Regulating Ph Patents (Class 210/724)
  • Patent number: 8182697
    Abstract: A method and an apparatus for treating selenium-containing wastewater, in which wastewater containing hexavalent selenium is subjected to reduction treatment, selenium can be effectively removed at a small amount of metal leached, and, preferably, sludge produced during treatment is white, thereby facilitating the disposal of the sludge. The selenium-containing wastewater is brought into contact with an alloy or a mixture of metallic titanium and a first metal other than metallic titanium to partially leach the first metal, thereby subjecting selenium in the wastewater to reduction treatment.
    Type: Grant
    Filed: June 28, 2007
    Date of Patent: May 22, 2012
    Assignee: Kurita Water Industries Ltd.
    Inventors: Yoshihiro Etou, Hiroyuki Asada, Yu Tanaka
  • Publication number: 20120103915
    Abstract: A method of purifying arsenic contaminated water is disclosed. The method comprises of adding to the arsenic contaminated water predetermined quantities of iron and alkali; and passing the water so obtained through a filter medium including rice husk ash. A device for purification of arsenic contaminated water is also disclosed.
    Type: Application
    Filed: March 23, 2010
    Publication date: May 3, 2012
    Applicant: TATA CONSULTANCY SERVICES LTD.
    Inventor: Kalyan Kumar Das
  • Patent number: 8153011
    Abstract: The invention relates to a method for separating off coloring components from aqueous plant extracts in which magnesium ions (Mg2+) are added to the plant extract, at least one alkaline component is added to the plant extract, a precipitate is formed, and the precipitate formed is separated off from the plant extract.
    Type: Grant
    Filed: April 27, 2007
    Date of Patent: April 10, 2012
    Assignee: Bayer Cropscience AG
    Inventors: Friedrich Meuser, Ingo Bauer
  • Patent number: 8147782
    Abstract: A process for producing a purified nickel hydroxide precipitate from a nickel-containing leach solution with impurities including one or more of the following: manganese, copper, zinc, iron and/or cobalt, so that the purified nickel hydroxide is suitable for pelletization with iron-containing ores and/or stainless steel production, includes treating the leach solution with a base to form a slurry of mixed hydroxide precipitate and low-nickel barren solution, thickening the slurry to form filter cake, washing the filter cake and contacting it with acid to dissolve nickel and other metals to produce a concentrated nickel-containing solution, subjecting the concentrated nickel-containing solution to solvent extraction with an organic acid extractant to remove metals other than nickel from the nickel-containing solution and form a solvent extraction raffinate of purified nickel solution and treating the solvent extraction raffinate with a base to precipitate the purified nickel hydroxide precipitate.
    Type: Grant
    Filed: September 23, 2008
    Date of Patent: April 3, 2012
    Assignee: Vale Inco Limited
    Inventors: Marc Murray Rishea, Indje Ognianov Mihaylov, Mohamed Buarzaiga, Flavia Dutra Mendes
  • Patent number: 8119011
    Abstract: Substitution of a single Ga-atom or single Ge-atom (GaAl12 and GeAl12 respectively) into the center of an aluminum Keggin polycation (Al13) produces an optimal water-treatment product for neutralization and coagulation of anionic contaminants in water. GaAl12 consistently shows ˜1 order of magnitude increase in pathogen reduction, compared to Al13. At a concentration of 2 ppm, GaAl12 performs equivalently to 40 ppm alum, removing ˜90% of the dissolved organic material. The substituted GaAl12 product also offers extended shelf-life and consistent performance. We also synthesized a related polyaluminum chloride compound made of pre-hydrolyzed dissolved alumina clusters of [GaO4Al12(OH)24(H2O)12]7+.
    Type: Grant
    Filed: February 11, 2009
    Date of Patent: February 21, 2012
    Assignee: Sandia Corporation
    Inventors: May D. Nyman, Thomas A. Stewart
  • Publication number: 20120037569
    Abstract: A method of removing mineral hardness of water comprises selecting a mineral hardness solubility constant modifier capable of at least partially precipitating insoluble mineral hardness material from water containing mineral hardness. A pressurized flow of the water containing mineral hardness is generated. The mineral hardness solubility constant modifier is added to the pressurized flow of water containing mineral hardness to form water bearing precipitate mineral hardness. The water bearing precipitate mineral hardness is filtered to at least partially remove the precipitated insoluble mineral hardness material from the water bearing precipitate mineral hardness to form post-filtered water.
    Type: Application
    Filed: August 16, 2011
    Publication date: February 16, 2012
    Inventor: David MORGAN
  • Publication number: 20120031850
    Abstract: Sulfate anions and divalent metal ions, such as magnesium, strontium and barium, in water are removed by treating the water with polyaluminum chloride, usually together with lime, to form ettringite and similar crystalline species which are readily removable by settling, filtration and the like. Iron is also removed by oxidation in a variation of the process. The process is particularly useful for treating aqueous solutions used in well treatment, where flowback fluids can provide some of the divalent metal ions necessary to form the ettringite-like materials, thus reducing the amount of lime otherwise necessary and further facilitating recycling of the fluid.
    Type: Application
    Filed: August 3, 2011
    Publication date: February 9, 2012
    Inventors: Kevin Smith, Jeffrey Snider, Jimmy Poindexter
  • Patent number: 8101085
    Abstract: Described is a process for treating an animal husbandry effluent slurry, such as hog manure, containing suspended solid particles. The process includes a) providing a liquid portion of the effluent, b) diluting the liquid to a Newtonian fluid, c) assuring the pH is under 10, d) adding to the fluid i) a soluble salt of alkaline earth metal (e.g. CaCl2) and ii) an insoluble basic salt of the same alkaline earth metal (e.g. CaCO3) to balance available cations and promote agglomeration of the suspended solid particles, e) adding a cationic coagulant to obtain a pre-treated destabilized colloid mixture with zero zeta potential value, and f) performing electroflotation to obtain a treated liquid and floated solids.
    Type: Grant
    Filed: May 8, 2008
    Date of Patent: January 24, 2012
    Assignee: Agriculture and Agri-Food Canada
    Inventors: Simon Guertin, Daniel Massé, François Lamarche
  • Patent number: 8101088
    Abstract: The present invention relates to a process for decontaminating aqueous media comprising organic contaminants. The process is targeted at reducing the COD and/or the TOC of an aqueous medium comprising organic molecules. It consists in subjecting the aqueous medium to an electron beam generated by an electron accelerator in the presence of a catalyst and in then removing the precipitates formed from the treated solution, said catalyst comprising a metal ion persulfate and optionally an Fe(II) salt or an Fe(III) salt.
    Type: Grant
    Filed: July 11, 2006
    Date of Patent: January 24, 2012
    Assignees: Centre National de la Recherche Scientifique, Universite de Poitiers
    Inventors: Nathalie Karpel Vel Leitner, Carole Catastini
  • Patent number: 8097168
    Abstract: A treatment method for wastewater employing sulfur dioxide and lime chemical dewatering technology in conjunction with an environmental photo biomass/algae biological treatment system growing photo biomass/algae to reduce dissolved solids, heavy metals, and ammonia in the wastewater to produce recovered treated wastewater for vegetation consumption, biofuel feedstock, and biofuel and carbon credits.
    Type: Grant
    Filed: June 4, 2009
    Date of Patent: January 17, 2012
    Assignee: Earth Renaissance Technologies, LLC
    Inventors: Marcus G. Theodore, Larry P. Wardle
  • Publication number: 20120006755
    Abstract: Provided is a process for efficiently removing an azole-type anticorrosive for copper from water containing the azole-type anticorrosive for copper, such as wastewater discharged from a CMP step in a fabrication process of a semiconductor device. Ferrous ions are added to water containing an azole-type anticorrosive for copper, and a resulting insoluble iron-azole complex is separated. After the insoluble iron-azole complex is separated, the remaining TOC components are subjected to ozonolysis. The azole-type anticorrosive for copper can be efficiently insolubilized in the form of an iron-azole complex using ferrous ions, and flocculation/solid-liquid separation can be performed. The water after removal of the insoluble matter formed by the addition of ferrous ions is water from which not only the azole-type anticorrosive for copper but also suspended solids have been removed.
    Type: Application
    Filed: October 21, 2009
    Publication date: January 12, 2012
    Applicant: KURITA WATER INDUSTRIES LTD.
    Inventors: Tomoharu Yasuike, Atsushi Nemoto
  • Patent number: 8062530
    Abstract: A method for neutralizing brines that contain high levels of silica accompanied with a high pH. Brine is processed through a reactor in which the pH is lowered and the resultant silica precipitate is adsorbed onto a sacrificial crystal structure. The resultant stream is then processed through a solids removal zone wherein the solids are removed and recovered for reuse. The neutralized solids-free brine is then suitable for down-hole injection in the heavy oil industry or further treatment by common water treatment methods if further adjustment is required for other industries.
    Type: Grant
    Filed: July 3, 2008
    Date of Patent: November 22, 2011
    Assignee: Aquatech International Corporation
    Inventors: Richard M. Schoen, Chandrakant Tiwari
  • Publication number: 20110272362
    Abstract: Oily and/or solids-containing water is clarified by chemical treatment to form flocculated and agglomerated solid phases and a clear water phase. In the clarification process, microbubbles of air or other gas are introduced at atmospheric pressure, via an eductor or other suitable device, together with a flocculant. During the subsequent formation of floes and their agglomeration into larger masses, microbubbles become entrained within and adhered to the solid flocculated materials. The resulting masses are very buoyant and easily separated from the water via a variety of approaches that include skimming, decanting, filtration, and screening. This process results in a solids phase that may be disposed of as waste, if desired, and a highly clarified water phase.
    Type: Application
    Filed: July 23, 2009
    Publication date: November 10, 2011
    Inventors: C. Steven Sikes, T. Daniel Sikes, Mark A. Hochwalt
  • Publication number: 20110271875
    Abstract: The present invention generally relates to processes for recovery of values from a fermentation mass obtained in producing ethanol. Further, the present invention relates to processes for the recovery of values from an inorganic- and lignin-containing mass. The present invention also relates to processes for the recovery of a fraction having enhanced silica content from a silica-containing mass. Still further, the present invention relates to processes for the recovery of crude ethanol from a fermentation mass. The present invention relates to various lignin-containing products and solutions and mineral-rich products.
    Type: Application
    Filed: May 4, 2011
    Publication date: November 10, 2011
    Applicant: ABENGOA BIOENERGY NEW TECHNOLOGIES, INC.
    Inventors: Aziz Ahmed, Quang A. Nguyen
  • Patent number: 8034158
    Abstract: There are provided a method of manufacturing an Fe/Ni-containing material having a low content of sulfur (S) from an Fe/Ni/SO4-containing liquid waste, a ferronickel mass using the Fe/Ni-containing material, and a method of manufacturing the ferronickel mass. The method of manufacturing an Fe/Ni-containing material from an Fe/Ni-containing liquid waste includes: removing SO4 from an Fe/Ni/SO4-containing liquid waste by adding an SO4 neutralizing agent to the liquid waste so that pH of the liquid waste can be maintained to a pH level of 0.5 to 2.5; precipitating Fe and Ni in the form of hydroxide [(Ni,Fe)(OH)] by adding NaOH to the SO4-free solution; washing the precipitate with water; and manufacturing an Ni/Fe-containing material by filtering and drying the washed Ni/Fe-containing sludge.
    Type: Grant
    Filed: May 15, 2008
    Date of Patent: October 11, 2011
    Assignee: Research Institute of Industrial Science & Technology
    Inventor: Jae Young Lee
  • Publication number: 20110239531
    Abstract: The object of the present invention is to provide a method for aggregating and separating algae dispersed in a liquid efficiently. According to the present invention, a method for aggregating and separating algae dispersed in a liquid, which comprises adding an alkaline inorganic aggregating agent to the liquid at pH of 2.0 to 4.0 in which algae are dispersed, followed by adding a cationic polymer aggregating agent, is provided. Further, according to the present invention, a method for producing biofuel utilizing algae is provided.
    Type: Application
    Filed: March 25, 2011
    Publication date: October 6, 2011
    Applicant: TOYOTA JIDOSHA KABUSHIKI KAISHA
    Inventors: Hiroshi URAYAMA, Minoru Kurata, Hiroaki Fukuda
  • Publication number: 20110215052
    Abstract: A process for recovering ionic liquids comprising the steps of: providing a first ionic liquid mixture, the first ionic liquid having a halogen metallate anion, the mixture containing an organic solvent; adjusting the pH of the mixture to pH 7-10 by the addition of a base to form a first precipitate; separating the first precipitate from the mixture; removing the organic solvent from the first mixture to form a second precipitate and separating the second precipitate from the first mixture; acidifying the resulting mixture to pH 2-7 by the addition of an acid; and drying the mixture to obtain a second ionic liquid having a halogen anion.
    Type: Application
    Filed: March 4, 2011
    Publication date: September 8, 2011
    Applicant: INSTITUTO MEXICANO DEL PETROLEO
    Inventors: Diego Javier Guzmán Lucero, Natalya Victorovna Likhanova, Rafael Martínez Palou, Eugenio Alejandro Flores Oropeza, Jorge Froylán Palomeque Santiago
  • Patent number: 8012358
    Abstract: A system is provided that includes: (a) a mobile platform; (b) an input pump operatively connected to be capable of pumping a treatment stream through the system; (c) a centrifugal separator operatively connected downstream of the input pump to centrifugally treat the treatment stream; (d) a borate filter operatively connected downstream of the centrifugal separator to filter the treatment stream capable of removing at least some of a borate when the treatment stream is at a pH of 8 or above; and (e) a chemical-additive subsystem operatively connected to be capable of: (i) selectively adding one or more chemical agents to the treatment stream upstream of the centrifugal separator, wherein the chemical agents can be selected to be capable of precipitating dissolved ions selected from the group consisting of: sulfate, calcium, strontium, or barium, magnesium, iron; and (ii) selectively adding a chemical agent to the treatment stream upstream of the borate filter to increase the pH of the treatment stream to 8 o
    Type: Grant
    Filed: August 26, 2010
    Date of Patent: September 6, 2011
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Billy F. Slabaugh, Arron L. Karcher, Michael J. R. Segura, Randy S. Rosine, Max L. Phillippi, Donna L. Harris
  • Publication number: 20110210076
    Abstract: The invention discloses a process to implement and maintain large water bodies with color, transparency, and cleanness characteristics similar to swimming pools or tropical seas, at low cost. The present invention also discloses a structure to contain large water bodies, comprising a system for the removal of impurities and surface oils by means of skimmers and a suction device to clean said structure.
    Type: Application
    Filed: March 30, 2011
    Publication date: September 1, 2011
    Applicant: CRYSTAL LAGOONS CORPORATION LLC
    Inventor: Fernando Benjamin FISCHMANN TORRES
  • Patent number: 7998439
    Abstract: A separation and recycling method for recycling uranium and fluoride from a waste liquid sequentially and separately is disclosed. The method comprises a uranium-recycling process and a fluoride-recycling process. In the uranium-recycling process, an alkali metal compound or monovalent cation and a coagulant aid are added into the waste liquid to promote the precipitation of uranium. In the fluoride-recycling process, an alkaline earth metal compound, a strong acid and a coagulant aid are added into the uranium-removed waste liquid to precipitate fluoride. By means of the method of the present invention, the uranium and fluoride contents of the uranium-removed and fluoride-removed waste liquid are compliant with the effluent standards of the environmental laws.
    Type: Grant
    Filed: December 29, 2009
    Date of Patent: August 16, 2011
    Assignee: Institute of Nuclear Energy Research
    Inventors: Chen-Te Lin, Kuo-Hao Tsao, Ben-Li Pen
  • Patent number: 7981295
    Abstract: Disclosed is an economical process for the purification of water containing soluble and sparingly soluble inorganic compounds using single-stage or two-stage membrane processes that integrate membrane water purification with chemical precipitation softening and residual hardness and silica removal from the membrane concentrates using ion exchange resins and silica sequestering media, respectively. The purified water recovery is not adversely affected by design and/or operational deficiencies in the chemical precipitation softening system that may result in higher residual hardness and silica in the supernatant from the clarifier.
    Type: Grant
    Filed: August 14, 2009
    Date of Patent: July 19, 2011
    Inventor: Riad A. Al-Samadi
  • Publication number: 20110163043
    Abstract: To provide a method for treating floor polish stripping wastewater and washing wastewater that is suitable for treating stripping wastewater produced in stripping with a strongly alkaline stripping agent when a floor polish coating film coated and formed on a floor surface is recoated and for treating washing wastewater produced in surface washing with a floor cleaner having neutral to alkaline properties during periodic or daily washing, this method making it possible to perform operations within a limited interval by treating wastewater within a short time and removing solids, thereby reducing environmental loads. A method for treating stripping wastewater or washing wastewater by which solid-liquid separation process can be performed within a short time and with good efficiency by adding a polyamidine polymer flocculant and converting aggregated particles into nonadhesive flocks of an appropriate size.
    Type: Application
    Filed: June 23, 2009
    Publication date: July 7, 2011
    Applicant: DIVERSEY, INC.
    Inventors: Satoshi Kayamori, Tetsuro Kondo, Susumu Komoda
  • Patent number: 7967990
    Abstract: A hybrid chemical/mechanical dewatering sewage treatment plant and method employing rapid sludge chemical dewatering technology in conjunction with slower conventional mechanical dewatering solids agglomeration and disposal methods to meet operating constraints and environmental permitting restrictions and siting limitations for disposal of sewage and wastewater.
    Type: Grant
    Filed: July 23, 2008
    Date of Patent: June 28, 2011
    Assignee: Earth Renaissance Technologies, LLC
    Inventor: Marcus G. Theodore
  • Patent number: 7967989
    Abstract: A sulfurous acid treated wastewater disposal method employing soil aquifer treatment (SAT) for artificial recharge of groundwater through infiltration basins allowing fully or partially-treated sewage effluent to infiltrate into the soil and move down to the groundwater through a “vadose” zone, which acts as a natural filter to remove essentially all suspended solids, biodegradable materials, bacteria, viruses, and other microorganisms.
    Type: Grant
    Filed: March 10, 2009
    Date of Patent: June 28, 2011
    Assignee: Earth Renaissance Technologies, LLC
    Inventors: Terry Gong, John Harmon, Marcus G. Theodore
  • Publication number: 20110147316
    Abstract: Methods of deoiling oily water such as SAGD and frac produce water. The oily water is treated with a natural coagulant selected from tannins and chitosan. A cationic and/or anionic flocculant may also be added to the treated oily water. The thus treated oily water may be subjected to conventional mechanical oil separation techniques such as hydrocyclonic separation, dissolved air flotation, entrapped air flotation, induced gas flotation, gravity filters, reverse osmosis filters, API, or Voraxial® bulk separators and the like.
    Type: Application
    Filed: December 18, 2009
    Publication date: June 23, 2011
    Applicant: General Electric Company
    Inventors: David M. Polizzotti, Abdul Rafi Khwaja
  • Publication number: 20110127223
    Abstract: A process for the treatment of phosphoric acid plant pond water where an increased recovery of phosphorus values from the input pond water is achieved through the dilution of the initial pond water with clarified water from the product generation stage and/or the final stage clarified water. The recycle of the product generation stage and/or final stage waters to dilute the feed pond water mitigates or eliminates the problems of silica gel formation and precipitation that occur when undiluted pond waters are processed. In addition, the dilution reduces phosphate losses in the first liming or neutralization stage rejected solids thereby increasing the yield of Di-Calcium Phosphate or ammonium magnesium phosphate or potassium magnesium phosphates.
    Type: Application
    Filed: November 24, 2010
    Publication date: June 2, 2011
    Applicant: VEOLIA WATER NORTH AMERICA OPERATING SERVICES, LLC
    Inventors: Vaughn V. Astley, Dennis H. Michalski, Robert Cook
  • Publication number: 20110114568
    Abstract: A wastewater treatment system includes a chemical treatment process tank for receiving and chemically treating wastewater. The wastewater treatment system also includes a blending system for receiving and activating a flocculating agent such as a polymer. The wastewater treatment system further includes a static mixer for introducing the flocculating agent into the wastewater and for promoting flocculation of the wastewater as the wastewater flows from the chemical treatment process tank to a clarification tank.
    Type: Application
    Filed: July 27, 2009
    Publication date: May 19, 2011
    Inventors: Brian D. Mize, Joe B. Downing
  • Patent number: 7943739
    Abstract: A method for precipitating casein from a suspension comprising milk is disclosed. The method includes the following steps: adding a phosphate solution to a suspension; mixing the phosphate solution with the suspension to form a mixture having a phosphate concentration greater or equal to 40 mM; freezing the mixture having a phosphate concentration greater or equal to 40 mM to obtain a frozen mixture; and thawing the frozen mixture to obtain casein-containing aggregates in the mixture, in which the phosphate solution is buffered at a pH value of no less than 4.4.
    Type: Grant
    Filed: February 20, 2008
    Date of Patent: May 17, 2011
    Assignee: Animal Technology Institute Taiwan
    Inventors: Chon-Ho Yen, Shou-Lun Lee, Mei-Yun Chen, Yin-Shen Lin, Xin-Hui Huang, Chen Hwang Shih, Hsiu-Fen Tai
  • Patent number: 7935261
    Abstract: A method is provided of recycling and cleaning up oil-based waste drilling mud and cuttings contaminated with oil-based waste drilling mud. A facility for performing the method is also provided. The method includes removing the coarse solids from the mud, breaking the emulsion, separating the hydrophobic phase from the water phase and the solid phase, vaporizing all residual oil and water from the solids, and burning off the vaporized oil. The method produces a solid “soil” product that is free from oil contamination, an oil product that is fit for reuse, and clean air emissions. A thermal desorber can be used to efficiently vaporize the oil at low temperature. Optionally the water fraction of the mud can be vaporized, solutes and salts can be captured as evaporite and then be mixed with the soil product. The method has the unique advantage of producing no persistent hazardous waste.
    Type: Grant
    Filed: November 24, 2008
    Date of Patent: May 3, 2011
    Assignee: Arkansas Reclamation Company, LLC
    Inventors: Thomas P. Jones, Richard T. Davis, Charles R. Richesin
  • Patent number: 7931822
    Abstract: Methods and compositions utilizing aluminum, magnesium, and calcium-based additives for the treatment and neutralization of wastewater are described for removing contaminants from wastewater, including reducing phosphorous-containing compounds, total suspended solids (TSS), biological oxygen demand (BOD), fats, oils, and greases (FOG), and total Kjedahl nitrogen (TKN) are described. Methods and compositions to control pH, sulfur and sodium loads present in wastewater and precipitatable solids are described. Concentrations of aluminum, magnesium, and calcium-based additives are maintained at mass action concentrations to the wastewater component levels present in the wastewater and bracketed approximately +/?0.5 pH units about the pK value of the soluble, buffering species.
    Type: Grant
    Filed: March 1, 2007
    Date of Patent: April 26, 2011
    Assignee: Inland Environmental Resources, Inc.
    Inventors: Douglas G. Kelley, Richard A. Handley
  • Patent number: 7906028
    Abstract: Hydraulic cement compositions that include a carbonate compound composition, e.g., a salt-water derived carbonate compound composition containing crystalline and/or amorphous carbonate compounds, are provided. Also provided are methods of making and using the hydraulic cements, as well as settable compositions, such as concretes and mortars, prepared therefrom. The cements and compositions produced therefrom find use in a variety of applications, including use in a variety of building materials and building applications.
    Type: Grant
    Filed: February 4, 2010
    Date of Patent: March 15, 2011
    Assignee: Calera Corporation
    Inventors: Brent R Constantz, Cecily Ryan, Laurence Clodic
  • Publication number: 20110042320
    Abstract: Systems and methods for treating contaminated water from gas wells by adding an inorganic coagulant and a low molecular weight polymer to the contaminated water to increase the size of solid particulates in the water and to thereby allow the solid particulates to be filtered or to otherwise be removed from the water are disclosed herein. While the inorganic coagulant can be any suitable coagulant, in some cases the coagulant is selected from aluminum chlorohydrate, polyaluminum chloride, aluminum sulfate, and ferric sulfate. Similarly, the polymer can comprise any suitable polymer, such as epi/dma, a condensation product of epichlorohydrin and dimethyl amine. The described systems and methods can clean the contaminated water so that the water can then be treated in a variety of other manners, which may include reverse osmosis, deionization, treatment with mixed bed deionizers, electro-separation, fraction distillation, distillation, and other suitable water cleansing processes.
    Type: Application
    Filed: August 18, 2010
    Publication date: February 24, 2011
    Applicant: WATER SOLUTIONS, INC.
    Inventor: Stephen D. Allen
  • Publication number: 20110042319
    Abstract: The invention relates to a method for processing sludge, comprising the addition of a lime-based basic agent to a sludge having a first pH value in order to raise the pH to a second value higher than the first one, adding at least one anionic organic flocculating agent that is active at said second pH value, flocculating the sludge, and separating the flocculated sludge between dehydrated sludge and a liquid phase, wherein the sludge to be dehydrated has a first above-mentioned pH value lower than 9, while the lime-based basic agent induces said pH raise to said above-mentioned second value within less than 5 minutes. The invention also relates to a composition for implementing said processing.
    Type: Application
    Filed: November 13, 2007
    Publication date: February 24, 2011
    Inventor: Marc Joseph, Henri Remy
  • Publication number: 20110031130
    Abstract: Method for purifying an aqueous composition by removing silicon therefrom, according to which a compound comprising aluminum is added to the aqueous composition in order to obtain a molar aluminum content greater than the molar silicon content in said composition, the pH of the composition is controlled and maintained at a value higher than or equal to 8 and lower than or equal to 10, and the precipitate formed is separated from the aqueous suspension obtained.
    Type: Application
    Filed: April 27, 2009
    Publication date: February 10, 2011
    Applicant: SOLVAY (SOCIETE ANONYME)
    Inventor: Alessandra Pastacaldi
  • Publication number: 20110024360
    Abstract: Methods and compositions utilizing aluminum, magnesium, and calcium-based additives for the treatment and neutralization of wastewater are described for removing contaminants from wastewater, including reducing phosphorous-containing compounds, total suspended solids (TSS), biological oxygen demand (BOD), fats, oils, and greases (FOG), and total Kjedahl nitrogen (TKN) are described. Methods and compositions to control pH, sulfur and sodium loads present in wastewater and precipitatable solids are described. Concentrations of aluminum, magnesium, and calcium-based additives are maintained at mass action concentrations to the wastewater component levels present in the wastewater and bracketed approximately +/?0.5 pH units about the pK value of the soluble, buffering species.
    Type: Application
    Filed: October 6, 2010
    Publication date: February 3, 2011
    Applicant: INLAND ENVIRONMENTAL RESOURCES, INC.
    Inventors: Douglas G. Kelley, Richard A. Handley
  • Patent number: 7867399
    Abstract: A method is provided of recycling and decontaminating oil-based waste drilling mud and cuttings contaminated with oil-based waste drilling mud. A facility for performing the method is also provided. The method includes removing the coarse solids from the mud, breaking the emulsion, and separating the hydrophobic phase from the water phase and the solid phase. The solids may then be treated by either or both of two approaches. One approach involves vaporizing all residual oil and water from the solids, and burning off the vaporized oil. Another approach involves at least partially vaporizing the residual oil from the solids and recondensing the oil. The method produces a solid “soil” product that is free from oil contamination (or is sufficiently decontaminated to allow reuse), an oil product that is fit for reuse, and clean air emissions. A thermal desorber or a soil dryer can be used to efficiently vaporize the oil at low temperature.
    Type: Grant
    Filed: October 30, 2009
    Date of Patent: January 11, 2011
    Assignee: Arkansas Reclamation Company, LLC
    Inventors: Thomas P. Jones, Charles R. Richesin, Richard T. Davis
  • Publication number: 20100319923
    Abstract: A system is provided that includes: (a) a mobile platform; (b) an input pump operatively connected to be capable of pumping a treatment stream through the system; (c) a centrifugal separator operatively connected downstream of the input pump to centrifugally treat the treatment stream; (d) a borate filter operatively connected downstream of the centrifugal separator to filter the treatment stream capable of removing at least some of a borate when the treatment stream is at a pH of 8 or above; and (e) a chemical-additive subsystem operatively connected to be capable of: (i) selectively adding one or more chemical agents to the treatment stream upstream of the centrifugal separator, wherein the chemical agents can be selected to be capable of precipitating dissolved ions selected from the group consisting of: sulfate, calcium, strontium, or barium, magnesium, iron; and (ii) selectively adding a chemical agent to the treatment stream upstream of the borate filter to increase the pH of the treatment stream to 8 o
    Type: Application
    Filed: August 26, 2010
    Publication date: December 23, 2010
    Inventors: Billy F. Slabaugh, Arron L. Karcher, Michael J.R. Segura, Randy S. Rosine, Max L. Phillippi, Donna L. Harris
  • Patent number: 7824552
    Abstract: A system is provided that includes: (a) a mobile platform; (b) an input pump operatively connected to be capable of pumping a treatment stream through the system; (c) a centrifugal separator operatively connected downstream of the input pump to centrifugally treat the treatment stream; (d) a borate filter operatively connected downstream of the centrifugal separator to filter the treatment stream capable of removing at least some of a borate when the treatment stream is at a pH of 8 or above; and (e) a chemical-additive subsystem operatively connected to be capable of: (i) selectively adding one or more chemical agents to the treatment stream upstream of the centrifugal separator, wherein the chemical agents can be selected to be capable of precipitating dissolved ions selected from the group consisting of: sulfate, calcium, strontium, or barium, magnesium, iron; and (ii) selectively adding a chemical agent to the treatment stream upstream of the borate filter to increase the pH of the treatment stream to 8 o
    Type: Grant
    Filed: September 5, 2007
    Date of Patent: November 2, 2010
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Billy F. Slabaugh, Arron L. Karcher, Michael J. R. Segura, Randy S. Rosine, Max L. Phillippi, Donna L. Harris
  • Patent number: 7820057
    Abstract: The invention relates to a method for removing at least one constituent from a solution, comprising:—forming a liquid mixture by bringing together said solution (1) and a particulate seed material (6) under conditions or in the presence of one or more substances which cause the constituent to be removed to crystallize out on the surface of the seed material; and—separating the seed material having the constituent to be removed crystallized out thereon from the liquid mixture by passing the liquid mixture through a filter (3), wherein the pore size of the filter (3) is greater than or equal to the particle size of the seed material (6). The invention also relates to a method for preparing a particulate material wherein use is made of the method according to the present invention. The invention also relates to the particulate material obtainable by this method. The invention further relates to an apparatus that can be used in the process of the present invention.
    Type: Grant
    Filed: October 8, 2004
    Date of Patent: October 26, 2010
    Assignee: Nederlandse Organisatie voor toegepastnatuurwetenschappelijk Onderzoek TNO
    Inventors: Dirk Verdoes, Johannes van der Meer, Earl Lawrence Vincent Goetheer
  • Patent number: 7799232
    Abstract: A reducing water purification material having a reducing iron-based precipitate selected from green rust, iron ferrite, reducing iron hydroxide, and a mixture thereof. A wastewater treatment process having steps of adding a reducing iron compound to wastewater, leading the wastewater to which the reducing iron compound is added to a reaction tank and forming a precipitate, separating the formed precipitate by a solid-liquid separation to obtain a sludge, and alkalinizing all or a portion of the separated sludge to form an alkaline sludge followed by returning to the reaction tank, wherein in the precipitation step, the wastewater to which the reducing iron compound is added and the alkaline sludge are mixed and are allowed to react in a non-oxidizing atmosphere under alkaline condition to form a reducing iron compound precipitate as the precipitate, thereby incorporating contaminants in the precipitate to remove the contaminants from the wastewater.
    Type: Grant
    Filed: July 31, 2009
    Date of Patent: September 21, 2010
    Assignee: Mitsubishi Materials Corporation
    Inventors: Hiroshi Hayashi, Hitoshi Takeuchi, Hajime Negishi, Shigeyuki Tsuzaki, Yoshio Aikawa, Ayako Mimoto, Shintaro Nakaya
  • Patent number: 7794604
    Abstract: The invention relates to a method for removing lignin from an aqueous solution. It is accomplished by adding a calcium compound and an aluminium compound to said solution. Said calcium compound is preferably calcium chloride and said aluminium compound is preferably a polymeric aluminium hydroxide salt.
    Type: Grant
    Filed: July 8, 2005
    Date of Patent: September 14, 2010
    Assignee: Kemira Oyj
    Inventors: Heikki Palonen, Arja Paloniemi, Reetta Taittonen, Päivi Rousu
  • Patent number: 7767092
    Abstract: A method of decolorizing a colored effluent comprising (i) a colored substance; and (ii) a polyvalent carboxylic acid or a polyvalent aminocarboxylic acid, the method including the steps of: (a) controlling a hydrogen ion exponent (pH) of the colored effluent to be in a range in which two or more carboxylic acid groups in the polyvalent carboxylic acid or the polyvalent aminocarboxylic acid does not dissociate; (b) adding an inorganic metal salt to the colored effluent so as to allow the inorganic metal salt to react with the colored substance to form a precipitation in the colored effluent, and (c) eliminating the precipitation from the colored effluent.
    Type: Grant
    Filed: October 4, 2007
    Date of Patent: August 3, 2010
    Assignee: Konica Minolta Business Technologies, Inc.
    Inventors: Eiichi Yoshida, Masahiko Nakamura, Kaori Soeda
  • Publication number: 20100155337
    Abstract: The present invention discloses a process of treating ternary combination flooding sewage, in particular, comprising treating the ternary combination flooding sewage after oil-water separation process in the following steps in order: (1) adding 1000-6000 mg/l pH regulator into the sewage to regulate pH to 5.0-7.5; ) (2) adding 500-5000 mg/l coagulant into the sewage; (3) adding 100-1000 mg/l organic flocculant into the sewage; (4) standing the sewage to deposit and separating out floccus from the sewage; and (5) filtering the sewage by delivering it to a known filtration device; the steps(1), (2) and (3) are always carried out under stirring and the added agents are maintained to be sufficiently mixed with the sewage. The effect of the present invention is that the process can treat the ternary combination flooding sewage which is extremely difficult to treat so as to meet the standard, and that the process has been put into the industrialized pilot with a treating capacity of 5000 m3/day.
    Type: Application
    Filed: December 18, 2008
    Publication date: June 24, 2010
    Applicants: HIGH GRADE TECHNOLOGY CO., LTD., DAQING DAFENG OILFIELD TECHNOLOGY CO., LTD.
    Inventors: Yanming GAO, Xingyu Liu, Shu-nan Gong
  • Publication number: 20100150818
    Abstract: A process and method for liquid-solid separation in raw water by chemical treatment, comprising adding into the water, separately or together, an effective amount of at least one aluminum polymer with an effective amount of an ammonium polymer, including at least one medium, high, or very high molecular weight ammonium polymer, to clarify said raw water to a settled turbidity standard, and including methods for blending and storing solution polymers.
    Type: Application
    Filed: February 10, 2010
    Publication date: June 17, 2010
    Inventor: Richard Alan Haase
  • Patent number: 7713419
    Abstract: A method and construction for treatment of sludge from waterworks and wastewater treatment plants is disclosed. The method for treatment of sludge from waterwork or wastewater treatment plant, comprising precipitated inorganic chemical coagulants and precipitated organic substances, comprises adding an acid to the sludge in such a way that a first sludge mixture with low pH is received. The first sludge mixture includes the inorganic chemical coagulants in solution and the organic substances. The sludge mixture is pumped, via heat exchangers to a pressure tank. An obtained first concentrate is fed to at least one membrane filtration process in which a second concentrate and a first permeate are obtained.
    Type: Grant
    Filed: November 18, 2004
    Date of Patent: May 11, 2010
    Assignee: Feralco AB
    Inventor: Hans David Ulmert
  • Patent number: 7713416
    Abstract: A process for transforming sludge into NPK type granulated fertilizer in which the energy consume is reduced a 90% thanks to the addition of a special filtration step in which the water content is reduced a 50% and the remaining water is evaporated by the exothermic reaction occurring in the process. Additionally, the process of the present invention includes mechanisms that allow some of the by products generated by some of the reactions, to adsorb crystallization water and reduce the humidity of the mass without using external energy.
    Type: Grant
    Filed: August 25, 2006
    Date of Patent: May 11, 2010
    Assignee: Chemical Biosolids Inc.
    Inventor: José Cabello-Fuentes
  • Publication number: 20100072142
    Abstract: A system and method that uses mature floc as seed particles to promote aggregation in a water treatment process is provided. The seed particles do not need to be recovered as they separate out with the waste steam after a spiral separation. One implementation is to prepare the mature floc off-line and inject periodically into the buffer tank, as needed. Another implementation is to tap into the more mature floc downstream and feedback, as needed, to the buffer tank.
    Type: Application
    Filed: September 19, 2008
    Publication date: March 25, 2010
    Applicant: PALO ALTO RESEARCH CENTER INCORPORATED
    Inventors: Meng H. Lean, Armin R. Volkel, Ashutosh Kole, Jeonggi Seo
  • Patent number: 7666311
    Abstract: Among flocculating agents reacting in a neutral region and also leaving treated water also in neutral region, a flocculating agent is proposed, which can be used simply and may carry out effective cleaning of mud water in particular. A flocculating agent is proposed, which is a flocculating agent in powder form and exhibiting a pH of 5 to 9 when added to pure water, containing in a mixed state an acidic powder comprising porous particles obtained by adsorbing a metal constituent and an alkaline powder comprising porous particles obtained by adsorbing calcium phosphate.
    Type: Grant
    Filed: December 25, 2006
    Date of Patent: February 23, 2010
    Assignees: Eccera Co., Ltd.
    Inventors: Sanai Fujita, Kazuhiro Fujita
  • Publication number: 20100038318
    Abstract: A method of cleaning drilling fluid including providing a flow of drilling fluid to a treatment loop, determining a flow rate of the drilling fluid, and injecting a polymer into the drilling fluid based on the determined flow rate of the drilling fluid. Additionally, the method includes injecting a coagulant into the drilling fluid based on the determined flow rate of the drilling fluid and adjusting the rate of polymer and coagulant injection based on a change in the flow rate of the drilling fluid. Also, a method of controlling a drilling fluid cleaning system, the method including inputting a polymer dosage rate and a coagulant dosage rate into a system controller and providing instructions to the system controller.
    Type: Application
    Filed: August 10, 2009
    Publication date: February 18, 2010
    Applicants: M-I L.L.C., M-I DRILLING FLUIDS CANADA, INC.
    Inventors: Alan Gilmour, Nicolas Christopher Wade Thiessen
  • Patent number: 7655145
    Abstract: Method and system for processing of a liquid (“contaminant liquid”) containing water and containing urine and/or other contaminants in a two step process. Urine, or a contaminated liquid similar to and/or containing urine and thus having a relatively high salt and urea content is passed through an activated carbon filter to provide a resulting liquid, to remove most of the organic molecules. The resulting liquid is passed through a semipermeable membrane from a membrane first side to a membrane second side, where a fortified drink having a lower water concentration (higher osmotic potential) than the resulting liquid is positioned. Osmotic pressure differential causes the water, but not most of the remaining inorganic (salts) contaminant(s) to pass through the membrane to the fortified drink. Optionally, the resulting liquid is allowed to precipitate additional organic molecules before passage through the membrane.
    Type: Grant
    Filed: September 28, 2006
    Date of Patent: February 2, 2010
    Assignee: United States Government as represented by the Administrator of the National Aeronautics and Space Administration (NASA)
    Inventors: Sherwin J. Gormly, Michael T. Flynn