Nitride Containing Patents (Class 419/13)
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Patent number: 8318082Abstract: A composition containing: about 45 to about 75 volume % of cubic boron nitride (CBN), where the CBN has finer and coarser particles having two different average particle sizes, the range of the average particle size of the finer particles being about 0.1 to about 2 ?m, the range of the average particle size of the coarser particles being about 0.3 to about 5 ?m, the ratio of the content of the coarser CBN particles to the finer CBN particles being 50:50 to 90:10; a secondary hard phase containing a nitride or carbonitride of a Group 4, 5 or 6 transition metal or a mixture or solid solution thereof, and a binder phase.Type: GrantFiled: October 28, 2005Date of Patent: November 27, 2012Assignee: Element Six Abrasives S.A.Inventors: Nedret Can, Stig Ake Andersin
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Patent number: 8309018Abstract: Methods of forming bit bodies for earth-boring bits include assembling green components, brown components, or fully sintered components, and sintering the assembled components. Other methods include isostatically pressing a powder to form a green body substantially composed of a particle-matrix composite material, and sintering the green body to provide a bit body having a desired final density. Methods of forming earth-boring bits include providing a bit body substantially formed of a particle-matrix composite material and attaching a shank to the body. The body is provided by pressing a powder to form a green body and sintering the green body. Earth-boring bits include a unitary structure substantially formed of a particle-matrix composite material. The unitary structure includes a first region configured to carry cutters and a second region that includes a threaded pin. Earth-boring bits include a shank attached directly to a body substantially formed of a particle-matrix composite material.Type: GrantFiled: June 30, 2010Date of Patent: November 13, 2012Assignee: Baker Hughes IncorporatedInventors: Redd H. Smith, John H. Stevens, James L. Duggan, Nicholas J. Lyons, Jimmy W. Eason, Jared D. Gladney, James A. Oxford, Benjamin J. Chrest
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Publication number: 20120276393Abstract: A multiphase composite system is made by binding hard particles, such as TiC particles, of various sizes with a mixture of titanium powder and aluminum, nickel, and titanium in a master alloy or as elemental materials to produce a composite system that has advantageous energy absorbing characteristics. The multiple phases of this composite system include an aggregate phase of hard particles bound with a matrix phase. The matrix phase has at least two phases with varying amounts of aluminum, nickel, and titanium. The matrix phase forms a bond with the hard particles and has varying degrees of hard and ductile phases. The composite system may be used alone or bonded to other materials such as bodies of titanium or ceramic in the manufacture of ballistic armor tiles.Type: ApplicationFiled: July 9, 2012Publication date: November 1, 2012Inventor: Robert G. LEE
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Patent number: 8298479Abstract: A process for forming a remateable machined titanium powder base alloy connecting rod using a titanium alloy powder having an average particle size of about 1-20 microns, a mean aspect ratio of about 5 to 300, and a specific surface area of at least about 25 m2/g.Type: GrantFiled: May 12, 2011Date of Patent: October 30, 2012Inventor: Gerald Martino
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Publication number: 20120251375Abstract: A method of producing a Pb-free copper-alloy sliding material containing 1.0 to 15.0% of Sn, 0.5 to 15.0% of Bi and 0.05 to 5.0% of Ag, and Ag and Bi from an Ag—Bi eutectic. If necessary, at least one of 0.1 to 5.0% of Ni, 0.02 to 0.2% P, 0.5 to 30.0% of Zn, and 1.0 to 10.0 mass % of at least one of a group consisting of Fe3P, Fe2P, FeB, NiB and AlN may be added.Type: ApplicationFiled: June 11, 2012Publication date: October 4, 2012Inventors: Hiromi YOKOTA, Ryo Mukai, Shinichi Kato, Nahomi Hamaguchi
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Publication number: 20120241670Abstract: The present invention provides a preparation method of a metal matrix composite. The method comprises the following steps of: 1) pulverizing a solid carbon material to a micrometer size; 2) plastic deforming a metal matrix powder and dispersing the pulverized nanometer-sized carbon material into the metal matrix powder during the plastic deformation; 3) integrating the metal/carbon nano-material composite powder obtained in step 2) by using a hot forming process; and 4) heat treating the integrated bulk material at a predetermined temperature to form a composite having a metal-carbon nanophase, a metal-carbon nanoband formed by growth of the metal-carbon nanophase, or a metal-carbon nano-network structure formed by self-coupling of the metal-carbon nanoband.Type: ApplicationFiled: October 22, 2010Publication date: September 27, 2012Applicant: Industry-Academic Cooperation Foundation, Yonsei UniversityInventors: Dong Hyun Bae, Hyun Joo Choi
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Patent number: 8273291Abstract: A controlled combustion synthesis apparatus comprises an ignition system, a pressure sensor for detecting internal pressure, a nitrogen supply, a gas pressure control valve for feeding nitrogen and exhausting reaction gas, means for detecting the internal temperature of the reaction container, a water cooled jacket, and a cooling plate. A temperature control system controls the temperature of the reaction container by controlling the flow of cooling water supplied to the jacket and the cooling plate in response to the detected temperature. By combustion synthesizing, while controlling the internal pressure and temperature, the apparatus can synthesize a silicon alloy including 30-70 wt. % silicon, 10-45 wt. % nitrogen, 1-40 wt. % aluminum, and 1-40 wt % oxygen.Type: GrantFiled: March 19, 2009Date of Patent: September 25, 2012Assignee: Sumikin Bussan CorporationInventors: Toshiyuki Watanabe, Masafumi Matsushita, Toshitaka Sakurai, Kazuya Sato, Yoko Matsushita
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Patent number: 8252225Abstract: A multi-layer precursor material for use in forming hardfacing on a tool including hard particles, metal particles and a polymer. Methods of forming a multi-layer precursor film. Methods of using a precursor material to form hardfacing on a tool, including brazing a precursor material onto a surface of the tool. Intermediate structures for use in forming earth-boring tools including a precursor material covering an internal surface of a body of the tools. Methods of forming earth-boring tools include forming a body having a fluid passageway extending therethrough and covering a surface of the body with a hardfacing material. The surface of the body may be located in a region susceptible to erosion when fluid is caused to flow through the fluid passageway.Type: GrantFiled: March 4, 2009Date of Patent: August 28, 2012Assignee: Baker Hughes IncorporatedInventors: Jimmy W. Eason, Travis E. Puzz
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Publication number: 20120207640Abstract: High strength aluminum alloys and methods for producing them. The alloys consist essentially of about 9.0 to 10.3 wt. % zinc, about 2.5 to 3.5 wt. % magnesium, about 1.5 to 3.0 wt. % copper and less than about 0.05 wt. % of any other alloying constituent. The balance consists of aluminum. These alloys are compatible with ceramic reinforcements used in metal matrix composites.Type: ApplicationFiled: February 14, 2011Publication date: August 16, 2012Applicant: Gamma Technology, LLCInventor: William C. Harrigan, JR.
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Patent number: 8241708Abstract: Metal and/or silicon oxides are produced by hydrolysis of alkoxide precursors in the presence of either an acid catalyst or a base catalyst in a supercritical fluid solution. The solubility of the acid catalysts in the supercritical fluid can be increased by complexing the catalyst with a Lewis base that is soluble in the supercritical fluid. The solubility of the base catalysts in the supercritical fluid can be increased by complexing the catalyst with a Lewis acid that is soluble in the supercritical fluid. The solubility of water in the solution is increased by the interaction with the acid or base catalyst.Type: GrantFiled: March 9, 2005Date of Patent: August 14, 2012Assignees: Micron Technology, Inc., Idaho Research FoundationInventors: Chien M. Wai, Hiroyuki Ohde, Stephen J. Kramer
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Publication number: 20120082586Abstract: The present invention comprises the nitridization of stainless steel with a gaseous nitrogen compound such as nitrogen gas (N2), or ammonia (NH3) at high temperature wherein the reaction pressure is lowered. A base powder with properties similar to those of a martensitic stainless steel is prepared from a molten metal with the subsequent incorporation of selective additives such as cobalt, chromium, boron, copper, vanadium, niobium and mixtures thereof to improve high temperature resistance to scuffing and adhesive wear. The molten mixture is then atomized by water- or air-atomization to yield a base powder which is mixed with nitrogen or ammonia gas at various pressures in a static or fluidized bed to provide a nitrogen alloyed particulate, i.e., a nitrided particulate alloy. The powder is heated in a hot isostatic press under vacuum with argon gas at reduced pressure and later cooled to ambient (room) temperature.Type: ApplicationFiled: November 22, 2010Publication date: April 5, 2012Applicant: Magna Tech P/M LabsInventor: Kenneth H. Moyer
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Publication number: 20120063943Abstract: Provided are a composite powder of a metal and carbide (carbonitride) for a structural material, a sintered body, and methods of preparing the composite powder and sintered body. The composite powder for a structural member has a composition of M1-x % M2C, M1-x % (M2,M1)C, M1-x % M2(CN), or M1-x % (M2,M1)(CN). A matrix-phase metal M1 is one selected from tungsten (W) and molybdenum (Mo) of the periodic table of the elements, an accessory-phase metal M2 is one selected from the group consisting of Group-IV to Group-VI metals of the periodic table of the elements and forms a carbide or carbonitride having an average particle size of about 1 ?m or less, and the matrix-phase metal M1 and the accessory-phase metal M2 coexist due to a reaction.Type: ApplicationFiled: September 28, 2009Publication date: March 15, 2012Applicant: SNU R&DB FOUNDATIONInventor: Shinhoo Kang
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Patent number: 8083831Abstract: The present invention relates to a lightweight, anti-scratch and fracture resistant material for use in manufacture of jewelry prepared by sintering a powered mixture consisting essentially of 20% by weight of titanium carbide, 25% by weight of tungsten carbide, 35% by weight of titanium nitride, and balance being a binder consisting essentially of nickel, molybdenum and cobalt.Type: GrantFiled: March 4, 2010Date of Patent: December 27, 2011Assignee: BTR LimitedInventor: Zhijian Xia
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Publication number: 20110262296Abstract: A titanium based carbonitride alloy containing Ti, Nb, Ta, W, C, N and Co, contains: Co 7 to 21 wt % W 14 to 20 wt % Ta 5 to 11 wt % Nb 2 to 7 wt % and, Ti 33 to 50 wt % whereby the overall N/C weight ratio is 0.6 to 0.75, the Ta/Nb weight ratio 1.8 to 2.1, the relative saturation magnetization 0.60 to 0.90 and the magnetic coercivity Hc=(18.2?0.2*Co wt %) +/? E kA/m, where E is 2.0. A method of making the alloy is also described.Type: ApplicationFiled: December 17, 2009Publication date: October 27, 2011Applicant: SECO TOOLS ABInventors: Bo Jansson, Jenni Zackrisson, Tomas Persson
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Publication number: 20110262295Abstract: A method of making a hard particle-dispersed metal matrix-bonded composite, includes the steps of mixing hard particles and ductile metal particles to yield a mixture, and sintering the mixture under a pressure of less than 2.0 GPa and at a temperature of less than 1200° C. for a sufficient time to yield the composite. A composite material made by the above method is disclosed.Type: ApplicationFiled: April 21, 2010Publication date: October 27, 2011Inventors: Oleg A. Voronov, Bernard H. Kear
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Patent number: 8043555Abstract: An earth-boring bit has a steel body and bearing pin for rotatably supporting a cone. The cone has an exterior surface containing rows of cutting elements. The cone and cutting elements are formed of cemented tungsten carbide. The cone may be manufactured by applying pressure to a mixture of hard particles and metal alloy powder to form a billet, then machining the billet to a desired over-sized conical shaped product. Then the conical-shaped product is liquid-phase sintered to a desired density, which causes shrinking to the desired final shape.Type: GrantFiled: December 7, 2009Date of Patent: October 25, 2011Assignee: Baker Hughes IncorporatedInventors: Redd H. Smith, Trevor Burgess, Jimmy W. Eason
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Patent number: 8034153Abstract: A composition for coating sliding or rolling or fretting or impacting members is formed by preparing a composite powder of TiB2 and BN, with a TiB2 to BN ratio ranging from 1:7 to 20:1, and a metallic matrix selected from the group consisting of nickel, chromium, iron, cobalt, aluminum, tungsten, carbon and alloys thereof.Type: GrantFiled: December 21, 2006Date of Patent: October 11, 2011Assignee: Momentive Performances Materials, Inc.Inventors: Robert Marchiando, Jon Leist
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Publication number: 20110243484Abstract: The present invention relates to a sliding bearing with improved wear resistance which is manufactured in a sintered body type, and more particularly, to a bush type of sliding bearing that has excellent friction and wear characteristics with a shaft usually made of an iron-based material even under very poor sliding conditions of high-surface pressure, low speed, and irregularity, such that the lubrication cycle of may be extended, and also has excellent hardness such that load feed capability, plastic deformation suppression, and fatigue strength can be improved.Type: ApplicationFiled: October 22, 2009Publication date: October 6, 2011Applicant: DOOSAN INFRACORE CO., LTD.Inventors: Chung Rae Lee, Dong Seob Shim, Sang Beom Kim
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Publication number: 20110214529Abstract: A process for forming a remateable machined titanium powder base alloy connecting rod using a titanium alloy powder having an average particle size of about 1-20 microns, a mean aspect ratio of about 5 to 300, and a specific surface area of at least about 25 m2/g.Type: ApplicationFiled: May 12, 2011Publication date: September 8, 2011Inventor: Gerald Martino
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Patent number: 8007714Abstract: The present invention relates to compositions and methods for forming a bit body for an earth-boring bit. The bit body may comprise hard particles, wherein the hard particles comprise at least one of carbide, nitride, boride, oxide, and solid solutions thereof, and a binder binding together the hard particles. The binder may comprise at least one metal selected from cobalt, nickel, and iron and, optionally, at least one melting point reducing constituent selected from a transition metal carbide in the range of 30 to 60 weight percent, boron up to 10 weight percent, silicon up to 20 weight percent, chromium up to 20 weight percent, and manganese up to 25 weight percent, wherein the weight percentages are based on the total weight of the binder.Type: GrantFiled: February 20, 2008Date of Patent: August 30, 2011Assignees: TDY Industries, Inc., Baker Hughes IncorporatedInventors: Prakash K. Mirchandani, Jimmy W. Eason, James J. Oakes, James C. Westhoff, Gabriel B. Collins, John H. Stevens, Steven G. Caldwell, Alfred J. Mosco
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Publication number: 20110150691Abstract: A method for preparing a rare earth permanent magnet material comprises the steps of: disposing a powder comprising one or more members selected from an oxide of R2, a fluoride of R3, and an oxyfluoride of R4 wherein R2, R3 and R4 each are one or more elements selected from among rare earth elements inclusive of Y and Sc on a sintered magnet form of a R1—Fe—B composition wherein R1 is one or more elements selected from among rare earth elements inclusive of Y and Sc, and then heat treating the magnet form and the powder at a temperature equal to or below the sintering temperature of the magnet in vacuum or in an inert gas. The result high performance, compact or thin permanent magnet has a high remanence and coercivity at a high productivity.Type: ApplicationFiled: February 24, 2011Publication date: June 23, 2011Applicant: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Hajime Nakamura, Koichi Hirota, Takehisa Minowa
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Publication number: 20110150692Abstract: A cemented carbide body is 1-30% by mass of binder consisting of Co, Co/Ni, Co/Fe, Co/Ni/Fe or Ni/Fe and a hard material having a hexagonal WC phase and having a face-centered cubic phase of the form (M1, M2, M3)C or (M1, M2, M3)(C, N) or (M1, M2, M3)(O, C, N) where M1=Ti and/or Zr and M2=W and M3 optionally means none or one or a plurality of the elements Ta, Nb, Hf, Cr, Mo or V, wherein the proportion of the face-centered cubic phase based on the total mass is 2% to 97%, preferably 5 to 12% by mass, and the microstructure of the hexagonal phase and of the face-centered cubic phase has a mean grain size of between 0.2 ?m and 1 ?m, preferably ?0.9 ?m, and the mean grain sizes of the hexagonal phase and of the face-centered cubic phase differ at most by 30%.Type: ApplicationFiled: July 14, 2009Publication date: June 23, 2011Inventors: Klaus Rödiger, Hendrikus Van Den Berg, Walter Lengauer, Klaus Dreyer, Dominic Janisch
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Publication number: 20110135530Abstract: A method of making a powder metal compact is disclosed. The method includes forming a coated metallic powder comprising a plurality of coated metallic powder particles having particle cores with nanoscale metallic coating layers disposed thereon, wherein the metallic coating layers have a chemical composition and the particle cores have a chemical composition that is different than the chemical composition of the metallic coating layers. The method also includes applying a predetermined temperature and a predetermined pressure to the coated powder particles sufficient to form a powder metal compact by solid-phase sintering of the nanoscale metallic coating layers of the plurality of coated powder particles to form a substantially-continuous, cellular nanomatrix of a nanomatrix material, a plurality of dispersed particles dispersed within the cellular nanomatrix and a solid-state bond layer extending throughout the cellular nanomatrix.Type: ApplicationFiled: December 8, 2009Publication date: June 9, 2011Inventors: Zhiyue Xu, Gaurav Agrawal, Bobby Salinas
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Publication number: 20110091345Abstract: A method for producing a high strength aluminum alloy tubing containing L12 dispersoids from an aluminum alloy powder containing the L12 dispersoids. The powder is consolidated into a billet having a density of about 100 percent. The tube is formed by at least one of direct extrusion, Mannesmann process, pilgering, and rolling.Type: ApplicationFiled: October 16, 2009Publication date: April 21, 2011Applicant: United Technologies CorporationInventor: Awadh B. Pandey
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Publication number: 20110064599Abstract: A method for producing a high strength aluminum alloy brackets, cases, tubes, ducts, beams, spars and other parts containing L12 dispersoids from an aluminum alloy powder containing the L12 dispersoids. The powder is consolidated into a billet having a density of about 100 percent. The billet is extruded using an extrusion die shaped to produce the component.Type: ApplicationFiled: September 15, 2009Publication date: March 17, 2011Applicant: UNITED TECHNOLOGIES CORPORATIONInventor: Awadh B. Pandey
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Patent number: 7871562Abstract: Process for manufacturing composite metal/ceramic thin films, consisting of: a) preparing a suspension (S) in an organic solvent starting from a substantially homogenous mixture of ceramic reinforcements, metallic particles, a binder, a plasticizer and a dispersant, the metallic particles constituting at least 5% by weight of the suspension; b) tape casting the suspension to form a thin film, and then de-binding said thin film; c) densifying the de-binded thin film in a furnace.Type: GrantFiled: May 4, 2009Date of Patent: January 18, 2011Assignee: Centre National de la Recherche ScientifiqueInventors: Jean-François Silvain, Thierry Chartier, Pierre-Marie Geffroy
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Patent number: 7867438Abstract: A method of manufacturing a powdered composition or starting material used in producing a CBN compact which comprises CBN, a secondary hard phase and a binder phase includes two steps of attrition milling. First, the attrition milling of the secondary hard phase and the binder phase. Second, adding CBN particles to the fine particle mixture of the first attrition milling and then attrition milling this mixture.Type: GrantFiled: October 28, 2005Date of Patent: January 11, 2011Inventors: Nedret Can, Stig Ake Andersin, Robert Fries, Iain Patrick Goudemond
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Publication number: 20100278679Abstract: There is provided cryogenic milled nanophase copper alloys and methods of making the alloys. The alloys are fine grained having grains in the size range from about 2 to about 100 nanometers, and greater. The nanophase alloys possess desirable physical properties stemming from the fine grain size, such as potentially high strength. Some embodiments of the cryogenic milled copper alloys may also be tailored for ductility, toughness, fracture resistance, corrosion resistance, fatigue resistance and other physical properties by balancing the alloy composition. In addition, embodiments of the alloys generally do not require extensive or expensive post-cryogenic milling processing.Type: ApplicationFiled: December 21, 2006Publication date: November 4, 2010Inventors: Barun Majumdar, James D. Cotton, Clifford C. Bampton
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Patent number: 7824507Abstract: A method of producing high strength nanophase metal alloy powder by cryomilling metal powder under conditions which cause the formation of intrinsic nitrides, and of producing high strength metal articles by subjecting the nitrided cryomilled powder to thermo-mechanical processing. The intrinsic nitrides present within the alloy significantly reduce grain growth during thermo-mechanical processing, resulting in formed metal products of high strength and improved ductility.Type: GrantFiled: January 25, 2008Date of Patent: November 2, 2010Assignee: The Boeing CompanyInventors: Thomas J. Van Daam, Clifford C. Bampton
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Publication number: 20100227188Abstract: An economic ferrous sintered multilayer roll-formed bushing, a producing method of the same and a connecting device are provided, in which a ferrous sintered sliding material layer is tightly sintered-bonded to a back metal steel, the ferrous sintered sliding material layer being intended to have low coefficient of friction, having excellent seizing resistance and abrasion resistance and providing self-lubricating property so as to prolong a lubrication interval or eliminate the necessity of lubricating. The ferrous sintered multilayer roll-formed bushing according to the present invention comprises: a back metal steel; a ferrous sintered sliding material layer sinter-bonded to the back metal steel; a diffusion layer of ferrous alloy particle formed at the vicinity of the bonding boundary between the ferrous sintered sliding material layer and the back metal steel; and a Cu alloy phase formed at the vicinity of the bonding boundary and extending in the direction of the bonding boundary.Type: ApplicationFiled: January 30, 2007Publication date: September 9, 2010Inventor: Takemori Takayama
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Patent number: 7776256Abstract: Methods of forming bit bodies for earth-boring bits include assembling green components, brown components, or fully sintered components, and sintering the assembled components. Other methods include isostatically pressing a powder to form a green body substantially composed of a particle-matrix composite material, and sintering the green body to provide a bit body having a desired final density. Methods of forming earth-boring bits include providing a bit body substantially formed of a particle-matrix composite material and attaching a shank to the body. The body is provided by pressing a powder to form a green body and sintering the green body. Earth-boring bits include a unitary structure substantially formed of a particle-matrix composite material. The unitary structure includes a first region configured to carry cutters and a second region that includes a threaded pin. Earth-boring bits include a shank attached directly to a body substantially formed of a particle-matrix composite material.Type: GrantFiled: November 10, 2005Date of Patent: August 17, 2010Assignee: Baker Huges IncorporatedInventors: Redd H. Smith, John H. Stevens, James L. Duggan, Nicholas J. Lyons, Jimmy W. Eason, Jared D. Gladney, James A. Oxford, Benjamin J. Chrest
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Patent number: 7771649Abstract: Disclosed herein is a method of producing an ultrafine crystalline TiN/TiB2 composite cermet. In the method, titanium nitride (TiN)/titanium boride (TiB2)/stainless steel composite nanopowder is produced through a reaction milling process using titanium (Ti), boron nitride (BN), and stainless steel powders as raw material powders, and the resulting composite nanopowder is liquid-phase sintered. The method comprises a first step of mixing titanium powder and boron nitride powder at a molar ratio of 3:2, a second step of mixing 5-60 wt % stainless steel powder and the powder mixture, a third step of feeding the powder mixture along with a ball having a predetermined diameter into a jar and conducting a high energy ball milling process to produce titanium nitride/titanium boride/stainless steel composite nanopowder, and a fourth step of shaping and sintering the resulting composite nanopowder.Type: GrantFiled: November 19, 2007Date of Patent: August 10, 2010Assignee: Korea Institute of Science and TechnologyInventors: Jae Hyeok Shim, Ji Woo Kim, Young Whan Cho
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Publication number: 20100154587Abstract: Methods of fabricating bodies of earth-boring tools include mechanically injecting a powder mixture into a mold cavity, pressurizing the powder mixture within the mold cavity to form a green body, and sintering the green body to a desired final density to form at least a portion of a body of an earth-boring tool. For example, a green bit body may be injection molded, and the green bit body may be sintered to form at least a portion of a bit body of an earth-boring rotary drill bit. Intermediate structures formed during fabrication of an earth-boring tool include green bodies having a plurality of hard particles, a plurality of matrix particles comprising a metal matrix material, and an organic material that includes a long chain fatty acid derivative. Structures formed using the methods of fabrication are also disclosed.Type: ApplicationFiled: December 22, 2008Publication date: June 24, 2010Inventor: Jimmy W. Eason
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Publication number: 20100124514Abstract: A method of uniformly dispersing a nano powder throughout a micron powder. Ordinary mixing or agitation does not succeed in attaining uniform dispersal: the nano powder agglomerates into microscopic masses. In one form of the invention, a charge of a micron powder, with fifty weight percent of charge of nanopowder is loaded into a ball mill. The mixture is ball milled for less than two hours, at room temperature in a dry condition, and produces a highly uniform distribution of the nano powder throughout the micron powder.Type: ApplicationFiled: September 14, 2006Publication date: May 20, 2010Applicants: THE TIMKEN COMPANY, IAP RESEARCH, INC.Inventors: Bhanumathi Chelluri, Edward Arlen Knoth, Edward John Schumaker, Ryan D. Evans, James. L. Maloney, III
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Patent number: 7635448Abstract: A compact is obtained from a mixed powder of a multi-component system ceramics composed of constitutive elements of at least two metal elements selected from the group consisting of Ti, Al, V, Nb, Zr, Hf, Mo, Ta, Cr, and W, N, and optionally C; and Fe, Ni, Co, or an alloy composed of a constitutive element of at least one metal element of Fe, Ni, and Co. A composite material is prepared by sintering the compact.Type: GrantFiled: September 10, 2004Date of Patent: December 22, 2009Assignee: Honda Giken Kogyo Kabushiki KaishaInventors: Mitsuo Kuwabara, Masanori Ohtsuka
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Patent number: 7585456Abstract: The invention concerns a method for making thin films in metal/ceramic composite, characterized in that it consists in: a) preparing a suspension (S) in an organic solvent from a substantially homogeneous mixture of ceramic reinforcements of metal particles, a binder, a plasticizing agent and an organic dispersant, the metal particles constituting at least 5 wt. % of the suspension; b) tape casting the suspension (S) to form a thing film (B), then culminating organic compounds contained in the binder and the plasticizing agent from said thin film; c) densifying the thin film from which said organic compounds have been removed in an oven.Type: GrantFiled: December 6, 2001Date of Patent: September 8, 2009Assignee: Centre National de la Recherche ScientifiqueInventors: Jean-François Silvain, Thierry Chartier, Pierre-Marie Geffroy
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Patent number: 7578867Abstract: A ceramic sintered product which comprises a first hard phase containing a nitride of titanium, a second hard phase containing at least one of alumina and zirconia, and a binding phase containing nickel; and a method for producing the ceramic sintered product. The ceramic sintered product is lightweight and exhibits good abrasion resistance in a wet atmosphere, and further can be produced at a low cost.Type: GrantFiled: September 28, 2006Date of Patent: August 25, 2009Assignee: Kyocera CorporationInventors: Kenichi Hamamura, Saburou Nagano
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Patent number: 7553563Abstract: The invention concerns a composite material consisting of intermetallic phases and ceramic, in particular in the form of a coating on metallic substrates, as well as an arc wire spraying process for production of the composite material in which the intermetallic phases and the ceramics to be deposited are newly formed during the deposit process from the components of the supplied wires by chemical reaction. The invention further concerns wear resistant layers formed by the composites, tribologic layers and plating or hard-facing materials.Type: GrantFiled: February 9, 2004Date of Patent: June 30, 2009Assignee: Daimler AGInventors: Stefan Grau, Michael Scheydecker, Karl Weisskopf
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Patent number: 7537726Abstract: A component is produced by powder metallurgy from hard metal. The alloy includes at least one grain growth-inhibiting additive from the group consisting of V, Cr, Ti, Ta and Nb with, at least locally, a graduated concentration profile. As a result, the mechanical properties also have a graduated profile. In the fabrication process, a dispersion or solution which contains the grain growth-inhibiting additive in finely distributed or dissolved form is applied to the surface of a green compact. Penetration of this dispersion or solution along open pores leads to a graduated distribution of the grain growth-inhibiting additive in the green compact. There is also described a process in which the grain growth-inhibiting additive in the form of a solution is distributed uniformly in the green compact and is then gradually broken down from edge regions by a heat treatment or a solvent.Type: GrantFiled: October 9, 2007Date of Patent: May 26, 2009Assignee: CERATIZIT Austria Gesellschaft m.b.H.Inventors: Johannes Glätzle, Rolf Kösters, Wolfgang Glätzle
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Publication number: 20090053089Abstract: A method of making a homogeneous granulated metal-based powder, comprises steps of: providing preselected amounts of at least one metal element or metal alloy, at least one ceramic compound, and/or at least one non-metallic element; forming a homogeneous slurry/suspension or wet mixture comprising the preselected amounts of metal element(s) and/or metal alloys, ceramic compound(s), and/or non-metallic element(s), a liquid phase comprising at least one liquid, and at least one binder material; drying the slurry/suspension or mixture to remove at least a portion of the liquid phase and form a powder mixture comprising partially or completely dried granules; and subjecting the granules to a thermal de-binder process for effecting: additional removal of any remaining liquid phase, if necessary; removal of the at least one binder material; reduction of carbon content; reduction of oxygen on the surfaces or interior of the metal or metal alloy phases in the granules; and optional partial sintering for strengtheningType: ApplicationFiled: August 20, 2007Publication date: February 26, 2009Applicant: HERAEUS INC.Inventors: Fenglin YANG, Carl Derrington, Bernd Kunkel
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Publication number: 20090011266Abstract: In a method of making a molybdenum, molybdenum silicide and molybdenum silicon boride composite material, a boron nitride powder, a silicon nitride powder and a molybdenum powder are mixed to form a composite precursor. The composite precursor is sintered in an atmosphere consisting essentially of hydrogen and argon to form a sintered material. The sintered material is hot isostatic pressed to form the composite material into a final shape.Type: ApplicationFiled: July 1, 2008Publication date: January 8, 2009Applicant: GEORGIA TECH RESEARCH CORPORATIONInventors: Joe K. Cochran, Kon J. Lee, Michael R. Middlemas
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Publication number: 20080314200Abstract: The present invention relates to a fine grained WC-Co cemented carbide. By adding an extremely small amount of Ti, V, Zr, Ta or Nb alone or in combinations, a grain refined cemented carbide structure with less abnormal WC-grains has been obtained.Type: ApplicationFiled: May 30, 2008Publication date: December 25, 2008Applicant: SANDVIK INTELLECTUAL PROPERTY ABInventors: Susanne NORGREN, Alexandra KUSOFFSKY, Alistair GREARSON
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Patent number: 7435376Abstract: A composite of a metal matrix with one or more incorporated secondary phases is referred to as a metal matrix composite (MMC). Secondary phase refers to all the particles or fibers which have a different composition than the metal matrix, and which are incorporated therein. As incorporation phases, elements and compounds are possible which, as a result of their material characteristics, are suited for improving individual properties of the metal matrix. Besides an improvement in individual properties of the pure metal matrix as a result of the incorporated secondary phase, certain properties of the metal are also degraded, in particular by particles having a size of 1 to 50 ?m. For example, the elongation at break decreases, the strength may decrease, or the tribology may become less favorable.Type: GrantFiled: December 15, 2003Date of Patent: October 14, 2008Assignee: CeramTec AGInventors: Dirk Rogowski, Ilka Lenke, Dieter Theil
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Publication number: 20080145261Abstract: A method for forming a carbide composite that includes providing a mixture of carbide particles and a metallic binder in a container; sintering the container contents at a first processing condition having a pressure of less than about 45,000 psi; and sintering the container contents at a second processing condition having a pressure of greater than about 100,000 psi is disclosed.Type: ApplicationFiled: December 15, 2006Publication date: June 19, 2008Applicant: Smith International, Inc.Inventors: Zhou Yong, Sike Xia, Sharath Kolachalam
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Patent number: 7364628Abstract: A solid material for a magnet, comprising a rare-earth/iron/nitrogen/hydrogen system magnetic material.Type: GrantFiled: April 24, 2002Date of Patent: April 29, 2008Assignee: Asahi Kasei Kabushiki KaishaInventors: Etsuji Kakimoto, Kiyotaka Dohke, Ichiro Shibasaki, Nobuyoshi Imaoka, Akira Chiba
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Patent number: 7354490Abstract: High strength aluminum alloy powders, extrusions, and forgings are provided in which the aluminum alloys exhibit high strength at atmospheric temperatures and maintain high strength and ductility at extremely low temperatures. The alloy is produced by blending about 89 atomic % to 99 atomic % aluminum, 1 atomic % to 11 atomic % of a secondary metal selected from the group consisting of magnesium, lithium, silicon, titanium, zirconium, and combinations thereof, and up to about 10 atomic % of a tertiary metal selected from the group consisting of Be, Ca, Sr, Ba, Ra, Sc, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Y, Nb, Mo, Tc, Ru, Rh, Pd, Ag, Cd, W, and combinations thereof. The alloy is produced by nanostructure material synthesis, such as cryomilling, in the absence of refractory dispersoids. The synthesized alloy is then canned, degassed, consolidated, extruded, and optionally forged into a solid metallic component. Grain size within the alloy is less than 0.5 ?m, and alloys with grain size less than 0.Type: GrantFiled: February 5, 2004Date of Patent: April 8, 2008Assignee: The Boeing CompanyInventors: Leslie G. Fritzemeier, Daniel E. Matejczyk, Thomas J. Van Daam
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Patent number: 7344675Abstract: A method of producing high strength nanophase metal alloy powder by cryomilling metal powder under conditions which cause the formation of intrinsic nitrides, and of producing high strength metal articles by subjecting the nitrided cryomilled powder to thermo-mechanical processing. The intrinsic nitrides present within the alloy significantly reduce grain growth during thermo-mechanical processing, resulting in formed metal products of high strength and improved ductility.Type: GrantFiled: March 12, 2003Date of Patent: March 18, 2008Assignee: The Boeing CompanyInventors: Thomas J. Van Daam, Clifford C. Bampton
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Publication number: 20080025802Abstract: It is an object to provide a CBN cutting tool using cBN-based sintered bodies which shows high resistance to chipping even when a hard ferric workpiece which is difficult to cut is cut at a high feed rate for high-speed, high-efficiency machining, and which can provide a machined surface that shows superior surface roughness, and improved fatigue life and sealability. A cBN-based sintered body of a cutting tip has an arcuate nose 5, a rake face 6, flanks 7 and a negative land 9. One of the cutting edges 10 defined between the negative land 9 and the flanks 7 that serves as an end cutting edge forms an inclination angle ?? of not less than 20 degrees and not more than 35 degrees with respect to the rake face. Further, the cutting edges 10 are positioned such that they are the lowest at the apex P of the arcuate nose and gradually rise from the apex P toward two points Q1 and Q2, respectively.Type: ApplicationFiled: March 14, 2006Publication date: January 31, 2008Inventor: Satoru Kukino
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Patent number: 7311873Abstract: The invention relates to manufacturing of fully dense strips, plates, sheets, and foils from titanium alloys, titanium metal matrix composites, titanium aluminides, and flat multilayer composites of said materials by direct powder rolling of blended powders followed by sintering. The resulting titanium alloy flat products have properties that meet or exceed the conventional ingot metallurgy alloys and are suitable for aerospace, automotive, sporting goods, and other applications. The process includes: (a) providing C.P.Type: GrantFiled: December 30, 2004Date of Patent: December 25, 2007Assignee: ADMA Products, Inc.Inventors: Vladimir S. Moxson, Volodymyr A. Duz
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Patent number: 7211218Abstract: Polycrystalline diamond (PCD) carbide composites of this invention have a microstructure comprising a plurality of granules formed from PCD, polycrystalline cubic boron nitride, or mixture thereof, that are distributed within a substantially continuous second matrix region that substantially surrounds the granules and that is formed from a cermet material. In an example embodiment, the granules are polycrystalline diamond and the cermet material is cemented tungsten carbide. PCD carbide composites of this invention display improved properties of fracture toughness and chipping resistance, without substantially compromising wear resistance, when compared to conventional pure PCD materials.Type: GrantFiled: September 5, 2002Date of Patent: May 1, 2007Assignee: Smith International, Inc.Inventors: Zhigang Fang, Anthony Griffo, Brian A. White, Stewart Middlemiss, Ron K. Eyre