Frosting Glass Patents (Class 216/98)
  • Patent number: 11629095
    Abstract: A method of etching a substrate comprises: contacting a substrate having a thickness with an etchant disposed in a vessel for a period of time until the thickness has reduced by at least 2 ?m and at an average rate of 1 ?m per minute to 6.7 ?m per minute, the etchant having a temperature of 170° C. to 300° C. and comprising a molten mixture of two or more alkali hydroxides; and ceasing contacting the substrate with the etchant. The etchant in some instances comprises a molten mixture of NaOH and KOH. For example, the etchant in some instances includes a molten mixture of 24 wt. % to 72 wt. % NaOH, and 76 wt. % to 28 wt. % KOH. In some instances, the method alters the weight percentage of Na+, K+ and Li+ in the composition of the surface of the substrate by less than 1%.
    Type: Grant
    Filed: May 28, 2020
    Date of Patent: April 18, 2023
    Assignee: CORNING INCORPORATED
    Inventors: Albert Joseph Fahey, Yuhui Jin
  • Patent number: 8992786
    Abstract: A glass article including: at least one anti-glare surface having haze, distinctness-of-image, surface roughness, and uniformity properties, as defined herein. A method of making the article having an anti-glare surface includes, for example, forming a protective film on selected portions of at least one surface of the article; contacting the at least one surface with a liquid etchant; and removing the protective film from the surface of the article to form the anti-glare surface. A display system that incorporates the glass article, as defined herein, is also disclosed.
    Type: Grant
    Filed: April 20, 2011
    Date of Patent: March 31, 2015
    Assignee: Corning Incorporated
    Inventors: Jeffrey Todd Kohli, Kelvin Nguyen, Lu Zhang
  • Patent number: 8821747
    Abstract: A method for manufacturing a glass substrate for a magnetic disk comprises a surface grinding step of processing a mirror-surface plate glass, having a main surface in the form of a mirror surface, to a required flatness and surface roughness using fixed abrasive particles. The method comprises, before the surface grinding step using the fixed abrasive particles, a surface roughening step of roughening the surface of the mirror-surface plate glass by frosting.
    Type: Grant
    Filed: October 5, 2009
    Date of Patent: September 2, 2014
    Assignee: Hoya Corporation
    Inventors: Takanori Mizuno, Yosuke Suzuki
  • Patent number: 8821735
    Abstract: An object of the invention is to effectively remove particles on the glass substrate surfaces, even in the case wherein abrasive particles having a small particle size is used in the polishing step of the glass substrate and a supersonic treatment is performed at a high frequency at the supersonic cleaning step after the polishing step. In a manufacturing method of a glass substrate for a magnetic disk comprising a polishing step for performing polishing of the glass substrate and a supersonic cleaning step for performing supersonic cleaning of the glass substrate after the polishing step, the polishing step uses abrasive particles having a particle size of 10 nm to 30 nm and a first supersonic cleaning is performed at a frequency of 300 kHz to 1,000 kHz to form secondary particles and then a second supersonic cleaning is performed at a frequency of 30 kHz to 100 kHz in the supersonic cleaning step.
    Type: Grant
    Filed: March 31, 2011
    Date of Patent: September 2, 2014
    Assignee: Hoya Corporation
    Inventor: Yosuke Suzuki
  • Patent number: 8465662
    Abstract: Provided is an etching composition for electively removing silicon dioxide at a high etch rate, more particularly, a composition for wet etching of silicon dioxide, including 1 to 40 wt % of hydrogen fluoride (HF); 5 to 40 wt % of ammonium hydrogen fluoride (NH4HF2); and water, and further including a surfactant to improve selectivity of the silicon dioxide and a silicon nitride film. Since the composition for wet etching of silicon dioxide has the high etch selectivity of the silicon dioxide to the silicon nitride film, it is useful for selectively removing silicon dioxide.
    Type: Grant
    Filed: September 21, 2010
    Date of Patent: June 18, 2013
    Assignee: Techno Semichem Co., Ltd.
    Inventors: Jung Hun Lim, Dae Hyun Kim, Chang Jin Yoo, Seong Hwan Park
  • Patent number: 8419965
    Abstract: A method for texturing a glass substrate includes cleaning the glass substrate with at least one surfactant and etching the glass substrate using a caustic solution. The percentage of caustic solution is provided by controlling a fluid flow and temperature to control the depth of the etching. The method also includes acid cleaning the etched glass substrate to remove glass residuals and surfactants.
    Type: Grant
    Filed: June 16, 2009
    Date of Patent: April 16, 2013
    Assignee: Rockwell Collins, Inc.
    Inventors: Paul R. Nemeth, John W. Sackfield
  • Patent number: 8246847
    Abstract: There are provided an aqueous solution for separation of a conductive ceramics sintered body in which a conductive ceramic sintered body separated form a glass can be collected in a recyclable condition, and a separating method therefor, and an aqueous solution for separation with which a dark ceramics sintered body, a conductive ceramics sintered body and a glass are separately collected from a glass with a dark ceramics sintered body in which a conductive ceramics sintered body is formed on the dark ceramics sintered body, and a separating method therefor. A treatment liquid having an etching ability for at least one of a glass and a conductive ceramic sintered body is prepared as an aqueous solution 20 for separation of the conductive ceramics sintered body, then the aqueous solution 20 for separation is filled in a container 11, and a glass with a conductive ceramics sintered body 30 is immersed into the aqueous solution 20 for separation in the container 11.
    Type: Grant
    Filed: September 11, 2006
    Date of Patent: August 21, 2012
    Assignee: Nippon Sheet Glass Company, Limited
    Inventors: Masahiro Hori, Kazuishi Mitani, Yasuhiro Saito, Nobuyuki Takatsuki, Kyouichi Shukuri, Shunji Kuramoto
  • Publication number: 20120045649
    Abstract: The present invention discloses a method for treating at least a portion of a surface of a glass article which comprises the following steps, whatever their order: application of a water solution comprising at least one high-pH solid material on said portion of the glass article; heating of said glass article to a temperature at least equal to the evaporation temperature of water.
    Type: Application
    Filed: June 2, 2010
    Publication date: February 23, 2012
    Applicant: AGC GLASS EUROPE
    Inventor: Ronny Pieters
  • Patent number: 7955440
    Abstract: After a water film is formed on a wafer front surface in a chamber, the water film is supplied sequentially with an oxidizing component of an oxidation gas, an organic acid component of an organic acid mist, an HF component of an HF gas, the organic acid mist, and the oxidizing component of the oxidation gas. As a result, the HF component and the organic acid component provide cleaning effect on the wafer surface, and a concentration of the cleaning components in the water film within a wafer surface can be even.
    Type: Grant
    Filed: November 21, 2008
    Date of Patent: June 7, 2011
    Assignee: Sumco Corporation
    Inventors: Shigeru Okuuchi, Kazushige Takaishi
  • Publication number: 20100297393
    Abstract: Provided is a method for surface frosting of glass product, wherein a glass product is first immersed in a pre-treatment solution having a composition including water (H2O) 60-80 wt %, hydrofluoric acid (HF) 10-20 wt %, and nitric acid (HNO3) 10-20 wt % for approximately 5 seconds to remove grease/oil and/or contamination from a surface of the glass product, then immersed in a frosting solution having a composition including nitric acid (HNO3) 15-40 wt %, ammonium hydrofluoride (NH4HF2) 30-60 wt %, hydrofluoric acid (HF) 0-10 wt %, water (H2O) 0-45 wt %, and hydrochloric acid (HCl) 0-1 wt % for approximately 1-5 minutes, and finally rinsed with water. As such, the surface of the glass product so treated forms a surface texture that provides smooth tactility of hand touch and shows an outer appearance of a scale like pattern formed on the surface of the glass product.
    Type: Application
    Filed: April 14, 2010
    Publication date: November 25, 2010
    Inventor: Chien-Ping WU
  • Patent number: 7824564
    Abstract: A method for flattening a glass substrate includes the steps of preparing plural kinds of etching liquids different from one another in an etching rate, preparing the glass substrate, and etching the glass substrate at least one time with each of the etching liquids and executing the etching a plurality of times in total. When the etchings are executed the plurality of times, an etching rate of the glass substrate with one etching liquid used for one etching of plural etchings is slower than that of the glass substrate with the another etching liquid used for another etching executed after the one etching process of the plural etching processes.
    Type: Grant
    Filed: September 26, 2006
    Date of Patent: November 2, 2010
    Assignees: Casio Computer Co., Ltd., Sanwa Frost Industries Co., Ltd., Nagase & Co., Ltd.
    Inventor: Kazuyuki Hiroki
  • Patent number: 7553428
    Abstract: A method of fabricating spacers for use in a flat panel device includes: preparing a core glass having a low solubility in a chemical etching solution and a tube glass having a high solubility in the chemical etching solution and having a larger inner diameter than an outer diameter of the core glass; inserting the core glass into the tube glass to obtain a cylindrical glass; drawing the cylindrical glass at a predetermined temperature until the core glass has a predetermined diameter; cutting the drawn cylindrical glass to a predetermined length; and removing the tube glass in the cylindrical glass using the chemical etching solution.
    Type: Grant
    Filed: August 10, 2005
    Date of Patent: June 30, 2009
    Assignee: Samsung SDI Co., Ltd.
    Inventors: Jeong-Hee Lee, Tae-Won Jeong, Jeong-Na Heo
  • Patent number: 7368393
    Abstract: A method for removing damages of a dual damascene structure after plasma etching is disclosed. The method comprises the use of sublimation processes to deposit reactive material onto the damaged regions and conditions to achieve a controlled removal of the damaged region. Furthermore a semiconductor structure comprising a dual damascene structure that has been treated by the method is disclosed.
    Type: Grant
    Filed: April 20, 2006
    Date of Patent: May 6, 2008
    Assignee: International Business Machines Corporation
    Inventors: William G. America, Steven H. Johnston, Brian W. Messenger
  • Patent number: 7276181
    Abstract: A method for preparing a decorative glass using a glass etching composition, wherein a frosting of elaborate patterns and designs is applied on the surface of the glass having an arbitrary shape, such a plane, a curved plane or a tube, by utilizing the silk-screen process or the like, using a glass etching composition characterized as comprising 1 to 20 w/v % (preferably, 2 to 5 w/v %) of a fluoride, 20 to 80 v/v % (preferably, 20 to 50 v/v %) of water and 20 to 80 v/v % (preferably, 50 to 80 v/v %) of an organic solvent miscible with water or another glass etching composition comprising the former composition and an additive. The glass etching composition is free from the problems of the danger to a human body and environmental pollution.
    Type: Grant
    Filed: December 25, 2001
    Date of Patent: October 2, 2007
    Inventor: Hiroshi Miwa
  • Patent number: 7022251
    Abstract: Disclosed is a method for forming a conductor on a dielectric. The method commences with the deposition of a conductive thickfilm on the dielectric, followed by a “subsintering” of the conductive thickfilm. Either before or after the subsintering, the conductive thickfilm is patterned to define at least one conductor. After subsintering, the conductive thickfilm is etched to expose the conductor(s), and the conductor(s) are then fired. A brief chemical etch may be used after the final firing step if improved wire-bondability is required.
    Type: Grant
    Filed: June 19, 2003
    Date of Patent: April 4, 2006
    Assignee: Agilent Technologies, Inc.
    Inventors: John F. Casey, Lewis R. Dove, Ling Liu, James R. Drehle, R. Frederick Rau, Jr., Rosemary O. Johnson
  • Patent number: 6807824
    Abstract: A glass etching composition free from health hazard and environmental pollution, and a frosting method using the composition for a glass surface are provided.
    Type: Grant
    Filed: December 21, 2000
    Date of Patent: October 26, 2004
    Inventor: Hiroshi Miwa
  • Patent number: 6652659
    Abstract: A method of rinsing an electronic substrate recognizes that adding a buffer to a rinsing fluid eliminates fluctuations in the amount of residues on an electronic substrate, and a buffered rinsing fluid is prepared by (a) providing water from a water source; (b) deionizing the water to produce deionized water; (c) adding a buffer to the deionized water at a concentration effective to eliminate fluctuations in the amount of residues on the electronic substrate. The electronic substrate is rinsed with the buffered rinsing fluid.
    Type: Grant
    Filed: November 30, 1999
    Date of Patent: November 25, 2003
    Assignee: Honeywell International Inc.
    Inventors: Glen Roeters, Raj Kumar
  • Publication number: 20020170883
    Abstract: A method of use for a reusable monitor wafer, having multiple crystal original pits (COP) on its surface, used for monitoring and measuring particle amounts in a chemical vapor deposition (CVD) process. First, a silicon oxide layer is formed on the surface of a monitor wafer. A first cleaning process and a thin film deposition process, forming a thin film layer on a surface of the silicon oxide layer, are then performed, respectively. Thereafter, a particle measurement process is performed to measure particle amounts on the surface of the thin film layer. After removing the thin film layer and the silicon oxide layer on the monitor wafer, respectively, a second cleaning process is performed.
    Type: Application
    Filed: May 17, 2001
    Publication date: November 21, 2002
    Inventor: Ching-Yu Chang
  • Patent number: 6428864
    Abstract: Glass bottles having undergone high-frequency heat sealing, to depress the dispersion of sealing strength as low as possible and to improve the ease of both sealing and unsealing. A rough surface having minute unevenness is formed in the proximity of the apical part of the mouth of a glass bottle, wherein the apical part contacts with a sealing material. Since (1) a contact area between the sealing material and the glass surface decreases, and the quantity of heat taken by the glass from the sealing material decreases, (2) a bond area increases; and (3) an anchor effect is generated, the sealing strength increases, and simultaneously the dispersion of the sealing strength decreases.
    Type: Grant
    Filed: March 29, 2001
    Date of Patent: August 6, 2002
    Assignee: Toyo Glass Company, Limited
    Inventor: Noriyuki Fujita
  • Patent number: 6281136
    Abstract: An apparatus for etching a glass substrate includes a first bath containing an etchant, at least one porous panel having a plurality of jet holes in the first bath, the porous panel containing the etchant to jet the etchant against the glass substrate, a container storing the etchant, and a pump supplying the etchant from the container to the porous panel, the pump being connected to the container and the porous panel.
    Type: Grant
    Filed: August 25, 2000
    Date of Patent: August 28, 2001
    Assignee: LG.Philips LCD Co., Ltd.
    Inventor: Woong Kwon Kim
  • Patent number: 6241903
    Abstract: A diffuser master is provided which is manufactured mechanically instead of holographically. The master can be made from a suitable substrate including relatively hard materials such as plastic, glass or metal. A substrate having a first side is worked to form a diffuser surface relief structure thereon. The substrate can be buffed using a buffing agent of a selected grit in order to form surface scratches in the first side of the substrate. The substrate can also be blasted with shot particles in order to form indentations and depressions in the first side. The substrate can alternatively be acid or alkali etched in order to form surface irregularities in the first side. The scratches, depressions or irregularities can be formed in order to create a desired surface relief and hence desired diffuser output characteristics.
    Type: Grant
    Filed: August 20, 1998
    Date of Patent: June 5, 2001
    Assignee: Physical Optics Corporation
    Inventors: Gajendra D. Savant, Kevin H. Yu, Andrew A. Kostrzewski