Vacuum Patents (Class 202/205)
  • Patent number: 4444623
    Abstract: Distilling equipment comprising input apparatus (21) including a boiling chamber (83) and means (80-82, 104-107, 110, 111) for supplying raw liquid to the boiling chamber at a predetermined level, a closed condensation chamber (22) above the predetermined level and connected to the top of the boiling chamber (96) to receive therefrom only vapor from the raw liquid, and output apparatus (20) including a liquid collection container (25) below the condensation chamber and liquid circulating structure (29-34, 44-55) for withdrawing liquid from the container, cooling the liquid, discharging it within the condensation chamber, and returning it to the container.
    Type: Grant
    Filed: November 9, 1981
    Date of Patent: April 24, 1984
    Inventor: Philip G. Youngner
  • Patent number: 4440601
    Abstract: A method and apparatus for high volume distillation of impure liquid, particularly of binary mixtures of relatively low boiling organic substances and water, comprises fractionally distilling the impure liquid to form a vapor of a low boiling organic substance; compressing the vapor; passing at least a portion of the compressed vapor through a vapor composition adjustment zone wherein the organic substance may catalytically or otherwise react or merely stabilize following compression; compressing the vapor exiting the adjustment zone to form a recompressed vapor; cooling the recompressed vapor in heat transfer relation with the impure liquid whereby the vapor at least partially condenses, transferring sufficient heat to the impure liquid for evaporating the liquid and to form the aforementioned low boiling organic vapor; and collecting the condensed low boiling organic vapor.
    Type: Grant
    Filed: January 15, 1981
    Date of Patent: April 3, 1984
    Inventors: Jerome Katz, Sidney J. Fogel
  • Patent number: 4439601
    Abstract: Disclosed is a multiple-stage flash devolatilization process, and apparatus for use therein, for recovering volatiles from mass processable polymers, which enables optimally low pressures to be employed without the necessity for refrigeration to condense the volatiles recovered thereby, comprising separating the volatiles from the polymeric material by flashing in a first flash devolatilization zone to remove the majority of the volatiles and then flashing in at least one additional flash devolatilization zone maintained at a lower pressure, preferably as low as practically possible, to remove residual volatiles, and then recovering the volatiles for further use by feeding the volatiles recovered from the additional flash zones back into the stream of volatiles leaving the first flash zone, the higher pressure of which allows the combined free volatiles present therein to then be condensed in a conventional non-refrigeration cooling process.
    Type: Grant
    Filed: July 15, 1981
    Date of Patent: March 27, 1984
    Assignee: Cosden Technology, Inc.
    Inventors: J. L. McCurdy, Marvin A. Jarvis
  • Patent number: 4420373
    Abstract: A mechanical energy conversion method and system for the restoration of dissipated heat energy, contained in natural or artificial water bodies at or near ambient temperatures, to industrial process heat, mainly in the form of steam up to 200.degree.-400.degree. C. The sensible heat contained in a water body is concentrated as latent heat in low pressure water vapor which is thermo-compressed by steam ejection to an intermediate pressure level, wherefrom mechanical compression takes over, generating highly superheated output steam. The ejecting steam is not generated in a boiler, but is continuously regenerated by the compressor and routed back for repeated ejection. The compressor is driven by a heat engine whose reject heat is collected and upgraded as well. The output of heat energy is essentially equal to the sun of the heating value of the fuel consumed and the intake of latent heat and amounts thus to substantially more than the heating value of the fuel alone.
    Type: Grant
    Filed: August 3, 1981
    Date of Patent: December 13, 1983
    Inventor: Dan Egosi
  • Patent number: 4383972
    Abstract: Disclosed is a multiple-stage flash devolatilization process, and apparatus for use therein, for recovering volatiles from mass processable polymers, which enables optimally low pressures to be employed without the necessity for refrigeration to condense the volatiles recovered thereby, comprising separating the volatiles from the polymeric material by flashing in a first flash devolatilization zone to remove the majority of the volatiles and then flashing in at least one additional flash devolatilization zone maintained at a lower pressure, preferably as low as practically possible, to remove residual volatiles, and then recovering the volatiles for further use by feeding the volatiles recovered from the additional flash zones back into the first flash zone, the higher pressure of which allows the combined free volatiles present therein to then be condensed in a conventional non-refrigeration cooling process.
    Type: Grant
    Filed: July 15, 1981
    Date of Patent: May 17, 1983
    Assignee: Polymer Research, Inc.
    Inventors: J. L. McCurdy, Marvin A. Jarvis
  • Patent number: 4381971
    Abstract: A water distillation system which includes a storage tank for impure water and a storage tank for distilled water. Impure water is pumped through a heater to an evaporator. Impure water is also pumped through an impure water jet ejector. Distilled water is pumped through a distilled water jet ejector. The impure water jet ejector withdraws water from the bottom of the evaporator. The distilled water jet ejector withdraws water vapor from the top of the evaporator. Distilled water from the distilled water jet ejector passes through a heat exchanger in the impure water tank to heat input water. Impure water from the impure water jet ejector passes through a heat exchanger in the distilled water tank to cool the distilled water.
    Type: Grant
    Filed: December 16, 1981
    Date of Patent: May 3, 1983
    Inventor: Gerald P. Dietrick
  • Patent number: 4366030
    Abstract: Method and apparatus for distillation of liquids such as sea water, brackish water, waste water, or the like, which also may be used for cooling purposes, are disclosed. The apparatus includes a vacuum tank, or vessel, into which liquid to be distilled, such as saline water, is fed to partially fill the tank. If desired, heating means may be included for heating the liquid adjacent the surface thereof to promote evaporation thereof. Vapor from the region above the liquid surface is fed to vapor condensing means adjacent the bottom of the tank for condensing the same. A condensate discharge tube extends downwardly from the condensing means for discharge of condensate therefrom. Means including a pressure head of condensate within the condensate discharge tube maintains a subatmospheric pressure within the tank to promote evaporation of liquid contained therein.
    Type: Grant
    Filed: October 12, 1979
    Date of Patent: December 28, 1982
    Inventor: Max F. Anderson
  • Patent number: 4366031
    Abstract: Distillation method and apparatus for separation of alcohol from an alcohol-water mixture are disclosed which include use of a fluid-tight vacuum tank within which a surface condenser is located adjacent the tank bottom. The condenser has a vapor inlet above the condenser, and a condenser outlet which communicates with a first pump having a pump discharge outside the tank. A second pump is provided for removal of mixture from the bottom of the tank. In operation, an alcohol-water mixture is fed into the tank to completely fill the same while air is vented therefrom. The vent is closed, and mixture then is pumped from the tank and condenser to empty the condenser and to lower the level of mixture in the tank beneath the vapor inlet to the condenser. With the removal of mixture, a vacuum is created whereupon alcohol rapidly evaporates from the mixture surface to rapidly reduce the temperature of remaining mixture.
    Type: Grant
    Filed: September 22, 1980
    Date of Patent: December 28, 1982
    Inventor: Max F. Anderson
  • Patent number: 4343683
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: May 7, 1980
    Date of Patent: August 10, 1982
    Inventor: Richard E. Diggs
  • Patent number: 4342624
    Abstract: A liquid containing a solvent to be evaporated is fed to a concentration chamber which is fluidly connected to an evaporation chamber maintained at a reduced pressure. A vapor compression means withdraws solvent vapor from the evaporation chamber, compresses the vapor and forces the compressed vapor to a liquification chamber. Regulator means responsive to the density of the liquid remaining within the concentration chamber will regulate the rate of solvent evaporation to provide a concentrate suitable for recycling.A method of operating the still of this invention utilizes the technique of increasing the compressor capacity until the compressor begins to surge and then reducing the capacity a fixed amount to provide the desired efficiency.
    Type: Grant
    Filed: August 7, 1981
    Date of Patent: August 3, 1982
    Assignee: Eaton Corporation
    Inventors: Richard Chute, Ralph P. Horan
  • Patent number: 4334962
    Abstract: A steam stripping process particularly useful for separating the volatile components of immiscible materials. In the disclosed embodiment of the invention peel oil emulsion, e.g., from a citrus juice extractor, is heated under pressure by the injection of steam while the emulsion is flowing. The major portion of the pressure on the flowing emulsion is then dropped through a back pressure valve, and the resultant vapor-liquid mixture is passed through a long turbulent passage under a slowly decreasing pressure where thorough mixing is provided and d-limonene, the volatile component of the peel oil emulsion, is stripped from the emulsion by the ad-mixed steam. The mixture is discharged at atmospheric pressure into a vapor collecting tank where the spent liquor is separated and drained off. The collected vapors are passed to a condenser, and the condensate therefrom is directed to a decant tank where the di-limonene is decanted off.
    Type: Grant
    Filed: July 20, 1978
    Date of Patent: June 15, 1982
    Assignee: FMC Corporation
    Inventor: Gordon P. Gerow
  • Patent number: 4329204
    Abstract: A multiple effect diffusion distillation system includes a plurality of parallel plates for continuous recovery of heat having opposed evaporation and condensation faces for alternately evaporating and condensing phases of a liquid fed on to the upper end of the plates in a thin film for gravity flow along the evaporator face of the plates with vapor condensing on the condensation faces and with means for collecting and recovering the condensed product from the system. Alternate embodiments including a solar heat input system and others include multiple modular systems.
    Type: Grant
    Filed: February 19, 1980
    Date of Patent: May 11, 1982
    Inventors: John P. Petrek, Clifford M. Cantrell
  • Patent number: 4319965
    Abstract: The invention relates to a system for purifying salty or brackish water which may, also, contain solids and living organisms making the water unpalatable for agriculture or long term animal consumption. The system includes a cyclic mechanism which causes an evaporable liquid to boil at a predetermined pressure and temperature in a first vertical elongated column, vapor cross over means to a second vertical elongated column, said vapor being condensed at a predetermined pressure and temperature in the second vertical elongated column, means for supplying heat to the first column, heat rejection means for the second column for reliquefying the material. Heat may be supplied to the first column by low temperature geothermal heat, heat from solar ponds, heat from solar collecting devices, as well as heat from the ambient air, or any form of low temperature heat for vaporizing the subject liquid.
    Type: Grant
    Filed: September 18, 1980
    Date of Patent: March 16, 1982
    Inventor: Sidney A. Parker
  • Patent number: 4318781
    Abstract: A desalinazation apparatus has the bulk of its piping circuitry composed of black iron pipe, or similar pipe, which is normally subject to corrosion by sea water. Heat transfer to a salt water still includes indirect heat transfer by a thermal oil which is contained in the black iron pipe. A solar collector heat source is used to heat the heat transfer oil. The heat transfer rate from the heat transfer oil is maintained by using turbulence inducing fins in the interior of the heat transfer tubes in the salt water still and by directing high pressure gas at the exterior of the heat transfer tubes in the salt water still. A manifold of jets placed beneath the heat transfer tubes in the salt water still projects the high pressure gas, such as high pressure high temperature steam, onto the exterior of the heat exchange tubes.
    Type: Grant
    Filed: January 11, 1980
    Date of Patent: March 9, 1982
    Inventor: Tomimaru Iida
  • Patent number: 4318780
    Abstract: A multi-stage flash evaporator design wherein two flash evaporator stages are paired in tandem with each individual condenser tube bundle. The condenser tube bundle is enclosed in a housing that is partitioned to define two separate condenser chambers and the housing is also partitioned to define two cross-flow evaporator stages. The condenser tubes extend to opposite ends of the housing and each evaporator chamber has a width substantially equal to the full extent of the condenser tubes with the brine entry port extending the full width of such chamber; however, the vapor from each flash chamber is directed to only a portion (i.e. generally one-half) of the condenser bundle with the partitions maintaining each condenser portion generally sealed from the vapor of the adjacent evaporator chamber. An internal vent orifice directs the non-condensible vapors of the high temperature chamber into the low temperature chamber.
    Type: Grant
    Filed: July 3, 1980
    Date of Patent: March 9, 1982
    Assignee: Westinghouse Electric Corp.
    Inventor: Robert E. Bailie
  • Patent number: 4316774
    Abstract: A urine-water recovery system is described which provides efficient potable water recovery from waste liquids. The design allows use over extended durations such as encountered in space flights. The system has advantages such as low power consumption, compactness, and gravity insensitive operation. The system comprises a vacuum distillation system combining a hollow fiber polysulfone membrane evaporator with a thermoelectric heat pump and condenser. With the system of the present invention, water purified from urine can be produced at a rate of more than 0.5 kg/hr at a total system energy of less than 400 w-hr/kg.
    Type: Grant
    Filed: July 5, 1979
    Date of Patent: February 23, 1982
    Assignee: United Technologies Corporation
    Inventor: Raymond B. Trusch
  • Patent number: 4302297
    Abstract: An apparatus for desalinating ocean waters by distillation and furnishing electrical power, utilizes an evaporator, barometric leg conduits, a closed condenser, ocean water circulating circuits for circulating warm surface water to the evaporator and cool ocean water to the condenser and using the mass flow of vapors evolved from the evaporator to drive a prime mover which in turn drives an electrical generator. A portion of the electrical power so-generated is used to control the operation of respective pumps and valves in the apparatus. The liquid level of the condensate water is controlled in a barometric leg condensate outlet conduit. The system is also provided with a vacuum pump at least for initiating a reduced pressure and particle separator channel means is provided to prevent liquid entrainment in the condenser.
    Type: Grant
    Filed: July 3, 1980
    Date of Patent: November 24, 1981
    Inventor: Gerald F. Humiston
  • Patent number: 4301298
    Abstract: A normally liquid hydrocarbon having a minimum boiling point of about 425.degree. F. is utilized to provide the liquid seal in a vacuum pump which intakes a gaseous light ends stream resulting from a process for the production of ethyl acrylate by the reaction of ethylene with acrylic acid in the presence of a sulfuric acid catalyst. Upon contact in the vacuum pump, the gaseous light ends are partially absorbed into the normally liquid hydrocarbon, with the normally liquid hydrocarbon being recovered by fractionation.
    Type: Grant
    Filed: May 23, 1980
    Date of Patent: November 17, 1981
    Assignee: Celanese Corporation
    Inventors: Theodore Horlenko, James L. Paul, James W. Gordon
  • Patent number: 4292121
    Abstract: A solids/liquid admixture is introduced into an atmosphere (temperature and reduced pressure) in which the liquid is immediately converted to a saturated vapor and thus relieved of associated solids, which are withdrawn. The saturated vapor is then conducted to a surface on which it condenses and from which it is collected. Suitable apparatus is provided in the form of modules, which are efficiently operated in multiples of four in a common temperature-stabilizing medium.
    Type: Grant
    Filed: September 21, 1979
    Date of Patent: September 29, 1981
    Assignee: The Caffes Trust
    Inventor: Peter J. Caffes
  • Patent number: 4285776
    Abstract: Salinated or other contaminated water is fed to a chamber and sprayed into an evaporation chamber that is maintained at a relatively low pressure by means of a vacuum pump or the like. This evaporates the water so that desalinated water vapor is drawn out through the pump and discharged into a collection chamber at a higher pressure whereupon it condenses and may be discharged into a storage area The solids removed by the evaporation of the water collect at the base of the evaporation chamber and can be removed periodically through an air lock.
    Type: Grant
    Filed: November 6, 1979
    Date of Patent: August 25, 1981
    Inventor: George Atwell
  • Patent number: 4285775
    Abstract: A mixture of xylenol, water, alcohol and other substances is put into an evaporator tank which is adjusted to a pressure and temperature to evaporate the water and alcohol. The water and alcohol vapors flow through an expansion chamber into a condenser and the condensate flows back through a distributor and a control valve into a collector tank. Through a two-stage control dial a second temperature and pressure is imposed upon the evaporator tank to evaporate the xylenol which is similarly condensed and the condensate flows back through the distributor which control valve has been actuated to direct the xylenol into a second collector tank. A second evaporator is connected through a selectively operable shut-off valve to the expansion chamber. The second evaporator tank is provided with an inlet funnel which can be heated to melt solid paraffin therein. A filter is within this funnel to filter out solid foreign matter.
    Type: Grant
    Filed: June 3, 1980
    Date of Patent: August 25, 1981
    Inventor: Wolfgang Hamann
  • Patent number: 4286066
    Abstract: Apparatus for continuously fermenting a moist particulate feed and distilling the fermentation product is disclosed in which a pressure-locked auger forces a moist particulate feed from a hopper into a fermentation tank, liquor is removed from the tank and solids are separated therefrom to produce a beer which is distilled in a distillation column. A combustion engine powers the auger and the means for separating solids, and the engine exhaust surrounds an inlet section of said auger to help heat the pressurized feed therein to produce fermentable sugar within the auger, and the auger includes a section passing to the tank in heat exchange relation to the distillation column to provide heat for distillation. The column is a multistage column angled to face the sun and has an upper glass plate to allow solar radiation to enter and penetrate between the foraminous plates of the column.
    Type: Grant
    Filed: June 24, 1980
    Date of Patent: August 25, 1981
    Inventors: Robert S. Butler, Lance B. Crombie
  • Patent number: 4282067
    Abstract: A method and closed system for high volume distillation of impure liquids comprises evaporating the impure liquid in an evaporator to form a vapor at a temperature above the freezing point and below the critical point, preferably the boiling point, of the liquid at ambient pressure and at a pressure not exceeding a pressure corresponding to the evaporation temperature under saturated conditions; compressing the vapor in compression means which preferably has a compression ratio variable in the range 1.
    Type: Grant
    Filed: August 10, 1979
    Date of Patent: August 4, 1981
    Inventors: Jerome Katz, Sidney J. Fogel
  • Patent number: 4269664
    Abstract: Liquid treating apparatus especially useful for water purification, including an output section and an input section interconnected at their tops by a closed condensation chamber. The input section includes raw liquid supply and return columns, opening at their bottoms into a raw liquid supply open to the atmosphere, and the output section includes treated liquid supply and return columns open at their bottoms into a treated liquid container also open to the atmosphere.Treated liquid is cooled and circulated in the output section to produce and maintain negative pressure at one end of the condensation chamber, and raw water in mixed liquid and vapor form is supplied by aspiration in the input section, the vapor phase passing through the condensation chamber, and the liquid phase being used to drive the pump which causes the circulation in the output section. Several embodiments of the invention are shown.
    Type: Grant
    Filed: December 1, 1978
    Date of Patent: May 26, 1981
    Inventor: Philip G. Younger
  • Patent number: 4267022
    Abstract: Method and apparatus for desalinizing water. Salt water in an evaporation zone is provided with heat of vaporization by a heat pump which transfers heat to the water from a thermal sink. The evaporation zone is maintained at subatmospheric pressure so that the salt water boils at a temperature at least about 10 degrees above the ambient dew point. The pressure in the evaporation zone is maintained at a low level by a vacuum pump and by condensing the vapor in a condensation zone from which fresh water is collected. The heat of condensation is dissipated into a "cold" sink if available or by a heat dissipating means such as an evaporative cooling apparatus. Energy efficiency results from the ability of the heat pump or pumps in the system to operate at a high coefficient of performance.
    Type: Grant
    Filed: April 26, 1978
    Date of Patent: May 12, 1981
    Inventor: Frederick L. Pitcher
  • Patent number: 4261814
    Abstract: The invention provides an improvement in the conventional operation of a vacuum pipestill, whereby when used with, for example, an atmospheric residuum either (a) conventional yields are obtainable with less stripping steam utilization, or (b) a deeper cut into the residuum is obtainable for conventional steam utilization. Some of the gaseous mixture normally withdrawn from the top of the vacuum pipestill for washing and removal is fed into compression and recycle means and recycled to the stripping zone of the pipestill to replace, or augment, the conventionally used stripping steam.
    Type: Grant
    Filed: November 22, 1978
    Date of Patent: April 14, 1981
    Assignee: Exxon Research and Engineering Co.
    Inventor: Klaus A. Pfeifer
  • Patent number: 4254943
    Abstract: The invention provides apparatus and a process for removing mercury from solid waste material. The solid waste material is placed in a vacuum chamber. The chamber is heated above the vaporization temperature of mercury. A vacuum condition is formed and then, while the temperature is maintained above the vaporization temperature of mercury, an inert gas is placed in the vacuum chamber. During this heating period, the pressure in the vacuum chamber is periodically varied from a maximum to a minimum. The apparatus utilized is a vacuum chamber, a vacuum pump, and a pipe that contains a mercury condenser. The pipe also functions through a side inlet as a means for introducing the inert gas into the vacuum chamber, while the vacuum pump is closed off. A control unit for controlling the alternate periods of mercury vapor withdrawal and inert gas introduction into the vacuum chamber is provided.
    Type: Grant
    Filed: July 17, 1979
    Date of Patent: March 10, 1981
    Assignee: Lumalampan AB
    Inventor: Karl-Ake G. Bjorkman
  • Patent number: 4239603
    Abstract: A fuel-efficient method and apparatus for the generation, actually re-generation, of ejecting steam used in a steam ejection system to evacuate process vapor from an enclosed space. In the method, all of the ejecting steam is not generated continuously in a boiler, but a predetermined quantity of steam is reused by continuous mechanical recompression, without intervening condensation, in a returning cycle while alternating between a pressure low after ejection (i.e. expansion) and a pressure high after recompression, whereas the evacuated vapor is branched off from the ejecting steam cycle after ejection and condensed. Parts of the condensate are reconverted to additional steam by heat exchange with all or part of the superheat and friction heat contained in the recompressed ejecting steam and/or by heat exchange with the exhaust and cooling system of a heat engine serving as a prime mover for the compressor.
    Type: Grant
    Filed: February 22, 1978
    Date of Patent: December 16, 1980
    Inventor: Dan Egosi
  • Patent number: 4235680
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: January 12, 1978
    Date of Patent: November 25, 1980
    Inventor: Richard E. Diggs
  • Patent number: 4235678
    Abstract: A low pressure, low temperature, solar powered evaporating-condensation system to provide relatively large scale conversion of brackish and seawater to fresh water, utilizes a solar radiation frequency selective material covered evaporation chamber, a throat connected elevated condenser containing energy transferring devices for vapor volume reduction to form a condensate which flows through a water-locked barometric leg to maintain the system at the sub-atmospheric pressure. The system is regenerative and includes means whereby the energy removed from the vapor during condensation is returned to the evaporating chamber and is again utilized in the cycle. Egress valves and locks are provided to maintain balanced flower of raw water, condensate and ejection of residuals. Suitable elevation of the condenser above the evaporator would provide for power generation.
    Type: Grant
    Filed: March 17, 1978
    Date of Patent: November 25, 1980
    Inventor: Joseph E. McKeen
  • Patent number: 4232598
    Abstract: This invention relates to an improved process for the separation and isolation of coffee aroma constituents from roasted coffee, combining the aroma constituents with an edible substance and subsequently incorporating the aromatized substance in a food product.The process involves improving the condensation of vapors generated from the distillation of coffee oil by condensing the distilled aroma constituents onto a sleeve cooled by and snugly surrounding a container filled with coolant. The sleeve is removed and the aroma constituents condensed thereon are then preferably combined with an edible substance by manipulating the condensed constituents quickly and efficiently thus minimizing aroma loss and degradation caused by undesirable prolonged contact with air.
    Type: Grant
    Filed: May 1, 1978
    Date of Patent: November 11, 1980
    Assignee: General Foods Limited
    Inventors: Gerald S. Hurlow, Jean R. Blain, Michael Coombes, Jean-Claude Richard, Patrick W. Hitchinson
  • Patent number: 4233267
    Abstract: Volatile reactants are heated under reflux in a reactor and form volatile reaction by-products which are continuously removed in a vapor effluent from a reflux column and partial condenser. The effluent, which entrains some of the reactants, is condensed in a first total condenser and is fed to a distillation apparatus for separation of the volatile reactants and by-products and return of the separated reactants to the reactor. Before the condensate reaches the distillation apparatus, it is temporarily stored in a receiver from which it is controllably fed to a pre-heater where it is evaporated and then fed as a vapor to the distillation column of the distillation apparatus for separation. The distillation column includes at one end a reboiler which retains the reactants. The other end of the distillation column is coupled to a second total condenser in which the volatile by-products are condensed and withdrawn through a cooler for disposal.
    Type: Grant
    Filed: January 18, 1978
    Date of Patent: November 11, 1980
    Assignee: Fiberglas Canada Limited
    Inventors: Robert J. Coker, Gary W. Bate, Henk J. Deuzeman
  • Patent number: 4211609
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: January 12, 1978
    Date of Patent: July 8, 1980
    Inventor: Richard E. Diggs
  • Patent number: 4204914
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: January 12, 1978
    Date of Patent: May 27, 1980
    Inventor: Richard E. Diggs
  • Patent number: 4203805
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: January 12, 1978
    Date of Patent: May 20, 1980
    Inventor: Richard E. Diggs
  • Patent number: 4203806
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: January 12, 1978
    Date of Patent: May 20, 1980
    Inventor: Richard E. Diggs
  • Patent number: 4201628
    Abstract: This invention relates to a distillation column for removing vinyl chloride monomer or other volatile material from an emulsion, suspension or dispersion containing such material. The apparatus comprises a column in which a series of inverted cones are mounted. The dispersion or emulsion is pulled downwardly over the cones and steam is fed into the column through sparges and flows upwardly against the descending stream of material. The low boiling materials are distilled out and recovered for reuse. The stripped emulsion or dispersion are collected at the bottom of the column.
    Type: Grant
    Filed: October 7, 1977
    Date of Patent: May 6, 1980
    Assignee: The Goodyear Tire & Rubber Company
    Inventors: Shirley L. Church, Loren M. Hilts
  • Patent number: 4200496
    Abstract: This invention relates to a vaporizer for generating developer gas, containing ammonia, from aqueous ammonia for developing diazo copying material comprising a first vaporizer unit including a rectifying column and a column head, a gas outlet for taking off the developer gas and an inlet opening into the column head for feeding in aqueous ammonia, and a heatable, steam-generating sump vessel having a base and a residual water outlet, a second unit including a volatilizer with means for heating a base zone thereof, a residual water inlet opening in said base zone, a residual water line connecting said residual water inlet opening to said residual water outlet of said rectifying column, said residual water outlet of said rectifying column projecting upwardly in said sump vessel and having an orifice above the base thereof, said two units being arranged side by side with parallel axes in a single casing, a first connecting branch as said gas outlet for taking off the developer gas and a second connecting branch
    Type: Grant
    Filed: February 10, 1978
    Date of Patent: April 29, 1980
    Assignee: Hoechst Aktiengesellschaft
    Inventor: Eckehard Stein
  • Patent number: 4199406
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: January 12, 1978
    Date of Patent: April 22, 1980
    Inventor: Richard E. Diggs
  • Patent number: 4199407
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: January 12, 1978
    Date of Patent: April 22, 1980
    Inventor: Richard E. Diggs
  • Patent number: 4186058
    Abstract: A method and closed system for high volume distillation of impure liquids comprises evaporating the impure liquid in an evaporator to form a vapor at a temperature above the freezing point and below the critical point, preferably the boiling point, of the liquid at ambient pressure and at a pressure not exceeding a pressure corresponding to the evaporation temperature under saturated conditions; compressing the vapor in compression means which preferably has a compression ratio variable in the range 1.
    Type: Grant
    Filed: April 18, 1977
    Date of Patent: January 29, 1980
    Inventors: Jerome Katz, Sidney J. Fogel
  • Patent number: 4181577
    Abstract: A water distillation system in which the heat supplied to the evaporator and the cooling of the condenser is provided by a refrigeration unit having its condensing coils in the evaporator and its evaporative coils in the condenser.
    Type: Grant
    Filed: March 25, 1977
    Date of Patent: January 1, 1980
    Assignee: Auscoteng Pty. Ltd.
    Inventor: Norman L. Foley
  • Patent number: 4170522
    Abstract: A diffusion pump capable of separating impurities from its pump fluid during operation is disclosed. Skimming drains are provided in the pump's boiler for periodically skimming the evaporative surface of the working fluid. This eliminates nearly all contaminants of higher molecular weight than the pump fluid. In the foreline of the pump, a series of peripheral gutters are provided for trapping, separating and draining off condensates. The gutters facilitate the removal of impurities of lower molecular weight than that of the pump fluid. Means are also provided for further removing trace quantities of residual volatile impurities which tend to backstream up the diffusion pump barrel. The highly purified pump fluid allows for a more vigorously working evaporative surface, thereby increasing the throughput of the diffusion pump. Together with the elimination of volatile impurities from the pump barrel, this facilitates the attainment of significantly higher ultimate chamber vacuum.
    Type: Grant
    Filed: October 6, 1975
    Date of Patent: October 9, 1979
    Inventor: Alvin E. Buggele
  • Patent number: 4140212
    Abstract: A simplified, essentially maintenance-free yet highly efficient distillation tower and method for waste oil rerefining is provided which allows direct vacuum distillation of additive-supplemented waste oils without chemical pretreatment thereof and yields a highly refined intermediate oil suitable for immediate use or final polishing, along with a valuable bottoms fraction usable in greases or asphalts, for example. The tower includes an upright, cylindrical chamber with a tangential waste oil inlet and cooperating internal baffle for creating a whirling oil flow pattern therewithin, along with means for maintaining the proper temperature conditions within the tower for maximizing vaporization and recovery of hydrocarbons from the waste oil while also preventing undesirable decomposition or cracking of the oil.
    Type: Grant
    Filed: August 19, 1977
    Date of Patent: February 20, 1979
    Assignee: Vacsol Corporation
    Inventors: Richard H. O'Blasny, Timothy F. Sparks, Timothy J. Tierney, John S. Hunter
  • Patent number: 4138293
    Abstract: Desalination apparatus utilizing solar heating of metal member(s) such as balls, rollers, or metal endless belt(s) in a heating chamber and vaporizing saline water with the latent heat in said metal member(s) by spraying saline water thereon in a vaporizing chamber, a water-cooled condenser to condense the vapors, a trough to collect the condensate, a rinse tank to remove salt deposits and/or saline water from the metal member(s), and means for returning the rinsed metal member(s) for solar reheating.
    Type: Grant
    Filed: January 27, 1978
    Date of Patent: February 6, 1979
    Inventor: Kurt F. Ziehm, Jr.
  • Patent number: 4118283
    Abstract: An apparatus and method for removing contaminants from water having solid contaminants dissolved therein. Contaminated water flows across a grid and into a storage tank. The grid utilizes solar energy to heat that water to a predetermined temperature. A heat transfer structure which is dome-shaped and receives water from the storage tank and a preheater means utilizing solar energy heats the water to a further predetermined temperature. An evaporator means receives the heated water and exposes it to a vacuum condition so that the temperature of the water is above the saturation temperature. The water is thus vaporized, and solid contaminants dissolved therein are separated therefrom. The solids are deposited on a plurality of moving belts and are then moved into a solids removal system. The solids removal system comprises a plurality of trap door pairs upon which the solids are deposited and which are sequentially opened so that the vacuum conditions existing in the evaporator are not disturbed.
    Type: Grant
    Filed: October 28, 1975
    Date of Patent: October 3, 1978
    Inventor: Richard E. Diggs
  • Patent number: 4108718
    Abstract: A process and system for recovering the materials from an aqueous solution is disclosed. Dissolved materials in the aqueous solution are solidified as the aqueous solution is caused to be changed from liquid to vapor state, and the solidified materials along with suspended materials, if any, are collected. The aqueous solution is caused to be changed from liquid to vapor state at a filter which passes the vapor but blocks passage of liquid, and the filter has a vacuum at the side opposite to that of the aqueous solution so that the vapor is withdrawn through the filter and the solid materials collected on the filter. The system includes a thin film filter that is releasably clamped against a container so that one side of the filter contacts aqueous solution such as water in the container with a vacuum pumping device exerting vacuum pressure on the other side of the filter of less than about 4 mm of Hg. The system is particularly useful for determining impurities in water.
    Type: Grant
    Filed: January 27, 1976
    Date of Patent: August 22, 1978
    Assignee: Purdue Research Foundation
    Inventors: Frank A. Rickey, Jr., Paul C. Simms, Neal R. Butler
  • Patent number: 4096039
    Abstract: An electronic system for automatically controlling the operation of a desalination system, and particularly such systems utilizing waste heat from internal combustion engines. The automatic control system is responsive to physical parameters within the desalinator and is particularly useful during warm-up and cooling periods at the beginning and end of use of such a desalination system for minimizing wear on system components and for maximizing the operational life of the system.
    Type: Grant
    Filed: December 18, 1975
    Date of Patent: June 20, 1978
    Assignee: Carnine Corporation
    Inventors: Howard H. Carnine, Carter R. Robinson
  • Patent number: 4094748
    Abstract: Impurities or unwanted by-products are distilled off from an oily liquid by means of an ancillary stripping agent. The vaporization temperatures of the impurities and of the ancillary stripping agent lie below that of the oily liquid. Spontaneous distillation takes place in a decompressor to which the materials to be treated are supplied from a mixer or contactor. The decompressor comprises two nozzles arranged in series. In the decompressor the materials to be treated are subjected to a pressure considerably below the mixer pressure and somewhat below the separator pressure. Decomposition of the oil stream occurs in the decompressor into a non-volatile liquid phase and a vapor phase containing the ancillary stripping agent and the impurities originally in the oil feed. The mixed vapor/liquid stream enters the separator which is at a pressure which lies considerably below the pressure obtaining in the mixer.
    Type: Grant
    Filed: June 11, 1976
    Date of Patent: June 13, 1978
    Inventor: Heinz Schumacher
  • Patent number: 4088542
    Abstract: Unwanted contaminants or by-products of oily streams can be removed by distillation at reduced pressure and elevated temperatures using an ancillary distilling agent which lowers the boiling temperatures of the impurities. The efficiency of such removal is enhanced by the formation of a true solution of the ancillary agent in the oily stream at the molecular level. To bring about this solution, the ancillary agent in the superheated gaseous state is brought into intimate contact with the oily stream in a mixing vessel or contactor at substantially equal pressures but at slightly differing temperatures. The oil temperature is such as to cause condensation of the ancillary agent, but not to significantly cool the oil.
    Type: Grant
    Filed: June 7, 1976
    Date of Patent: May 9, 1978
    Inventor: Heinz Schumacher