Powder Shape Or Size Characteristics Patents (Class 419/23)
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Patent number: 4818628Abstract: A process for making a composite bearing material comprising a steel backed, prealloyed, lead-bronze sintered powder metal matrix whereby the first sinter step includes induction heating the prealloyed powder and steel backing to above 650.degree. C. and thereafter sintering the same at temperatures of about 850.degree. C. in a second sintering furnace. A composite bearing material made by the same process and comprising a lead particle size averaging less than about 8 microns and having no lead islands larger than about 44 microns.Type: GrantFiled: August 31, 1987Date of Patent: April 4, 1989Assignee: Federal-Mogul CorporationInventors: Robert G. Alexander, George C. Pratt
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Patent number: 4810289Abstract: A process of hot isostatic pressing of powders to form electrical contacts is characterized by the steps: (A) mixing powders, 1 in the Drawing, from metal containing powder or metal containing powder plus carbon powder, where at least one of Ag and Cu is present, (B) thermal cleaning treatment of the powder, 2 in the Drawing, (C) granulating the thermally treated powder, 3 in the Drawing, (D) uniaxially pressing the powders without heating, 5 in the Drawing, to provide a compact, (E) placing at least one compact in a pressure-transmitting, pressure-deformable container, 6 in the Drawing, and surrounding each compact with fine particles of a separating material, (F) evacuating air from the container, 7 in the Drawing, (G) sealing the compacts inside the container, 8 in the Drawing, (H) hot isostatic pressing, 9 in the Drawing, the compacts through the pressure transmitting material at a pressure from 352 kg/cm.sup.2 to 2,115 kg/cm.sup.2 and a temperature from 0.5.degree. C. to 100.degree. C.Type: GrantFiled: April 4, 1988Date of Patent: March 7, 1989Assignee: Westinghouse Electric Corp.Inventors: Norman S. Hoyer, Natraj C. Iyer
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Patent number: 4808226Abstract: A process of fabricating steel stock for bearing components from highly alloyed steel powders supersaturated in carbon up to 0.5 weight percent in ferrite and up to 1.0 weight percent in austenite type combinations is disclosed. Rapid solidification of an atomized molten composition yields a metal powder with a diameter ranging between 75 and 105 microns. The metal powder is then compressed and heated to a low forging temperature between 1,600.degree. and 1,800.degree. F. to yield the steel stock.Type: GrantFiled: November 24, 1987Date of Patent: February 28, 1989Assignee: The United States of America as represented by the Secretary of the Air ForceInventor: Colin M. Adam
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Patent number: 4808249Abstract: A method for producing an integral titanium alloy article having at least two regions, each region having a distinct microstructure is provided. The method comprises heat treating one or more selected region(s) of the article at a temperature greater than the beta-transus temperature of the region(s), while simultaneously heat treating the remaining region(s) of the article at a temperature below the beta-transus temperature of the remaining region(s).Type: GrantFiled: May 6, 1988Date of Patent: February 28, 1989Assignee: The United States of America as represented by the Secretary of the Air ForceInventors: Daniel Eylon, Francis H. Froes
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Patent number: 4801340Abstract: A method for manufacturing a permanent magnet using alloys of the formula R(T.sub.1-y M.sub.y).sub.z, wherein R denotes one or two species of rare earth metals, including Y, T denotes transition metals, principally Fe or Fe and Co, M denotes metalloid elements, principally B, and wherein 0.02<y<0.15, and 5<z<9), to obtain permanent magnets with high orientation properties through the formation of 50-1000 .mu.m crude grains by spraying the alloys in a hot melt state using an inert gas atomization process, forming grains of less than 30 .mu.m by a mechanical pulverizing process after crystal texture in the crude grains has grown to over 30 .mu.m granules by a heat-treatment of the crude grains in a vacuum or in an inert atmosphere below 1000.degree. C., whereupon the grain powder is compression molded and heat treated at 500.degree.-900.degree. C. under a magnetic field to yield a compacted powder permanent magnet.Type: GrantFiled: June 11, 1987Date of Patent: January 31, 1989Assignee: Namiki Precision Jewel Co., Ltd.Inventors: Nobuyuki Inoue, Katsumi Takahashi, Nobuo Imaizumi
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Patent number: 4793967Abstract: The present invention is directed to a cermet material comprising a matrix of aluminum alloy with ceramic particles distributed therein. The cermet is adapted for use as a semiconductor substrate and is manufactured using powder technology procedures. The cermet comprises from about 40 to about 60 volume % of aluminum or aluminum alloy, from an effective amount up to about 10 volume % of binder for enhancing bonding between the aluminum alloy and ceramic particles, and the balance essentially ceramic particles.Type: GrantFiled: December 31, 1987Date of Patent: December 27, 1988Assignee: Olin CorporationInventors: Michael J. Pryor, Eugene Shapiro, Deepak Mahulikar
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Patent number: 4792367Abstract: High energy product, magnetically anisotropic permanent magnets are produced by hot working overquenched or fine grained, melt-spun materials comprising iron, neodymium and/or praseodymium, and boron to produce a fully densified, fine grained body that has undergone plastic flow.Type: GrantFiled: March 17, 1986Date of Patent: December 20, 1988Assignee: General Motors CorporationInventor: Robert W. Lee
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Patent number: 4780437Abstract: A porous layer of catalyst material suitable for use as an electrode in a molten carbonate fuel cell includes elongated pores substantially extending across the layer thickness. The catalyst layer is prepared by depositing particulate catalyst material into polymeric flocking on a substrate surface by a procedure such as tape casting. The loaded substrate is heated in a series of steps with rising temperatures to set the tape, thermally decompose the substrate with flocking and sinter bond the catalyst particles into a porous catalytic layer with elongated pores across its thickness. Employed as an electrode, the elongated pores provide distribution of reactant gas into contact with catalyst particles wetted by molten electrolyte.Type: GrantFiled: February 11, 1987Date of Patent: October 25, 1988Assignee: The United States of America as represented by the United States Department of EnergyInventor: James L. Smith
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Patent number: 4777014Abstract: Self-supporting bodies are produced by reactive infiltration of a parent metal with a boron source typically resulting in a composite comprising a parent metal boride and metal. The mass to be infiltrated may contain one or more inert fillers admixed with the boron source to produce a composite by reactive infiltration, which composite comprises a matrix of metal and parent metal boride embedding the filler. The relative amounts of reactants and process conditions may be altered or controlled to yield a body containing varying volume percents of ceramic, metal and/or porosity.Type: GrantFiled: March 7, 1986Date of Patent: October 11, 1988Assignee: Lanxide Technology Company, LPInventors: Marc S. Newkirk, Michael K. Aghajanian, Danny R. White
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Patent number: 4775598Abstract: A process is described in which hollow spheres or hollow-sphere composites (moldings) having high-strength walls are produced. Additional layers are applied to metallized spherical lightweight particles having a core of foamed polymer. In order to increase the strength of the wall of the spherical particle and the strength of the molding, metallized lightweight spherical particles having a metal wall thickness of 5 to 20 microns are treated (coated) with a dispersion of particulate metal or metal oxide or particulate ceramic or refractory material, the lightweight spherical particles coated in a thickness from 15 to 500 microns are dried, the dried particles are heated to a temperature of about 400.degree. C. to effect a pyrolysis of the polymer core, and the particles are subsequently sintered at a temperature from 900.degree. to 1400.degree. C.Type: GrantFiled: November 25, 1987Date of Patent: October 4, 1988Assignee: Norddeutsche Affinerie AkitiengesellschaftInventor: Manfred Jaeckel
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Patent number: 4765954Abstract: A rapidly solidified magnesium based alloy contains finely dispersed magnesium intermetallic phases. The alloy has the form of a filament or a powder and is especially suited for consolidation into bulk shapes having superior combination of strength, ductility and corrosion resistance.Type: GrantFiled: September 30, 1985Date of Patent: August 23, 1988Assignee: Allied CorporationInventors: Santosh K. Das, Chin-Fong Chang
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Patent number: 4762557Abstract: A high temperature, oxidation resistant alloy useful in high temperature, oxidizing environments such as those encountered in gas turbines, advanced jet engines, high temperature furnaces and glass melting and processing equipment, among others.The alloy is characterized by selecting a refractory alloy from the group consisting of molybdenum, tungsten, niobium and tantalum having dispersed therein a second phase additive of titanium nitride and a third phase additive of aluminum and titanium. Alternatively, the refractory metals may be molybdenum or tungsten and the second phase additive and third phase additive may be silicon nitride and silicon, or chromium nitride and chromium respectively.Type: GrantFiled: October 1, 1987Date of Patent: August 9, 1988Assignee: Battelle Memorial InstituteInventors: Vaidyanathan Nagarajan, Ian G. Wright
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Patent number: 4762558Abstract: Reactive sintering process for producing a shaped body containing the nickel aluminide compound Ni.sub.3 Al, which comprises sintering a compacted shaped mass containing an intimate mixture of substances, e.g. including elemental nickel powder and elemental aluminum powder in a stoichiometric atomic ratio generally corresponding to the compound Ni.sub.3 Al, by heating the mass, e.g. in a vacuum, to an elevated sintering temperature, e.g. 500-750.degree. C., sufficiently to initiate an exothermic reaction, and at a heating rate sufficiently for consequent progressive generation of a transient liquid below the melting point of the aluminum powder and at the corresponding eutectic temperature, and upon initiation of the exothermic reaction continuing the sintering sufficiently to form a densified shaped body containing the nickel aluminide compound Ni.sub.Type: GrantFiled: May 15, 1987Date of Patent: August 9, 1988Assignee: Rensselaer Polytechnic InstituteInventors: Randall M. German, Animesh Bose, David Sims
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Patent number: 4761262Abstract: A method for sintering a metal powder, a ceramic powder, or a mixture thereof accomplishes compact sintering of even a high melting substance by heating the powder at an elevated temperature for a short time under not less than 10,000 atmospheres of pressure. To attain the quick high-temperature heating under the ultrahigh pressure, a Thermit reaction is generated in an ultrahigh pressure generating apparatus which is provided with a gasket made of pyrophyllite and cylinders and anvils protected with heat insulators.For the purpose of preventing the Thermit reaction from inducing a reaction between the Thermit composition and the powder under treatment and the heater and ensuring electrical insulation of these components, barriers made of hexagonal boron nitride and/or tantalum are suitably disposed within the apparatus.Type: GrantFiled: October 8, 1986Date of Patent: August 2, 1988Assignee: Kabushiki Kaisha Komatsu SeisakushoInventors: Masaru Ogata, Shuichi Takeda
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Patent number: 4759905Abstract: Apparatus is provided for the production of ultrafine powder. The powder is produced by spark erosion within an electric discharge cell. The starting material for production of the powder is a body in chunk form of the material to be pulverized. The material is contained in an electric discharge cell having a fine mesh screen bottom. The cell and its contents are immersed in a dielectric fluid such as water, liquified gas or an organic base liquid. The cell and its contents are vibrated to cause the chunks to separate repeatedly and momentarily. A sparking voltage is impressed repeatedly through the body to develop sparks between confronting portions of separated chunk surfaces. Small particles produced as a result of the sparking fall through the screen of the cell and are collected as product.Type: GrantFiled: April 3, 1987Date of Patent: July 26, 1988Assignee: General Electric CompanyInventors: John L. Walter, Ami E. Berkowitz
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Patent number: 4756753Abstract: An aluminum matrix composite containing evenly dispersed reinforcement particles in the aluminum matrix wherein the contents of oxygen and carbon are controlled so that their volume percentage is not larger than 20% and wherein the contents of the reinforcement particles, oxygen and carbon are controlled so that their volume percentage is not larger than 40%. The control of oxygen and carbon is effected by carrying out the main process at a non-oxidizing atmosphere and minimizing the addition of an anti-seizure agent required to facilitate the mechanical alloying treatment.Type: GrantFiled: August 26, 1987Date of Patent: July 12, 1988Assignee: Showa Aluminum Kabushiki KaishaInventor: Tsunemasa Miura
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Patent number: 4755368Abstract: A process for formation of a silica filler product comprising the steps of subjecting fluidized silicon powder to combustion at a temperature of about 3000.degree. K. and quenching the combustion products to form a silica powder characterized by a large proportion of discrete, non-agglomerated primary particles.Type: GrantFiled: June 26, 1986Date of Patent: July 5, 1988Assignee: Ulrich Research & Consulting, Inc.Inventors: Gael D. Ulrich, Dennis W. Molesky
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Patent number: 4755221Abstract: Composite powder particles which are essentially spherical in shape are disclosed which consist essentially of particles of a matrix phase which consists essentially of a metal selected from the group consisting of aluminum and aluminum based alloys and a reinforcement phase which is relatively uniformly dispersed in and bonded to the matrix, the reinforcement phase comprising titanium diboride.A process is disclosed for producing the above composite particles which involves entraining in a carrier gas a plurality of agglomerated powders, at least one of the powders supplying aluminum, at least one of the powders supplying titanium without boron and at least one of the powders supplying boron without titanium. The powders are fed through a high temperature zone to cause essentially complete melting and coalescence of the powders wherein at least a part of the titanium and at least a part of the boron combine to form titanium diboride and thereafter resolidified to form the composite powder particles.Type: GrantFiled: March 24, 1986Date of Patent: July 5, 1988Assignee: GTE Products CorporationInventors: Muktesh Paliwal, Walter A. Johnson
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Patent number: 4755353Abstract: A process is disclosed for producing discontinuous metal foils. The process involves entraining metal powder particles in a carrier gas and passing the powder particles through a high temperature zone at a temperature above the melting point of the powder particles to melt at least about 50% by weight of the powder particles and thereafter resolidifying the resulting high temperature treated material by impacting the material against a substrate to form the foils.Type: GrantFiled: April 3, 1987Date of Patent: July 5, 1988Assignee: GTE Products CorporationInventors: Nelson E. Kopatz, Jack E. Vanderpool, Philip E. Stermer, Howard H. Shaw
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Patent number: 4752333Abstract: The invention concerns alloys comprising a matrix based on at least one conductor metal M, formed by a homogeneous dispersion in the matrix of stable coherent particles of one or more associations of ions of type M, M', O in which M represents the metal or metals of the matrix, M' represents a different metal from M, which is capable of undergoing internal oxidation, and O represents oxygen.It also concerns the process for the production of such alloys which comprises subjecting a starting alloy powder to the action of an oxidizing agent formed by a powder with a granulometry of the order of 1 .mu.m of a metal oxide capable by thermal decomposition of providing the oxygen necessary for the internal oxidization of M', the starting alloy being based on at least one metal M, if appropriate hardened by one or more elements R or A as defined hereinbefore.Use of such alloys for the electrical, electronic and connection arts.Type: GrantFiled: January 9, 1987Date of Patent: June 21, 1988Assignee: TrefimetauxInventors: Jules Caisso, Martine Cahoreau, Edmond Dedieu, Michel Grosbras
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Patent number: 4749410Abstract: An article of tungsten heavy alloy material is disclosed, the article having essentially elongated tungsten grains, the alloy material comprising tungsten, nickel, and iron, the elongated tungsten grains having a length to diameter ratio of at least about 2 to 1.A method is disclosed for producing the above article which involves rolling a pressed and sintered body of tungsten heavy alloy material comprising tungsten, iron, and nickel in a tandem rolling mill having a succession of roll stands, each stand consisting essentially of three rolls positioned at about 120.degree. to each other so that the gap between the rolls is a triangle, each stand being rotated about 180.degree. with respect to the adjacent roll stands, the rolling being done at a sufficient temperature to produce the article which has essentially elongated tungsten grains.Type: GrantFiled: February 17, 1987Date of Patent: June 7, 1988Assignee: GTE Products CorporationInventors: James A. Mullendore, James R. Spencer
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Patent number: 4749545Abstract: This invention relates to metal matrix composites containing at least 40% v/v of a hard material such as SiC and a matrix of aluminium, magnesium or alloys of either. The invention also covers a method of making such composites by ball milling powders of the respective components. Other mixing techniques do not enable such a high proportion of hard material to be incorporated into the composite. The composites are useful to produce components resistant to wear.Type: GrantFiled: March 26, 1987Date of Patent: June 7, 1988Assignee: British Petroleum Co. p.l.c.Inventors: Alan R. Begg, Andrew D. Tarrant
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Patent number: 4746363Abstract: Cermet body formed by reaction sintering at pressures ranging from subatmospheric to superatmospheric of admixed and shaped particulate exothermic reactants, which have maximum particle size substantially not greater than 150 .mu.m and can be elements, compounds, intermetallic compounds and/or alloys, in stoichiometric proportions to substantially form 40-95 mole percent of first phase or phases being boride, nitride, silicide, sulfide or combination thereof of one or more of the elements of Groups 2a, 3a exclusive of B, 4a, 2b, 3b including lanthanide and actinide series elements, 4b, 5b, 6b, 7b and 8, and 5-60 mole percent of second phase or phases being metal, alloy, intermetallic compound or combination thereof of one or more of the elements of Groups 3a exclusive of B, 4a, 2b, 4b, 5b, 6b, 7b, iron, cobalt and nickel, wherein the maximum grain size of the first phase or phases is substantially not greater than 10 .mu.m and which body contains 0 to 4 weight percent oxygen.Type: GrantFiled: June 19, 1987Date of Patent: May 24, 1988Assignee: Corning Glass WorksInventor: Thomas P. DeAngelis
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Patent number: 4744944Abstract: A process is disclosed for producing tungsten heavy alloy billets. The process involves forming a uniform blend of elemental powders to form a tungsten alloy having a tungsten content of equal to or less than about 91% by weight and wherein the particle size of the tungsten is no less than about 2 micrometers in diameter. This blend is uniformly packed into a container having thermal expansion similar to that of the powder. The blend is then sintered in a hydrogen atmosphere at a temperature sufficient to impart strength to the powder and to reduce oxides and remove volatile impurities from the powder without significant densification in the powder. The powder is then solid state sintered in a reducing atmosphere at a sufficient temperature to densify the powder to at least about 90% of the theoretical density but at a temperature below the liquid phase sintering temperature of the powder, to form the billet.Type: GrantFiled: August 5, 1987Date of Patent: May 17, 1988Assignee: GTE Products CorporationInventors: James R. Spencer, De Wayne R. Grover
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Patent number: 4743185Abstract: An electrochemical cell comprising a zinc electrode in an electrolyte solution wherein the electrode is formed from a zinc powder compacted to a density of at least about 6.5 g/cc to substantially reduce the corrosion of the zinc electrode and the consequent evolution of hydrogen gas without resorting to the addition of mercury to the electrode.Type: GrantFiled: February 27, 1987Date of Patent: May 10, 1988Assignee: Sab Nife Inc.Inventors: Viet Vu, Paul F. Hettwer
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Patent number: 4743425Abstract: A method of producing ferrous sintered alloys comprises the steps of preparing mixed alloy powder containing Fe-P-C eutectic alloy powder which includes phosphorus within the range of 2.0% to 3.0% by weight, carbon not more than 4.0% by weight and one of molybdenum within the range of 8.0% to 11.0% by weight and boron within the range of 0.5% to 3.0% by weight, graphite, and ferroalloy powder containing chromium within the range of 11% to 14% by weight; causing the mixed alloy powder to be subjected to compression molding to have a green compact; and sintering the green compact to have a ferrous sintered alloy containing compound carbides in a matrix structure thereof. The graphite is so selected that the sum total of the graphite and the carbon included in the Fe-P-C eutectic alloy powder constitutes a part within the range of 5% to 8% by weight of the sum total of the graphite and the Fe-P-C eutectic alloy powder.Type: GrantFiled: September 3, 1987Date of Patent: May 10, 1988Assignees: Mazda Motor Corporation, Kawasaki Steel Corp.Inventors: Shigemi Ohsaki, Sumio Kamino, Minoru Nitta
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Patent number: 4739641Abstract: A novel process is disclosed by which contorted or distorted sheet gauge steel and other metal scrap material, generated by stamping and other deforming metal-working operations, is flattened by rolls for the purpose of increasing its bulk density and to provide a scrap product that can more efficiently be transported and used for remelting in steel-making and foundry furnaces. The process involves the steps of feeding contorted sheet metal scrap between a pair of moving compressive surfaces, compressing the scrap to substantial flatness, and discharging the flattened steel scrap. The novel apparatus for performing the process is also disclosed.Type: GrantFiled: April 25, 1986Date of Patent: April 26, 1988Assignee: Connell Limited PartnershipInventor: Alfred G. Hering
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Patent number: 4740352Abstract: The present invention is concerned with a method of molding metallic powders, in which a binder fluid having a specific freezing point, typically water, is added to the metallic powder to be molded to form a mixture, after which a die having the desired cavity is filled with said mixture. The mixture is then pressure molded and rapidly cooled, freezing the binder fluid to produce a frozen molded shape, which is then dried to remove the binder fluid and sintered.The amount of the binder fluid of specific freezing point to be added to the said metallic powder is the minimum amount that will satisfy the dual demands of flowability during molding and shape retention after the removal of the binder fluid, with from 25 to 50 vol% generally being appropriate. Molding is achieved by injection molding, compression molding or other technique in which pressure is applied to the material in the mold.Type: GrantFiled: April 10, 1985Date of Patent: April 26, 1988Assignee: Mitsubishi CorporationInventor: Nobuyuki Takahashi
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Patent number: 4737339Abstract: A workpiece consisting of a heat-resistant aluminum alloy is produced by a powder-metallurgical process wherein an alloy containing 8 to 14% by weight Fe, 0.5 to 2% by weight V and 0.2 to 1% by weight Mn is melted, the melt is cooled in a gas stream at a rate of at least 10.sup.5 .degree.C/s and is atomized to form particles having a diameter of 1 to 40 .mu.m, whereupon the powder is consolidated a temperature of 350.degree. to 450.degree. C. at a pressure of 2000 to 6000 bar, to form a pressed article. In this process, the intermetallic compound Al.sub.6 Fe stabilized by Mn occurs in fine distribution. This dispersoid imparts high ductility and toughness to the grain.Type: GrantFiled: August 11, 1987Date of Patent: April 12, 1988Assignee: BBC Brown Boveri AGInventor: Malcolm J. Couper
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Patent number: 4735770Abstract: By the inventive method, an amorphous material in powder form can be produced, whereby at least two starting components in powder form are mechanically alloyed by means of a milling process so that a boron component which cannot be alloyed mechanically can nevertheless be alloyed. According to the invention, a boron component in powder form is admixed to the starting components; this powder mixture is subjected to the milling process, an amorphous alloying component being formed from the starting components with embedded or deposited fine particles of the boron components; and the mixture powder so produced is subjected to an annealing treatment below the crystallization temperature of the amorphous alloy component for diffusing the boron into the amorphous alloy component.Type: GrantFiled: January 29, 1987Date of Patent: April 5, 1988Assignee: Siemens AktiengesellschaftInventors: Ludwig Schultz, Egon Hellstern
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Patent number: 4735656Abstract: An abrasive material comprised of a metal matrix and evenly distributed ceramic particulates, is made by mixing powder metal with the ceramic powder and heating to a temperature sufficient to melt most, but not all of the powder. In this way the ceramic does not float to the top of the material, yet a dense material is obtained. A nickel superalloy matrix will have at least some remnants of the original powder metal structure, typically some equiaxed grains, along with a fine dendritic structure, thereby imparting desirable high temperature strength when the abrasive material is applied to the tips of blades of gas turbine engines. Preferred matrices have a relatively wide liquidus-solidus temperature range, contain a melting point depressant, and a reactive metal to promote adhesion to the ceramic.Type: GrantFiled: December 29, 1986Date of Patent: April 5, 1988Assignee: United Technologies CorporationInventors: Robert P. Schaefer, David A. Rutz, Edward Lee, Edward J. Johnson
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Patent number: 4732610Abstract: Loose metal particles, or a consolidated metal particle composition, of an aluminum alloy consisting essentially of about 5 to 13% zinc, 1 to 3.5% magnesium, 0.5 to 3.0% copper, with iron being present up to 0.5%, with silicon being present up to 0.4%, plus nickel or cobalt or both being present in an amount effective essentially to place the iron in the incoherent dispersoid Al.sub.9 (Fe,M).sub.2, M being nickel or cobalt or both, M being present up to 0.75%, plus means being present for forming coherent dispersoids, said means being present up to 1%, balance aluminum.Type: GrantFiled: February 24, 1986Date of Patent: March 22, 1988Assignee: Aluminum Company of AmericaInventors: Gregory J. Hildeman, Linda C. Labarre, David J. Brownhill, Arshad Hafeez
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Patent number: 4732818Abstract: The present invention relates to a composite bearing material comprising three layers: (1) a metal backing, (2) a porous metal interlayer bonded to the metal backing which includes bronze or other copper alloy particles from two distinct particle size ranges and (3) a PTFE based composition intermixed with and overlying the porous metal interlayer. In accordance with the method of the present invention, the porous metal interlayer substantially comprises a relatively non-homogeneous mixture of particles from the two distinct particle size ranges, wherein a substantial portion of the relatively fine powder is segregated adjacent the metal backing. The present invention includes a significant thickness of the PTFE based composition applied to and remaining above the surface of the porous metal backing.Type: GrantFiled: September 29, 1986Date of Patent: March 22, 1988Assignee: Federal-Mogul CorporationInventors: George C. Pratt, Michael C. Montpetit, Michael D. Lytwynec
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Patent number: 4726843Abstract: Aluminum alloy, suitable for rapid quenching from a melt supersaturated with alloy components, which contains 2 to 5.5% by weight of Cr and 2 to 5.5% by weight of V, the remainder being Al, and may contain further added amounts of Mo, Zr, Ti or Fe, individually or in combination, up to a total content of not more than 1% by weight, the total content of all alloy elements being no more than 10% by weight. The simultaneous occurrence of the phases Al.sub.13 Cr.sub.2 and Al.sub.10 V in silid solution and as hardness-imparting dispersoids having a particle diameter of not more than 0.1 .mu.m results in good high-temperature strength and thermal stability coupled with good ductility and toughness of the material. The comparatively Low Vickers hardness of, on average, only about 130 (HV) for the rapidly solidified alloys initially obtained make the powders readily processable. After the heat treatment, the Vickers hardness of the workpiece reaches values up to about 200 (HV).Type: GrantFiled: June 18, 1986Date of Patent: February 23, 1988Assignee: BBC Brown, Boveri & Company LimitedInventor: Malcolm J. Couper
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Patent number: 4721599Abstract: Metal or alloy articles having complicated shapes can be produced with high precision by injection molding a kneaded mixture of a metal or alloy powder and an organic binder comprising a special methylcellulose, a plasticizer, a lubricant and water, followed by removal of the organic binder and sintering.Type: GrantFiled: April 24, 1986Date of Patent: January 26, 1988Assignee: Hitachi Metals, Ltd.Inventor: Hideki Nakamura
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Patent number: 4719077Abstract: An alloy of nickel and titanium in the atomic ratio of 49:51 to 56:44 can be prepared at a temperature much lower than the eutectic point of the corresponding alloy. Thus, a green compact of a powdery mixture of the component metals is subjected to a heat treatment under high vacuum first at a rate of temperature elevation of 5.degree. to 30.degree. C./minute up to a temperature of, for example, 600.degree. C. and then at a rate of temperature elevation of at least 40.degree. C./minute up to a temperature of 815.degree.-900.degree. C. The surface of the metal particles is activated at the first stage along with degassing and the surface-activated metal particles are brought into an exothermic reaction at the second stage to cause explosive fusion and alloying.Type: GrantFiled: June 9, 1987Date of Patent: January 12, 1988Assignee: Agency of Industrial Science and TechnologyInventors: Yoshikazu Suzuki, Hidero Unuma
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Patent number: 4716019Abstract: A process is disclosed for producing composite agglomerates of molybdenum and molybdenum carbide (Mo.sub.2 C). The process involves forming a relatively uniform mixture of non-agglomerated molybdenum powder and carbon powder having a particle size of no greater than the particle size of the molybdenum powder. The amount of carbon powder is proportional to the amount of molybdenum carbide desired in the composite agglomerate. A slurry is formed of the mixture, an organic binder, and water with the amount of the binder being no greater than about 2% by weight of the mixture; and the powders are agglomerated from the slurry. The agglomerated powders are then classified to remove the major portion of the agglomerates having a size greater than about 170 mesh and less than about 325 mesh from the balance of the agglomerates. The balance of the agglomerates in which the particle size is -170 +325 mesh is then reacted at a temperature of no greater than about 1400.degree. C.Type: GrantFiled: June 4, 1987Date of Patent: December 29, 1987Assignee: GTE Products CorporationInventors: David L. Houck, David J. Port, Jen S. Lee
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Patent number: 4716133Abstract: When a composite nitride obtained by nitriding a fine powder of an alloy comprising metallic silicon and a metal of the group IIIa of the Periodic Table is sintered, a highly homogeneous silicon nitride sintered body having a high strength can be obtained. This fine powder of the alloy and this composite nitride exert a function of promoting sintering of Si.sub.3 N.sub.4.Type: GrantFiled: March 31, 1986Date of Patent: December 29, 1987Assignee: Kyocera CorporationInventors: Akito Horiuchi, Kiyoshi Yokoyama, Makoto Yoshida
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Patent number: 4710223Abstract: A sintered, metal infiltrated article and a method for preparing same is disclosed. The method permits mass production by injection molding, of metal infiltrated sintered articles of complex shape without excessive machining of the final product. The articles so produced have desirable physical properties such as abrasion resistance, high hardness, and high resistance to erosion at extreme temperatures encountered in use.Type: GrantFiled: March 21, 1986Date of Patent: December 1, 1987Assignee: Rockwell International CorporationInventor: Daniel E. Matejczyk
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High speed steel sintering powder made from reclaimed grinding sludge and objects sintered therefrom
Patent number: 4705565Abstract: A method of producing a sintering powder made from high speed steel and alumina. This sintering powder is sinterable over a broader range of temperatures than conventional high speed steel sintering powders and at lower temperatures, thereby making sintered objects which are crack resistant and also highly wear resistant. Additionally, the sintering powder flows readily when poured into a mold for production of a green object for sintering.Type: GrantFiled: June 25, 1986Date of Patent: November 10, 1987Inventors: Robert J. Beltz, Joseph D. Dankoff -
Patent number: 4704251Abstract: Method for the production of a wear resistant part of a soil working tool comprising forming a mixture of 67-90% by volume of iron particles consisting of at least 97% Fe and 10-33% by volume of hard particles having a desired particle size distribution, and subsequently pressing the mixture at a pressure of at least 3500 kp/cm.sup.2 to form a compact, sintering the compact at a temperature of 900.degree.-1200.degree. C., and optionally sinter forging the sintered compact. The sintered part consists of an iron matrix in which hard particles with a predetermined particle size distribution are embedded.Type: GrantFiled: July 14, 1986Date of Patent: November 3, 1987Assignee: Teknologisk InstitutInventor: Ole Kr mer
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Patent number: 4702885Abstract: A process for producing an aluminum alloy comprises: producing an aluminum alloy powder, consisting of (A) 10 to 36 wt % of Si, 1 to 12 wt % of Fe, 2 to 10 wt % of at least one of metal selected from the group consisting of Ni, Co, Cr and Mn, reminder of the alloy powder consisting of aluminum, or consisting of (B) 10 to 36 wt % of Si, 2 to 10 wt % of Ni, 2 to 10 wt % of at least one of metal selected from the group consisting of Fe, Co, Cr, and Mn, and remainder of the alloy powder consisting of aluminum; compressing a mass of the powder by either compacting the power or accumulating the powder in a can where in case of compacting the powders are so as to have its actual density ratio of 65% to 90%, and in case of the accumulation the powders are compressed so as to have its actual density ratio of not more than 90%; heating the thus compressed mass of powder in convection type heating furnace at a temperature of 250.degree. C. to 550.degree. C.Type: GrantFiled: June 27, 1986Date of Patent: October 27, 1987Assignee: Sumitomo Electric Industries, LTD.Inventors: Yusuke Odani, Kiyoaki Akechi, Nobuhito Kuroishi
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Patent number: 4702772Abstract: The present invention relates to an iron-base powder containing Ni, Mo and C for producing highly resistant sintered bodies under normal pressing and sintering conditions. The powder contains 7-12% by weight of Ni, 0.4-1.5% by weight of Mo, and 0.3-0.7% by weight of C.Type: GrantFiled: March 6, 1986Date of Patent: October 27, 1987Assignee: Hoganas ABInventors: Ulf F. I. Engstrom, Sven E. Allroth, Olavi M. Mustonen
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Patent number: 4702770Abstract: Low-density composites are produced consisting chiefly of boron carbide and aluminum, or aluminum alloy, and minor amounts of ceramic material. The method allows control of the rate of reaction between boron carbide and metal so that the final components of the composite, and hence the mechanical properties, are controlled. The invention includes modification of the carbon content of the boron carbide composition, dispersion of boron carbide and formation of a compact, infiltration of the compact by aluminum or aluminum alloy, and heat treatments. The invention produces low-density boron carbide-aluminum composites with a homogeneous microstructure possessing desired mechanical properties.Type: GrantFiled: July 26, 1985Date of Patent: October 27, 1987Assignee: Washington Research FoundationInventors: Aleksander J. Pyzik, Ilhan A. Aksay
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Patent number: 4699657Abstract: Very fine grain metal billets are produced by loading alloy metal powder of desired composition into a metal extrusion container in successive layers of two or four inches deep. Each layer after loading is compacted by a high energy rate forming ram so as to introduce energy on the order of 3.times.10.sup.6 psi per layer and at least 18.times.10.sup.6 psi total. An inner plate is then loosely placed on the compacted powder. On top of the inner plate is placed a cover plate which is welded to the container. The filled container is then heated in a furnace to an extrusion temperature below the melting point of the alloy and is extruded in an extrusion press having a ratio of about 3:1 with a force of about 3,000 tons. The inner plate does not move at the same rate as the container and in effect is partially extruded against the powder so as to raise the density of the extruded billet to substantially 100% of its theoretical density.Type: GrantFiled: November 3, 1986Date of Patent: October 13, 1987Assignee: Worl-Tech LimitedInventor: Vincent N. DiGiambattista
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Patent number: 4693747Abstract: Disclosed is a metal alloy product having increased resistance to fatigue crack growth and having coarse grains distributed in a fine grain structure, the coarse grains having a different alloy composition from the fine grain structure.Type: GrantFiled: November 18, 1985Date of Patent: September 15, 1987Assignee: Aluminum Company of AmericaInventors: Philip E. Bretz, Jocelyn I. Petit, Ralph R. Sawtell, Asuri K. Vasudevan
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Patent number: 4693746Abstract: A cBN sintered compact for an end mill obtained by sintering mixed powder prepared by mixing about 35 to 50 percent by volume of cubic boron nitride powder smaller than about 2 .mu.m in average particle size with about 50 to 65 percent by volume of a binder under cBN-stable superhigh pressure conditions. The binder contains about 20 to 30 percent by weight of Al and one or more Ti compounds selected from a group of TiN.sub.z, Ti(C,N).sub.z, TiC.sub.z, (Ti,M)C.sub.z, (Ti,M) (C,N).sub.z and (Ti,M)N.sub.z (where M indicates a transition metal element of the group IVa, Va or VIa of the periodic table excepting Ti and z is within a range of about 0.7.ltoreq.z.ltoreq. about 0.Type: GrantFiled: January 5, 1987Date of Patent: September 15, 1987Assignee: Sumitomo Electric Industries, Ltd.Inventors: Tetsuo Nakai, Mitsuhiro Goto
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Patent number: 4693864Abstract: Mill scale, iron ore, or taconite is utilized in a powder metallurgy process to form steel articles having approximately the same density as that of conventional rolled steel. Particulate iron is mixed with manganese, carbon, additional alloying ingredients, and a binder to form a particulate admixture. The particulate admixture is then compressed, preferably under extreme pressure until the density of the compressed particulate admixture is from about 0.2408 lbs/in.sup.3 (6.67 g/cm.sup.3) to about 0.2833 lbs/in.sup.3 (7.83 g/cm.sup.3), which corresponds to a density of from about 85% to about 100% of the density of conventional rolled steel. The resultant coherent mass is subjected to sintering and below fusion heating to form an alloyed article which can be swaged, rolled, drawn, or worked at elevated temperature to decrease the grain size of the alloyed article. The resultant end-product will preferably have a density of from about 0.2408 lbs/in.sup.3 (6.67 g/cm.sup.3) to about 0.2833 lbs/in.sup.3 (7.Type: GrantFiled: December 5, 1985Date of Patent: September 15, 1987Assignee: Donald W. Lloyd Realty, Inc.Inventor: Donald W. Lloyd
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Patent number: 4690797Abstract: A method for the manufacture of large area silicon crystal bodies suitable for use in the manufacture of solar cells wherein silicon powder having a small grain size is used as the starting material. This powder is compressed to form a thin layer in a suitable form, the form having at least a surface composed of silicon or a silicon compound. The form is filled to a depth approximating the final dimensions of the article. The powder is sintered in the form, and the compressed, sintered layer is converted into a self-supporting silicon foil. This foil is melted partially up to at least half its thickness and recrystallized in a two-stage temperature treatment. The melting occurs by means of a single-sided energy irradiation. The silicon foil is not deteriorated in terms of its mechanical stability and shaped by means of the single-sided, optical type heating.Type: GrantFiled: September 17, 1986Date of Patent: September 1, 1987Assignee: Siemens AktiengesellschaftInventors: Achim Eyer, Armin Raeuber, Norbert Schillinger
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Patent number: 4690796Abstract: A process is disclosed for producing composite powder particles consisting essentially of a matrix phase and a reinforcement phase. The process involves entraining agglomerated particles in a carrier gas, the agglomerated particles consisting essentially of titanium diboride and particles of a metal selected from the group consisting of aluminum and aluminum based alloys. The agglomerated particles are fed through a high temperature zone having a temperature sufficient to allow the metal particles to melt, coalesce together, and encapsulate the titanium diboride particles. The metal is then resolidified, resulting in the formation of the composite powder particles wherein the matrix phase consists essentially of the metal and the reinforcement phase consists essentially of the titanium diboride particles.Type: GrantFiled: March 13, 1986Date of Patent: September 1, 1987Assignee: GTE Products CorporationInventor: Muktesh Paliwal