Date of Patent: July 19, 2011Assignee: ExxonMobil Research & Engineering CompanyInventors: Arun K. Sharma, Theodore Sideropoulos, Rutton D. Patel, Brian D. Albert, Alvin U. Chen
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Patent number: 7972445Abstract: The present invention consists of an improved vertical continuous vacuum pan apparatus consisting of eight chambers (2) (instead of four or five) and a storage or buffer tank (27) at the top, within the existing conventional height, characterized in that each chamber has a bottom mounted mechanical circulator housed in an insulated pocket (28) in the vapour space segment (29) of each chamber and not in additional space above the chamber.Type: GrantFiled: September 25, 2006Date of Patent: July 5, 2011Assignee: Spray Engineering Devices LimitedInventors: Jai Parkash Singh, Vipin Kumar Gupta, Saroj Kumar Singh
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Patent number: 7955476Abstract: A multiple application recycling and purification device has a coaxial core that is horizontally oriented, non-rotating, cylindrical distillation chamber. The enhanced, completely coaxial configuration continuously cleans the entire distillation chamber and spreads a thin film of liquid to enhance distillation and positively aid in the removal of remaining contaminants. Through a timed and positioned valve, the device removes and purges lower-temperature contaminants. Timed valves and sensors control all phases of the distillation to provide a coaxially integrated, stand-alone, adaptable, scalable and maintenance free distillation unit that self-monitors, self-cleans and economically functions to produce the pure distilled liquid, e.g., water. This device can be modified to purify any numerous array of liquids and can be scaled to produce any amount of purified liquids for either household, commercial, or industrial applications.Type: GrantFiled: January 18, 2007Date of Patent: June 7, 2011Assignee: Mansur CorporationInventor: Pierre G. Mansur
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Patent number: 7931782Abstract: A method of recovering a liquid medium from a mixture containing the liquid medium, the method including: (a) blowing a first gas into the mixture containing the liquid medium to vaporize the liquid medium, in a first vaporizing means, thereby to form a second gas containing which is a mixture of the first gas and vaporized liquid medium; (b) continuously dropwise feeding the mixture containing the liquid medium into a second vaporizing means and counter-flowingly contacting the mixture containing the liquid medium, with the second gas to vaporize additional liquid medium to form a third gas which is a mixture of the second gas and additional vaporized liquid medium; and (c) feeding the third gas into a condensing means to condense the vaporized liquid medium into a liquid and separate the first gas, which is then blown into the first vaporizing means in step (a).Type: GrantFiled: March 26, 2004Date of Patent: April 26, 2011Assignee: The Institute of Creative Chemistry Co., Ltd.Inventors: Sigeru Torii, Kouichi Miki
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Publication number: 20110031100Abstract: The present invention provides composite membranes for membrane distillation and related methods of manufacture. In particular, there is provided a composite hydrophilic/hydrophobic membrane comprising a hydrophilic polymer layer and a hydrophobic polymer layer comprising fluorinated surface-modifying macromolecules, wherein said composite membrane has a high vapour flux. Also provided herein are methods of manufacturing and optimizing the composite membranes and a membrane distillation system comprising the composite membranes.Type: ApplicationFiled: December 2, 2009Publication date: February 10, 2011Applicant: UNIVERSITY OF OTTAWAInventors: Moh'd Rasool QTAISHAT, Mohamed KHAYET, Takeshi MATSUURA
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Patent number: 7875153Abstract: The invention relates to a method and a device for the purification of an aqueous solution of an organic acid having a boiling point at atmospheric pressure of less than 450° C., which-further has approximately 275 g carboxylate ions/1 or less, preferably 250 g carboxylate ions/1 or less, and preferably less than 1% by weight ionic impurities, calculated on the basis of the total solution. In particular, the invention relates to a method and a device for the continuous purification and concentration, on an industrial scale, of an aqueous solution of an organic acid having a boiling point at atmospheric pressure of less than 450° C. According to the method, this solution is subjected to two or more distillation steps, the first distillation step being carried out at a temperature of from 80° to 150° C. and a pressure of from 50 to 250 mbar, and the second distillation step being carried out at a temperature of from 80° to 200° C. and a pressure of from 0.01 to 50 mbar.Type: GrantFiled: July 19, 2007Date of Patent: January 25, 2011Assignee: Purac Biochem B.V.Inventors: Hendrik Martinus Winkelaar, Jan Van Breugel, Jose Maria Vidal Lancis, Margarita Camprubi Vila
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Publication number: 20110008241Abstract: A catalytically activated vacuum distillation system, several novel component parts of said system, a process for producing carbon based products and novel carbon black that is produced from such a system and process.Type: ApplicationFiled: September 16, 2010Publication date: January 13, 2011Inventors: Michael P. Maskarinec, Bart M. Taylor
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Patent number: 7811420Abstract: A method of and apparatus is disclosed for water desalination including steps of transferring water vapor from salt-water in a vaporization zone 7, via a water vapor transfer zone 12, to a condensation zone 11, and condensing the water vapor into fresh-water. The water vapor transfer zone 12 is maintained substantially free of any gas other than water vapor. Heat is supplied to the vaporization zone 7 and extracted from the condensation zone 11, at relative rates such that there is a net transfer of water from the vaporization zone to the condensation zone. Also disclosed is a method of and apparatus for degassing salt water using at least two degassing chambers 17A, 17B each provided with a valved vent 47 and a valved inlet 21,29,90,91, with a valved pipe circuit 17a, 72-82,85-87, having a pump 71.Type: GrantFiled: August 21, 2006Date of Patent: October 12, 2010Inventor: Sven Olof Sonander
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Patent number: 7770872Abstract: A flow device intended for a two-phase flow processing enclosure of the natural counter-flow type, in which an ascending gaseous flow and a descending liquid flow circulate. The device is formed by an appreciably horizontal tray having openings for the passage of the ascending gaseous flow, and a channel for recovering the descending liquid flow, the channel discharging into a flow orifice. The flow device includes a single guide device extending beneath the tray and connected to the flow orifice in such a way that the liquid flows on its outer wall. Also, a processing enclosure, particularly for processing a hydrocarbonated or aqueous type liquid flow, containing the flow device.Type: GrantFiled: December 20, 2006Date of Patent: August 10, 2010Assignee: Total Raffinage MarketingInventor: Romain Delatour
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Patent number: 7749360Abstract: A vapor based liquid purification system and process utilizes an evaporator for evaporating a liquid into a vapor and a vapor condenser for condensing the vapor into the processed liquid. The vapor condenser has a stator and a rotor, with the rotor disposed for rotation about the stator. The stator and the rotor each have protrusions proximate to an inlet of the vapor condenser. These protrusions cooperate to draw vapor from the evaporator into the vapor condenser. The stator and the rotor each further have at least one axially extending ridge. These ridges cooperate to move a mixture of the vapor and the processed liquid towards at least one drain in the rotor where the processed liquid is communicated to an outlet of the vapor condenser. A multi-level vapor based purification system may also be utilized.Type: GrantFiled: April 5, 2006Date of Patent: July 6, 2010Inventor: Wesley K. Waldron
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Patent number: 7718033Abstract: A one step method and system for producing nanofluids by a particle-source evaporation and deposition of the evaporant into a base fluid. The base fluid such (i.e. ethylene glycol) is placed in a rotating cylindrical drum having an adjustable heater-boat-evaporator and heat exchanger-cooler apparatus. As the drum rotates, a thin liquid layer is formed on the inside surface of the drum. A heater-boat-evaporator having an evaporant material (particle-source) placed within its boat evaporator is adjustably positioned near a portion of the rotating thin liquid layer, the evaporant material being heated thereby evaporating a portion of the evaporant material, the evaporated material absorbed by the liquid film to form nanofluid.Type: GrantFiled: July 12, 2006Date of Patent: May 18, 2010Assignee: The United States of America as represented by the United States Department of EnergyInventors: Milivoje Kostic, Mihajlo Golubovic, John R. Hull, Stephen U. S. Choi
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Patent number: 7670463Abstract: When fresh water is produced from salt water or similar by evaporation of untreated or crude liquid in an evaporation device under partial vacuum and by vapor condensation in a condensation device connected with the vapor outlet of the evaporation device a high degree of evaporation and cost effectiveness can be obtained in that the evaporation device and the condensation device in a disconnected condition, are filled with crude or clean liquid, respectively, and are subsequently exposed to a partial vacuum created by volume enlargement under hermetically sealed conditions and that the evaporation device and the condensation device are not flow-connected with each other until they are under partial vacuum.Type: GrantFiled: December 6, 2003Date of Patent: March 2, 2010Inventor: Kurt Hausmann
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Publication number: 20100012476Abstract: Disclosed is a simplified apparatus for recovering acrylic acid from a mixture containing acrylic acid, acrylic acid dimer and impurities with high boiling point, in a stable and efficient manner. An apparatus for recovering an acrylic acid from a mixture containing acrylic acid, acrylic acid dimer and impurities with high boiling point, which comprises: an acrylic acid recovering device that comprises an acrylic acid distillation unit being present within an acrylic acid dimer pyrolysis tank, and is operated under reduced pressure; and a line for introducing the mixture into the acrylic acid recovering device, wherein decomposition of the acrylic acid dimer is carried out under reduced pressure at a lower part of the acrylic acid recovering device, while the acrylic acid is recovered by distillation under reduced pressure from a top of the acrylic acid recovering device.Type: ApplicationFiled: September 23, 2009Publication date: January 21, 2010Inventors: Seong Pil KANG, Seok Kwan Choi, Kyoung Su Ha, Jun Seok Ko, Boo Gon Woo, Young Bae Kim
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Patent number: 7641771Abstract: A system for generating purified water from polluted water which includes an entry chamber communicating with a source of polluted water, a pump for delivering water vapor from the entry chamber to the vapor chamber, and a passageway for delivering condensed water from the vapor chamber to a reservoir of purified water.Type: GrantFiled: June 17, 2008Date of Patent: January 5, 2010Inventors: Joel Vance Miller, Robert Samuel Smith
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Patent number: 7610768Abstract: A rotary multi-stage distiller for recovery of water from wastewater is provided. The rotary multi-stage distiller of the present invention can recover water from a wide variety of aqueous wastewaters such as, but not limited to, urine, condensate from air conditioning systems, wash water containing foaming soaps, seawater or polluted water. The multi-stage distiller can operate under vacuum conditions permitting the distillation to occur at low temperatures. The multi-stage distiller uses centrifugal forces for fluid pumping and for vapor/liquid separation. The multi-stage distiller comprises hydraulic seals for each stage which eliminate contamination of clean, recovered water by condensed waste water during the regeneration process. The multi-stage distiller also comprises a stationary shaft of stacked segments where each segment is associated with an individual stage of the multi-stage distiller.Type: GrantFiled: November 9, 2005Date of Patent: November 3, 2009Assignee: Honeywell International Inc.Inventors: Alex M. Lubman, Allen K. MacKnight, Volodimir G. Rifert, Ivan V. Zolotukhin, Vladimir I. Usenko, Petr A. Barabash, Aleksandr P. Strikun
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Patent number: 7597783Abstract: Methods for processing oils and apparatus for carrying out such methods are disclosed herein. One embodiment provides a method for processing a partially processed oil, wherein the oil includes glycerides and a volatilizable impurity fraction. The partially processed oil may be processed by driving off a first volatiles stream having a portion of the glycerides and at least a portion of the volatilizable impurity fraction, leaving a deodorized oil. The first volatiles stream may be introduced into a first condensing chamber and a glyceride-rich, impurity-poor fraction may be condensed from the first volatiles stream, leaving a glyceride-poor, impurity-rich second volatiles stream. The second volatiles stream may be passed into a second condensing chamber and a glyceride-poor, impurity-rich second condensate may be condensed from the second volatiles stream.Type: GrantFiled: November 13, 2001Date of Patent: October 6, 2009Assignee: Cargill, IncorporatedInventor: Marco Kruidenberg
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Patent number: 7588664Abstract: A vacuum column for oil distillation incorporates a thickened plate that has a layer of erosion-resistant material that is thicker than the corrosion-resistant thickness of an adjacent column section. Use of thickened, explosive- or roll-bonded clad plates may provide better service than either conventional plug-welded liners or conventional shell plates with weld overlays.Type: GrantFiled: July 27, 2005Date of Patent: September 15, 2009Assignee: Chicago Bridge & Iron CompanyInventors: Fahim E. Shadid, Alan W. Green
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Patent number: 7553396Abstract: A system for generating purified water from polluted water which includes an entry chamber communicating with a source of polluted water, a pump for delivering water vapor from the entry chamber to the vapor chamber, and a passageway for delivering condensed water from the vapor chamber to a reservoir of purified water.Type: GrantFiled: May 20, 2008Date of Patent: June 30, 2009Inventor: Joel Vance Miller
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Patent number: 7531065Abstract: A fluid distillation apparatus includes at least one each of a fluid inlet port Through which the fluid to be distilled is transferred from a container containing the fluid to be distilled to distillation chamber, a fluid outlet port through which the distilled fluid is transferred to a container to hold the distilled fluid, an air supply port to which compressed air supply is to be connected, a power cord through which the electric power is supplied, preferably an outlet through which air pressure for fluid agitation is supplied to said container containing the fluid to be distilled, and preferably art outlet through which air pressure is supplied to a pump means for transferring the distilled fluid from the receiving container to the duty fluid container. The apparatus includes a debris draining system for automatically draining debris from said distillation tank.Type: GrantFiled: October 18, 2002Date of Patent: May 12, 2009Assignee: Uni-Ram CorporationInventor: Soichiro Yamamoto
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Publication number: 20090032387Abstract: The present invention is an improved type of distillation of water. Usual distillation is related to a liquid's boiling point. However, it is possible to distill significant quantities of water at temperatures well below the boiling point. During distillation a compound is taken from a liquid-phase to the gas phase and then condensed to the liquid again to get a pure liquid. The present invention uses water sprayed and adsorbed onto a solid surface such as micro-powder made from wood as a starting material. Absorbing water onto such a surface results in rapid evaporation with a relatively low temperature gradient when the water and particles are agitated. The present invention could be characterized as solid-phase distillation.Type: ApplicationFiled: October 6, 2008Publication date: February 5, 2009Applicant: BIOMASS CONVERSIONS LLCInventor: Seiji HATA
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Publication number: 20090000940Abstract: A method of oil and/or oil product treatment is carried out by producing a physico-mechanical effect on a moving flow of oil and/or oil products by changing pressure along the flow, wherein the pressure of at least 0.35 MPa being created at the flow inlet, which is subsequently reduced to a value not in excess of 0.05 MPa to provide the formation of the vapor-liquid mixture, followed by pressure increase at the flow outlet to at least 0.1 MPa. The unit for producing effect on the moving flow by pressure drops comprises an inlet piping with a multi-nozzle block hermetically fixed in its cross-section connected to a cylindrical channel and an expanding diffusor having a half-angle not in excess of 4 degrees. The ratio of the cylindrical channel cross-section area to the sum of nozzle hole area at the outlet from the multi-nozzle block ranges from 2.1 to 5.9.Type: ApplicationFiled: March 30, 2006Publication date: January 1, 2009Inventors: Alexandr Vladimirovich Koss, Roman Andreevich Penzin
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Patent number: 7464237Abstract: A system and method for implementing a fast file synchronization in a data processing system. A memory management unit divides a file stored in system memory into a collection of data block groups. In response to a master (e.g., processing unit, peripheral, etc.) modifying a first data block group among the collection of data block groups, the memory management unit writes a first block group number associated with the first data block group to system memory. In response to a master modifying a second data block group, the memory management unit writes the first data block group to a hard disk drive and writes a second data block group number associated with the second data block group to system memory. In response to a request to update modified data block groups of the file stored in the system memory to the hard disk drive, the memory management unit writes the second data block to the hard disk drive.Type: GrantFiled: October 27, 2005Date of Patent: December 9, 2008Assignee: International Business Machines CorporationInventors: Jos M. Accapadi, Mathew Accapadi, Andrew Dunshea, Dirk Michel
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Patent number: 7435317Abstract: An improved distillation of water. involves distilling significant quantities of water at temperatures well below the boiling point. During distillation, a compound is taken from a liquid-phase to a gas-phase and then condensed to the liquid-phase again to get a pure liquid. The present invention uses water sprayed (105) and absorbed onto a solid surface such as micro-powder (104) made from wood as a starting material. Absorbing water onto such a surface results in rapid evaporation with a relatively low temperature gradient when the water and particles are agitated. The present invention could be characterized as solid-phase distillation.Type: GrantFiled: March 29, 2001Date of Patent: October 14, 2008Assignee: Biomass Conversions, L.L.C.Inventor: Seiji Hata
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Patent number: 7429312Abstract: The present group of inventions relates to processing of multi-component liquid mixtures (MCLM) employing reforming process, preferably for vacuum distillation of hydrocarbon mixtures and in petroleum refining and chemical industries. The inventions include the method for processing of multi-component liquid mixtures. The method of MCLM separation includes pressure feeding of a hydrocarbon liquid mixture to an a liquid-gas jet device nozzle which discharges to a vacuum chamber of liquid-gas jet device. A counter pressure jointly with the liquid-gas jet device forms a pressure surge in the vacuum chamber. The counter pressure is 0.4 to 0.7 of the magnitude of the feed pressure generated by the pump. The plant for MCLM processing includes a feed pump, a head delivery main, a discharge main, control instrumentation and a vacuum-generating device including a vacuum chamber, a liquid-gas jet device with a nozzle in the front end wall of the vacuum chamber.Type: GrantFiled: December 27, 2002Date of Patent: September 30, 2008Assignee: Energy Savings Technologies Financial Industrial Group LLCInventors: Yuriy Pavlovich Skakunov, Chamil Khakimovich Iskhakov, Sergey Vladimirovich Tishkin
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Patent number: 7422663Abstract: A compact array of vertical rising film evaporators is disclosed in an evacuated multi-effect process, for desalination of seawater, using waste heat of thermal machines. Vapor produced in one stage is the heat source for the next. This invention is based on a concentric disposition of three different evaporators, at which the first stage is a shell and tube evaporator built in a ring format, where is inserted inside the intermediate stage that is a bundle of vertical tubes in a ring format, and the last stage that is a bundle of vertical tubes placed inside the intermediate stage. By this arrangement, vapor pipelines are eliminated, dimensions are reduced, and heat transfer is improved per the rising film evaporators compared to falling film.Type: GrantFiled: August 1, 2003Date of Patent: September 9, 2008Inventor: Sergio Martins Costa
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Patent number: 7416642Abstract: A system for cooling a heated juice by partial low-pressure evaporation, the system includes a vat with at least two compartments that are connected to each other through a variably positioned shutter element, where the juice is subjected to decreasing pressure reductions within the vat and the movement of the variably positioned shutter element creates a pulsed effect that removes solid particles contained in the juice.Type: GrantFiled: May 29, 2002Date of Patent: August 26, 2008Assignee: Centre National de la Recherche Scientific (CNRS)Inventors: Jean-Pierre Nadeau, Dominique Cadiot, Patrick Sebastian, David Callede
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Patent number: 7413634Abstract: A multiple effect distillation chamber includes a plurality of separate distilling chambers and a drain chamber at a downstream end of the distilling chambers. The drain chamber functions to create a vacuum to draw volatile gases and impurities collected at the end of the distilling chambers into the drain chamber. The drain chamber cools the volatile gases via cooling water, whereby the cooling water and volatile gases are not mixed during the cooling process, such that the cooling water may be recycled and reused. The drain chamber may include two heat exchangers, each receiving cooling water from a separate water source. Utilizing separate water sources in conjunction with the dual heat exchangers of the drain chamber enables the flow rates of the cooling water sources to be adjusted to enable the disposal of waste water from the distiller at any desired temperature without affecting other functions of the distillation system.Type: GrantFiled: September 17, 2002Date of Patent: August 19, 2008Inventor: Mark W Napier
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Patent number: 7297236Abstract: A process arrangement for distilling fuel grade ethanol includes a fermentation portion, a distillation portion, a condensation and dehydration portion, a separation and drying portion and an evaporation portion. The fermentation portion produces beer. The distillation portion, the condensation and dehydration portion and the separation and drying portion receives beer from the fermentation portion and produces hot ethanol vapor and thin stillage. In the evaporation portion, a set of first effect evaporators which are heated either by plant steam or hot ethanol vapor, concentrate thin stillage into mid stillage while producing first effect steam. The first effect steam from the first effect evaporators provides heat to a set of second effect evaporators which concentrate the mid stillage into a syrup for further drying. The second effect evaporators produce second effect steam which is used to heat the distillation portion of the process arrangement.Type: GrantFiled: June 28, 2002Date of Patent: November 20, 2007Assignee: ICM, Inc.Inventor: Dennis Lee Vander Griend
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Patent number: 7291250Abstract: The present invention relates to a vacuum distillation plant and a process for concentrating organic aqueous solutions, especially spissum extracts, using said plant. The vacuum distillation plant of the invention comprises a flash evaporator, a means for vapor concentration and a multi-stage condenser positioned down-stream of said means for vapor concentration, means for recycling at least part of the condensate from a condensation stage into the bottoms product being provided. In addition, the present invention relates to a process for concentrating organic aqueous solutions such as concentrated extracts using said plant.Type: GrantFiled: October 20, 1999Date of Patent: November 6, 2007Assignee: Bionorica AGInventors: Michael A. Popp, Heinz Walter Joseph, Michael R. Rannow
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Patent number: 7288169Abstract: A distillation apparatus for subjecting a crude readily polymerizable compound to distillation under vacuum conditions to purify the same includes a distillation column and a vacuum generator, an exhaust gas conduit of the vacuum generator being connected to a connecting conduit therebetween through a pressure control valve. The purification method includes using the disclosed distillation apparatus and controlling the action of the pressure control valve based on a pressure of the distillation column, thereby controlling the amount of the exhaust gas to be introduced to control the pressure of the distillation column.Type: GrantFiled: February 20, 2004Date of Patent: October 30, 2007Assignee: Mitsubishi Chemical CorporationInventors: Shuhei Yada, Yasushi Ogawa, Yoshiro Suzuki, Kenji Takasaki, Kiyoshi Takahashi