Consolidation Of Powders Patents (Class 419/66)
  • Patent number: 5302341
    Abstract: The subject invention relates to method for briquetting fines and ultrafines comprising mixing the fines and ultrafines on a continuous basis with a binder system having low viscosity of up to about 200 cps and at least 50% solids, such that the resulting briquette contains less than about 3% binder by weight of the briquette.
    Type: Grant
    Filed: October 29, 1992
    Date of Patent: April 12, 1994
    Assignee: Palsat International, Inc.
    Inventors: Francis S. Palowitz, Sudarshan R. Sathe
  • Patent number: 5284532
    Abstract: A rapidly solidified aluminum based alloy consists essentially of the formula Al.sub.bal Fe.sub.a M.sub.b Si.sub.c R.sub.d, wherein M is at least one element selected from the group consisting of V, Mo, Cr, Mn, Nb, Ta, and W; R is at least one element selected from the group consisting of La, Ce, Pr, Nd, Sm, Gd, Dy, Er, Yb, and Y; "a" ranges from 3.0 to 7.1 atom %; "b" ranges from 0.25 to 1.25 atom %; "c" ranges from 1.0 to 3.0 atom %; "d" ranges from 3.0 to 0.3 atom % and the balance is aluminum plus incidental impurities, with the provisos that (i) the ratio [Fe+M]:Si ranges from about 2.0:1 to 5.0:1 and (ii) the ratio Fe:M ranges from about 16:1 to 5:1. The alloy exhibits improved elevated temperature strength due to the rare earth element additions without an increase in the volume fraction of dispersed intermetallic phase precipitates therein.
    Type: Grant
    Filed: January 14, 1993
    Date of Patent: February 8, 1994
    Assignee: Allied Signal Inc.
    Inventor: David J. Skinner
  • Patent number: 5277717
    Abstract: A rapidly solidified, low density aluminum base alloy consists essentially of the formula Al.sub.bal Li.sub.a Cu.sub.b Mg.sub.c Zr.sub.d wherein "a" ranges from about 2.2 to 2.5 wt %, "b" ranges from about 0.8 to 1.2 wt %, "c" ranges from about 0.4 to 0.6 wt % and "d" ranges from about 0.4 to 0.8 wt %, the balance being aluminum plus incidental impurities. The alloy is especially suited to be consolidated to produce a strong, tough, low density aircraft landing wheel.
    Type: Grant
    Filed: August 4, 1992
    Date of Patent: January 11, 1994
    Assignee: AlliedSignal Inc.
    Inventors: Jerry C. LaSalle, Santosh K. Das
  • Patent number: 5264021
    Abstract: A compacted and consolidated aluminum-based alloy material is obtained by compacting and consolidating a rapidly-solidified material having a composition represented by the general formula: Al.sub.a Ni.sub.b X.sub.c M.sub.d or Al.sub.a' Ni.sub.b X.sub.c M.sub.d Q.sub.e, where X is one or two elements selected from La and Ce or an Mm; M is Zr or Ti; Q is one or more elements selected from Mg, Si, Cu and Zn, and a, a', b, c, d and e are, in atomic percentages, 84.ltoreq.a.ltoreq.94.8, 82.ltoreq.a'.ltoreq.94.6, 5.ltoreq.b .ltoreq.10, 0.1.ltoreq.c.ltoreq.3, 0.1.ltoreq.d.ltoreq.3, and 0.2.ltoreq.e.ltoreq.2. According to the production process of the invention, powder or flakes obtained by rapidly solidifying are compacted, followed by compressing, forming and consolidating by conventional plastic working operations. The consolidated material has an elongation sufficient to withstand secondary working operations. Moreover, the material retains the excellent properties of its raw material as they are.
    Type: Grant
    Filed: August 14, 1992
    Date of Patent: November 23, 1993
    Assignee: Yoshida Kogyo K.K.
    Inventors: Kazuhiko Kita, Makoto Kawanishi, Hidenobu Nagahama
  • Patent number: 5259860
    Abstract: A sintered metal part has a magnesium metasilicate mineral, or a magnesium metasilicate mineral and a magnesium orthosilicate mineral, or at least one of a magnesium metasilicate mineral and a magnesium orthosilicate mineral and at least one of boron nitride and manganese sulfide dispersed throughout the metal matrix. An iron-based sintered sliding member is of a structure that free graphite and an intercrystalline inclusion have been dispersed throughout the metal matrix that consists essentially of, in weight ratio, 1.5 to 4% of carbon, 1 to 5% of copper, 0.1 to 2% of tin, 0.1 to 0.5% of phosphorus, 0.
    Type: Grant
    Filed: October 9, 1991
    Date of Patent: November 9, 1993
    Assignee: Hitachi Powdered Metals Co., Ltd.
    Inventors: Yutaka Ikenoue, Ryoji Satoh, Koichiro Hayashi, Katsunao Chikahata
  • Patent number: 5250255
    Abstract: Green compacts for sintered ceramic bodies and for sintered permanent magnets are produced by first preparing outside a die press machine a mold which contains a rubber portion in at least a side portion. The mold cavity is then filled with the fine powder which is to form the compact to a density which is at least 1.2 times the natural filling density of the powder. The filled rubber mold is then placed in the die press machine and compacted in the die press machine to produce the green compact. The natural filling density is obtained by allowing the powder to fall from a powder pan into the rubber mold until the powder reaches the top of the rubber mold, where the distance from the powder pan to the bottom of the rubber mold is 3.7 times the depth of the cavity of the rubber mold.
    Type: Grant
    Filed: December 2, 1991
    Date of Patent: October 5, 1993
    Assignee: Intermetallics Co., Ltd.
    Inventors: Masato Sagawa, Hiroshi Nagata, Hiroo Shirai
  • Patent number: 5217664
    Abstract: Process for the production of a component, in which metal or ceramic powder (6) is applied under centrifugal force to the inner wall of a gas-permeable mold (13), which is under reduced pressure and is located in a reduced-pressure vessel (10), and precompacted, after which the mold (13) is removed from the vessel (10) and sintered. The mold (13) consists of a heap of ceramic grains with an organic binder having high strength between room temperature and a temperature just below the sintering temperature, in order to support the powder (6) to be sintered to give the component. When sintering starts, the binder evaporates or burns away, as a result of which the mold (13) substantially loses its supporting action for the component. Binder: aminolic, phenolic, furan resin.
    Type: Grant
    Filed: March 13, 1991
    Date of Patent: June 8, 1993
    Assignee: Asea Brown Boveri Ltd.
    Inventor: Heinrich Feichtinger
  • Patent number: 5215697
    Abstract: A shaped body is formed from fine particles such as powder, whiskers or short fibers of ceramics or metal, by preparing a mold having a mold chamber, an inlet port open to the mold chamber at its first portion and adapted to introduce a mixture of the fine particles and a carrier fluid into the mold chamber, and an outlet port open to the mold chamber at its second portion substantially opposite to the first portion and adapted to exhaust substantially only the carrier fluid in a gaseous state out of the mold chamber; preparing the mixture of the fine particles and the carrier fluid; and supplying the mixture under a pressure elevated substantially above atmospheric pressure into the mold chamber through the inlet port while exhausting the carrier fluid out of the mold chamber through the outlet port.
    Type: Grant
    Filed: March 11, 1992
    Date of Patent: June 1, 1993
    Assignee: Toyota Jidosha Kabushiki Kaisha
    Inventors: Kazuyuki Toki, Mikio Murachi
  • Patent number: 5180446
    Abstract: Improvement of Nb-alloys, which are known as heat-resistant alloys, by giving anti-oxidation property thereto and increasing the high temperature strength thereof. In addition to a determined amount of Al, one of (1) suitable amounts of Ti, Cr and V, and (2) suitable amounts of Cr and Co, are added to Nb-matrix, and a high melting temperature metal oxide such as Y.sub.2 O.sub.3 or Al.sub.2 O.sub.3 is dispersed in the matrix. Preferable method of preparing the alloys is combination of mechanical alloying and subsequent hot processing.
    Type: Grant
    Filed: January 27, 1992
    Date of Patent: January 19, 1993
    Assignee: Daido Tokushuko Kabushiki Kaisha
    Inventors: Kenji Tsukuta, Tomohito Iikubo
  • Patent number: 5174955
    Abstract: A heat-resisting aluminum alloy contains manganese ranging from 6 to 8% by weight, iron ranging from 0.5 to 2% by weight, zirconium ranging from 0.03 to 0.5% by weight, and copper ranging from 2 to 5% by weight, the balance being essentially aluminum. The aluminum alloy has been confirmed to be high in mechanical strength both at ordinary temperatures and at high temperatures while to be suitable for producing an article by using so-called atomization process.
    Type: Grant
    Filed: July 22, 1986
    Date of Patent: December 29, 1992
    Assignee: Nissan Motor Co., Ltd.
    Inventors: Masahiko Shioda, Syunsuke Suzuki, Akira Matsuyama, Yoshihiro Maki
  • Patent number: 5152959
    Abstract: The present invention relates to a process for forming a composite strip material without any sintering step. The process includes blending a powdered high conductivity material such as powdered copper with a powdered low thermal expansion phase material such as a nickel-iron alloy, compacting the powders to form a green composite strip, heating the green strip to a hot rolling temperature and hot rolling the heated strip to a desired gauge. The heated strip is reduced less than about 45% to minimize the deformation of the low thermal expansion phase particles.
    Type: Grant
    Filed: June 24, 1991
    Date of Patent: October 6, 1992
    Assignee: AMETEK Speciality Metal Products Division
    Inventor: Clive R. Scorey
  • Patent number: 5126104
    Abstract: A method is disclosed for preparing an intimate mixture of powders of nickel-chromium-boron-silicon alloy, molybdenum metal powder, and Cr.sub.3 C.sub.2 /NiCr alloy suitable for thermal spray coatings which comprises milling a starting mixture of the above two alloys with molybdenum powder to produce a milled mixture wherein the average particle size is less than about 10 micrometers in diameter, forming an aqueous slurry of the resulting milled mixture and a binder which can be an ammoniacal molybdate compound or polyvinyl alcohol, and agglomerating the milled mixture and binder. The intimate mixture and binder may be sintered in a reducing atmosphere at a temperature of about 800.degree. C. to 950.degree. C. for a sufficient time to form a sintered partially alloyed mixture wherein the bulk density is greater than about 1.2 g/cc.
    Type: Grant
    Filed: June 6, 1991
    Date of Patent: June 30, 1992
    Assignee: GTE Products Corporation
    Inventors: Vidhu Anand, Sanjay Sampath, David L. Houck, Jack E. Vanderpool
  • Patent number: 5122319
    Abstract: A method of forming a cylindrical compact for a cylindrical magnet is improved by moving a core pin and a die of a mold at the same time of pressing magnet materials with a pressing punch in the same direction as that of the pressing punch at travelling speed Vc and Vd indicated by following equation:Vc=m.multidot.Vp(0.5.ltoreq.m.ltoreq.1.0)Vd=n.multidot.Vp(0.5.ltoreq.n.ltoreq.1.0)where Vc is the travelling speed of the core pin, Vd is the travelling speed of the die and Vp is the pressing speed of the pressing punch. It is possible to form the thin-walled elongated cylindrical compact by utilizing the frictional force caused between the mold and the magnet materials for forming the compact very effectively in order to obtain a thin walled elongated cylindrical magnet.
    Type: Grant
    Filed: March 22, 1991
    Date of Patent: June 16, 1992
    Assignee: Daido Tokushuko K.K.
    Inventors: Teruo Watanabe, Yasuaki Kasai, Hiyoshi Yamada, Norio Yoshikawa, Yutaka Yoshida
  • Patent number: 5118468
    Abstract: The subject of the invention is a method of making a clad metal, neutron absorbing element, and the neutron absorbing element produced by preparing compactable metal products comprising (weight %) HF at least 25%, Zr and/or Zr alloys=0 to 75%; Ti and/or Ti alloys=0 to 75%; Hf-ZR alloys containing <55% Zr=0 to 75%; Hf-Ti alloys containing <55% Ti=0 to 75%; neutron absorbing metal elements melting at over 400.degree. C.: <0.2% and other metal elements melting at over 400.degree. C.: 0 to the balance, the balance being less than 5%; introducing at least some of these products into a metal container with an open end; compressing the products in the container, or compressing them before putting them into the container; if necessary repeating the introduction and compression of the products until the container is at least 95% full; and closing the open end of the container by welding on a metal lid or plug and providing an internal vacuum. The element is used, e.g.
    Type: Grant
    Filed: July 20, 1989
    Date of Patent: June 2, 1992
    Assignee: Compagnie Europeenne Du Zirconium Cezus
    Inventors: Jean Boutin, Luc Moulin
  • Patent number: 5114470
    Abstract: A method of producing nitrogenated metal alloys which involves melting a al alloy under a nitrogen atmosphere and subsequently gas atomizing the molten alloy with nitrogen gas has been found to produce alloys powders having a high nitrogen content and a minimum amount of hollow particles. The resulting alloy powders which demonstrate superior mechanical properties and heat and chemical resistance are easily fabricated into articles utilizing powder metallurgical processes.
    Type: Grant
    Filed: October 4, 1990
    Date of Patent: May 19, 1992
    Assignee: The United States of America as represented by the Secretary of Commerce
    Inventors: Francis S. Biancaniello, Gregg N. Janowski, Stephen D. Ridder
  • Patent number: 5112572
    Abstract: The invention provides a method for removing the oxide surface from water atomized metal powders containing an oxidizer capable of oxidizing chromium from a trivalent to a soluble hexavalent state, whereby chromium oxides are removed from the metal powder surface. The powder is then treated with a dilute acid solution essentially devoid of hydrofluoric acid to remove other hydrated oxides from the metal powder surface. The powder is then water washed and dried.
    Type: Grant
    Filed: October 1, 1991
    Date of Patent: May 12, 1992
    Assignee: Inco Limited
    Inventors: Thijs Eerkes, James A. E. Bell, Carlos M. Diaz
  • Patent number: 5102863
    Abstract: A process for fabricating superconducting composite wire by the steps of placing a superconductive precursor admixture capable of undergoing a self propagating combustion in stoichiometric amounts sufficient to form a superconductive product within a metal tube, sealing one end of said tube, igniting said superconductive precursor admixture whereby said superconductive precursor admixture endburns along the length of the admixture, and cross-section reducing said tube at a rate substantially equal to the rate of burning of said superconductive precursor admixture and at a point substantially planar with the burnfront of the superconductive precursor mixture, whereby a clad superconductive product is formed in situ, the product characterized as superconductive without a subsequent sintering stage, is disclosed.
    Type: Grant
    Filed: March 19, 1991
    Date of Patent: April 7, 1992
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Richard B. Cass, Kevin C. Ott, Dean E. Peterson
  • Patent number: 5100602
    Abstract: A method and apparatus for filling generally cylindrical molds with powder particles is disclosed. A stream of powder particles is fed into a mold, and the powder particles are compacted in spirally formed layers so that the particles are compacted continuously in localized adjacent areas. The powder filling apparatus is comprised of a blade means configured to direct powder particles to spread evenly in the mold and urge the powder particles to compact while the blade means is rotated about an axis. A shaft is attached to the blade means for rotation of the blade means about the axis. A chuck means is slideably mounted on the shaft means through an axial channel, the chuck means being configured for applying force to the shaft while permitting movement of the shaft axially through the channel. A drive means is operatively connected to the chuck means for applying force to rotate the chuck about the axis.
    Type: Grant
    Filed: January 28, 1991
    Date of Patent: March 31, 1992
    Assignee: General Electric Company
    Inventors: James Day, Bernard P. Bewlay
  • Patent number: 5094811
    Abstract: The invention is a method for making an electrically conductive path on the wall of a passage through a substrate. It is especially useful for connecting electrically conductive paths (25) on opposite sides of a circuit board (20). The method is characterized by the steps of forming a tapered passage (21) through the substrate (20) that connects to at least one conductive path on each side of the substrate (20), filling the tapered passage (21) with an electrically conductive powder (10), applying pressure with a tapered die (30) to compact the powder (11) against the wall of the passage (21) without blocking the passage, and then heating the compacted powder (11) to a temperature that increases the conductivity and ductility of the compacted powder (11) and its adhesion to the substrate (20) without adversely affecting the shape or condition of the substrate (20).
    Type: Grant
    Filed: December 30, 1985
    Date of Patent: March 10, 1992
    Assignee: Allied-Signal
    Inventors: Robert P. Kane, Bruce E. Kurtz
  • Patent number: 5093076
    Abstract: This invention describes a practice for the hot pressing and/or hot working of rare earth element-containing alloy powders using open-to-the-air presses. The rare earth-containing powder is pressed into a compact at ambient temperatures using a solid lubricant only on the die wall. This compact is then hot pressed in an open air press utilizing a heated die flooded with argon.
    Type: Grant
    Filed: May 15, 1991
    Date of Patent: March 3, 1992
    Assignee: General Motors Corporation
    Inventors: Kevin A. Young, Joseph J. Worden, Donald S. Kirk, Larry J. Eshelman
  • Patent number: 5092023
    Abstract: A process for the production of, in particular, ceramic parts having a cavity by press molding or pressing sealed sheaths.The core used for defining the cavity and preventing subsequent machining operations is initially more voluminous than the desired cavity and has an adequate ductility to allow partial extrusion during pressing. This avoids often excessive mechanical stresses, which can lead to a bursting or shattering of the densified part when the sheath is removed. This process has, application to the hot isostatic pressing of fragile materials.
    Type: Grant
    Filed: November 21, 1990
    Date of Patent: March 3, 1992
    Assignee: Commissariat a l'Energie Atomique
    Inventors: Marcel Boncoeur, Frederic Valin
  • Patent number: 5085828
    Abstract: A rare earth-containing powder is pressed into a compact at ambient temperatures using a solid lubricant applied only to the die wall and/or a core. The solid lubricant is applied by suspending lubricant powder in a fluorinated hydrocarbon liquid.
    Type: Grant
    Filed: May 15, 1991
    Date of Patent: February 4, 1992
    Assignee: General Motors Corporation
    Inventors: Jon C. Shain, James W. Herchenroeder
  • Patent number: 5080859
    Abstract: A process for hardening sponge refractory metal and making it more susceptible to crushing by the addition of oxygen and/or nitrogen gas to either the reduction stage of the production of the metal from a tetrachloride thereof with magnesium, or to the treatment of a regulus of such metal following vacuum distillation thereof.
    Type: Grant
    Filed: June 1, 1990
    Date of Patent: January 14, 1992
    Assignee: Westinghouse Electric Corp.
    Inventors: Hani A. M. Abodishish, Randall W. Wahlquist
  • Patent number: 5071618
    Abstract: A method of manufacturing dispersion-strengthened material wherein a first material having a metal matrix M and at least one metal X capable of reacting with boron is supplied in a molten state to a mixing region at a first velocity. A second material having a metal matrix M and boron is supplied to the mixing region at a second velocity. The materials impinge on one another to produce a reaction between the metal X and the boron to form a boride in the metal matrix M. The mixture is solidified and pulverized to a powder which is then cleaned and consolidated.
    Type: Grant
    Filed: September 20, 1990
    Date of Patent: December 10, 1991
    Assignee: Sutek Corporation
    Inventors: Luis E. Sanchez-Caldera, Arthur K. Lee, Nam P. Suh, Jung-Hoon Chun
  • Patent number: 5069868
    Abstract: Thermoelectric elements with excellent thermoelectric characteristics such as Seebeck coefficient thermoelectromotive force and thermal conductivity can be produced by molding a powder of metal or metal alloy as the raw material and then sintering; by using as such raw material, ultra fine powders containing Fe and Si as main components and having a mean particle diameter of 50 to 5,000.ANG..
    Type: Grant
    Filed: November 29, 1990
    Date of Patent: December 3, 1991
    Assignee: Idemitsu Petrolchemical Co., Ltd.
    Inventors: Takeo Tokiai, Takashi Uesugi
  • Patent number: 5068071
    Abstract: A process for making a hollow spherical shell of silicate glass composition in which an aqueous suspension of silicate glass particles and an immiscible liquid blowing agent is placed within the hollow spherical cavity of a porous mold. The mold is spun to reduce effective gravity to zero and to center the blowing agent, while being heated so as to vaporize the immiscible liquid and urge the water carrier of the aqueous suspension to migrate into the body of the mold, leaving a green shell compact deposited around the mold cavity. The green shell compact is then removed from the cavity, and is sintered for a time and a temperature sufficient to form a silicate glass shell of substantially homogeneous composition and uniform geometry.
    Type: Grant
    Filed: April 25, 1990
    Date of Patent: November 26, 1991
    Assignee: KMS Fusion, Inc.
    Inventor: Thomas P. O'Holleran
  • Patent number: 5061438
    Abstract: The invention is a method for providing an electrically conductive path through a substrate. It is especially useful for electrically connecting together electrically conductive paths (25) on opposite sides of a circuit board (20). The method is characterized by the steps of forming a passage (21) through a substrate (20) that connects to at least one conductive path (25) on each side of the substrate (20), filling the passage (21) with an electrically conductive powder (10), applying pressure with a die (30) to obtain a compacted powder (11) in the passage (21), and then heating the compacted powder (11) to a temperature that increases the conductivity and ductility of the compacted powder (11) and its adhesion to the substrate (20) without adversely affecting the shape or condition of the substrate (20).
    Type: Grant
    Filed: December 30, 1985
    Date of Patent: October 29, 1991
    Assignee: Allied-Signal Inc.
    Inventors: Edwin D. Lillie, Joseph M. Ilardi, Robert P. Kane
  • Patent number: 5047182
    Abstract: A process for forming articles from inorganic sinterable particulates includes providing a well-dispersed, low pressure injectable slurry, freeze-forming the slurry into a desired geometry, and drying the piece so formed by a predominantly sublimative process, to produce a green article that can be conventionally sintered. The vehicle has a volume change on freezing of not more than .+-.10% by volume; to further control the volume change on freezing, an emulsion derived from different vehicles can be tailored. The slurries preferably have a solids content of at least about 35 v/o, a viscosity of preferably not more than about 1000 cP at 100 s.sup.-1, and are preferably injectable at not more than about 1000 psi, usually at less than 100 psi.
    Type: Grant
    Filed: March 7, 1991
    Date of Patent: September 10, 1991
    Assignee: Ceramics Process Systems Corporation
    Inventors: Cathryn A. Sundback, Bruce E. Novich, Angelica E. Karas, Richard W. Adams
  • Patent number: 5047181
    Abstract: Dense, flaw free, complex, 3-dimensional, metal or refractory shapes are formed by preparing a low viscosity, pourable aqueous-based suspension. The aqueous suspension preferably contains ceramic or metal particulates, water, and a compatible mixture of additives for performing dispersant, cryoprotectant, and strength enhancing functions. The low viscosity slip is cast or injection molded at low pressure into a complex mold, frozen, demolded, and freeze dried without the formation of a continuous liquid phase. The green part is subsequently sintered by conventional techniques to achieve a dense part.
    Type: Grant
    Filed: February 25, 1991
    Date of Patent: September 10, 1991
    Assignee: Ceramics Process Systems Corporation
    Inventors: Mark A. Occhionero, Bruce E. Novich, Cathryn A. Sundback
  • Patent number: 5045277
    Abstract: A method for producing metal carbide grade powders which comprises forming a wax mixture consisting essentially of in percent by weight about 5 to about 15 paraffin oil, with the balance being an esterified wax and paraffin, heating the wax mixture to a temperature above the melting point to melt the wax mixture and maintain it in the molten state, forming a powder-wax mixture consisting essentially of metal carbide powder, a binder metal, and the wax mixture while heating to a temperature above the melting point of the wax mixture to maintain the wax mixture in the molten state to result in a uniform distribution of the wax mixture on the carbide and binder metal particles, forming a slurry of the powder-wax mixture and water, attritor milling the slurry at a temperature below the melting point of the wax mixture, and removing water and agglomerating to produce metal carbide grade powder wherein a densified article made therefrom exhibits less linear shrinkage than articles made from carbide grade powder abs
    Type: Grant
    Filed: September 10, 1990
    Date of Patent: September 3, 1991
    Assignee: GTE Products Corporation
    Inventors: Joseph J. Penkunas, Theodore E. Smith, Jr.
  • Patent number: 5043123
    Abstract: The present invention relates to a method and apparatus for the manufacture of finished parts by the sintering of compacts which are formed as composite moldings of a pulverulent base material and at least one other pulverulent material, particularly different metal powders. The compacts are produced in the manner that at least one of the powder materials is introduced in pourable condition directly alongside of an already pre-compacted part of the compact into the mold which has a shell-shaped matrix and the powder materials are subjected together to final compacting by plug forces acting from on top and on bottom to the size desired for the sintering.
    Type: Grant
    Filed: May 24, 1990
    Date of Patent: August 27, 1991
    Assignee: Mannesmann Aktiengesellschaft
    Inventors: Theodor Gormanns, Siegfried Radewahn, Walter Solty
  • Patent number: 5035847
    Abstract: A mold for slip casting comprising a compact formed out of a mixture having an organic matter and powders, the organic matter being capable of being extracted by supercritical fluid and the powders being incapable of being extracted by the supercritical fluid, and furthermore, a method for slip casting comprising a compact formed out of an organic matter capable of being extracted by supercritical fluid and having a melting point of 0.degree. to 150.degree. C. The organic matter is any one selected from the group of methyl carbonate, t-butyle alcohol, stearic acid stearyl alcohol and paraffin.
    Type: Grant
    Filed: February 5, 1991
    Date of Patent: July 30, 1991
    Assignee: Nippon Kokan Kabushiki Kaisha
    Inventors: Hiroaki Nishio, Takeshi Kawashima
  • Patent number: 5035845
    Abstract: This invention relates to compacts obtained from nonmetallic and metallic powders by die pressing. In particular, it describes an improved method of manufacturing parts from powders where the properties of powders and green compacts can be readily controlled and modified to obtain final products according to desired specifications and dimensions. Introduction of an uniform procedure for determination of powder and green compact properties: slide coefficient, compactibility coefficient and cohesiveness, by a simple compaction test allows to optimize the selection of binders, plasticizers, lubricating substances and the methods of powder preparation prior to pressing operation. With the powder properties known, the pressing parameters can be precisely established and an optimum material and surface treatment for the compacting die can be chosen. With the value of cohesiveness given by the test, the process can be designed to eliminate mechanical defects in compacts such as cracks and laminations.
    Type: Grant
    Filed: March 1, 1990
    Date of Patent: July 30, 1991
    Assignee: KZK Powder Technologies Corporation
    Inventor: Slawomir Gasiorek
  • Patent number: 5032352
    Abstract: The method of consolidating a powder material to form a composite part includes forming a pattern which is a scaled-up version of the part to be formed; employing the pattern to produce a flexible mold with interior conformation matching the pattern exterior; introducing a previously formed shape, insert or body into the mold; introducing consolidatable powder material into the mold; compacting the mold to thereby compress the powder and previously formed shape into a preform which is to be consolidated; separating the preform from the mold; providing a bed of pressure transmission particles, and positioning the preform in the bed; and compacting the preform in the bed of particles by transmission of pressure to the preform via the bed, to thereby consolidate the preform into a dense, desired shape part.
    Type: Grant
    Filed: September 21, 1990
    Date of Patent: July 16, 1991
    Assignee: Ceracon, Inc.
    Inventors: Henry S. Meeks, Stephen P. Swinney
  • Patent number: 5028363
    Abstract: A method of casting a powdered material. A slurry is formed by dispersing metal powder or ceramic powder into a dispersing medium mainly consisting of a substance extractable by a liquid or supercritical carbon dioxide and having a melting point between 0.degree. C. and 100.degree. C., and the slurry is poured into a liquid non-absorbing mold where the slurry is cooled to freeze and solidify into a molding. The main constituent of the dispersing medium in the molding is extracted and removed by the liquid or supercritical carbon dioxide.
    Type: Grant
    Filed: January 16, 1990
    Date of Patent: July 2, 1991
    Assignee: NKK Corporation
    Inventors: Hiroaki Nishio, Takeshi Kawashima, Yoshio Takagi
  • Patent number: 5026518
    Abstract: The invention relates to a method of making permanent magnets, especially rare-earth ion permanent magnets composed of compacted Fe-B-R type alloy particles. Accordingly, the method provides compacting the magnetic particles into a desired shape having voids between some of the compacted particles. The voids between the particles are filled with a sealing agent and the compact is further coated with either an organic coating or metallic coating.
    Type: Grant
    Filed: June 22, 1989
    Date of Patent: June 25, 1991
    Assignee: Seiko Instruments Inc.
    Inventors: Teruo Suzuki, Matsuo Kishi, Katsuyoshi Muraishi, Kenichi Ogawa, Hiroshi Takashio
  • Patent number: 5024811
    Abstract: Precision compacts are produced from powdered material in a mold having at least one top plug and at least one bottom plug between which plugs the powdered material is compressed. The course of the pressing force of at least one of the plugs is detected as a function of the path of its travel during compression, and compared with a predetermined path-dependent tolerance range of the pressing force. Upon exceeding such tolerance range, the final pressing position of the plug in question is changed in such a manner that the height of the compact in such final pressing position is reduced by an amount corresponding to the increased springing back of the compact upon its removal from the mold that results from the greater final pressing force.
    Type: Grant
    Filed: June 15, 1990
    Date of Patent: June 18, 1991
    Assignee: Mannesmann Aktiengesllschaft
    Inventors: Gerd Hinzmann, Norbert Nies, Siegfried Radewahn
  • Patent number: 5022918
    Abstract: A heat-resistant aluminum alloy sinter comprises 5 to 12% by weight of Cr, less than 10% by weight of at least one selected from the group consisting of Co, Ni, Mn, Zr, V, Ce, Fe, Ti, Mo, La, Nb, Y and Hf, and the balance of Al containing unavoidable impurities. A silicon carbide fiber is included for reinforcing the sinter in a fiber volume fraction range of 2 to 30%.
    Type: Grant
    Filed: December 1, 1988
    Date of Patent: June 11, 1991
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventors: Seiichi Koike, Hiroyuki Horimura, Masao Ichikawa, Noriaki Matsumoto
  • Patent number: 5004580
    Abstract: A method and apparatus for packing a permanent magnet powder wherein a solenoid coil is provided near the opening of a cylindrical molding space of a mold in such a manner that the direction of the central axis of the solenoid coil substantially coincides with the central axis of the molding space, and an alternating current magnetic field is applied, so that a permanent magnet powder above the opening is packed into the molding space. A magnetic pole may be provided in the center of the solenoid coil. The method of the present invention can be applied to not only a powder for a sintered magnet but also a powder for a bonded magnet.
    Type: Grant
    Filed: April 13, 1990
    Date of Patent: April 2, 1991
    Assignee: Fuji Electrochemical Co. Ltd.
    Inventors: Yoshio Matsuo, Hirofumi Nakano, Masakuni Kamiya, Kezuo Matsui
  • Patent number: 4999156
    Abstract: Apparatus and methods for compressing a mass utilizing a plurality of interfitting anvils mounted for movement relative to one another along co-planar paths and include faces which, when the anvils are operatively moved relative to one another, exert compression on a mass positioned between the faces in at least two directions in a plane simultaneously. The faces of the apparatus can be so shaped that the cross section of the mass being compressed is urged toward a shape other than that of a regular polygon. Methods of the invention include the consolidation of a mass of compactable material enclosed within a hollow tube having deformable walls, the extraction of juice or oil from fruit or seeds and the internal fracturing of solids so as to swell materials such as solid rocket propellants.
    Type: Grant
    Filed: March 1, 1990
    Date of Patent: March 12, 1991
    Assignee: University of Tennessee Research Corporation
    Inventor: Kenneth H. G. Ashbee
  • Patent number: 4999157
    Abstract: A method for molding powders comprises the steps of forming a mold support having at least an opening and a cavity, forming a film of latex on inner surfaces of the mold support by pouring the latex from the opening into the cavity of the mold support and discharging a substantial portion of the latex poured into the cavity, forming a thin-wall resilient mold inside the mold support by drying the film of latex formed, charging powders as materials for a compact from the opening into the thin-wall resilient mold, exhausting air out of the thin-wall resilient mold filled up with the powders through the opening and sealing the opening of the thin-wall resilient mold, separating the thin-wall resilient mold filled up with the powders from the mold support, and subjecting the thin-wall resilient mold to a cold isostatic press method treatment.
    Type: Grant
    Filed: March 5, 1990
    Date of Patent: March 12, 1991
    Assignee: NKK Corporation
    Inventors: Hiroaki Nishio, Akira Kato, Sazo Nakamura
  • Patent number: 4996014
    Abstract: The invention concerns a method for the manufacture of a rivet for a fixed spike or for a sleeve-mounted spike, respectively, by pressing in a mold. In the method of the invention, the cavity space in the mold (10,20), corresponding to the shape of the spike to be manufactured, is first filled to the desired extent with a first material (1) to form the body part of the spike. Thereupon a first punch (30), whose diameter is substantially smaller than the diameter of the cavity space in the mold, is fitted into the cavity space concentrically with the cavity space, and the annular space between said first punch (30) and the cavity space is filled with a second material (20) so as to form the wear-resistant surface layer for the spike. Next, the first punch (30) is removed, and the space remaining after said punch is filled with a third material. Ultimately the spike is pressed to the desired shape and density, whereinafter the spike is removed from the mold.
    Type: Grant
    Filed: April 12, 1990
    Date of Patent: February 26, 1991
    Assignee: Neste Oy
    Inventor: Erkki Suvanto
  • Patent number: 4994398
    Abstract: An assistant combustion agent for use in a high-frequency combustion furnace is characterized by a blending together of tungsten powder and tin powder. The blended mixture is then molded into a form and a plurality of the molded forms are added to a sample in the furnace. The ratio of tungsten powder to tin powder is between about 80:20 to 60:40.
    Type: Grant
    Filed: February 18, 1988
    Date of Patent: February 19, 1991
    Assignee: Horiba, Ltd.
    Inventors: Takeshi Yamada, Mitsuhiko Chishiro, Katsuya Tsuji
  • Patent number: 4985072
    Abstract: The polycrystalline magnetic substance for magnetic refrigeration in or gas refrigeration accordance with the present invention comprises a plurality of magnetic alloy fine crystalline powders that include at least one kind of rare-earth element selected from the group of Y, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, and Yb, with the remainder metal consisting substantially of 2 kinds selected from Al, Ni, Co, and Fe, and a metallic binder which forms a compact together with the fine crystalline particles, where the abundance ratio of the metallic binder in the compact is 1 to 80% by volume.
    Type: Grant
    Filed: September 22, 1988
    Date of Patent: January 15, 1991
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Masashi Sahashi, Hiromi Niu, Koichiro Inomata
  • Patent number: 4976917
    Abstract: Quench-solidifed Al-Si alloy powder which contains more than 12 wt % Si is preformed, and the preforming is compression-molded into an aluminum alloy part. The aluminum alloy part is repeatedly subjected to a heating-and-cooling cycle of heating the aluminum alloy part to a temperature between 440.degree. C. and 500.degree. C. and cooling it to a temperature not higher than 380.degree. C.
    Type: Grant
    Filed: May 2, 1990
    Date of Patent: December 11, 1990
    Assignee: Mazda Motor Corporation
    Inventor: Makoto Fujita
  • Patent number: 4968481
    Abstract: Ingot-derived and sodium-reduced agglomerated tantalum powders having improved flow characteristics and lead pull-out strength that find particular utility in manufacture of anodes for capacitors. Powder size distribution is in the range of -60 to +400 mesh, preferably -60 to +250 mesh, containing less than 5 wt % powder above the upper and below the lower range limits.
    Type: Grant
    Filed: September 28, 1989
    Date of Patent: November 6, 1990
    Assignee: V Tech Corporation
    Inventor: Carlos F. Rerat
  • Patent number: 4950327
    Abstract: A creep-resistant alloy having a tiered structural arrangement of one or several refractory metals Mo, W, Nb, Ta, V, Cr containing certain doping agents, as well as a process for producing the same. The special doping agents are compounds and/or mixed phases of such compounds selected from the group of oxides, nitrides, carbides, borides, silicates or aluminates having a melting point higher than 1500.degree. C. The size of their grains is .ltoreq.1.5 .mu.m, their proportion in the alloy is comprised between 0.005 and 10% by weight. Unlike in the known state of the art, the use of porassium as doping agent is avoided in this alloy. A good reproducible consolidation and in particular high densities during sintering can thus be obtained. Furthermore, this alloy has better ambient temperature, heat and creep resistance properties than known alloys of refractory metal with a tiered structual arrangement.
    Type: Grant
    Filed: September 27, 1988
    Date of Patent: August 21, 1990
    Assignee: Schwarzkopf Development Corporation
    Inventors: Ralf Eck, Gerhard Leichtfried
  • Patent number: 4943319
    Abstract: Disclosed is herein a process for producing a molding product of Al or Cu composite material, which comprises admixing a functional material capable of improving the desired property of the composite material by dispersion into a matrix to a powder of metal selected from Al, Cu or alloys thereof constituting the matrix, charging the dust directly into a molding die, applying cold dust core molding under the pressure of greater than 5 t/cm.sup.2 of facial pressure and applying a diffusing treatment at a temperature higher than 300.degree. C.
    Type: Grant
    Filed: December 30, 1988
    Date of Patent: July 24, 1990
    Assignee: Kabushiki Kaisha Kobe Seiko Sho
    Inventors: Masahiro Yanagawa, Mutsumi Abe, Kenichi Aota, Takashi Motoda
  • Patent number: 4940563
    Abstract: An article is molded by contacting it with a solid polymer medium, such as an especially low strength unfilled silicone rubber which is solid and able to flow readily. Thermal expansion of the medium or mechanical force is used to create molding pressure and thereby provides a substantially uniform pressure on the article precursor. Various temperature and pressure cycles can be attained; constant high pressures can be maintained on the article precursor during cooldown, optionally aided by flowing of medium to and from a vessel in which the article precursor is being molded. The method is particularly adapted to molding filler or fiber reinforced thermosetting polymer composite articles.
    Type: Grant
    Filed: May 26, 1988
    Date of Patent: July 10, 1990
    Assignee: United Technologies Corporation
    Inventor: Robert V. Kromrey
  • Patent number: RE33243
    Abstract: The invention relates to a process for the treatment of a metal oxide powder, particularly a UO.sub.2 or PuO.sub.2 powder, with a view to its fritting.This process consists of oxidizing the powder, so as to form on its surface a hydrated oxide layer of the same metal. When the oxide is UO.sub.2 or PuO.sub.2 and mixtures thereof, as well as those prepared with ThO.sub.2, the treated powder can be used for producing nuclear fuel pellets by cold compression, followed by fritting.
    Type: Grant
    Filed: January 13, 1989
    Date of Patent: June 26, 1990
    Assignee: Commissariat a l'Energie Atomique
    Inventors: Camille Braun, Joel Danroc, Bernard Francois, Jean Michel