Powder Shape Or Size Characteristics Patents (Class 419/23)
-
Patent number: 5436080Abstract: A structural member is produced using starting powder consisting of composite particulates each containing AlN grain within its surface covered by an Al layer of a single crystal structure, and Al alloy particulates of a single crystal structure, and then by sintering the Al layers of the composite particulates with the Al alloy particulates. The Al layers and the Al alloy particulates of the single crystal structure have no dislocation fault, crystal grain boundary. etc., produced therein, and for this reason, they have a low chemical activity. Therefore, the Al layers and the like have a characteristic that they are extremely difficult to oxidize. This ensures that the Al layers and the Al alloy particulates can be reliably sintered to achieve the densification of the resulting structural member.Type: GrantFiled: September 10, 1992Date of Patent: July 25, 1995Assignees: Tsuyoshi Masumoto, Akihisa Inoue, Yoshida Kogyo K.K., Honda Giken Kogyo Kabushiki KaishaInventors: Akihisa Inoue, Tsuyoshi Masumoto, Jun Sasahara, Katsutoshi Nosaki, Tadashi Yamaguchi
-
Patent number: 5427734Abstract: The object of the invention is to provide a manufacturing method of a complex shaped R--Fe--B type sintered anisotropic magnet improved the moldability of injection molding and preventing the reaction between R ingredients and binder and controlled the degradation of magnetic characteristics due to residual carbon and oxygen. Utilizing the R--Fe--B type alloy powder or the resin coated said alloy powder, and methylcellulose and/or agar and water, instead of the usual thermoplastic binder, it is mixed and injection molded. The molded body is dehydrated by the freeze vacuum dry method to control the reaction between R ingredients and of the R--Fe--B alloy powder and water; furthermore, by administering the de-binder treatment in the hydrogen atmosphere, and sintering it after the dehydrogen treatment, residual oxygen and carbon in the R--Fe--B sintered body is drastically reduced, improving the moldability during the injection molding to obtain a three dimensionally complex shape sintered magnet.Type: GrantFiled: June 24, 1993Date of Patent: June 27, 1995Assignee: Sumitomo Special Metals Co., Ltd.Inventors: Osamu Yamashita, Masahiro Asano, Tsunekazu Saigo
-
Patent number: 5421852Abstract: Disclosed is a hard alloy with high hardness, high abrasion resistance, high corrosion resistance and high rigidity, which is excellent in performance in use for tools. The hard alloy contains more than 80% by weight of WC with less than 2 .mu.m of average particle size, more than 0.2% by weight and less than 2% by weight of Co and the remaining part of one or more metals, carbides, nitrides and carbonitrides of the metals in the IVa, Va and VIa families in the periodic table, such as 2.0 to 7.0% by weight of one or more of Mo and Mo.sub.2 C, and the alloy contains Co.sub.x W.sub.y C.sub.z in the sintered product. By the addition of Mo or Mo.sub.2 C and VC the growth of particles in the hard phase is inhibited and at the same time the wettability of WC--Co is increased.Type: GrantFiled: January 25, 1993Date of Patent: June 6, 1995Assignee: Sumitomo Electric Industries, Ltd.Inventors: Masao Maruyama, Hiroshi Nakagaki, Minori Shirane
-
Patent number: 5421851Abstract: The present invention relates to a sintered titanium-based carbonitride alloy for milling and turning where the hard constituents are based on Ti, Zr, Hf, V, Nb, Ta, Cr, Mo and/or W and the binder phase based on Co and/or Ni. The structure comprises 10-50% by volume hard constituent grains with core-rim-structure with a mean grain size for the cores of 2-8 .mu.m in a more fine-grained matrix with a mean grain size of the hard constituents of <1 .mu.m and where said mean grain size of the coarse hard constituents grains is >1.5 .mu.m, preferably >2 .mu.m, larger than the mean grain size for the grains in the matrix. The coarse grains can be Ti(C,N), (Ti,Ta)C, (Ti,Ta)(C,N) and/or (Ti,Ta,V)(C,N).Type: GrantFiled: May 6, 1992Date of Patent: June 6, 1995Assignee: Sandvik ABInventors: Rolf G. Oskarsson, Gerold Weinl, Ake Ostlund
-
Patent number: 5418070Abstract: An impregnated cathode comprising three layers: a very thin emitting surface layer of metal such as an alloy of tungsten with a high fraction of an activating metal of the platinum group to provide low workfunction; an underlying, thin buffer layer of porous tungsten alloyed with a fraction of activating metal, to retard diffusion loss of activating metal from the emitting layer; and a substrate of porous tungsten impregnated with barium aluminate.Type: GrantFiled: April 28, 1988Date of Patent: May 23, 1995Assignee: Varian Associates, Inc.Inventor: Michael C. Green
-
Patent number: 5415831Abstract: The method serves to produce a material based on a doped intermetallic compound. In carrying out the method, at least two differently doped powders each based on the intermetallic compound are selected. One of the two powders predominantly has coarse-grained particles. On the other hand, another powder is formed from comparatively fine-grained particles composed of a material having a lower creep strength but a higher ductility than the material of the coarse-grained powder. The at least two powders are mixed with one another in a ratio serving to establish a desired mixed microstructure and then hot-compacted and heat-treated to form the material.Material produced by this method is suitable for components which are exposed to high mechanical loads at high temperatures, such as, in particular, gas-turbine blades or turbine wheels of turbo chargers.Type: GrantFiled: December 13, 1993Date of Patent: May 16, 1995Assignee: ABB Research Ltd.Inventors: Robert Baumann, Joachim Rosler, Christoph Tonnes
-
Patent number: 5415829Abstract: A method of manufacturing metal silicide targets or alloy targets for sputtering use comprises the steps of (a) mechanically alloying silicon and a metal to provide a metal silicide powder or mechanically alloying silicon and a plurality of metal powders to provide an alloy powder, (b) and then pressing the metal silicide powder or alloy powder. The invention also relates to the metal silicide targets or alloy targets so manufactured. In the mechanical alloying step, rapid and fine division and agglomeration of the mixed powder is repeated until the particles of the material powders are finely divided to a submicron level. They form aggregates tens of microns in diameter. The aggregates gradually take an equi-axed shape. Homogenization of the material powder mixture progresses to mixing on the atomic level, until alloying takes place.Type: GrantFiled: December 22, 1993Date of Patent: May 16, 1995Assignee: Nikko Kyodo Co., Ltd.Inventors: Tateo Ohhashi, Takakazu Seki, Takeo Okabe, Koichi Yasui, Hideaki Fukuyo
-
Patent number: 5413751Abstract: High density heatsinks for microcircuit packages are formed by first mold-pressing a composite powder of free-flowing spray-dried particles of copper and at least one other denser material such as tungsten and/or molybdenum, the proportions of which are adjusted to match the thermal expansion characteristics of the microcircuit material. The pressed compacts are then heated in a sintering furnace at 1,200.degree. C. to 1,350.degree. C. in order to effect an homogeneous distribution of the melting copper throughout the structure. The process results in a readily usable component having good thermal conductivity and matched thermal expansion that requires no further machining.Type: GrantFiled: May 20, 1993Date of Patent: May 9, 1995
-
Patent number: 5405572Abstract: A method for the reduction of oxides in a powder metal requires a predetermined quantity of powder to be loaded into a retort tube or other type of furnace which is pumped down to a vacuum less than about 5.times.10.sup.-6 Torr. The retort is ramped up to a temperature of about 500.degree.-750.degree. C. and maintained at that temperature under high vacuum for about 30-60 minutes to obtain reduction of oxides and de-gasing of copper powders of screen mesh sizes of -100. A hydrogen partial pressure of 150 microns to 20 mm of Hg may be valved into the system from standard grade hydrogen gas 15 minutes into approximately the 30-60 minute hold temperature ramp and then valved off on cooling to 400.degree. C. to improve oxide removal. The system is returned to the high vacuum mode and furnace cooled to room temperature.Type: GrantFiled: March 18, 1992Date of Patent: April 11, 1995Assignee: Printron, Inc.Inventor: Gerald A. DeVolk
-
Patent number: 5403543Abstract: Disclosed is a manufacturing process of an alloy material comprising a chromium component and a base component which comprises at least one element selected from tile group consisting of copper and silver, the manufacturing process comprising steps of: subjecting a chromium material with a carbon material to heat treatment; and manufacturing the alloy material using the chromium material treated at the heat treatment subjecting step and a raw material for tile base component. At the heat treatment subjecting step, the chromium material, mixed with 50 ppm to 5,000 ppm of the carbon material, is heated to a temperature within the range of 800.degree. C. to 1,400.degree. C. in a non-oxidizing atmosphere. According to this manufacturing process, the level of oxygen content in the alloy material are decreased to be not more than 200 ppm. The obtained alloy material can be used as a contact material for vacuum circuit breakers.Type: GrantFiled: June 3, 1992Date of Patent: April 4, 1995Assignee: Kabushiki Kaisha ToshibaInventors: Tsutomu Okutomi, Tsuneyo Seki, Atsushi Yamamoto, Mikio Okawa, Tadaaki Sekiguchi, Yoshiko Majima
-
Patent number: 5403544Abstract: A method for forming a wear surface on a metal substrate has a slurry which includes wear resistant particles, powdered steel, and binder system positioned on the metal substrate by retaining walls for a time sufficient for drying the slurry and forming a composite material of preselected thickness "T". The retaining walls are then removed and the substrate and the composite material are heated and passed through a rolling mill compressing the composite material.Type: GrantFiled: December 20, 1993Date of Patent: April 4, 1995Assignee: Caterpillar Inc.Inventors: Richard L. Adrian, James C. Henehan, Phillip J. Shankwitz
-
Patent number: 5403374Abstract: A watch exterior part is formed of cemented carbide or stellite alloy, and has a three-dimensionally curved as-sintered surface or a small hole with an as-sintered interior peripheral surface, or has a three-dimensionally curved polished surface obtained by polishing an as-sintered surface. The watch exterior part is manufactured by a method in which organic binder is milled into a material powder, and a molded body obtained by injection molding is subjected to a binder removing process and then sintered. By the manufacturing method, a watch exterior part formed of cemented carbide or stellite alloy has a high strength and a complicated configuration such as a three-dimensional curved surface and a small hole, without applying secondary machining operations such as discharge operations.Type: GrantFiled: May 28, 1992Date of Patent: April 4, 1995Assignees: Sumitomo Electric Industries, Ltd., Namiki Precision Jewel Co., Ltd.Inventors: Nobuyuki Kitagawa, Toshio Nomura, Yoichi Yaguchi, Hidehiro Uchiumi, Naoko Iwashimizu
-
Patent number: 5393485Abstract: A process for the production of foamable elements, in which a metal powder is mixed with a foaming agent powder, the powder mixture is brought to an elevated temperature in a receiver and is extruded through a die, so that the extruded part can be subsequently foamed by decomposition of the foaming agent powder by heating of the extruded part and then cooled to yield a finished foam element. The powder mixture is continuously introduced into a channel, leading to the die, which has a moving wall component by which the powder mixture is transported in the channel by friction with precompacting and is extruded through the die. The speed of the wall component is selected so that the heating necessary for the precompacting comes from heat generated in the transport operation.Type: GrantFiled: April 23, 1993Date of Patent: February 28, 1995Assignee: Mepura Metallpulvergesellschaft M.G.H.Inventors: Helmut Worz, Hans P. Degischer
-
Patent number: 5387272Abstract: The present invention provides an Al-Si based sintered alloy of high strength and high ductility, a method for production thereof and use thereof. The alloy comprises 1-45% of Si, 0.1-20% of an element of Group IIIa, 0.01-5% of at least one element of Groups IVa and Va, the balance of substantially Al. This alloy can further contain at least one of 0.01-5% of Cu, 0.01-5% of Mg, 2.0% or less of Fe, 1.5% or less of Mn and 1.5% or less of Co and the oxygen content is reduced to 0.15% or less by sintering under vacuum. The present invention is applied to automobile parts such as a piston and scroll compressors. The alloy has a tensile strength of about 40 kg/mm.sup.2 or higher and an elongation of 1.5% or more at 150.degree. C.Type: GrantFiled: April 8, 1992Date of Patent: February 7, 1995Assignees: Hitachi, Ltd., Hitachi Powdered Metals Company, LimitedInventors: Yasuo Kamitsuma, Yusaku Nakagawa, Mitsuo Chigasaki, Tadashi Iizuka, Kooichi Inaba, Keiichi Nakamura, Masaki Minabe, Tsuyoshi Kagaya
-
Patent number: 5384087Abstract: The present invention relates to a process for making an aluminum silicon carbide composite material in strip form. The process comprises blending a powdered aluminum matrix material and a powdered silicon carbide material, roll compacting the blended powdered materials in an inert atmosphere to form a green strip having a first thickness, and directly hot working the blended and roll compacted materials to bond the aluminum matrix material particles and the silicon carbide particles and to form a thin strip material having a desired thickness.Type: GrantFiled: April 6, 1992Date of Patent: January 24, 1995Assignee: Ametek, Specialty Metal Products DivisionInventor: Clive Scorey
-
Patent number: 5382405Abstract: A method of manufacturing a shaped article from a powdered precursor, wherein the components of the powdered precursor are subjected to a self-propagating high-temperature synthesis (SHS) reaction and are consolidated essentially simultaneously. The shaped article requires essentially no machining after manufacture.Type: GrantFiled: September 3, 1993Date of Patent: January 17, 1995Assignee: Inland Steel CompanyInventors: Kenneth F. Lowrance, II, Eric C. Knorr, William M. Goldberger, Daniel Boss, Doreen Edwards
-
Patent number: 5364586Abstract: A filter membrane and a process for making the filter membrane are provided. The filter membrane comprises a metal substrate having a filtering layer thereon comprising sintered ultra-fine particles of metal or ceramic compounds. The filtering layer preferably has an average pore size of from about 30 nanometers to about 200 nanometers. The filter membranes can withstand pressure drops of up to about 0.6 MPa and are useful for a variety of filtering applications.Type: GrantFiled: August 17, 1993Date of Patent: November 15, 1994Assignee: Ultram International L.L.C.Inventors: Lev I. Trusov, Vladimir N. Lapovok, Victor I. Novikov
-
Patent number: 5364442Abstract: A composite electrode for electrochemical processing having improved high temperature properties, and a process for making the electrode by combustion synthesis. A composition from which the electrode is made by combustion synthesis comprises from about 4% to about 90% by weight of a particulate or fibrous combustible mixture which, when ignited, is capable of forming an interconnected network of a ceramic or metal-ceramic composite, and from about 10% to about 60% by weight of a particulate or fibrous filler material capable of providing the electrode with improved oxidation resistance and maintenance of adequate electrical conductivity at temperatures above 1000.degree. C. The filler material is molybdenum silicide, silicon carbide, titanium carbide, boron carbide, boron nitride, zirconium boride, cerium oxide, cerium oxyfluoride, or mixtures thereof.Type: GrantFiled: October 26, 1993Date of Patent: November 15, 1994Assignee: Moltech Invent S.A.Inventor: Jainagesh A. Sekhar
-
Patent number: 5356453Abstract: A mixed powder for powder metallurgy comprising a Fe powder and an alloy powder mixed together in which the mean particle size and the solidus line temperature of the alloy powder and the amount of the liquid phase formed during sintering are so defined as to attain most suitable sintering behavior, that is, the mean particle size of the alloy powder is smaller than 20 .mu.m, the solidus line temperature of the alloy powder is set to higher than 950.degree. C. and lower than 1300.degree. C. and the amount of the liquid phase formed during sintering is more than 20%. A sintered product having desired properties can be obtained by using the mixed powder described above.Type: GrantFiled: May 28, 1992Date of Patent: October 18, 1994Assignee: Kabushiki Kaisha Kobe Seiko ShoInventor: Jinsuke Takata
-
Patent number: 5354534Abstract: The invention provides a method for manufacturing sintered parts, which uses as a debinder solvent a substance harmless to the human body and which can enhance the strength of an injection-molded product.Type: GrantFiled: September 18, 1992Date of Patent: October 11, 1994Assignee: Sumitomo Electric Industries, Ltd.Inventors: Nobuyuki Kitagawa, Toshio Nomura, Katuyosi Saito
-
Patent number: 5342573Abstract: A method of producing a tungsten heavy alloy product according to a powder metallurgical procedure utilizing the injection molding technique which enables production of tungsten heavy alloy products having high dimensional accuracy and complex configuration and yet having high physical strength and toughness in high productivity and at low cost. A powder mixture of tungsten powder and nickel powder, iron powder or copper powder is mixed with an organic binder and they are kneaded together. The kneaded mixture is injection molded into a predetermined shape, and thereafter the binder is removed from the molded product. Subsequently, the molded product is sintered in a temperature range of from the melting point of the bond phase of nickel, iron or copper to +50.degree. C. relative to the melting point.Type: GrantFiled: August 20, 1992Date of Patent: August 30, 1994Assignee: Sumitomo Electric Industries, Ltd.Inventors: Yoshinari Amano, Masahiro Omati, Junzo Matsumura
-
Refractory metal reinforced MoSi.sub.2 /SiC composite with matched thermal coefficients of expansion
Patent number: 5340531Abstract: A method for producing a substantially silica-free composition of matter comprising a matrix of MoSi.sub.2 having SiC dispersed therein, the matrix being reinforced with a particulate ductile refractory metal, the method comprising providing a composite of the particulate ductile refractory metal and a substantially silica-free composite mechanical alloy powder comprising MoSi.sub.2 and SiC having a composition in that segment of the ternary diagram of FIG. 1 designated A, and consolidating the composite of particulate ductile refractory metal and mechanical alloy powder; the coefficient of thermal expansion of the MoSi.sub.2 matrix having SiC dispersed therein being substantially equivalent to that of the particulate ductile refractory metal. The composition of matter formed by the method and an article of manufacture comprising the same are also disclosed.Type: GrantFiled: June 1, 1993Date of Patent: August 23, 1994Assignee: University of FloridaInventors: S. Jayashankar, Michael J. Kaufman -
Patent number: 5338505Abstract: A silver base electrical contact material with superior resistance to arc erosion along with improved wear and welding resistance. The contact material consists essentially of 0.5 to 39.9 wt % of nickel, 0.14 to 7.0 wt % of nickel oxides, and balance silver. The material contains not less than 0.4 wt % of nickel responsible for constituting minute nickel and nickel particles which have a particle size of not more than 1 .mu.m and are dispersed in a silver matrix for strengthening the material to give improved wear and welding resistance. The dispersed minute nickel oxide particles are included to stabilize arcing occurring at the time of opening and closing contacts in such a manner as to anchor one end of an arc substantially at any immediately available point over the entire contact surface as soon as the arcing occurs, thereby preventing the arc end from moving violently across or beyond the contact surface and therefore minimizing arc related damages or arc erosion.Type: GrantFiled: December 28, 1992Date of Patent: August 16, 1994Assignee: Matsushita Electric Works, Ltd.Inventors: Koji Tsuji, Yoshinbou Takegawa, Hayato Inada, Shuji Yamada
-
Patent number: 5336465Abstract: A slurry compound prepared by a sintering powdery material and a binder is press-molded to obtain a contour for the final product applicable to a bone-implant such as hip prosthesis. The molded body is given a programmed movement of rotation and/or swinging to impart a centrifugal force to the sintering particles which direct toward the inner wall of the mold cavity. The final product obtained after sintering has a hollow interior having no communication to the outside. Imparting conditions of rotating/swinging movement may be changed or programmed in order to achieve a desired structure or constitution of the final product. By way of example, larger particles concentrate near the inner wall of the mold to provide a rough, porous surface of the body, whereas it has a dense core consisting mainly of sintered fine particles. A hip prosthesis having a ceramic-rich femoral head and a metal-rich stem may also be produced by so programming the movement imparting conditions.Type: GrantFiled: December 3, 1992Date of Patent: August 9, 1994Assignees: Janome Sewing Machine Co., Ltd., Terumo CorporationInventors: Noboru Matsunaga, Kazuyoshi Azeyanagi, Ichirou Sogaishi, Takeo Katakura, Yoshihisa Ueda, Takaaki Ohsawa
-
Patent number: 5336091Abstract: A moldable dental composition for use in forming or repairing dental restorations composed of a mixture of high- and low-fusing temperature metal particles and a volatile binder, composed substantially or entirely of wax, with the binder having a concentration of between thirty (30%) to eighty percent (80%) by volume of the mixture. The average particle size of the high-fusing metal particles are above one micron, and preferably between four microns and eighty microns in size. The composition is heat treated at a temperature to melt the low-fusing temperature metal particles and to eliminate the binder, leaving a porous metal structure with a void volume above thirty percent (30%). The voids are filled using a filler material of metal or ceramic.Type: GrantFiled: November 17, 1992Date of Patent: August 9, 1994Inventors: Itzhak Shoher, Aharon E. Whiteman
-
Patent number: 5330700Abstract: A porous electrode for pacemakers is comprised of a plurality of platinum globules sintered together to form a porous mass of semi-hemispherical shape at the end of a platinum electrode stem. The globules, which are themselves made by sintering together spherically-shaped particles of approximately one micron diameter, provide the globules with an irregular outer surface of high total surface area. The globules have diameters within a critical range of 40-200 microns. The large total surface area of the globules improves the sensing function of an electrode configuration of given size and surface area, while the globule diameters of 40-200 microns have been found to beneficially accommodate tissue ingrowth within the electrode. In a preferred method of making the electrode, the platinum globules, which are formed by sintering together platinum particles of much smaller size, are mixed with organic solvent and organic binder to form a paste.Type: GrantFiled: September 18, 1991Date of Patent: July 19, 1994Assignee: Siemens Pacesetter, Inc.Inventors: Thomas M. Soukup, Paul E. Kreyenhagen
-
Patent number: 5326525Abstract: A process is disclosed for fabricating a metal aluminide composite which comprises providing a metal aluminide, such as titanium aluminide, or a titanium aluminide alloy, and a reinforcing fiber material, such as silicon carbide fiber, and placing an interlayer or diffusion barrier layer in the form of a metal selected from the group consisting of silver, copper and gold, and alloys thereof, between the metal aluminide and the reinforcing fiber material. The interlayer metal can be a foil of the metal or in the form of a coating, such as a silver coating, on the reinforcing fiber material. The metal aluminide, the reinforcing fiber material, and the metal interlayer, e.g., in the form of a packet of a plurality of alternate layers of metal aluminide alloy and reinforcing fiber material, each layer being separated by the metal interlayer, is pressed and heated at an elevated temperature, e.g., ranging from about 900.degree. to about 1200.degree. C., at which diffusion bonding occurs.Type: GrantFiled: July 11, 1988Date of Patent: July 5, 1994Assignee: Rockwell International CorporationInventor: Amit K. Ghosh
-
Patent number: 5318743Abstract: A process for producing a thermoelectric material comprises molding a material powder comprising two or more elements selected from the group consisting of bismuth, tellurium, antimony and selenium and having average diameter in the range from 0.05 to 100 .mu.m and sintering the molded material powder with or without hot isostatic pressing. The material powder may be calcinated before the molding. A process for producing a thermoelectric element comprises cutting out pieces of a pillar-like shape from each of a p-type thermoelectric material and a n-type thermoelectric material, connecting the pieces cut out from the p-type thermoelectric material and the pieces cut out from the n-type thermoelectric material alternately with electrodes at the upper faces or the lower faces of the pieces and attaching insulating base plates to the surfaces of the electrodes. The p-type thermoelectric material and the n-type thermoelectric material are respectively produced by the process described above.Type: GrantFiled: November 27, 1992Date of Patent: June 7, 1994Assignees: Idemitsu Petrochemical Co., Ltd., Director-General, Agency of Industrial Science and Technology, Ministry of International Trade and IndustryInventors: Takeo Tokiai, Takashi Uesugi, Kazuyuki Fukumoto, Toshitaka Ohta, Takenobu Kajikawa
-
Patent number: 5314658Abstract: Tungsten and molybdenum powders are advantageously conditioned for metal injection molding by fluid energy milling the powder prior to batching. A preferred method of conditioning, jet milling, has been found to beneficially effect the particle characteristics to render the metal powder more suitable for injection molding.Type: GrantFiled: April 3, 1992Date of Patent: May 24, 1994Assignee: AMAX, Inc.Inventors: David N. Meendering, Deepak Malhotra, Linda K. Baltich
-
Patent number: 5292478Abstract: The present invention relates to a copper-molybdenum composite material having utility in electrical applica- tions and the process for forming the composite material. The composite material is characterized by a continuous copper matrix having a plurality of discrete molybdenum particles embedded therein. The molybdenum particles have an aspect ratio in the range of from about 1:1 to about 4:1 so as to create a thermal path through the matrix from a first side of the composite material to a second side of the composite material. The resulting composite material exhibits improved through-thickness thermal conductivity as a result of the molybdenum particles being within the aforementioned range.Type: GrantFiled: June 24, 1991Date of Patent: March 8, 1994Assignee: Ametek, Specialty Metal Products DivisionInventor: Clive Scorey
-
Patent number: 5290507Abstract: Method of forming and a new class of tool steel macrocomposites having improved thermal fatigue resistance and improved wear resistance, formed of tool steel powder mixed with carbide powder under hot isostatic pressing.Type: GrantFiled: February 19, 1991Date of Patent: March 1, 1994Inventor: Joseph C. Runkle
-
Patent number: 5284615Abstract: The present invention presents a method of processing ferrous powder materials to produce small component parts exhibiting excellent soft magnetic properties, in particular, residual magnetic flux density. The processing steps involve, in part, mixing with a binder, dewaxing or presintering at a temperature higher than in the conventional dewaxing process, followed by final sintering and a further conversion sintering, at a temperature lower than in the conventional sintering process, to produce parts having density values of over 96% theoretical density and excellent soft magnetic properties. The invented method is suitable for producing small component parts having sufficient strength and excellent soft magnetic properties to make them suitable for miniaturized electrical and electronic equipment.Type: GrantFiled: July 15, 1992Date of Patent: February 8, 1994Assignee: Mitsubishi Materials CorporationInventors: Koshiro Ueda, Mutsumi Moribayashi, Tohru Kohno
-
Patent number: 5279786Abstract: Multi-layer, porous material and process of manufacturing same produced from aluminum scrap powder by means of a centrifugal atomizer for use in noise absorbing devices and filter elements. The multi-layers are arranged according to increasing particle size so that a first layer contains the largest particle size and a last layer contains the smallest particle size. Arranging the layer sin this manner produces a multilayer porous material having a shell configuration of a conch which effectively absorbs noise.Type: GrantFiled: October 13, 1992Date of Patent: January 18, 1994Assignee: Jae Chang ByunInventor: Seong S. Cho
-
Patent number: 5269830Abstract: A process for synthesizing intermetallic compounds from elemental powders. The elemental powders are initially combined in a ratio which approximates the stoichiometric composition of the intermetallic compound. The mixed powders are then formed into a compact which is heat treated at a controlled rate of heating such that an exothermic reaction between the elements is initiated. The heat treatment may be performed under controlled conditions ranging from a vacuum (pressureless sintering) to compression (hot pressing) to produce a desired densification of the intermetallic compound. In a preferred form of the invention, elemental powders of Fe and Al are combined to form aluminide compounds of Fe.sub.3 Al and FeAl.Type: GrantFiled: October 26, 1990Date of Patent: December 14, 1993Assignee: The United States of America as represented by the United States Department of EnergyInventors: Barry H. Rabin, Richard N. Wright
-
Patent number: 5252119Abstract: A high speed tool steel produced by sintering powder, consisting essentially, by weight, of more than 1.5% but not more than 2.2% C, not more than 1.0% Si, not more than 0.6% Mn, 3.0 to 6.0% Cr, an amount of W and Mo in which the content of W+2Mo is in the range of 20 to 30% and in which the ratio of W/2Mo is not less than 1, not more than 5.0% V, 2.0 to 7.0% Nb, the ratio of Nb/V being not less than 0.5, and the balance Fe and incidental impurities, the value of C-Ceq, which Ceq is defined by 0.24+0.033.times.W+0.063.times.Mo+0.2.times.V+0.1.times.Nb, being in a range of -0.20 to 0.05, the density of carbides in the sintered steel having grain size of 2 to 5 .mu.m being in a range of 10,000 to 30,000 pieces/mm.sup.2.Type: GrantFiled: October 29, 1991Date of Patent: October 12, 1993Assignee: Hitachi Metals, Ltd.Inventors: Junichi Nishida, Norimasa Uchida
-
Patent number: 5234487Abstract: Tungsten-titanium sputter targets of at least 95% theoretical density are provided with little or no .beta.(Ti, W) phase constituent. Such targets will minimize troublesome particulate emissions during sputter coating conditions.Type: GrantFiled: April 15, 1991Date of Patent: August 10, 1993Assignee: Tosoh SMD, Inc.Inventors: Charles E. Wickersham, Jr., John J. Mueller
-
Patent number: 5226947Abstract: Superconductors formed by powder metallurgy have a matrix of niobium-titanium alloy with discrete pinning centers distributed therein which are formed of a compatible metal. The artificial pinning centers in the Nb-Ti matrix are reduced in size by processing steps to sizes on the order of the coherence length, typically in the range of 1 to 10 nm. To produce the superconductor, powders of body centered cubic Nb-Ti alloy and the second phase flux pinning material, such as Nb, are mixed in the desired percentages. The mixture is then isostatically pressed, sintered at a selected temperature and selected time to produce a cohesive structure having desired characteristics without undue chemical reaction, the sintered billet is reduced in size by deformation, such as by swaging, the swaged sample receives heat treatment and recrystallization and additional swaging, if necessary, and is then sheathed in a normal conducting sheath, and the sheathed material is drawn into a wire.Type: GrantFiled: February 17, 1992Date of Patent: July 13, 1993Assignee: Wisconsin Alumni Research FoundationInventors: Paul D. Jablonski, David C. Larbalestier
-
Patent number: 5207821Abstract: Disclosed is a sintered alloy composition and method of manufacturing the same, the sintered alloy composition having a multi-phase structure, comprising: a first phase composed of aluminum and copper; and a second phase being dispersed in the first phase and composed of molybdenum, chromium, silicon and cobalt. This alloy composition has excellent abrasion and corrosion resistance, preferably to be used for making machine parts such as valve seats for engines.Type: GrantFiled: July 9, 1991Date of Patent: May 4, 1993Assignees: Hitachi Powdered Metals Co., Ltd., Honda Giken Kogyo Kabushiki KaishaInventors: Yutaka Ikenoue, Keitaro Suzuki, Yoshimasa Aoki, Hideo Urata, Koji Koishikawa, Makoto Tsuji
-
Patent number: 5204162Abstract: Non-spherical bodies having a circular cross-section that is 0.5-200 microns in diameter and that are longer than the cross-sectional diameter, and a method of making such bodies by reshaping non-spherical bodies. The method comprises positioning a monolayer of unsintered, deformable, spherical bodies between smooth facing surfaces on two flat formers, and applying a mild shearing force to at least one of the formers.Type: GrantFiled: October 3, 1991Date of Patent: April 20, 1993Assignee: Corning IncorporatedInventor: Thomas D. Ketcham
-
Patent number: 5199971Abstract: The present invention relates to parts, such as a drive gear and driven gear, for use in a rotary gear pump exhibiting good sliding characteristics against a pump case made of light metals such as aluminum alloys. These parts are obtained by subjecting aluminum alloy powders, which have been solidified at a cooling rate of 100.degree. C./sec or more, or aluminum alloy powders having particle diameters of 350 .mu.m or less, to powder compacting and hot extrusion and optionally further to hot forging, or subjecting the aluminum alloy powders to powder forging.Type: GrantFiled: December 19, 1989Date of Patent: April 6, 1993Assignee: Sumitomo Electric Industries, Ltd.Inventor: Kiyoaki Akechi
-
Patent number: 5174953Abstract: A method is disclosed of making a sintered composite unitary artifact having an alpha-alumina component fast with a metal component. Particulate alpha-alumina and a glass-forming additive are mixed together; and a green artifact is pressed having an alumina portion formed from the mixture and a metal portion formed from a particulate metal. The green artifact is then heated under a non-oxidizing atmosphere to a temperature at which both portions undergo densification. This provides a sintered artifact having a debased alpha-alumina component sintered to a metal artifact.Type: GrantFiled: October 9, 1991Date of Patent: December 29, 1992Assignee: Lillywyte Societe AnonymeInventors: Jonathan L. Albain, Adrian W. Paterson
-
Patent number: 5174952Abstract: A process for the powder-metallurgical production of a workpiece by filling a binder-free and solvent-free, dry metal powder or ceramic powder into a mold, precompacting the powder by tapping and presintering it for 1/2 hour to 1 hour at 0.65 to 0.85 times the absolute melting temperature without significant shrinkage, adjacent powder particles being joined merely at their contact points by necking to give a skeletal formed body. The formed body is taken out of the mold and finish-sintered at at least 0.9 times the absolute melting temperature for at least 1 hour without additional support by a mold. Advantageously, the sintered body is additionally hot-isostatically pressed containerless in order to reach at least 98% of the theoretical density.Type: GrantFiled: September 6, 1990Date of Patent: December 29, 1992Assignee: Asea Brown Boveri Ltd.Inventors: Peter Jongenburger, Christoph Tonnes, Clemens Verpoort
-
Patent number: 5167885Abstract: Monolithic bodies of sinterable materials are formed by a sintering process in which little or no shrinkage of the body occurs during sintering. In the method, large particles are placed in particle-to-particle contact with finer size powder particles at the interstices to form a molded shape which is then fired. During firing, the large particles are substantially stable, but the fine powder particles sinter to bond the large particles together. The method is especially useful for producing large and/or intricately shaped bodies. The method is also especially useful for making monolithic bodies using large hollow spherical particles.Type: GrantFiled: January 7, 1992Date of Patent: December 1, 1992Assignee: W. R. Grace & Co.-Conn.Inventors: Roy W. Rice, Rasto Brezny
-
Patent number: 5160534Abstract: Ti-W target material for sputtering includes a structure composed of a W phase, a Ti phase, and a Ti-W alloy phase of which 20% or more consist of the area ratio of a micro structure covering the cross section of the Ti-W target material. The Wi-W target material further includes dispersed tungsten particles, the Ti-W alloy phases substantially surrounding the W grains, and the Ti phases dispersed adjacent to the Ti-W alloy phase or the W grains. The formation of the Ti-W alloy phases is capable of reducing a substantial amount of the Ti phase in the target material. It is thus possible to prevent the generation of particles attributable to a difference between sputtering speeds of Ti and Ti-W.Type: GrantFiled: May 31, 1991Date of Patent: November 3, 1992Assignee: Hitachi Metals Ltd.Inventor: Akitoshi Hiraki
-
Patent number: 5147446Abstract: A method of producing a dense compact of ultra-fine powder employs low temperatures and high pressures to produce a very dense, nearly ideally packed compact from a starting nano-sized powder. The final product is capable of being easily hot-pressed or sintered to full density.Type: GrantFiled: August 6, 1991Date of Patent: September 15, 1992Assignee: The United States of America as represented by the Secretary of the CommerceInventors: Alexander Pechenik, Gasper J. Piermarini
-
Patent number: 5145506Abstract: A non-magnetic, wear resistant composite of from 10 to 45 volume percent of titanium carbide or tungsten carbide particles bonded in a matrix of a nickel-titanium alloy wherein nickel comprises from 53 to 62 weight percent of the alloy with the remainder being essentially titanium.Type: GrantFiled: July 5, 1984Date of Patent: September 8, 1992Assignee: The United States of America as represented by the Secretary of the NavyInventors: David Goldstein, Scott M. Hoover
-
Patent number: 5143692Abstract: A method of making a substructure for a dental restoration which comprises a substructure of a dental metal and a fired on coating of a dental ceramics, which method comprises applying a powder-form mixture of a dental metal powder and a thermoplastic polymeric material having a melting point above 50.degree. C., in the shape of the dental restoration to be made, to a porous refractory model, by means of a heated instrument, heating the assembly so obtained to a temperature at which the thermoplastic polymeric material liquefies and is sucked from the coating into the model, followed by raising the temperature of the assembly to a temperature at which the thermoplastic polymeric material disappears, and raising the temperature further to a sintering temperature at which the dental metal powder is sintered into a solid metal mass. The substructure so formed can be provided with a fired on coating of dental ceramics.Type: GrantFiled: July 2, 1991Date of Patent: September 1, 1992Assignee: Elephant Edelmetaal B.V.Inventor: Joseph M. van der Zel
-
Patent number: 5141702Abstract: A method for depositing a composite coating on a substrate is provided. The coating contains a mixture of ductile metal particles and a uniformly dispersed polymer particles. The polymer is present in a concentration effective to reduce frictional forces. The coating mixture is compacted such as by isostatic pressing, formed into strips and then clad to the substrate. One preferred coating contains 0.5 weight percent polytetrafluoro-ethylene in a tin matrix.Type: GrantFiled: May 28, 1991Date of Patent: August 25, 1992Assignee: Olin CorporationInventors: Bruce M. Guenin, Julius C. Fister
-
Patent number: 5137565Abstract: According to the present invention there is now provided a method of making a sintered titanium-based carbonitride alloy. According to the method, melt-metallurgical raw materials containing the metallic alloying elements for hard constituent-forming as well as binder phase-forming elements are melted and cast, using no intentional additions of the elements C, N, B and O, to form a pre-alloy which in solidified condition of brittle intermetallic phases with hard constituent-forming and binder phase-forming elements mixed in atomic scale. The pre-alloy is crushed and/or milled to powder with grain size <50 .mu.m. The powder is carbonitrided for simultaneous formation in situ of extremely fine-grained <0.1 .mu.m, hard constituent particles enclosed in their binder phase.Type: GrantFiled: December 17, 1991Date of Patent: August 11, 1992Assignee: Sandvik ABInventors: Anders G. Thelin, Rolf G. Oskarsson, Gerold Weinl
-
Patent number: 5126104Abstract: A method is disclosed for preparing an intimate mixture of powders of nickel-chromium-boron-silicon alloy, molybdenum metal powder, and Cr.sub.3 C.sub.2 /NiCr alloy suitable for thermal spray coatings which comprises milling a starting mixture of the above two alloys with molybdenum powder to produce a milled mixture wherein the average particle size is less than about 10 micrometers in diameter, forming an aqueous slurry of the resulting milled mixture and a binder which can be an ammoniacal molybdate compound or polyvinyl alcohol, and agglomerating the milled mixture and binder. The intimate mixture and binder may be sintered in a reducing atmosphere at a temperature of about 800.degree. C. to 950.degree. C. for a sufficient time to form a sintered partially alloyed mixture wherein the bulk density is greater than about 1.2 g/cc.Type: GrantFiled: June 6, 1991Date of Patent: June 30, 1992Assignee: GTE Products CorporationInventors: Vidhu Anand, Sanjay Sampath, David L. Houck, Jack E. Vanderpool