Etching Of Substrate Containing At Least One Compound Having At Least One Oxygen Atom And At Least One Metal Atom Patents (Class 216/76)
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Patent number: 6287476Abstract: A method to form a passivation layer using an electrochemical process over a MR Sensor so that the passivation layer defines the MR track width. The passivation layer is formed by anodizing the MR sensor. The passivation layer is an electrical insulator (preventing Sensor current (I) from shunting through the overspray) and a heat conductor to allow MR heat to dissipate away from the MR sensor through the overspray. The method comprises: forming a passivation layer on the MR sensor; the passivation layer formed using an electrochemical process. Then we spinning-on and printing a lift-off photoresist structure over the passivation layer. The passivation layer is etched to remove the passivation layer not covered by the lift-off structure thereby defining a track width of the MR sensor. Then we deposit a lead layer over the passivation layer and MR sensor. The lift-off structure is removed where by the passivation layer defines a track width.Type: GrantFiled: June 14, 1999Date of Patent: September 11, 2001Assignee: Headway Technologies, Inc.Inventors: Kochan Ju, Shou-Chen Kao, Cherng-Chyi Han, Jei-Wei Chang, Mao-Min Chen
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Publication number: 20010009249Abstract: A metal etching process. A glue/barrier layer, a metal layer and an anti-refeletion layer are formed on a substrate. A three-stage etching step is performed. A break through step of etching is performed to pattern the glue/barrier layer. A main etching step is performed on the metal layer with chlorine, boron trichloride, and trifluoro-methane as etching gases. The trifluoro-methane is advantageous to produce a polymer during etching, so that the profile of the metal layer appears atilt. An over-etching step is then performed to ensure an insulation between neighboring wiring lines.Type: ApplicationFiled: March 23, 2001Publication date: July 26, 2001Inventors: Wen-Pin Kuo, Yueh-Feng Ho, Jy-Hwang Lin
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Publication number: 20010008227Abstract: Dry etching of a metal oxide film exposed without being coated with a photoresist is carried out with plasma of a gas obtained by mixing hydrogen iodide with at least one gas selected from the group consisting of a group consisting of fluorine gas and fluorine-based compound gases and a group consisting of nitrogen gas and nitrogen-based compound gases, and then after the exposing of the above mentioned photoresist film to plasma of oxygen gas, the remaining photoresist film is removed by etching with plasma of a gas obtained by mixing oxygen gas with at least one gas selected from the group consisting of a group consisting of fluorine gas and fluorine-based compound gases and a group consisting of nitrogen gas and nitrogen-based compound gases.Type: ApplicationFiled: August 4, 1998Publication date: July 19, 2001Inventors: MITSURU SADAMOTO, NORIYUKI YANAGAWA, SATORU IWAMORI, KENJU SASAKI
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Patent number: 6255221Abstract: Disclosed are methods and systems for etching dielectric layers in a high density plasma etcher. A method includes providing a wafer having a photoresist mask over a dielectric layer in order to define at least one contact via hole or open area that is electrically interconnected down to the silicon substrate of the wafer. The method then proceeds to inserting the wafer into the high density plasma etcher and pulsed application a TCP power source of the high density plasma etcher. The pulsed application includes ascertaining a desired etch performance characteristic, which includes photoresist selectivity and etch rate which is associated with a continuous wave application of the TCP source. Then, selecting a duty cycle of the pulsed application of the TCP source and scaling a peak power of the pulsed application of the TCP source in order to match a cycle-averaged power that would be delivered by the continuous wave application of the TCP source.Type: GrantFiled: December 17, 1998Date of Patent: July 3, 2001Assignee: Lam Research CorporationInventors: Eric A. Hudson, Jaroslaw W. Winniczek, Joel M. Cook, Helen L. Maynard
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Patent number: 6251796Abstract: A method for fabrication of ceramic tantalum nitride and improved structures based thereon is disclosed. According to the disclosed method, an ionized metal plasma (“IMP”) tool is used to create a plasma containing tantalum ions where the plasma is sustained by a mixture of nitrogen and argon gases. The percentage of nitrogen partial flow in the mixture of gases is adjusted so as to result in a layer of tantalum nitride with a nitrogen content of at least 30%. With a nitrogen content of at least 30%, the tantalum nitride becomes ceramic. The ceramic tantalum nitride presents a number of advantages. For example, the fabrication of ceramic tantalum nitride can be easily incorporated into fabrication of semiconductor chips using copper as the interconnect metal. Also, ceramic tantalum nitride can be used as an effective etch stop layer.Type: GrantFiled: February 24, 2000Date of Patent: June 26, 2001Assignee: Conexant Systems, Inc.Inventors: Hadi Abdul-Ridha, David T. Young, Maureen R. Brongo
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Patent number: 6251793Abstract: A plasma processing chamber includes a substrate holder and a member of silicon nitride such as a liner, focus ring or a gas distribution plate, the member having an exposed surface adjacent the substrate holder and the exposed surface being effective to minimize particle contamination during processing of substrates. The chamber can include an antenna which inductively couples RF energy through the gas distribution plate to energize process gas into a plasma state.Type: GrantFiled: June 9, 1999Date of Patent: June 26, 2001Assignee: Lam Research CorporationInventors: Thomas E. Wicker, Robert A. Maraschin
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Patent number: 6174448Abstract: A method of removing a diffusion aluminide coating on a component designed for use in a hostile environment, such as superalloy turbine, combustor and augmentor components of a gas turbine engine. The method selectively removes an aluminide coating by stripping aluminum from the coating without causing excessive attack, alloy depletion and gross thinning of the underlying superalloy substrate. Processing steps generally include contacting the coating with a mixture that contains a halogen-containing activator and a metallic powder containing an aluminide-forming metal constituent, such as by pack cementation-type process. The mixture is then heated to a temperature sufficient to vaporize the halogen-containing activator and for a duration sufficient to cause the halogen-containing activator to provide a transfer mechanism for the removal of aluminum from at least a portion of the diffusion aluminide coating, while the metallic powder absorbs the removed aluminum.Type: GrantFiled: March 2, 1998Date of Patent: January 16, 2001Assignee: General Electric CompanyInventors: Nripendra N. Das, Howard J. Farr, Raymond W. Heidorn
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Patent number: 6171511Abstract: The invention relates to a process for thermal etching under oxidizing conditions of a ceramic, more particularly with the aim of revealing its grain boundaries and for the study of its granular microstructure. The invention applies to technical and nuclear ceramics and in particular UO2 and to (U, Pu) O2 mixtures. The thermal etching is performed in a furnace or kiln under a controlled atmosphere constituted by an oxidizing gas supplying a chemical oxygen potential of −75 to −125 kJ/mole and comprises the following successive stages: rapid rise in the temperature of the furnace to a rate of 900 to 1500° C./h from the initial temperature to a temperature plateau, maintaining the temperature at said plateau at a value of 1250 to 1450° C. for between 30 and 15 minutes, lowering the temperature to the final temperature.Type: GrantFiled: October 21, 1998Date of Patent: January 9, 2001Assignees: Commissariat a l'Energie Atomique, Compagnie Generale des Matieres NucleairesInventors: François Charollais, Mireille Bauer, Michel Coster, Pascal Piluso, Claude Fort
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Patent number: 6143191Abstract: A method of forming an iridium-based electrode structure on a substrate, from an iridium-containing precursor thereof which is decomposed to deposit iridium on the substrate. The iridium-based material is formed on the substrate in a desired environment, e.g., an oxidizing ambient environment which may for example contain an oxidizing gas such as oxygen, ozone, air, or nitrogen oxide, or alternatively a reducing environment containing a reducing agent such as H.sub.2, CO or NH.sub.3. The iridium deposited on the substrate is contacted with an etching reagent such as halogen-based etch species (e.g., Cl.sub.2, Br.sub.2, F.sub.2, CCl.sub.4, Si.sub.2 F.sub.6, SiCl.sub.4, NF.sub.3, C.sub.2 F.sub.6, SF.sub.6, or CF.sub.4) formed by exposing halogen to light, laser radiation, plasma, or ion beam, or alternatively with XeF.sub.2, for sufficient time and under sufficient conditions to etch the deposited iridium-based material and form the etched iridium-based electrode structure.Type: GrantFiled: November 10, 1997Date of Patent: November 7, 2000Assignee: Advanced Technology Materials, Inc.Inventors: Thomas H. Baum, Frank Dimeo, Jr.
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Patent number: 6046116Abstract: A method for minimizing the critical dimension growth of a feature on a semiconductor wafer includes performing an etch operation in a reactor 20 and controlling the temperature of the wafer 26 by controlling the pressure of the gas contacting the backside of the wafer 26 and/or providing a heat source 56 such as for example in the chuck 46 or electrode 28 associated with the wafer 26 in order to heat the wafer 26.Type: GrantFiled: November 19, 1997Date of Patent: April 4, 2000Assignee: Tegal CorporationInventors: Stephen P. DeOrnellas, Alfred Cofer, Leslie G. Jerde, Kurt A. Olson, Paritosh Rajora
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Patent number: 6036876Abstract: An etch method includes providing a material layer consisting essentially of a group member selected from the group consisting of an indium oxide (InO), a tin oxide (SnO), a mixture of indium and tin oxides, a compound of indium and of tin and of oxygen having the general formulation In.sub.x Sn.sub.y O.sub.z where z is substantially greater than zero but less than 100% and where the sum x+y fills the remainder of the 100%, and a mixture of the preceding ones of the group members. A reactive gas including a halogen-containing compound and an oxygen-containing compound is supplied to a vicinity of the material layer. Also, an electric field is supplied to react the supplied reactive gas with the material layer so as to form volatile byproducts of reactive gas and the material layer.Type: GrantFiled: June 25, 1997Date of Patent: March 14, 2000Assignee: Applied Komatsu Technology, Inc.Inventors: Jie Chen, Yuen-Kui Wong
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Patent number: 6027660Abstract: A method of patterning a ceramic slider by plasma etching is disclosed. The ceramic slider contains alumina and titanium carbide. The method includes the steps of forming an etch pattern by depositing and developing a photoresist on the ceramic slider, and reactive ion etching a first surface on the ceramic slider using an etchant gas. The etchant gas generally includes argon, and a fluorine containing gas. The power source density, during etching ranges from about 0.5 W/(cm.sup.2) to 8 W/(cm.sup.2). Another aspect of the invention is a ceramic slider resulting from the method of the invention having a smoothness ranging from about 20 to 300 .ANG. as measured by atomic force microscopy.Type: GrantFiled: May 11, 1998Date of Patent: February 22, 2000Assignee: International Business Machines CorproationInventors: Richard Hsiao, Cherngye Hwang, Son Van Nguyen, Diana Perez
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Patent number: 6022485Abstract: A catalytic method and an apparatus for selectively removing material from a solid substrate is provided. The method comprises contacting a surface of a solid substrate with a catalyst material in the presence of a reactant under conditions effective to selectively remove material from those areas of said solid substrate in contact with said catalyst material and said reactant.Type: GrantFiled: October 17, 1997Date of Patent: February 8, 2000Assignee: International Business Machines CorporationInventor: Roger W. Cheek
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Patent number: 6019906Abstract: A method for forming a patterned microelectronics layer within a microelectronics fabrication. There is first provided a substrate employed within a microelectronics fabrication. There is then formed over the substrate an oxygen containing plasma etchable microelectronics layer. There is then formed upon the oxygen containing plasma etchable microelectronics layer a hard mask layer. There is then formed upon the hard mask layer a patterned photoresist layer. There is then etched through use of a first anisotropic plasma etch method the hard mask layer to form a patterned hard mask layer while employing the patterned photoresist layer as a first etch mask layer. The first anisotropic plasma etch method employs an etchant gas composition appropriate for etching a hard mask material from which is formed the hard mask layer.Type: GrantFiled: May 29, 1998Date of Patent: February 1, 2000Assignee: Taiwan Semiconductor Manufacturing CompanyInventors: Syun-Ming Jang, Ming-Hsin Huang
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Patent number: 6010635Abstract: The plasma descaling process of the present invention removes surface oxides selectively from structural metal surfaces, especially titanium and its alloys, and, with appropriate control of the reaction temperature, is self-limiting to avoid cracking problems otherwise associated with intergranular attack. In a preferred embodiment of the present invention, a fluoride plasma reacts with surface oxides on a titanium alloy to remove scale and alpha case in a temperature controlled chamber without attacking the underlying crystalline metal to cause intergranular attack. Properly controlled by regulating the chamber temperature, the plasma reaction terminates when the plasma has removed the surface oxides and encounters the underlying crystalline metal. The product is a metal surface free of scale and alpha case and free of intergranular attack. The plasma descaling process replaces conventional metal finishing processes, such as chemical milling or etching.Type: GrantFiled: November 21, 1997Date of Patent: January 4, 2000Assignee: The Boeing CompanyInventors: Herbert S. Goode, Jr., Jean A. Nielsen, Larry E. Nitzsche
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Patent number: 6008135Abstract: A method for etching a metal layer of a semiconductor device is provided. A metal layer formed on a substrate is etched using a hard mask and a mixed etching gas containing chlorine and oxygen in which the ratio of oxygen gas is preferably about 0.5-0.8. Under such conditions, a metal layer pattern of a fine profile is formed. Since the hard mask is thin, it is possible to prevent etch reactants generated in a process of etching the metal layer from being deposited on the side surface of the resultant formed of the metal layer pattern and the hard mask. As a result, no additional processing is required to remove the etch reactants from the side surfaces and the metal layer etching process is simplified.Type: GrantFiled: August 26, 1998Date of Patent: December 28, 1999Assignee: Samsung Electronics Co., Ltd.Inventors: Sang-Jeong Oh, Yong-tak Lee
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Patent number: 6001268Abstract: The invention is a method of patterning the air bearing surface of a ceramic slider preferably including alumina and titanium carbide. The method includes the steps of forming an etch pattern by depositing and developing a photoresist on the ceramic slider, and reactive ion etching the slider air bearing surface using an etchant gas of argon, sulfur hexafluoride, and methyltrifluoride flowing at a rate which provides a smooth patterned surface on the slider air bearing surface.Type: GrantFiled: June 5, 1997Date of Patent: December 14, 1999Assignee: International Business Machines CorporationInventors: Son Van Nguyen, Diana Perez, Andrew Chiuyan Ting, Cherngye Hwang, Martin Straub, Gerd Dworschak
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Patent number: 5996212Abstract: Method of manufacturing a multilayer structure, in which method gold is deposited on a basic layer (3, 11) for forming a gold layer (7, 13), whereafter aluminium oxide is deposited on the gold layer for forming an aluminium oxide layer (9, 15). Silicon oxide is deposited on the aluminium oxide layer by means of PE-CVD for forming a silicon oxide layer (11, 13), and the aluminium oxide layer constitutes an adhesive layer between the gold layer and the silicon oxide layer. Together with the aluminium oxide layer, the silicon oxide layer constitutes an insulating and/or protective cladding layer for the gold layer.Type: GrantFiled: March 18, 1998Date of Patent: December 7, 1999Assignee: U.S. Philips CorporationInventor: Peter S. A. Knapen
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Patent number: 5932492Abstract: A method for forming a capacitor structure includes the steps of forming a conductive layer in a substrate, and forming a dielectric layer on the conductive layer opposite the substrate. An aluminum layer is formed on the dielectric layer, and this aluminum layer is patterned so that portions of the dielectric layer are exposed. The patterned aluminum layer is then oxidized to form an alumina masking layer. The alumina masking layer can then be used to selectively etch portions of the dielectric and conductive layers exposed thereby. Related systems are also disclosed.Type: GrantFiled: October 23, 1996Date of Patent: August 3, 1999Assignee: Samsung Electronics Co., Ltd.Inventors: Jin-hwan Hahm, Kyeong-koo Chi
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Patent number: 5906948Abstract: A method for etching dielectric layers is disclosed. A first etch of the dielectric layers is performed with a gas chemistry comprising C.sub.4 F.sub.8 flowing at about 10 sccm to about 25 sccm and CH.sub.3 F flowing at about 5 sccm to about 20 sccm. A second etch of the dielectric layers is performed with the gas chemistry and flow rates of gases which are about 10% to about 40% greater than the flow rates of gases in the first etch.Type: GrantFiled: April 17, 1998Date of Patent: May 25, 1999Assignee: Vanguard International Semiconductor CorporationInventors: Hao-Chieh Liu, Erik S. Jeng
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Patent number: 5888410Abstract: A dry etching method performing dry etching of a material containing zinc forms and patterns a resist on the material to be etched, and etches the material using an etching gas which is a mixed gas of methane gas and an inert gas. A dry etching method that dry etches a material containing zinc etches the material using an etching gas that consists only of methane gas, an inert gas, and hydrogen gas alone. Another dry etching method that dry etches a material containing zinc introduces an etching gas that contains methane gas, an inert gas, and hydrogen gas into a dry etching device, in which the flow rate of the hydrogen gas is set such that it is equal to or greater than the value at which the amount of dissociated hydrogen becomes saturated, and etches the material using the etching gas.Type: GrantFiled: March 31, 1997Date of Patent: March 30, 1999Assignee: Denso CorporationInventors: Hajime Ishihara, Kazuhiro Inoguchi, Yutaka Hattori, Nobuei Ito, Tadashi Hattori
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Patent number: 5874010Abstract: A method for trimming a pole used in a read-write head comprises the step of depositing a metallic layer on a layer of pole material, patterning the metallic layer so that it can serve as a mask, and ion beam etching the pole material with nitrogen ions. Of importance, a thin nitride layer forms on the metallic layer so that the etch rate of the metallic layer during ion beam etching is slowed. Alternatively, in lieu of the metallic layer, a nitride layer can be used.Type: GrantFiled: July 17, 1996Date of Patent: February 23, 1999Assignee: Headway Technologies, Inc.Inventors: Arthur Hungshin Tao, Yong-Chang Feng, Cheng Tzong Horng, Cherng-Chyi Han
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Patent number: 5849207Abstract: A method for the plasma etching of a ferrodielectric perovskite oxide thin film such as PZT which comprises providing a resist pattern from on a perovskite oxide thin film as an etching mask, and subjecting the thin film to plasma etching using an etching gas which includes a compound having at least carboxyl group in the molecule, so that the carbonyl group formed by dissociation of the compound having at least carboxyl group in the molecule reacts with constituent metals of the perovskite oxide to efficiently form a reaction product in the form of a metal complex, enabling one to effect plasma etching at a practical etching rate while ensuring good anisotropic processing.Type: GrantFiled: July 1, 1996Date of Patent: December 15, 1998Assignee: Sony CorporationInventor: Junichi Sato
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Patent number: 5846443Abstract: A method in a plasma processing chamber, for etching through a selected portion of an aluminum-containing layer and a titanium-containing layer. The titanium-containing layer is disposed above the aluminum-containing layer. The method includes a first etching step that etches at least partially through the titanium-containing layer using a first source gas composition. The first source gas composition consists essentially of the Cl.sub.2 etchant and a first mixture. The first mixture consists essentially of HCl and CHF.sub.3. The first source gas composition has a first flow ratio of the Cl.sub.2 etchant to the first mixture. There is further included a second etching step that etches at least partially through the aluminum-containing layer using a second source gas composition. The second source gas composition consists essentially of a Cl.sub.2 etchant and a second mixture. The second mixture consists essentially of HCl and CHF.sub.3. The second source gas composition has a second flow ratio of the Cl.sub.Type: GrantFiled: July 9, 1996Date of Patent: December 8, 1998Assignee: Lam Research CorporationInventor: Susan C. Abraham
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Patent number: 5843289Abstract: A method of obtaining a porous titanium surface suitable for medical implants is provided. The titanium surface is exposed to a plasma comprising a reactive plasma gas, the reactive plasma gas comprising an active etching species and a sputtering gas. The plasma conditions are effective to modify the titanium surface and provide surface porosity. The plasma conditions are effective to non-uniformly etch and sputter the titanium surface.Type: GrantFiled: January 22, 1996Date of Patent: December 1, 1998Assignee: Etex CorporationInventors: Dosuk D. Lee, Atul Nagras
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Patent number: 5843277Abstract: An RIE method and apparatus for etching through the material layer of a transparent-electrode (ITO) in a single continuous step at a rate better than 100 .ANG./min and with a selectivity better than 20 to 1 is disclosed. Chamber pressure is maintained at least as low as 60 mTorr. A reactive gas that includes ethyl iodide C.sub.2 H.sub.5 I) is used alone or in combination with another gas such as O.sub.2. Plasma-induced light emissions of reaction products and/or the reactants are monitored to determine the time point of effective etch-through.Type: GrantFiled: December 22, 1995Date of Patent: December 1, 1998Assignee: Applied Komatsu Technology, Inc.Inventors: Haruhiro Harry Goto, Yuh-Jia Su, Yuen-Kui Wong, Kam S. Law
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Patent number: 5840200Abstract: A device insulating film, a lower-layer platinum film, a ferroelectric film, an upper-layer platinum film, and a titanium film are sequentially formed on a semiconductor substrate in this order. On the titanium film, a photoresist mask is further formed in a desired pattern. The thickness of the titanium film is adjusted to be 1/10 or more of the total thickness of a multilayer film consisting of the upper-layer platinum film, the ferroelectric film, and the lower-layer platinum film. The titanium film is then subjected to dry etching and the photoresist film is removed by ashing process. The titanium film thus patterned is used as a mask in etching the upper-layer platinum film, the ferroelectric film, and the lower-layer platinum film by a dry-etching method using a plasma of a gas mixture of chlorine and oxygen in which the volume concentration of oxygen gas is adjusted to be 40%. During the dry-etching process, the titanium film is oxidized to provide a high etching selectivity.Type: GrantFiled: January 24, 1997Date of Patent: November 24, 1998Assignee: Matsushita Electronics CorporationInventors: Satoshi Nakagawa, Toyoji Ito, Yoji Bito, Yoshihisa Nagano
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Patent number: 5785871Abstract: A process for the minute processing of diamonds which comprisespreparing a substrate;forming a first buffer layer on the substrate;forming a second buffer layer, having a higher charge transfer rate than both the substrate and the first buffer layer, on the first layer;selectively removing the first and second buffer layers to selectively expose the surface of the substrate;depositing diamonds on the whole surface of the exposed surface of the substrate and the remaining first and second buffer layer; andremoving the by-products formed on the surface of the second buffer layer and surface thereof.Type: GrantFiled: August 27, 1996Date of Patent: July 28, 1998Assignee: LG Semicon Co., Ltd.Inventor: Hyun Pil Noh
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Patent number: 5776356Abstract: A method for etching a ferroelectric film made of a compound containing lead of the present invention, includes the steps of: forming an insulating film, metal films, and a ferroelectric film on a substrate in this order; forming an etching resistant film on the ferroelectric film, followed by patterning; and etching the ferroelectric film with a mixed gas containing an inert gas and a halogen gas or a halogenated gas as an etching gas, using the patterned etching resistant film as an etching mask.Type: GrantFiled: February 15, 1995Date of Patent: July 7, 1998Assignee: Sharp Kabushiki KaishaInventors: Seiichi Yokoyama, Yasuyuki Itoh, Shigeo Onishi, Jun Kudo, Keizo Sakiyama, Hitoshi Urashima
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Patent number: 5762813Abstract: By using first mixed gas containing carbon atoms and fluorine atoms, a semiconductor substrate is etched. In order to remove a damage layer formed on the surface of the semiconductor substrate by this etching processing, the semiconductor substrate is etched by second mixed gas including gas containing fluorine atoms and oxygen gas having a partial pressure ratio of at least 70%. Thereafter, a semiconductor oxide film is formed on the semiconductor substrate to fabricate a semiconductor device.Type: GrantFiled: March 13, 1996Date of Patent: June 9, 1998Assignee: Nippon Steel CorporationInventors: Makoto Takiyama, Hideki Fujikake
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Patent number: 5705443Abstract: A plasma-assisted dry etching process for etching of a metal containing material layer on a substrate to remove the metal containing material from the substrate, comprising (i) plasma etching the metal containing material and, (ii) contemporaneously with said plasma etching, contacting the metal containing material with an etch enhancing reactant in a sufficient amount and at a sufficient rate to enhance the etching removal of the metal containing material, in relation to a corresponding plasma etching of the metal containing material layer on the substrate in the absence of the etch enhancing reactant metal material being contacted with the etch enhancing reactant.Type: GrantFiled: May 30, 1995Date of Patent: January 6, 1998Assignee: Advanced Technology Materials, Inc.Inventors: Gregory Stauf, Robin A. Gardiner, Peter S. Kirlin, Peter C. Van Buskirk
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Patent number: 5681486Abstract: The invention provides a method of removing surface scale from a titanium or titanium alloy substrate. The method includes the steps of heating the substrate to a temperature in the range from about 100.degree. C. to about 600.degree. C., and thereafter subjecting the heated surface to a plasma formed from a gas selected from the group of consisting of CF.sub.4 and SF.sub.6. The plasma reacts with the surface scale, removing the scale, without attacking the underlying crystalline titanium or titanium alloy. Properly controlled, the plasma reaction terminates when the plasma has penetrated the scale and encounters the underlying crystalline metal. As a result, the method of the invention is capable of uniform removal of the entire surface scale of a crystalline titanium-containing substrate, without intergranular attack of the substrate.Type: GrantFiled: February 23, 1996Date of Patent: October 28, 1997Assignee: The Boeing CompanyInventors: Herbert S. Goode, Jr., Jean A. Nielsen, Larry E. Nitzsche
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Patent number: 5679267Abstract: A novel reticulated array comprises islands of ceramic (e.g. BST 40) which are fabricated from novel materials using unique methods of patterning. A shallow etch stop trench (46) is first ion milled around each ceramic island on the front side and then filled with an etch step material (e.g. parylene 48). An optical coat (e.g transparent metal layer 54, transparent organic layer 56 and conductive metallic layer 58) is elevated above the etch step material by an elevation layer (e.g. polyimide 49). For some applications, it has been experimentally verified that there is no loss, and sometimes a measured increase, in optical efficiency when the optical coating is not planar in topology. Novel fabrication methods also provide for the convenient electrical and mechanical bonding of each of the massive number of ceramic islands to a signal processor substrate (e.g. Si 86) containing a massive array of sensing circuits.Type: GrantFiled: January 16, 1996Date of Patent: October 21, 1997Assignee: Texas Instruments IncorporatedInventors: James F. Belcher, Robert A. Owen
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Patent number: 5676855Abstract: A process for producing a metal coated substrate with an improved resistivity to cyclic temperature stress is provided. The substrate is provided with at least one insulating layer and at least one metal layer attached to at least one side of the insulating layer. The metal layer is made at least 0.2 millimeters thick, and is weakened in places by openings formed in at least one border area.Type: GrantFiled: October 25, 1995Date of Patent: October 14, 1997Inventor: Jurgen Schulz-Harder
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Patent number: 5674407Abstract: A method of fabricating an anode plate 80 for use in a field emission device comprising the steps of providing a substantially transparent substrate 70, depositing a layer of a transparent, electrically conductive material 90 on a surface of the substrate, and then removing portions of said layer of conductive material to leave stripes of said conductive material 90.sub.R, 90.sub.G, 90.sub.B. The stripes of conductive material have a first and second corner 84, 88 distal from the substrate 70. The first and second corners 84, 88 of the stripes of conductive material are rounded and luminescent material 74 is applied on the conductive stripes 90. The first and second corners 84, 88 are rounded by applying voltage to the stripes 90 and then etching the stripes to form the rounded corners 84, 88.Type: GrantFiled: July 3, 1995Date of Patent: October 7, 1997Assignee: Texas Instruments IncorporatedInventor: Kenneth G. Vickers
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Patent number: 5667700Abstract: A process for the fabrication of a structural element, in particular an optical element comprises a carrier substrate as well as a layer system, with at least one dielectric layer stepped with respect to its thickness in at least one region opposite at least one second region. The dielectric layer is of the type MeO.sub.x and is applied onto a base, where Me is a metal whose atomic mass is at least 44, and x is selected so that the coefficient of absorption of the layer material at light of wavelength .lambda.=308 nm is k.sub.308 .ltoreq.0.01. The layer is built up through reactive etching by means of an activated gas for the step formation of the thickness. Other related processes and examples of the elements themselves are also disclosed.Type: GrantFiled: February 14, 1994Date of Patent: September 16, 1997Assignee: Balzers AktiengesellschaftInventors: Helmut Rudigier, Johannes Edlinger
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Patent number: 5667631Abstract: A method for dry etching an indium tin oxide (ITO) layer disposed above a substrate in a low pressure plasma reactor is disclosed. The method includes a step of placing a substrate having the ITO layer into the low pressure plasma reactor, a step of introducing an etchant gas into the low pressure plasma reactor; a step of striking a plasma from the etchant gas in the low pressure plasma reactor; and a step of etching the ITO layer with the plasma.Type: GrantFiled: June 28, 1996Date of Patent: September 16, 1997Assignee: Lam Research CorporationInventors: John P. Holland, Alex T. Demos
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Patent number: 5653851Abstract: A method to anisotropically etch a titanate wafer (16 or 39) is provided. The method includes the steps of generating a plasma (32) and mixing an organic acid reagent with the plasma (32). The titanate wafer (16 or 39) is then exposed to the plasma (32) and organic acid reagent mixture thereby etching (42) the titanate wafer (16 or 39).Type: GrantFiled: July 5, 1994Date of Patent: August 5, 1997Assignee: Texas Instruments IncorporatedInventor: Gail D. Shelton
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Patent number: 5653892Abstract: A novel reticulated array comprises islands of ceramic (e.g. BST 40) which are fabricated from novel materials using unique methods of patterning. A front side optical coating (e.g. transparent metal layer 44, transparent organic layer 46 and conductive metallic layer 48) is elevated above the substrate between the ceramic islands. This allows additional material (e.g. polyimide 38) between the optical coating and the substrate above the regions where cavities are to be etched. Etching of the cavities (72) is performed from the back side of the substrate without damaging the front side optical coating. Novel fabrication methods also provide for the convenient electrical and mechanical bonding of each of the massive number of ceramic islands to a signal processor substrate (e.g. Si 80) containing a massive array of sensing circuits.Type: GrantFiled: January 16, 1996Date of Patent: August 5, 1997Assignee: Texas Instruments IncorporatedInventors: James F. Belcher, Robert A. Owen
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Patent number: 5635081Abstract: In a fabrication method of a field-emission cold cathode, a conductive material for an emitter is first deposited on a Si substrate and then dry etched to form a conical emitter. An insulating layer and a gate electrode are deposited in such a manner as to cover over the emitters, and the surfaces of the emitters are flattened with a resist. Then, the insulating layer and the gate electrode are opened by etching back to expose the end of the conical emitter. Ta can be used as the conductive material to be deposited on the Si substrate. Meanwhile, the insulating layer to be deposited on the emitter can be formed by anodic oxidation. Further, where the height of the surface of the gate electrode from the surface of the Si substrate is set equal to the height of the emitter, detection of the end point at the later etching back step is facilitated.Type: GrantFiled: July 11, 1995Date of Patent: June 3, 1997Assignee: NEC CorporationInventor: Takuya Yoshihara
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Patent number: 5624583Abstract: A method of manufacturing a semiconductor device containing a ruthenium oxide includes the step of dry-etching the ruthenium oxide using a gas mixture containing oxygen or ozone gas and at least one material selected from the group consisting of fluorine gas, chlorine gas, bromine gas, iodine gas, a halogen gas containing at least one of the fluorine, chlorine, bromine, and iodine gases, and a hydrogen halide.Type: GrantFiled: September 6, 1995Date of Patent: April 29, 1997Assignee: NEC CorporationInventors: Ken Tokashiki, Kiyoyuki Sato
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Patent number: 5618446Abstract: The present invention relates to a method for foxing a step on a deposition surface of a substrate for depositing a thin film on it. According to the method, the step is formed by etching a portion of the deposition surface of the substrate by emitting a laser beam to the portion.Type: GrantFiled: February 24, 1995Date of Patent: April 8, 1997Assignee: Sumitomo Electric Industries, Ltd.Inventor: Tatsuoki Nagaishi
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Patent number: 5607602Abstract: An RIE method and apparatus for etching through the material layer of a transparent-electrode (ITO) in a single continuous step at a rate better than 80 .ANG./min is disclosed. Chamber pressure is maintained at least as low as 30 mTorr. A reactive gas that includes a halogen hydride such as HCl is used alone or in combination with another reactive gas such as Cl.sub.2. Plasma-induced light emissions of reaction products and/or the reactants are monitored to determine the time point of effective etch-through.Type: GrantFiled: June 7, 1995Date of Patent: March 4, 1997Assignee: Applied Komatsu Technology, Inc.Inventors: Yuh-Jia Su, Yuen-Kui Wong, Kam S. Law, Haruhiro Goto
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Patent number: 5607600Abstract: An infrared sensing array 46 is coupled to a sensing integrated circuit structure 48, and then inter-pixel thermal isolation slots 62 are etched in the optical coating 32 of the infrared sensing array 46. An optional protective material 64 may be deposited over at least the sensing integrated circuit structure 48 for additional protection.Type: GrantFiled: January 31, 1995Date of Patent: March 4, 1997Assignee: Texas Instruments IncorporatedInventors: James F. Belcher, Craig Osborn
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Patent number: 5578225Abstract: A field emission display that may be viewed through the back plate, thus providing increased luminous efficiency, and methods for making such a display, are described. A glass substrate is provided as a base for the display faceplate. There is a reflective, conductive layer over the glass substrate. A phosphor layer is formed over the reflective, conductive layer. A second glass substrate acts as a transparent base for the display baseplate, which is mounted opposite and parallel to the faceplate. A first transparent insulating layer is formed over the second glass substrate. There are parallel, transparent cathode electrodes with auxiliary metal electrodes, over the first insulating layer. Parallel, transparent gate electrodes are formed over, separate from, and orthogonally to the parallel, transparent cathode electrodes, and also have auxiliary metal electrodes. A second transparent insulating layer is between the gate electrodes and the cathode electrodes.Type: GrantFiled: January 19, 1995Date of Patent: November 26, 1996Assignee: Industrial Technology Research InstituteInventor: Ho-Ching Chien
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Patent number: 5567659Abstract: A method of accurately controlling the depth of etched gratings in uniform or layered quaternary III-V material. A native oxide is selectively grown on the area of the quaternary to be patterned and this native oxide is subsequently removed to engrave the surface. Periodic repetition of the oxide growth/removal steps results in gratings of the desired depths.Type: GrantFiled: May 25, 1995Date of Patent: October 22, 1996Assignee: Northern Telecom LimitedInventors: Grzegorz Pakulski, Cornelis Blaauw, Agnes Margittai, Ronald Moore
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Patent number: 5567333Abstract: A magnetic head element has one or more rails formed on the surface thereof. Each rail is formed so as to have a tapered angle of 55.degree.-85.degree.. To form such a rail, ion milling is conducted; the rail substrate used is allowed to have an inclination angle to 15.degree.-60.degree. and is rotated; and there is used, as the ion milling gas, a fluorinated hydrocarbon (e.g. CH.sub.2 FCF.sub.3) gas alone or a mixed gas of said fluorinated hydrocarbon gas and Ar, SF.sub.6 or the like. Accordingly, a magnetic head rail shape gives a small variation in flying height between magnetic head and magnetic disc.Type: GrantFiled: June 22, 1994Date of Patent: October 22, 1996Assignee: Hitachi, Ltd.Inventors: Yasuo Hira, Tamaki Toba, Hirotaka Imayama, Atsuko Ohkawa, Masayasu Fujisawa, Kazuo Nate, Hideki Sonobe, Saburo Suzuki, Eisei Togawa, Hiroshi Ishizaki, Yoshiki Hagiwara
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Patent number: 5567332Abstract: A gaseous process for removing and vaporizing at least a portion of a silicon oxide film from between a substrate and a superstructure leaving a space between the substrate and the superstructure. The silicon oxide layer is removed in two steps. In the first step the bulk of the silicon oxide layer is removed by a rapid liquid or gaseous etching process, leaving at least a portion of the silicon oxide layer directly underlying the superstructure in place so as to support the superstructure during a wash cycle. In the second silicon oxide removal step the substrate is introduced to a high flow rate gaseous environment containing a relatively high concentration of anhydrous HF to which no, or only a relatively very low amount of, additional water vapor is provided until the silicon oxide directly underlying the superstructure has been removed.Type: GrantFiled: June 9, 1995Date of Patent: October 22, 1996Assignee: FSI InternationalInventor: Jitesh Mehta
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Patent number: 5496437Abstract: A method of reactive ion etching both a lead zirconate titanate ferroelectric dielectric and a RuO.sub.2 electrode, and a semiconductor device produced in accordance with such process. The dielectric and electrode are etched in an etching gas of O.sub.2 mixed with either CClF.sub.2 or CHClFCF.sub.3.Type: GrantFiled: June 10, 1993Date of Patent: March 5, 1996Assignees: Ceram Incorporated, Sharp Kabushiki Kaisha, Virginia Tech Intellectual Properties, Inc.Inventors: Seshu B. Desu, Wei Pan, Dilip P. Vijay
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Patent number: RE36746Abstract: The invention provides a method of removing surface scale from a titanium or titanium alloy substrate. The method includes the steps of heating the substrate to a temperature in the range from about 100.degree. C. to about 600.degree. C., and thereafter subjecting the heated surface to a plasma formed from a gas selected from the group of consisting of CF.sub.4 and SF.sub.6. The plasma reacts with the surface scale, removing the scale, without attacking the underlying crystalline titanium or titanium alloy. Properly controlled, the plasma reaction terminates when the plasma has penetrated the scale, and encounters the underlying crystalline metal. As a result, the method of the invention is capable of uniform removal of the entire surface scale of a crystalline titanium-containing substrate, without intergranular attack of the substrate.Type: GrantFiled: September 16, 1998Date of Patent: June 27, 2000Assignee: The Boeing CompanyInventors: Herbert S. Goode, Jr., Jean A. Nielsen, Larry E. Nitzsche