Hot Isostatic Pressing (hip) Patents (Class 419/49)
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Patent number: 4938673Abstract: The invention includes an isostatic press supply of heat to a workpiece by microwave energy and a method for isostatically pressing a powdered ceramic or powdered metal material that is heated by microwave energy. The isostatic press includes a pressure vessel. A fluid medium is available for supply to the pressure vessel under pressure. The invention further includes a means for transmitting microwave energy into the pressure vessel. The method includes preparing a workpiece comprising a microwave coupler material. Desirably, the workpiece is a composition comprising a powdered coupler or semiconductor and a powdered insulator. The workpiece is immersed in an additional powdered insulator which is transparent to the microwave energy. The workpiece and immersing powdered insulator are contained in a closed, compressible container. The contained, immersed workpiece is then placed into a pressure vessel.Type: GrantFiled: January 17, 1989Date of Patent: July 3, 1990Inventor: Donald J. Adrian
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Patent number: 4935199Abstract: In a process for producing a sintered body using a gas-impermeable membrane formed by softening of a powder layer provided on the surface of a porous body, a metal polymer selected from polysilanes, polycarbosilanes, polysilazanes and hydrolyzates of metal alkoxides is added as a binder to the powder layer. According to the process of the invention, the gas-impermeable membrane is formed with high reliability, and high density sintered bodies can be obtained in a simple process.Type: GrantFiled: July 14, 1989Date of Patent: June 19, 1990Assignee: NKK CorporationInventors: Hiroaki Nishio, Keiji Watanabe, Michitaka Satoh
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Patent number: 4933139Abstract: A process for the production of at least a one kilogram block of Chevrel-phase Pb.sub.x Mo.sub.y S.sub.z, wherein x=0.9 to 1.2, y=6.0 to 6.4, and z=7 to 8, includes mixing thoroughly stoichiometric quantities of starting materials in powdered form. The starting materials are selected from elemental Pb, Mo and S, sulfides of elemental Pb and Mo, and mixtures thereof. The starting mixture is introduced into a metallic container and evacuated to a pressure to 10.sup.4 Pa or less. The evacuated container is subjected to hot isostatic pressing at a constant pressure selected from a pressure ranging from 100 to 300 MPa, at a heating rate ranging from 10.degree. to 100.degree. C./hr., at a final pressing temperature ranging from 800.degree. to 1200.degree. C., and for a pressing period ranging from 10 to 100 hours, whereby the starting materials react to form the block of Chevrel-phase Pb.sub.x Mo.sub.y S.sub.z. The block is cooled at a cooling rate ranging from 50.degree. to 500.degree. C./hr.Type: GrantFiled: September 1, 1987Date of Patent: June 12, 1990Assignee: Kernforschungszentrum Karlsruhe GmbHInventors: Rene Flukiger, Wilfried Goldacker
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Patent number: 4931238Abstract: Method for manufacturing a sintered body with high density comprises: turning first powder into a first slurry by dispersing the first powder in a first dispersion medium composed mainly of substances capable of being extracted by supercritical fluid and forming a compact which contains the first dispersion medium, by casting the first slurry; turning second powder into a second slurry by dispersing the second powder in a second dispersion medium composed mainly of substances capable of being extracted by supercritical fluid, and forming a film layer by coating the surface of the compact with the second slurry; extracting and removing the substances contained in the compact and the substances contained in the film layer by means of the supercritical fluid; turning the film layer on the surface of the compact into an impermeable film layer to gas by heating the compact, from which the substances have been extracted and removed; and applying a hot isostatic pressing process to the compact, the film layer on theType: GrantFiled: June 6, 1988Date of Patent: June 5, 1990Assignee: Nippon Kokan Kabushiki KaishaInventors: Hiroaki Nishio, Takeshi Kawashima
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Patent number: 4931253Abstract: A method for producing a titanium alloy powder metallurgy article having high resistance to loading and creep at high temperature is described and comprises the steps of simultaneously pressing a preselected quantity of titanium alloy powder at from 15 to 60 ksi and heating the powder to a temperature just below the beta transus temperature of the alloy to promote beta to alpha phase transformation in the alloy, and then slowly cooling the compacted powder under pressure.Type: GrantFiled: August 7, 1989Date of Patent: June 5, 1990Assignee: United States of America as represented by the Secretary of the Air ForceInventors: Daniel Eylon, Francis H. Froes, Gerhard Welsch
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Patent number: 4929394Abstract: A process for compacting radioactive waste by precompressing the waste in each of capsules while filling the waste into the capsule to thereby compress the waste to the desired bulk/true density ratio under a small total pressing load and diminish damage to the inner surface of the die used, each of the capsules having a cross sectional form corresponding to a divided segment of the cross section of an HIP treatment container, then placing the capsules into the HIP treatment container, subsequently filling the HIP treatment container with a metal powder as a filler, thereafter degassing and sealing the HIP treatment container and subjecting the container to an HIP treatment in its entirety. The process precludes scattering of the radioactive substance from the waste and release of waste fragments to assure improved safety.Type: GrantFiled: January 31, 1989Date of Patent: May 29, 1990Assignees: Kabushiki Kaisha Kobe Seiko Sho, Doryokuro Kakunenryo Kaihatsu JigyodanInventors: Kazuo Kitagawa, Fumiaki Komatsu, Takayoshi Masaki, Yoshihisa Sawada, Eiichi Inada, Masao Shiatsuki
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Patent number: 4929596Abstract: Production of a sheathed wire or multiple-filament conductor composed of ceramic high-temperature superconductor by mixing Y.sub.2 O.sub.3, CuO and BaO.sub.2 or BaO.sub.2 +BaO, loading the powder mixture (3) into the interior of a metal sheath (1) lined with Ag intermediate layer (2), slowly heating to a maximum permissible reaction/sintering temperature of 950.degree. C. in a period of at least 0.1 h, holding the sintering temperature for at least 1 h, cooling down to 200.degree. C. at at most 10.degree. to 100.degree. C./h to form a conducting core (4) composed of YBa.sub.2 Cu.sub.3 O.sub.6.5-7.5. Variants having a layer composed of CuO, diffusion barrier composed of Ni, Ta, Nb, V or having Ag intermediate layer doped with AgO or BaO.sub.2. Preferably reactive sintering under a pressure of 10 to 10.000 bar as hot isostatic pressing. Variant: reactive annealing of the powder mixture under oxygen pressure of 10 to 3000 bar at 600.degree. to 950.degree. C.Type: GrantFiled: July 18, 1988Date of Patent: May 29, 1990Assignee: Asea Brown Boveri AGInventors: Gundolf Meyer, Erwin Schonfeld, Clemens Verpoort
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Patent number: 4927600Abstract: The invention is concerned with the method of compression molding a metallic or ceramic powders. The method includes the step of maintaining a negative pressure within a first mold of noncompactable powders for intimately contacting on its inner surface a pouch-like member of thin-walled resilient material for producing a second mold, and the step of compactly charging starting powders into the second mold and exhausting air from and sealing the second mold, taking out a pre-molded body of the metallis or ceramic powders together with the second mold and the step of processing the pre-molded body by a cold or hot isostatic press.Type: GrantFiled: October 8, 1987Date of Patent: May 22, 1990Assignee: Nippon Kokan Kabushiki KaishaInventors: Tsuneo Miyashita, Hiroaki Nishio, Kazuya Yabuta, Yoshio Takagi
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Patent number: 4921666Abstract: A process for high efficiency hot isostatic pressing in a hot isostatic pressing treatment for sintering or densifying a ceramic or metallic work in a high temperature and high pressure gas atmosphere, comprising preheating the work outside a high pressure vessel prior to the hot isostatic pressing treatment, transferring the preheated work as surrounded with the gas in a hot state into the high pressure vessel, then treating the work at high temperature and high pressure in a gas atmosphere, thereafter taking out the work from the high pressure vessel together with the gas atmosphere, then cooling the work if necessary, and subsequently taking it out from the gas atmosphere, as well as an apparatus for practicing the above process, wherein a treating chamber for effecting the hot isostatic pressing treatment is covered with a hermetic casing, and at least one valve mechanism capable of providing communication and cut-off between the interior and exterior of the treating chamber is provided in each of upper aType: GrantFiled: November 29, 1984Date of Patent: May 1, 1990Assignee: Kabushiki Kaisha Kobe Seiko ShoInventor: Takahiko Ishii
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Patent number: 4917722Abstract: A method for producing a single crystal of chromium is disclosed, comprising sintering a chromium molding to thereby apply thereto a thermal strain and heat treating the resulting thermally strained chromium molding. The method achieves high efficiency of crystal growth and produces a single-crystal chromium molding of complicated shape.Type: GrantFiled: May 18, 1989Date of Patent: April 17, 1990Assignee: Tosoh CorporationInventors: Tsutomu Kuniya, Koichi Hanawa, Tomoyuki Oikawa
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Patent number: 4915605Abstract: A method of consolidating metal powders selected from the group consisting essentially of aluminum, aluminum alloys, and aluminum metal matrix composites includes: pressing the powder into a preform, and preheating the preform to elevated temperatures; providing a bed of flowable pressure transmitting particles; positioning the preform in such relation to the bed that the particles encompass the preform; and pressurizing the bed to compress the particles and cause pressure transmission via the particles to the preform, thereby to consolidate the body into desired shape. Typically, the metal powder has surface oxide, and such pressurizing is carried out to break up, partially or fully, the surface oxide.Type: GrantFiled: May 11, 1989Date of Patent: April 10, 1990Assignee: Ceracon, Inc.Inventors: Hing Chan, Brian L. Oslin, Raymond L. Anderson
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Patent number: 4911625Abstract: This case relates to tough, wear resistant graded structure composites, to a process for preparing the same and to tools and products fabricated therefrom. The composites have a surface layer e.g. of WC and a binder, an interface layer, e.g. which is a stepwise transition from the surface layer whereby the binder content thereof gradually increases, a substrate layer which is a combination of e.g. an initial high carbon steel layer and finally a base layer of bainitic steel. The composites are substantially non-porous and can be used to fabricate components such as drill bits, wear plates, pump components machine tools, seals, washers, bearings and the like.Type: GrantFiled: May 17, 1989Date of Patent: March 27, 1990Assignee: The British Petroleum Company, p.l.c.Inventors: Alan R. Begg, Colin W. Brown, Neil E. S. Charman
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Patent number: 4911990Abstract: A microstructurally toughened metallic article is disclosed. The article includes discrete metal regions which are enclosed within and separated from each other by a network of metal. The regions are bonded to the network to form stable interfacial boundaries. The article exhibits high impact resistance. The process for making the article is also disclosed. The process includes positioning a plurality of structural elements within a container to define one or more void spaces within the container, introducing a quantity of metallic particles into the void spaces, and then consolidating the container, structural elements, and particles to form the microstructurally toughened article.Type: GrantFiled: February 5, 1988Date of Patent: March 27, 1990Assignee: United Technologies CorporationInventors: Karl M. Prewo, Vincent C. Nardone, James R. Strife
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Patent number: 4909840Abstract: A process for the production of a secondary powder composition having a nanocrystalline structure and being comprised of binary or quasi-binary substances composed of at least one of the elements Y, Ti, Zr, Hf, Nb, Mo, Ta and W and at least one of the elements V, Cr, Mn, Fe, Co, Ni, Cu and Pd, optionally also containing further ingredients, such as Si, Ge, B and/or oxides, nitrides, borides, carbides, and their possible mixed crystals. The components are in powdered form and are mixed in elementary form or as pre-alloys and have particle sizes ranging from 2 to 250 .mu.m. The powder components are subjected to high mechanical forces in order to produce secondary powders having a nanocrystalline structure. The secondary powders obtained in this way can be processed into molded bodies according to known compression molding processes, but at a temperature below the recrystallization temperature.Type: GrantFiled: April 7, 1988Date of Patent: March 20, 1990Assignee: Fried. Krupp Gesellschaft mit beschrankter HaftungInventor: Wolfgang Schlump
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Patent number: 4904538Abstract: A single step is relied on in the canning process for hot isostatic pressing powder metallurgy composites. The binders are totally removed while the HIP can of compatible refractory metal is sealed at high vacuum and temperature. This eliminates out-gassing during hot isostatic pressing.Type: GrantFiled: March 21, 1989Date of Patent: February 27, 1990Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space AdministrationInventor: John J. Juhas
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Patent number: 4891080Abstract: A workable, boron-containing, stainless steel alloy and an article formed therefrom are disclosed together with a process for manufacturing same. The alloy consists essentially of, in weight percent, about______________________________________ w/o ______________________________________ Carbon 0.10 max. Manganese 2.00 max. Silicon 1.00 max. Phosphorus 0.045 max. Sulfur 0.010 max. Chromium 16.00-22.00 Nickel 10.00-15.00 Molybdenum 0-3.0 Boron 0.2-2.0 Nitrogen 0.075 max. ______________________________________and the balance consisting essentially of iron. The as-worked alloy in accordance with the invention is characterized by having a boride particle areal density per weight percent boron (A.sub.N) defined by the relationshipA.sub.N .gtoreq.58,080-18,130 (%B).The as-worked alloy of the invention is further characterized by having a Charpy V-notch impact strength (CVN) defined by the relationshipCVN.gtoreq.85.917 x e.sup.-1.20297(%B).Type: GrantFiled: June 6, 1988Date of Patent: January 2, 1990Assignee: Carpenter Technology CorporationInventors: Gregory J. Del Corso, James W. Martin, David L. Strobel
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Patent number: 4891182Abstract: A process for making a porous mass of a metal of iron- or titanium-group comprises steps of forming a sinter of solvent-soluble particles, pressing in a molten metal of the iron- or titanium- group into open interstices in the sinter, and eluting the particles from the composite of the sinter and metal. Solvent-soluble magnesia particles whose surface is either covered or not with a film of boric anhydride or solvent-soluble calcia particles whose surface is either covered or not with film of calcium chloride are sintered and machined into the desired shape. The formed sinter is put in a case of a heat-insulating material that can withstand the melting temperature of a metal of iron- or titanium-group. After being heated to a given temperature together with the case, the sinter is immediately put in a metal mold where a molten metal of iron- or titanium-group is pressed into open interstices in the sinter. Then, only the particles are eluted from the sinter-metal composite by a solvent.Type: GrantFiled: March 20, 1989Date of Patent: January 2, 1990Assignee: Agency of Industrial Science & TechnologyInventors: Michiru Sakamoto, Akira Kitahara, Hidetoshi Ueno, Sumio Nagata
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Patent number: 4886639Abstract: Structural component made of powder metallurgical materials, particularly temperature resistant alloys, nickel base alloys, are produced by injection molding or pressing. The sintering is divided into individual work steps for producing dense and smooth structural components which are true to shape.Type: GrantFiled: April 30, 1987Date of Patent: December 12, 1989Assignee: MTU Motoren- und Turbinen-Union Muenchen GmbHInventors: Gerhard Andrees, Josef Kranzeder, Wilhelm Vogel
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Patent number: 4883639Abstract: An object is manufactured of a powdered material by isostatic pressing of a body (10), preformed from the powdered material, whereby the preformed body is surrounded by a casing (16) which at least for the main part is transferred to molten phase, before the isostatic pressing is carried out while sintering the powder. As material in the casing there is used glass or a material forming glass when being heated and containing 48-52 percent by weight B.sub.2 O.sub.3, 46-50 percent by weight SiO.sub.2 and 1.5-2.5 percent by weight Al.sub.2 O.sub.3. It can be removed from the finished object by water or water vapor and has a low coefficient of thermal expansion at temperatures below the melting temperature of the glass. To counteract the penetration of molten glass from the casing into the preformed body, a barrier layer (18) may be arranged on the preformed body inside the casing. (FIG.Type: GrantFiled: December 16, 1988Date of Patent: November 28, 1989Assignee: ABB Cerama ABInventors: Jan Adlerborn, Hans Larker, Jan Nilsson
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Patent number: 4879091Abstract: This invention relates to substantially full-dense, near-net shape bodies made of dispersion strengthened copper (D.S.C.) powder and products which are cold formed and/or machined from these bodies, such as resistance welding electrodes. The invention includes processes for manufacturing substantially full-dense, near-net shape, substantially equiaxed bodies from D.S.C. powder.Type: GrantFiled: December 14, 1987Date of Patent: November 7, 1989Assignee: SCM Metal Products, Inc.Inventors: Prasan K. Samal, Anil V. Nadkarni
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Patent number: 4874430Abstract: A silver base electrical contact material is described which contains a dispersion of particles consisting of cadmium oxide and nickel. The nickel particles are surrounded by a continuous adherent coating of nickel oxide which eliminates the detrimental reaction which would otherwise occur between nickel and cadmium oxide. The invention contact materials have improved lives and are fabricated by any one of several different powder metallurgy techniques.Type: GrantFiled: January 23, 1989Date of Patent: October 17, 1989Assignee: Hamilton Standard Controls, Inc.Inventor: Norman S. Bornstein
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Patent number: 4869869Abstract: A method of treating a preform consisting essentially FeNeB alloy particles to produce a magnet having superior magnetic properties, the steps:(a) removing O.sub.2 from the preform and applying an O.sub.2 resistant coating to the preform surface, or removing O.sub.2 and maintaining an O.sub.2 -free environment,(b) heating the coated preform to elevated temperature and in a non-oxidizing atmosphere, to facilitate subsequent bonding of the particles during their consolidation,(c) providing a consolidation zone containing a grain bed and transferring the heated and coated or uncoated preform to said zone to be embedded in the grain bed,(d) applying pressure to the grain bed sufficient to be transferred via the bed and to the heated preform, thereby to consolidate the preform.Type: GrantFiled: September 26, 1988Date of Patent: September 26, 1989Assignee: Ceracon, Inc.Inventors: Raymond L. Anderson, Joanna R. Groza, Brian Oslin
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Patent number: 4868065Abstract: An alloy tool of hard metal has a working part and a non-working part. The working part is made of a hard metal containing carbide of at least a metal selected from a group of elements belonging to the groups IVa, Va and VIa of the periodic table as a basis metal of the hard phase and an iron family metal as a basis metal of the binder phase. The working part includes a region for working a work piece. The non-working part is made of a hard metal containing carbide of at least a metal selected from a group of elements belonging to the groups IVa, Va and VIa of the periodic table as a basis metal of the hard phase of the non-working part and of an iron family metal as a basis metal of the binder phase of the non-working part. A diffused junction between the working and non-working parts bonds the two parts together.Type: GrantFiled: October 20, 1987Date of Patent: September 19, 1989Assignee: Sumitomo Electric Industries, Ltd.Inventors: Masao Maruyama, Atsushi Seki, Yoshihiro Minato
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Patent number: 4867788Abstract: To control grain size during recrystallization annealing of a consolidated metallurgical, dispersion-strengthened powder allow material, the initial powder is seeded with a powder alloy in which the dispersoid is absent or is in a coarser form or is present in a lesser quantity so that the seeds provide sites at which nucleation of recrystallization is promoted.Type: GrantFiled: September 26, 1988Date of Patent: September 19, 1989Assignee: United Kingdom Atomic Energy AuthorityInventor: Andrew R. Jones
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Patent number: 4863882Abstract: Rare earth oxysulfide ceramic material prepared by covering the material with a foil of a metal selected from the group consisting of molybdenum, tungsten, platinum, and rhenium, sealing it into an airtight vessel of tantalum or niobium, and then subjecting it to a hot isostatic press process.Type: GrantFiled: March 15, 1988Date of Patent: September 5, 1989Assignee: Kabushiki Kaisha ToshibaInventors: Naotoshi Matsuda, Masaaki Tamatani, Kazuto Yokota
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Patent number: 4861546Abstract: A container for holding powdered metal is formed by electroplating a layer of metal over a pattern having a configuration which corresponds to the configuration of an article to be formed. A rigid core is surrounded by the pattern material and the layer of metal. The pattern material is removed from the layer of metal to form a container in which the core is disposed. The core and container may be held against relative movement by gripping the core with the layer of metal or by pin elements extending between the core and layer of metal. The container is filled with metal powder. The metal powder is cold compacted to plastically deform the particles of metal powder without significant bonding between the particles of metal powder. The metal powder is cold compacted by exposing the container to fluid at a relatively low temperature and high pressure.Type: GrantFiled: December 23, 1987Date of Patent: August 29, 1989Assignee: Precision Castparts Corp.Inventor: Gerald I. Friedman
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Method for manufacturing metallic products from powder by hot isostatic pressing using ceramic cores
Patent number: 4855103Abstract: Method of manufacturing metal products from a powder (19) which is received in a mould cavity formed by a gas-tight casing (10, 11, 12, 13) and is isostatically hot pressed in the casing to form a monolithic body. A body (14) of graphite, hexagonal boron nitride, or another similar ceramic material is provided as a core in the mould cavity, and after the isostatic hot pressing this core is removed from the produced monolithic body by blasting.Type: GrantFiled: December 21, 1987Date of Patent: August 8, 1989Assignee: Asea Stal ABInventor: Ragnar Ekbom -
Patent number: 4853178Abstract: A method of consolidating a body in any of initially powdered, sintered, fibrous, sponge, or other form capable of compaction, including the steps: providing a bed of flowable particles within a contained zone, the particulate including flowable and resiliently compressible carbonaceous particles; positioning the body in the bed, to be surrounded by the particles; effecting pressurization of the bed to cause pressure transmission via the particles to said body, thereby to compact the body into desired shape, increasing its density; the particles being heated to elevated temperature prior to compacting of the body into desired shape; and the heating of the particles being effected by passing electric current through same, with heat generated in the particles also to be transferred to the body.The electrically heated mass of particles may be fluidized; the particles may consist of graphite; and the body may consist of metal, ceramic, or synthetic resin.Type: GrantFiled: November 17, 1988Date of Patent: August 1, 1989Assignee: Ceracon, Inc.Inventor: Brian L. Oslin
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Patent number: 4851190Abstract: The disclosure relates to a turbine disk and a method of making the turbine disk comprising the steps of rotating a mold, adding a first powdered metal to the rotating mold at a first rate, reducing the rate of addition of the first metal to a second rate, and adding a second powdered metal to the mold at a third rate substantially equal to the difference between the first and second rates.Type: GrantFiled: July 27, 1987Date of Patent: July 25, 1989Assignee: Williams International CorporationInventors: Kim E. Bowen, Steven M. Foster, Said Izadi
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Patent number: 4851189Abstract: Method of manufacturing cams for camsshafts by powder metallurgy, wherein the formed cams have constant properties over the volume thereof and are well polishable, includes molding into a cam blank a powder mixture made up of iron powder alloyed with carbide-forming elements of the fifth and sixth secondary groups of the periodic table, and graphite powder in a quantity necessary for carbide formation; sintering the blank at a temperature of at most 50 K above a solidus temperature of the blank; and compacting the blank by hot-isostatic compression at a temperature below the solidus temperature to at least 99% of a theoretical density.Type: GrantFiled: August 17, 1988Date of Patent: July 25, 1989Assignee: Ringsdorff-Werke GmbHInventors: Jurgen Donch, Bernhard Schelb, Wolfgang Zimmermann
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Patent number: 4847962Abstract: A method for producing porous bearing shells with a compacted surface for gas-static bearings from sintered hollow blanks includes heating a blank with an inside diameter smaller than a rated diameter of a bearing and slipping the blank in the heated state onto a mandrel having an outside diameter equal to the rated diameter of the bearing. Subsequently the blank is cooled to the operating temperature of the bearing. The blank is reheated and the blank is finally pulled off the mandrel.Type: GrantFiled: April 29, 1988Date of Patent: July 18, 1989Assignee: Interatom GmbHInventor: Heinrich Puetz
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Patent number: 4847044Abstract: A softer metal such as aluminum, or a metal forming a metal aluminide, or an alloy containing these metals is added to a metal aluminide composite during fabrication to promote easy consolidation of the metal aluminide matrix with the reinforcing phase. The metal aluminide may be titanium aluminide, nickel aluminide, or iron aluminide. The softer metal, the metal aluminide matrix, and the reinforcing phase are pressed together at a temperature above the softening temperature of the softer metal. The softened metal promotes flow and consolidation of the matrix and the reinforcement at relatively low temperatures. The composite is held at an elevated temperature to diffuse and convert the soft metal phase into the metal aluminide matrix. By consolidating at a lower temperature, cracking tendencies due to thermal expansion differences between the matrix and reinforcement is reduced. By consolidating at a lower pressure, mechanical damage to the fibers is avoided.Type: GrantFiled: April 18, 1988Date of Patent: July 11, 1989Assignee: Rockwell International CorporationInventor: Amit K. Ghosh
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Patent number: 4844863Abstract: A method of producing clad metal comprises the steps of forming a cladding on the surface of a metal substrate by subjecting powder of a metal which is of a different type from that of the metal substrate and is selected from among Ni-base alloys, Co-base alloys, Ti-base alloys, Fe-base superalloys and stainless steels to hot isostatic pressing under a gas pressure load of not less than 300 Kg/cm.sup.2 at a temperature not higher than the solidus thereof, thereby to obtain a composite material, and elongating the composite material by hot working. Optionally the composite material is subjected to soaking or solution treatment before being subjected to hot working.Type: GrantFiled: March 24, 1988Date of Patent: July 4, 1989Assignee: Nippon Steel CorporationInventors: Akihiro Miyasaka, Hiroyuki Ogawa, Hiroyuki Homma, Saburo Kitaguchi, Hiroshi Morimoto, Satoshi Araki
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Patent number: 4836978Abstract: A production method of a vacuum circuit breaker electrode comprises the steps of mixing conductive metal powder, and refractory material powder with a higher melting point than said conductive metal powder, compacting the resultant mixture to form a compact, presintering the compact in a atmosphere of high purity hydrogen, sealing a presintered body in a capsule while exhausting, heating and degassing, and subjecting the sealed capsule to hot isostatic pressing treatment. The conductive metal powder is one or both of Cu and Ag. The hot isostatic pressing treatment is effected at a temperature higher than a melting point of the conductive metal so that the presintered body is sintered under liquid phase, and a part of molten conductive metal component is seeped out on a sintered body surface.Type: GrantFiled: September 2, 1987Date of Patent: June 6, 1989Assignee: Hitachi, Ltd.Inventors: Ryuji Watanabe, Hisashi Andoh, Kiyoji Iwashita, Kinko Shimizu
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Patent number: 4834917Abstract: Waste material such as toxic compounds, radioactive waste materials and spent nuclear fuel rods are encapsulated in a container system which is subjected to a hot pressure process to cause a protective powder material located around the waste material to form a dense matrix and function as a highly corrosion resistant and protective shroud. Embodiments include hot isostatic pressing and hot uniaxial pressing, the use of metal powder such as copper powder for the protective powder material or alternatively ceramic powder and, depending upon the embodiment chosen, the use of a single container or dual container system in which a first container is located within an outer container. Either or both of such containers may be cylindrical with a bellows-like side wall to facilitate compression thereof in an axial direction.Type: GrantFiled: June 23, 1987Date of Patent: May 30, 1989Assignees: Australian Nuclear Science & Technology Organization, The Australian National UniversityInventors: Eric J. Ramm, Albert E. Ringwood
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Patent number: 4820484Abstract: Method in producing a molding of an iron alloy, wherein the molding is produced by hot isostat pressing of a prealloyed powder comprising 0.5 to 2.8% coal by weight, 24 to 35% chromium by weight, from effective amount to 2% silicon by weight, from effective amount to 1.5% manganese by weight, 0 to 2.3% nickel weight, and 0 to 3.0% molybdenum by weight, and the residue iron.Type: GrantFiled: October 2, 1986Date of Patent: April 11, 1989Assignee: Asea Stal ABInventor: Ragnar Ekbom
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Patent number: 4820393Abstract: The present invention provides a sputter target for the deposition of titanium nitride films. The sputter target has a target face comprising titanium nitride having a density of at least 90% of the theoretical density of 100% pure titanium nitride. The sputter target is prepared by subjecting titanium nitride powder to hot isostatic pressure.Type: GrantFiled: May 11, 1987Date of Patent: April 11, 1989Assignee: Tosoh SMD, Inc.Inventors: Teodoro E. Brat, Charles E. Wickersham
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Patent number: 4813124Abstract: A bakeable evacuative fabrication assembly for the production of permanent agnets formed by assembling discrete magnetic elements on a core, enclosing such assembly in a close-fitting container, providing end closures on said container, and providing a one of said end closures with a sealably closeable cold mold vent means.Type: GrantFiled: July 20, 1987Date of Patent: March 21, 1989Assignee: The United States of America as represented by the Secretary of the ArmyInventor: Joseph P. Klimek
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Patent number: 4810289Abstract: A process of hot isostatic pressing of powders to form electrical contacts is characterized by the steps: (A) mixing powders, 1 in the Drawing, from metal containing powder or metal containing powder plus carbon powder, where at least one of Ag and Cu is present, (B) thermal cleaning treatment of the powder, 2 in the Drawing, (C) granulating the thermally treated powder, 3 in the Drawing, (D) uniaxially pressing the powders without heating, 5 in the Drawing, to provide a compact, (E) placing at least one compact in a pressure-transmitting, pressure-deformable container, 6 in the Drawing, and surrounding each compact with fine particles of a separating material, (F) evacuating air from the container, 7 in the Drawing, (G) sealing the compacts inside the container, 8 in the Drawing, (H) hot isostatic pressing, 9 in the Drawing, the compacts through the pressure transmitting material at a pressure from 352 kg/cm.sup.2 to 2,115 kg/cm.sup.2 and a temperature from 0.5.degree. C. to 100.degree. C.Type: GrantFiled: April 4, 1988Date of Patent: March 7, 1989Assignee: Westinghouse Electric Corp.Inventors: Norman S. Hoyer, Natraj C. Iyer
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Patent number: 4808224Abstract: A method of treating a preform consisting essentially FeNeB alloy particles to produce a magnet having superior magnetic properties, the steps:(a) removing O.sub.2 from the preform and applying an O.sub.2 resistant coating to the preform surface, or removing O.sub.2 and maintaining an O.sub.2 -free environment,(b) heating the coated preform to elevated temperature and in a non-oxidizing atmosphere, to facilitate subsequent bonding of the particles during their consolidation,(c) providing a consolidation zone containing a grain bed and transferring the heated and coated or uncoated preform to said zone to be embedded in the grain bed,(d) applying pressure to the grain bed sufficient to be transferred via the bed and to the heated preform, thereby to consolidate the preform.Type: GrantFiled: September 25, 1987Date of Patent: February 28, 1989Assignee: Ceracon, Inc.Inventors: Raymond L. Anderson, Joanna R. Groza, Brian Oslin
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Patent number: 4799956Abstract: A gasket or other sealing member containing intercalated graphite exhibits improved strength and safety properties and simplified manufacture. Such a gasket may be formed by filling a mold of the appropriate shape with intercalated graphite powder and applying sufficient pressure and heat to produce a coherent mass. The properties of an intercalated graphite gasket may be further improved by incorporating metal reinforcement, metal powders, organic polymers ceramic powders or even exfoliated graphite into the intercalated graphite gasket.Type: GrantFiled: February 17, 1987Date of Patent: January 24, 1989Assignee: Intercal CompanyInventor: Ferdinand L. Vogel
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Patent number: 4785574Abstract: Methods and apparatus are disclosed for consolidating loose or pre-compressed particulate materials, such as metal powder or metal flakes, in press equipment utilizing a reusable canister means that is sealed in vacuum from the atmosphere and heated prior to consolidation in the press equipment at elevated pressures and temperatures, thereby improving utilization of the press equipment.Type: GrantFiled: March 2, 1987Date of Patent: November 22, 1988Assignee: Battelle Memorial InstituteInventor: Robert J. Fiorentino
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Patent number: 4781886Abstract: A method is disclosed for producing a high hardness refractory metal part, the method comprising hot isostatic pressing a refractory metal part having a density greater than about 98% of the theoretical density in the presence of a pressurizing gas having an atomic size great enough to strain the lattice of the refractory metal at a pressure to exceed the yield strength of the metal to result in the densification of the part to a density of greater than about 98% of the theoretical density. The part is then rapidly cooled. The resulting part has a hardness approaching the hardness of mechanically worked material.Type: GrantFiled: February 29, 1988Date of Patent: November 1, 1988Assignee: GTE Products CorporationInventors: Thomas J. Patrician, Vito P. Sylvester
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Patent number: 4778650Abstract: In the manufacture of an object of a powdered material by isostatic pressing of a body (10) preformed from the powdered material with a gaseous pressure medium, the preformed body is provided with a casing (13) of glass which is made gas-impenetrable by heating before carrying out the isostatic pressing. Inside the glass casing there is arranged on the preformed body an intermediate layer (12) which counteracts the penetration of molten glass from the casing into the preformed body. The intermediate layer comprises a layer of one or more intermediate phases in the system Al.sub.2 O.sub.3 --SiO.sub.2, for example mullite 3Al.sub.2 O.sub.3.2SiO.sub.2, or a layer containing one or more such intermediate phases as main constituent. In a preferred embodiment a layer of boron nitride is arranged inside the intermediate layer. In a preferred embodiment, the powdered object consists of aluminium oxide or an aluminium oxide-based ceramic.Type: GrantFiled: February 12, 1988Date of Patent: October 18, 1988Assignee: ASEA Cerama ABInventors: Leif Hermansson, Anna-Karin Tjernlund
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Patent number: 4772450Abstract: In forming an article, such as a turbine blade, of metal powder, a container is first formed by electroplating a thin layer of metal over a pattern having a configuration which corresponds to the configuration of the article. The pattern is then removed to leave a container having a cavity with a configuration corresponding to the configuration of the article. The container is filled with metal powder and sealed. The container is then at least partially enclosed with a rigid body of fluid permeable material having inner side surface areas disposed in abutting engagement with the container. Heat and fluid pressure are transmitted through the rigid body to compact the container and metal powder. The fluid pressure causes the side walls of the container to move away from the inner side surfaces of the rigid body of fluid permeable material.Type: GrantFiled: July 25, 1984Date of Patent: September 20, 1988Assignee: TRW Inc.Inventor: Gerald Friedman
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Patent number: 4772437Abstract: A solid flowable polymeric material useful as a pressurizing medium that is ultraviolet detectable and is particularly adapted for use in a molding process. The polymeric material comprises a substantially uniform mixture of a solid, flowable, particulate silicone having a nominal flow rate of at least 0.6 gram per second through a 1.1 cm diameter pipe 7.6 cm long under applied pressure of 10.34 MPa at room temperature and an ultraviolet detectable compound. The polymeric material is especially useful for molding composites. A composite is disposed with a pressure vessel which is substantially filled with the above mixture. The silicone is caused to produce a substantially uniform, predetermined medium pressure on the surface of said composite prepreg. The composite prepreg is cured to form a composite which is removed from the pressure vessel and exposed to ultraviolet light.Type: GrantFiled: September 10, 1986Date of Patent: September 20, 1988Assignee: United Technologies CorporationInventors: Richard T. Reavely, David J. Parker, Robert V. Kromrey
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Patent number: 4770835Abstract: A method of molding an article utilizing two types of solid flowable particulate polymer pressurizing media wherein one medium is protected from thermal degradation by a second medium. The method comprises disposing an article precursor within a pressure vessel and disposing a first solid flowable polymer medium that is substantially thermally stable at temperatures in excess of about 316.degree. C. so that it is capable of transferring a substantially uniform, predetermined medium pressure to the surface of the article precursor. A second solid flowable polymer medium is disposed so that it is capable of transferring a substantially uniform, predetermined medium pressure to the first polymer medium. The second medium is caused to produce a substantially uniform medium pressure so that said pressure is transferred to the surface of the article precursor and the article precursor is exposed to temperatures in excess of about 316.degree. C.Type: GrantFiled: September 10, 1986Date of Patent: September 13, 1988Assignee: United Technologies CorporationInventor: Robert V. Kromrey
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Patent number: 4770850Abstract: A novel magnesium alloy consisting essentially of about 6 to 14 weight percent calcium, about 4 to 8 weight percent of copper or nickel, balance magnesium.There is also provided a process for producing a magnesium alloy article having improved properties which comprises the steps of providing a rapidly solidified product having the composition defined above and having a maximum average thickness of about 200 microns in at least one dimension, introducing the rapidly solidified product into a mold, and consolidating the rapidly solidified product to obtain a desired densification of the rapidly solidified product. Consolidation may be carried out by hot isostatic pressing (HIP'ing) the rapidly solidified product at a pressure of about 100 to 300 MPa and a temperature of about 150.degree. to 350.degree. C. for a time sufficient to obtain the desired densification. Alternatively, consolidation may be accomplished by extrusion using the same temperature range, and an extrusion ratio of about 10:1 to 30:1.Type: GrantFiled: October 1, 1987Date of Patent: September 13, 1988Assignee: The United States of America as represented by the Secretary of the Air ForceInventors: Franz J. Hehmann, Setumadhavan Krishnamurthy, Erica Robertson, Steven J. Savage, Francis H. Froes
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Patent number: 4767456Abstract: A corrosion and wear resistant sintered powdered metal alloy having a density of at least 99.9 percent of theoretical density is provided. The alloy comprises, in weight percent, from about 13 to about 17 percent chromium, from about 5.5 to about 8.5 percent molybdenum, from about 1.25 to about 2.5 percent vanadium, and from about 1.2 to about 1.65 percent carbon, with the balance being iron plus trace elements. The foregoing alloy is used to produce corrosion and wear resistant bearings which are characterized by high hot hardness and toughness.Type: GrantFiled: March 26, 1987Date of Patent: August 30, 1988Assignee: MRC Bearings IncorporatedInventor: Ronald F. Spitzer
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Patent number: 4762679Abstract: A process for manufacturing powder metallurgy (P/M) preforms which are conditioned for optimum intrinsic workability is described which comprises steps of heating a quantity of P/M material in a can to a first preselected temperature under vacuum to degas the material, compacting the canned material at a second preselected temperature under pressure to provide a compact of the material; or cold compacting the powder to about 75% density and degassing it at suitable temperature and then vacuum hot pressing the powder at about 0.Type: GrantFiled: July 6, 1987Date of Patent: August 9, 1988Assignee: The United States of America as represented by the Secretary of the Air ForceInventors: Harold L. Gegel, Yellapregada V. R. K. Prasad, Sokka M. Doraivelu, Raghavan Srinivasan, J. S. Gunasekera, Douglas R. Barker, James T. Morgan, Jr., James C. Malas, Kristine A. Lark, Lawrence E. Matson