Alloying Occurs During Sintering Patents (Class 419/46)
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Patent number: 4597938Abstract: Permanent magnet materials of the Fe-B-R type are produced by:preparing a metallic powder having a mean particle size of 0.3-80 microns and a composition of 8-30 at % R, 2-28 at % B, and the balance Fe,compacting, andsintering, at a temperature of 900-1200 degrees C.Co up to 50 at % may be present. Additional elements M (Ti, Ni, Bi, V, Nb, Ta, Cr, Mo, W, Mn, Al, Sb, Ge, Sn, Zr, Hf) may be present. The process is applicable for anisotropic and isotropic magnet materials.Type: GrantFiled: September 15, 1983Date of Patent: July 1, 1986Assignee: Sumitomo Special Metals Co., Ltd.Inventors: Yutaka Matsuura, Masato Sagawa, Setsuo Fujimura
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Patent number: 4595556Abstract: A composite camshaft having a plurality of ferrous fitting members, such as cam lobes and journals, firmly bonded to a steel shaft by sintering in the presence of a liquid phase. The fitting members are fabricated as a green compact from metal powders and pre-sintered to axially shrink the compact by one-half a preselected allowance of shrinkage. Thereafter the pre-sintered fitting members are fitted on the shaft and sintered to axially shrink the compact by the remaining allowance of shrinkage and metallurgically join the shaft.Type: GrantFiled: January 2, 1985Date of Patent: June 17, 1986Assignee: Nippon Piston Ring Co., Ltd.Inventors: Genkichi Umeha, Shigeru Urano, Osamu Hirakawa, Shunsuke Takeguchi
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Patent number: 4585480Abstract: The aforementioned invention comprises an iron based powder mixture with up to 8% silicon, addition of which is in the form of ferrosilicon with a silicon content of approximately 50% and a particle size mainly less than 150 .mu.m.Type: GrantFiled: April 3, 1985Date of Patent: April 29, 1986Assignee: Hoganas ABInventors: Jan Tengzelius, Sten-Ake Kvist, Patricia Jansson
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Patent number: 4585617Abstract: Amorphous metal alloy compositions are synthesized by solid state incorporation/reduction reactions wherein a high-surface area support is brought in contact with a precursor metal-bearing compound in such a manner that the compound is incorporated into the support or caused to deposit metal onto the surface of the support. The composition obtained is an amorphous alloy composition or can be made so by heat treating at a temperature below the crystallization temperature of the amorphous metal alloy desired to be formed.Type: GrantFiled: July 3, 1985Date of Patent: April 29, 1986Assignee: The Standard Oil CompanyInventors: Michael A. Tenhover, Richard S. Henderson, Robert K. Grasselli
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Patent number: 4584172Abstract: An improved inert electrode composition is suitable for use as an inert electrode in the production of metals such as aluminum by the electrolytic reduction of metal oxide or metal salt dissolved in a molten salt bath. The composition comprises one or more metals or metal alloys and metal compounds which may include oxides of the metals comprising the alloy. The alloy and metal compounds are interwoven in a network which provides improved electrical conductivity and mechanical strength while preserving the level of chemical inertness necessary for such an electrode to function satisfactorily.Type: GrantFiled: May 3, 1984Date of Patent: April 22, 1986Assignee: Aluminum Company of AmericaInventors: Siba P. Ray, Robert A. Rapp
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Patent number: 4569822Abstract: A method is provided for preparing computer disk substrates having low surface amplitude which comprises: (a) forming a liquid suspension containing aluminum powder, an aluminum alloying element and a borate composition by initially admixing the borate composition with a volatile liquid medium to obtain a borate solution and thereafter admixing the aluminum powder and aluminum alloying element with the borate solution to produce the liquid suspension; (b) heating the liquid suspension to remove the liquid medium and to obtain a dry aluminum powder composition; (c) isostatically pressurizing the dry aluminum powder composition and roller compacting the same into sheet form; (d) heating and sintering the sheet form in a non-oxidizing atmosphere; and (e) cutting and compressing the sintered sheet into computer disk substrate configuration.Type: GrantFiled: May 11, 1984Date of Patent: February 11, 1986Inventors: Sanford W. Brown, Robert W. Hill
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Patent number: 4561889Abstract: A sintered ferrous alloy which is high in wear resistance and relatively weak in the tendency to abrade another metal material with which the sintered alloy makes rubbing contact and suitable for rocker arm tips in automotive engines for example. The sintered alloy is produced by compacting and sintering a powder mixture of 15-50 parts by weight of a Fe-Cr-B alloy powder, which contains 10-35% of Cr and 1.0-2.5% of B, 1.0-3.5 parts by weight of graphite powder, such an amount of a Cu-P alloy powder that the powder mixture contains 0.2-1.5% of P and 1.0-20.0% of Cu and the balance of an iron powder.Type: GrantFiled: October 25, 1983Date of Patent: December 31, 1985Assignee: Nissan Motor Co., Ltd.Inventors: Takaaki Oaku, Yasuzi Hokazono, Masahiko Shiota, Yoshihiro Maki
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Patent number: 4552719Abstract: A stainless steel powder is mixed with at least a Ni--Mn and a Ni--Cr powder, and the powder mixture is formed by loose packing into a required configuration. The powder mixture is sintered in a non-oxidizing atmosphere at the melting point of the Ni--Mn powder or at a higher temperature thereby to obtain a porous body.Type: GrantFiled: August 31, 1983Date of Patent: November 12, 1985Assignee: N.D.C. Co., Ltd.Inventors: Toru Morimoto, Tsuyoshi Ohsaki, Toshio Ohkawa, Masahito Fujita
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Patent number: 4544524Abstract: The solid cathodes built into reduction cells for aluminum production have at least one workface which can be wet by the precipitated metal. The starting materials, which contain titanium, boron and carbon in powder form, are first intimately mixed in such proportions that the sum of the powdered carbon and any carbon extracted from the substrate is in excess with respect to the amount required by the starting materials to form titanium diboride. This mixture is heated under a neutral or reducing atmosphere to 1600.degree.-2200.degree. C. and held for 5-45 min at this temperature. The reaction product containing pores and channels is then heated further, to 2250.degree.-2600.degree. C., and held there for 10-60 min to form a compact titanium diboride/carbon eutectic. Subsequently, the solid cathode is cooled to room temperature.Type: GrantFiled: October 9, 1984Date of Patent: October 1, 1985Assignee: Swiss Aluminium Ltd.Inventors: Tiberiu Mizrah, Matthias Hoffmann, Peter Kaser, Klemens Heilig
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Patent number: 4541877Abstract: A method of producing high performance permanent magnets is disclosed in which particles of a master alloy consisting of Fe.sub.2 B having a maximum particle size of 50 microns is admixed with Fe powder and particles of a rare earth capable of combining with Fe and B to form a tetragonal compound of Fe.sub.14 R.sub.2 B type. The admixture is compacted and a magnetic material is formed of the master alloy, Fe powder and rate earth particles which includes a major phase of at least one intermetallic compound of the Fe-R-B type having a crystal structure of the substantially tetragonal system and while the particle size of the crystal structure is controlled by sintering the compacted admixture at a temperature of about 700.degree. C. to 1000.degree. C. for from a fraction of an hour to 36 hours. The magnetic material is then annealed at a temperature of about 550.degree. C. to 650.degree. C. for a fraction of an hour to 2 hours.Type: GrantFiled: September 25, 1984Date of Patent: September 17, 1985Assignee: North Carolina State UniversityInventors: Hans H. Stadelmaier, Nadia A. ElMasry
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Patent number: 4537743Abstract: The disclosed electrode composition for a vacuum switch comprises copper, as a principal ingredient, a low melting point metal such as Bi, Pb, In, Li, Sn or any of their alloys, in a content not exceeding 20% by weight, a first additional metal such as Te, Sb, La, Mg or any of their alloys and a refractory metal such as Cr, Fe, Co, Ni, Ti, W or any of their alloys in a content less than 40% by weight.Type: GrantFiled: June 25, 1984Date of Patent: August 27, 1985Assignee: Mitsubishi Denki Kabushiki KaishaInventors: Takashi Yamanaka, Yasushi Takeya, Mitsumasa Yorita, Toshiaki Horiuchi, Kouichi Inagaki, Eizo Naya, Michinosuke Demizu, Mitsuhiro Okumura
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Patent number: 4512805Abstract: A process for the production of valve metal powder, which is doped with boron or boron compounds, for electrolytic capacitors having a low relative leakage current and a high specific charge. The doping with boron or boron compounds in amounts of up to 0.5 percent by weight, relative to the metal content, can take place either during the production of the metal powder or the green valve metal anodes.Type: GrantFiled: June 13, 1984Date of Patent: April 23, 1985Assignee: Hermann C. Starck BerlinInventors: Wolf-Wigand Albrecht, Uwe Papp, Dieter Behrens
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Patent number: 4492670Abstract: The solid cathodes built into reduction cells for aluminum production have at least one workface which can be wet by the precipitated metal. The starting materials, which contain titanium, boron and carbon in powder form, are first intimately mixed in such proportions that the sum of the powdered carbon and any carbon extracted from the substrate is in excess with respect to the amount required by the starting materials to form titanium diboride. This mixture is heated under a neutral or reducing atmosphere to 1600.degree.-2200.degree. C. and held for 5-45 min at this temperature. The reaction product containing pores and channels is then heated further, to 2250.degree.-2600.degree. C., and held there for 10-60 min to form a compact titanium diboride/carbon eutectic. Subsequently, the solid cathode is cooled to room temperature.Type: GrantFiled: January 23, 1984Date of Patent: January 8, 1985Assignee: Swiss Aluminium Ltd.Inventors: Tiberiu Mizrah, Matthias Hoffmann, Peter Kaser, Klemens Heilig
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Patent number: 4491477Abstract: An anti-wear sintered alloy comprising from 2.5 to 25.0% of Cr, from 0.10 to 3.0% of Mn, from 0.1 to 0.8% of P, from 1.0 to 5.0% of Cu, from 0.5 to 2.0% of Si, from 0 to 3% of Mo, 1.5 to 3.5% of C, one selected from the group consisting of from 0.5 to 3.0% of S and from 1.0 to 5.0% of Pb, and the balance being Fe with less than 2% of impurities, wherein S or Pb is distributed uniformly in the sintered alloy in form of sulfide or lead particle of less than 100 .mu.m and a manufacturing process thereof.Type: GrantFiled: August 24, 1982Date of Patent: January 1, 1985Assignee: Toyota Jidosha Kabushiki KaishaInventors: Tetsuya Suganuma, Koji Kazuoka, Shuichi Fujita, Yoshitaka Takahashi, Takeshi Okujo
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Patent number: 4472351Abstract: Metal-ceramic composites may be prepared by treating the ceramic component of the composite with a second metal prior to subjecting the metal-ceramic composite to a sintering operation. By pretreating the ceramic component of the composite, it is possible to obtain a composite which will undergo sintering at an elevated temperature to form a composite which will possess desirable characteristics such as increased density, hardness and low thermal coefficient of expansion, thus enabling the composites to be utilized in a wide variety of applications.Type: GrantFiled: May 5, 1983Date of Patent: September 18, 1984Assignee: UOP Inc.Inventor: Stephen T. Gonczy
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Patent number: 4440572Abstract: A process for making a novel alloy of a dispersion strengthened copper by blending dispersion strengthened copper powder and a powdered modifying metal, heat treating the blend to form the alloy, and the compacting and working the compact to densify it.Type: GrantFiled: June 18, 1982Date of Patent: April 3, 1984Assignee: SCM CorporationInventors: Anil V. Nadkarni, Prasanna K. Samal
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Patent number: 4439237Abstract: A metallurgically bonded diamond-metal composite sintered material suitable for lapping comprises a Ni and/or Co base, an intermetallic compound dispersed in said base and diamond powder, and the method of making said material comprises specifying the particle size of the base powder and then sintering same at a low temperature not exceeding a diamond graphitization temperature.Type: GrantFiled: September 25, 1981Date of Patent: March 27, 1984Assignee: Mitsui Mining & Smelting Co., Ltd.Inventors: Shiro Kuminitsu, Izumi Hayakawa, Seizo Kitatani, Akira Emura
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Patent number: 4432794Abstract: A hard alloy including at least one hard phase and a binary or multicomponent binder metal alloy, in which the hard substance comprises a finely dispersed, homogeneous distribution in the binder metal. The hard phase comprises a carbide of a Group IVb, Vb or VIb transition metal, and the binder metal alloy comprises a solid alloy of a Group IVb, Vb or VIb transition metal, with Re, Ru, Rh, Pd, Os, Ir, or Pt.Type: GrantFiled: July 17, 1981Date of Patent: February 21, 1984Assignee: Kernforschungszentrum Karlsruhe GmbHInventor: Helmut Holleck
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Patent number: 4432935Abstract: A porous body, for a solid electrolytic capacitor, is made from a combination of titanium and aluminum in order to reduce dependence upon tatalum, a material which is now in extremely short supply. First, the titanium hydride and aluminum are milled into an extremely fine micro-powder. Then, the powders are mixed with the aluminum content in the range of 45%-65%, compressed into the desired body shape, and given a three-step heat treatment. In the first step, the body is heated at a temperature of 400.degree. to 500.degree. C. for a dehydrogenation. In the second step, the dehydrogenated body is heated to an alloying temperature which is higher than 500.degree. C., but lower than the melting point of aluminum. In the third step, the alloyed body is heated to a temperature which is higher than the melting point of aluminum (about 1000.degree. C.).Type: GrantFiled: March 31, 1981Date of Patent: February 21, 1984Assignee: Nippon Electric Co., Ltd.Inventors: Yoshimi Kubo, Shigeaki Shimizu, Tetsuo Suzuki, Hitoshi Igarashi
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Patent number: 4432795Abstract: A sintered powdered titanium alloy article is provided which has a density approaching theoretical and which is characterized by having physical properties similar to those of a wrought titanium alloy article having the same chemical composition.Type: GrantFiled: February 16, 1982Date of Patent: February 21, 1984Assignee: Imperial Clevite Inc.Inventor: Phillip J. Andersen
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Patent number: 4430295Abstract: In the preferred embodiment, a method is presented for forming an iron-base article by powder metallurgy, which includes compacting a powder mixture comprising a major portion of iron particles and between about 2 to about 5 weight percent of a powder consisting of hypereutectic tricopper phosphide Cu.sub.3 P compound. The compact is sintered at a temperature between about 970.degree. C. to about 1100.degree. C., whereupon the copper phosphide forms a liquid that flows and wets the iron particle surfaces. During sintering, phosphorus from the copper phosphide diffuses into the iron particles and resulting copper-enriched liquid forms a film coating pore surfaces in the compact. The sintered article displays an improved combination of ductility and strength, particularly in view of the relatively low sintering temperature.Type: GrantFiled: November 19, 1981Date of Patent: February 7, 1984Assignee: General Motors CorporationInventor: William F. Jandeska, Jr.
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Patent number: 4415528Abstract: A method of forming precision metal alloy shaped parts starting with small particles of the individual metals and/or individual compounds containing the metals of the targeted metal alloy and a binder. A mix is initially formed of metals and/or compounds of the metals required to form a targeted alloy wherein the metal percent of each metal and/or compound is provided whereby the targeted alloy will be provided. The sizes of the particles of the metals and/or alloys are as small as possible and preferably in the range from one tenth of a micron to ten microns. These particles are mixed with an appropriate binder to form a homogeneous mass.Type: GrantFiled: March 20, 1981Date of Patent: November 15, 1983Assignee: Witec Cayman Patents, LimitedInventor: Raymond E. Wiech, Jr.
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Patent number: 4381942Abstract: The invention relates to a process for the production of titanium-based alloy members by powder metallurgy.This process consists of:(a) preparing a titanium or titanium alloy powder having a grain size distribution between 100 and 1000 .mu.m,(b) depositing on said powder a coating of a material such that on contact with the titanium or titanium alloy it forms a liquid phase at a temperature T.sub.1 which is below the allotropic transformation temperature T of the titanium or titanium alloy constituting the said powder,(c) introducing the thus coated powder into a mould, and(d) hot compressing this powder in the mould at a pressure of 10 to 30 MPa at a temperature between T.sub.1 and T for a time such that a complete densification of the powder is obtained.Application to the construction of discs for turbines with integrated blades.Type: GrantFiled: August 22, 1980Date of Patent: May 3, 1983Assignee: Commissariat a l'Energie AtomiqueInventors: Pierre Blum, Jacques Devillard