Consolidation Of Powders Patents (Class 419/66)
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Patent number: 4927461Abstract: The machinability characteristics of P/M ferrous sintered compacts are improved when the compact is prepared from a ferrous powder having a maximum particle size less than about 300 microns, and from at least about 0.01 weight percent of a boron nitride powder comprising agglomerates of irregular-shaped, submicron particles.Type: GrantFiled: November 2, 1988Date of Patent: May 22, 1990Assignee: Quebec Metal Powders, Ltd.Inventors: Cavit Ciloglu, Martin Gagne, Edy Laraque, Joel Poirier, Sylvain Tremblay, Yves Trudel
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Patent number: 4925501Abstract: This invention relates to a method of making large, fully dense compacts of substantially amorphous to very finely crystalline rare earth alloys using explosive compaction and hot working.Type: GrantFiled: March 3, 1988Date of Patent: May 15, 1990Assignee: General Motors CorporationInventor: Elizabeth F. Harasek
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Patent number: 4909840Abstract: A process for the production of a secondary powder composition having a nanocrystalline structure and being comprised of binary or quasi-binary substances composed of at least one of the elements Y, Ti, Zr, Hf, Nb, Mo, Ta and W and at least one of the elements V, Cr, Mn, Fe, Co, Ni, Cu and Pd, optionally also containing further ingredients, such as Si, Ge, B and/or oxides, nitrides, borides, carbides, and their possible mixed crystals. The components are in powdered form and are mixed in elementary form or as pre-alloys and have particle sizes ranging from 2 to 250 .mu.m. The powder components are subjected to high mechanical forces in order to produce secondary powders having a nanocrystalline structure. The secondary powders obtained in this way can be processed into molded bodies according to known compression molding processes, but at a temperature below the recrystallization temperature.Type: GrantFiled: April 7, 1988Date of Patent: March 20, 1990Assignee: Fried. Krupp Gesellschaft mit beschrankter HaftungInventor: Wolfgang Schlump
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Patent number: 4907731Abstract: Shock wave formation of thin layers of materials with improved superconducting and permanent magnetic properties and improved microstructures.The material fabrication system includes a sandwiched structure including a powder material placed between two solid members to enable explosive shock consolidation. The two solid members are precooled to about 80.degree.-100.degree. K. to reduce the residual temperatures attained as a result of the shock wave treatment, and thereby increase the quench rate of the consolidated powder.Type: GrantFiled: October 14, 1987Date of Patent: March 13, 1990Assignee: The United States of America as represented by the United States Department of EnergyInventors: William J. Nellis, Theodore H. Geballe, M. Brian Maple
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Patent number: 4906294Abstract: A cutting bit (1) has a bottom side (2), flanks (3) that are inclined at a positive clearance angle (.alpha.) with respect to the bottom side (2), and a top side (7). The top side (7) has cutting edges (5 and 5') which are inclined with respect to one another at an angle of inclination (.lambda.). The cutting bit is made by sintering a blank which is formed using a pressing tool (10). The pressing tool includes a mold member (11), an upper die (12), and a lower die (13). The upper die (12) has a pressure face (20) which corresponds precisely, except for an allowance for the shrinkage ratio of the sinter material, to the actual surface of the upper side of the cutting bit (1). When the upper die (12) is fully inserted into the mold (11), a free space (31) exists between the upper die (12) and the mold member (11), the free space being disposed above the delimiting line (21) of pressure face (20) of the upper die (12).Type: GrantFiled: April 21, 1988Date of Patent: March 6, 1990Assignee: Fried. Krupp Gesellschaft mit beschrankter HaftungInventors: Rainer von Haas, Helmut Morbitzer, Jose A. Paya
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Patent number: 4902471Abstract: A method is disclosed for producing metal carbide grade powders, which comprises forming a wax mixture consisting essentially of in percent by weight about 10 to 60 of an organic compound additive which is a solid at room temperature and contains a C.dbd.Type: GrantFiled: September 11, 1989Date of Patent: February 20, 1990Assignee: GTE Products CorporationInventors: Joseph J. Penkunas, Theodore E. Smith, Jr.
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Patent number: 4894086Abstract: A method of producing dispersion hardened metal alloys which incorporate highly reactive metals or their alloys whose oxides are not adapted to be easily reduced. According to the method, the highly reactive metals of their alloys are added as powder particles to a solution of a salt of a reducible metal which is to form a metallic matrix in which the reactive metals or their alloys are to be integrated, after which the solution is atomized to form particles from which the solvent is removed to yield the final product of the metal matrix with the highly reactive metals or their alloys integrated therein as a second phase.Type: GrantFiled: May 6, 1988Date of Patent: January 16, 1990Assignee: MTU- Motoren-und Turbinen-Union Munchen GmbHInventors: Werner Huether, Wolfgang Betz, Gerhard Andrees
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Patent number: 4889582Abstract: A stable age hardenable aluminum alloy which has useful mechanical properties at temperatures up to at least 900.degree. F. (482.degree. C.). The alloy contains 5-15% iron, 1-5% molybdenum and 0.2-6% vanadium with balance aluminum and is processed by rapid solidification from the melt to form a particulate which is consolidated to form a bulk article.Type: GrantFiled: October 27, 1986Date of Patent: December 26, 1989Assignee: United Technologies CorporationInventors: James W. Simon, Jr., Kathleen Gorman
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Patent number: 4883621Abstract: In a method for forming a cast article by slip casting through casting of a slip of powders of ceramics, etc. as disporsed in a solvent such as water, etc. into a solvent-absorbable, porous casting mold of gypsum, etc., the casting mold as made is heated to considerably lower the strength of the casting mold in a shape-maintainable range, the slip is cast into the cavity of the casting mold and after solidification of the slip into a green body the casting mold is removed to obtain a defect-free green body. The casting mold can be removed with much ease.Type: GrantFiled: July 9, 1986Date of Patent: November 28, 1989Assignee: Hitachi, Ltd.Inventors: Tatsuo Natori, Takashi Shimaguchi, Akihide Watanabe, Toshihiro Yamada
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Patent number: 4880598Abstract: A tubular compact (14) obtained by compacting a powder is applied with one circumferential surface (16) at a minimum distance required for said application, from an abutment surface (15) corresponding to said one circumferential surface (16). The space between said one circumferential surface (16) and the abutment surface (15) is evacuated, such that the compact (14), while undergoing a certain deformation to bridge said space, is sucked against the abutment surface (15) so as to be firmly retained against it.Type: GrantFiled: December 15, 1988Date of Patent: November 14, 1989Assignee: Cips KBInventors: Flemming Hansen Kaad, Ola Pettersson
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Patent number: 4879095Abstract: A rapidly solidified aluminum-base alloy consists essentially of the formula Al.sub.bal Fe.sub.a Si.sub.b V.sub.c, wherein "a" ranges from 3.0 to 7.1 atom percent, "b" ranges from 1.0 to 3.0 atom percent, "c" ranges from 0.25 to 1.25 atom percent and the balance is aluminum plus incidental impurities, with the provisos that (i) the ratio (Fe+V): Si ranges from about 2.33:1 to 3:33:1 and (ii) the ratio Fe:V ranges from 11.5:1 to 5:1. The alloy exhibits high strength, ductility and fracture toughness and is especially suited for use in high temperature structural applications such as gas turbine engines, missiles, airframes and landing wheels.Type: GrantFiled: April 17, 1987Date of Patent: November 7, 1989Assignee: Allied-Signal Inc.Inventors: Colin M. Adam, Richard L. Bye, Santosh K. Das, David J. Skinner
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Patent number: 4878967Abstract: A rapidly solidified aluminum-base alloy consists essentially of the formula Al.sub.bal Fe.sub.a Si.sub.b X.sub.c wherein X is at least one element selected from the group consisting of Mn,V,Cr,Mo,W,Nb,Ta, "a" ranges from 2.0 to 7.5 atom percent, "b" ranges from 0.5 to 3.0 atom percent, "c" ranges from 0.05 to 3.5 atom percent and the balance is aluminum plus incidental impurities, with the proviso that the ratio {Fe+X}:Si ranges from about 2.0:1 to 5.0:1. The alloy exhibits high strength, ductility and fracture toughness and is especially suited for use in high temperature structural applications such as gas turbine engines, missiles, airframes and landing wheels.Type: GrantFiled: September 8, 1987Date of Patent: November 7, 1989Assignee: Allied-Signal Inc.Inventors: Colin M. Adam, Richard L. Bye, Santosh K. Das, David J. Skinner
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Patent number: 4871497Abstract: In a casting method comprising casting a slip containing water or an organic solvent as the medium into a mold and removing the mold after solidification of the slip, use of a mold formed with an organic binder soluble in the medium of the slip allows the slip to quickly solidify and afford a green body due to absorption of the medium in the slip by the mold. In this case, the mold softens with loss of the binding power thereof simultaneously with the absorption of the medium. Therefore, no cracks appear at all in the green body, and removal of the mold is very easy.Type: GrantFiled: February 10, 1986Date of Patent: October 3, 1989Assignee: Hitachi, Ltd.Inventors: Tatsuo Natori, Takashi Shimaguchi, Akihide Watanabe, Toshihiro Yamada
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Patent number: 4867806Abstract: Al-alloy containing Si, Fe, Cu and Mg and at least one kind of Mn and Co in the basic composition range of 8.0.ltoreq.Si.ltoreq.30.0 wt. %, 2.0.ltoreq.Fe.ltoreq.33.0 wt. %, 0.8.ltoreq.Cu.ltoreq.7.5 wt. %, 0.3.ltoreq.Mg.ltoreq.3.5 wt. %, 0.5.ltoreq.Mn.ltoreq.5.0 wt. % and 0.5.ltoreq.Co.ltoreq.3.0 wt. %, are provided in a powder state. A sindered member formed of these Al-alloys has a high strength and reveals excellent heat-resistivity and stress corrosion cracking resistivity. A structural member made of the sintered all-alloy is manufactured through the steps of subjecting a powder press-shaped body formed at a temperature of 350.degree. C. or lower and at a pressure of 1.5.about.5.0 ton/cm.sup.2 to hot extrusion working at a temperature of 300.degree..about.400.degree. C. to form a raw material for forging, and then forge shaping the raw material at a temperature of 300.degree..about.495.degree. C.Type: GrantFiled: May 31, 1988Date of Patent: September 19, 1989Assignee: Honda Giken Kogyo Kabushiki KaishaInventor: Haruo Shiina
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Die-upset manufacture to produce high volume fractions of RE-Fe-B type magnetically aligned material
Patent number: 4859410Abstract: A method to increase the volume fraction of magnetically aligned material in rare earth (RE), iron, boron type anisotropic permanently magnetic material includes forming an adaptively shaped fully dense substantially magnetically isotropic preform from relatively coarse powder particles of melt spun alloy with a very fine grain Re.sub.2 Fe.sub.14 B phase. The preform is heated and die upset to provide uniformity of strain in the perform as it is conformed to the die thereby to cause an increased percentage of the crystallites to be oriented along a crystallographically preferred magnetic axis which increases the energy product of a resultant magnet.Type: GrantFiled: March 24, 1988Date of Patent: August 22, 1989Assignee: General Motors CorporationInventors: Earl G. Brewer, Robert W. Lee -
Patent number: 4859238Abstract: Electrical contacts are formed from a silver-iron material which contains 3 to 30% by weight of iron and one or more of the components manganese, copper, zinc, antimony, bismuth oxide, molybdenum oxide, tungsten oxide or chromium nitride in amount totalling 0.05 to 5 weight percent, the balance being silver. These materials are suitable for forming electrical contacts of a wide variety. Tantalum is an optional component which may also be utilized particularly when 0.2 percent to 2 percent zinc is present.Type: GrantFiled: June 3, 1988Date of Patent: August 22, 1989Assignee: Degussa AktiengesellschaftInventors: Wolfgang Weise, Roger Wolmer, Peter Braumann
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Patent number: 4859411Abstract: A process for controlling fractionation in selenium alloys comprising providing pellets of an alloy comprising amorphous selenium and an alloying component selected from the group consisting of tellurium, arsenic, and mixtures thereof, the particles having an average particle size between about 300 micrometers and about 3,000 micrometers, exposing the pellets to an ambient temperature of between about 114.degree. C. and about 190.degree. C. until an exotherm occurs in the pellets resulting in substantially complete crystallization between about 104.degree. C. and about 180.degree. C., grinding the pellets into fresh powder having an average particle size of less than about 200 micrometers, and compressing the fresh powder into fresh pellets having an average weight between about 50 mg and about 1000 mg. The resulting fresh pellets may be heated in a vacuum chamber to vacuum deposit the alloy onto a substrate.Type: GrantFiled: April 8, 1988Date of Patent: August 22, 1989Assignee: Xerox CorporationInventors: Gerald H. Sweatman, Roy Hodgson, Robert H. Haste
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Patent number: 4857266Abstract: A composition of matter comprised of copper and particles which are dispersed throughout the copper, where the particles are comprised of copper oxide and copper having a coating of copper oxide, and a method for making this composition of matter.Type: GrantFiled: December 5, 1988Date of Patent: August 15, 1989Assignee: The United States of America as represented by the United States Department of EnergyInventors: Haskell Sheinberg, Thomas T. Meek, Rodger D. Blake
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Patent number: 4853180Abstract: A die assembly having a cavity in which powdered metal is compressed with upper and lower punches. A core extends through the lower punch to form the inner wall of a bushing, and a core extension rod having a lateral protrusion that extends into the cavity to form a groove in the upper portion of the bushing. The core and the core extension rod move in concert between positions to receive powder, compress it and moves upward to afford expelling the finishing bushing. One stationary protrusion extends from the die into the cavity to form a groove in the powdered metal along the full length of the completed bushing. Air passage means are used to direct air into the cavity to remove residue powder that may eventually build-up and cause inaccuracies. Also, in the preferred embodiment a powder feeder means is used on a die table to reciprocate between a retracted, inactive position and an extended position to deposit powdered metal into the cavity and later to bump a finished bushing across the table.Type: GrantFiled: September 15, 1988Date of Patent: August 1, 1989Assignee: Martin Sprocket & Gear, Inc.Inventor: Billy G. Howard
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Patent number: 4851190Abstract: The disclosure relates to a turbine disk and a method of making the turbine disk comprising the steps of rotating a mold, adding a first powdered metal to the rotating mold at a first rate, reducing the rate of addition of the first metal to a second rate, and adding a second powdered metal to the mold at a third rate substantially equal to the difference between the first and second rates.Type: GrantFiled: July 27, 1987Date of Patent: July 25, 1989Assignee: Williams International CorporationInventors: Kim E. Bowen, Steven M. Foster, Said Izadi
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Patent number: 4834941Abstract: An Al-alloy containing Si, Fe, Cu and Mg and at least one of Mn and Co in the basic composition range of 8.0.ltoreq.Si.ltoreq.30.0 wt. %, 2.0.ltoreq.Fe.ltoreq.33.0 wt. %, 0.8.ltoreq.Cu.ltoreq.7.5 wt. %, 0.3.ltoreq.Mg.ltoreq.3.5 wt. %, 0.5.ltoreq.Mn.ltoreq.5.0 wt. % and/or 0.5.ltoreq.Co.ltoreq.3.0 wt. %, provided in a powder state. A sindered member formed of these Al-alloys displays high strength, excellent heat-resistivity and stress corrosion cracking resistivity. A structural member made of the sintered Al-alloy is manufactured through the steps of subjecting a powder press-shaped body formed at a temperature of 350.degree. C. or lower and at a pressure of 1,5.about.5.0 ton/cm to hot extrusion working at a temperature of 300.degree..about.400.degree. C. to form a raw material for forging, and then forge shaping the raw material at a temperature of 300.degree..about.495.degree. C.Type: GrantFiled: February 1, 1988Date of Patent: May 30, 1989Assignee: Honda Giken Kogyo Kabushiki KaishaInventor: Haruo Shiina
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Patent number: 4834940Abstract: Tooling and a method are provided for producing powder metal compacts in which a fine hole is provided through the compact without the need for secondary operations. A top punch and bottom punch are used in an opposing relationship and a stem is provided on the top punch to form the hole through the compact. A resilient member is placed upon the bottom punch opposite the stem. When powder metal is introduced into the die cavity of the press, the powder is compressed by pressing the first punch against the second punch. During this powder compaction process, the stem of the first punch will press through the powder until it engages and penetrates the resilient member. When the first punch and second punch are released, a powder metal compact is formed having a hole provided the entire length therethrough. Such a powder metal compact is especially designed for use as a wire-drawing die.Type: GrantFiled: August 3, 1988Date of Patent: May 30, 1989Assignee: Newcomer Products, Inc.Inventor: Jack Krall
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Patent number: 4834939Abstract: A silver base electrical contact material is described which contains a dispersion of particles consisting of cadmium oxide and nickel. The nickel particles are surrounded by a continuous adherent coating of nickel oxide which eliminates the detrimental reaction which would otherwise occur between nickel and cadmium oxide. The invention contact materials have improved lives and are fabricated by any one of several different powder metallurgy techniques.Type: GrantFiled: May 2, 1988Date of Patent: May 30, 1989Assignee: Hamilton Standard Controls, Inc.Inventor: Norman S. Bornstein
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Patent number: 4834942Abstract: An aluminum-titanium alloy and a process of making it, the alloy consisting ssentially of aluminum, 4-6 wt. % titanium, 1-2 wt. % carbon, and 0.1-0.2 wt % oxygen. The alloy is an aluminum matrix supersaturated with titanium, and having throughout a fine, homogeneous dispersion of Al.sub.3 Ti particles. It is fine grained and has grain boundary dispersoids of carbides and oxides, predominantly of aluminum. An aluminum-titanium melt is rapidly solidified and then mechanically alloyed in the presence of a carbon-bearing agent. The resulting powder is degassed and hot consolidated to form articles which exhibit high strength, ductility, and creep resistance at temperatures greater than 200.degree. C.Type: GrantFiled: January 29, 1988Date of Patent: May 30, 1989Assignee: The United States of America as represented by the Secretary of the NavyInventors: William E. Frazier, Michael J. Koczak
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Patent number: 4832741Abstract: A green pressed article of high strength and of low relative density, formed from a heat-resistant aluminum alloy of the Al/Fe/X or Al/Cr/X type, where X is Ti, Ce, Zr, Hf, V, Nb, Cr, Mo or W, is produced by a powder-metallurgical process, wherein an alloy melt is atomized to form fine particles by means of an inert gas jet, with which 0.5 to 2% by volume of oxygen is admixed, and the powder produced in this manner is compacted. Nitrogen, argon or helium can be employed as inert gas. The green pressed article is preferably formed from a small proportion of coarser, non-spherical particles and a greater proportion of finer, spherical particles.Type: GrantFiled: May 6, 1988Date of Patent: May 23, 1989Assignee: BBC Brown Boveri AGInventor: Malcolm J. Couper
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Process for the production of chromium-aluminum balls for adding chromium into molten aluminum baths
Patent number: 4820483Abstract: The present invention relates to a process for the production of chromium-aluminum balls for adding chromium into molten aluminum baths.In order to obtain balls containing x% of chromium and y% of aluminum, where x and y are gravimetric contents corresponding to the following relationships:70.ltoreq.x.ltoreq.8020.ltoreq.y.ltoreq.30x+y=100an alloy of chromium and aluminum containing gravimetric chromium and aluminum contents approximating to x by an excess and to y by a deficit respectively is prepared by melting and this alloy is then finely ground into a crude powder; the chromium and aluminum contents of the alloy or of the crude powder are determined and, if required, an additional amount of finely divided aluminum is added so as to obtain a powder containing x% of chromium and y% of aluminum, the additional amount of finely divided aluminum corresponding to less than 10% by weight of the crude powder; a compacting is then carried out.Type: GrantFiled: December 22, 1987Date of Patent: April 11, 1989Assignee: Delachaux SAInventor: Alain Defrance -
Patent number: 4818283Abstract: A process for producing a dispersion hardened copper alloy includes admixing to a copper melt from 0.3 to 15 weight % of molybdenum to provide a mixture which is a melt; superheating the mixture to a temperature ranging from about 200.degree. C. to about 1000.degree. C. above the melting point of coper to provide a superheated melt; and subjecting the superheated melt to very rapid solidification at a cooling rate ranging from 104.degree. to 106.degree. C./sec. The above process produces dipsersion hardened copper alloy comprising copper and from 1 to 15 weight % of molybdenum which is present in the dispersion hardened copper alloy as particles having a diameter of less than 0.1 .mu.m embedded in the copper matrix. Such dispersion hardened copper alloys are useful for providing electrical conductors which are subjected to elevated temperatures, such as for providing spot welding electrodes, particularly for welding of zinc-galvanized sheet metal.Type: GrantFiled: October 16, 1987Date of Patent: April 4, 1989Assignee: Battelle-Institut e.V.Inventors: Karl-Heinz Grunthaler, Dieter Langbein, Fehmi Nilmen, Heinrich Winter
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Patent number: 4818482Abstract: A method for pickling and consolidating water atomized metallic powders to reduce surface oxides. The technique includes introducing the powder into an acid bath--preferably nitric acid and hydrofluoric acid, rinsing the powder, introducing the powder into an alkaline bath, rinsing the powder and then consolidating the powder into a workpiece. Alternatively, the powder can be additionally introduced into a second acid bath and/or placed into a finishing boric acid bath before consolidation.Type: GrantFiled: July 9, 1987Date of Patent: April 4, 1989Assignee: Inco Alloys International, Inc.Inventors: Jon M. Poole, Lindy J. Curtis
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Patent number: 4808225Abstract: A process for producing an alloy product of improved ductility from metal powder. It includes the steps of: providing metal powder having at least 5 wt. % of one or more reactive elements from the group consisting of titanium, aluminum, hafnium, niobium, tantalum, vanadium and zirconium; consolidating the powder to an essentially fully dense shape; and progressively melting and solidifying localized areas of the consolidated shape so as to produce a product of improved ductility.Type: GrantFiled: January 21, 1988Date of Patent: February 28, 1989Assignee: Special Metals CorporationInventors: Stephen J. Donachie, James W. Fesko, James J. Furgal, Francis E. Sczerzenie
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Patent number: 4799955Abstract: Disclosed is a composite metal powder made from a base iron powder milled with an alloying component such as nickel, copper, managnese, chromium, silicon, phosphorus, boron, vanadium, and molybdenum, where the composite metal powder has a compressibility comparable to the compressibility of the soft base iron powder prior to milling. Such a composite is obtained by using a short mill time followed by an annealing step.Type: GrantFiled: October 6, 1987Date of Patent: January 24, 1989Assignee: Elkem Metals CompanyInventor: Melvin L. McClellan
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Patent number: 4798694Abstract: A molded composite material comprising a plural number of constituents is provided in which at least two of the constituents are distributed with a relative existing ratio varying at least in one direction in the composite material. A process for producing the composite material is also provided.Type: GrantFiled: August 6, 1986Date of Patent: January 17, 1989Assignee: Canon Kabushiki KaishaInventors: Hiroyuki Sugata, Kouhei Nakata, Nobutoshi Mizusawa, Satoshi Yuasa, Masahiro Haruta, Takashi Hamamoto, Kuniji Osabe
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Patent number: 4780274Abstract: A method of manufacturing by a powder metallurgy process a rotary drill bit including a bit body having a plurality of cutting elements mounted on the outer surface thereof comprises the steps of forming a hollow mould for moulding at least a portion of the bit body, packing the mould with powdered matrix material, and infiltrating the material with a metal alloy in a furnace to form a matrix. Before packing the mould with powdered matrix material, there are postioned in spaced locations on the interior surface of the mould a plurality of cutting element, each of which is formed of a material, such as a polycrystalline diamond material, which is thermally stable at the temperature necessary to form the matrix. Also positioned in the mould, adjacent the rearward side of each cutting element, is a support material such that, at least after formation of the matrix, the support material has a higher modulus of elasticity than the matrix.Type: GrantFiled: October 24, 1986Date of Patent: October 25, 1988Assignee: Reed Tool Company, Ltd.Inventor: John D. Barr
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Patent number: 4775598Abstract: A process is described in which hollow spheres or hollow-sphere composites (moldings) having high-strength walls are produced. Additional layers are applied to metallized spherical lightweight particles having a core of foamed polymer. In order to increase the strength of the wall of the spherical particle and the strength of the molding, metallized lightweight spherical particles having a metal wall thickness of 5 to 20 microns are treated (coated) with a dispersion of particulate metal or metal oxide or particulate ceramic or refractory material, the lightweight spherical particles coated in a thickness from 15 to 500 microns are dried, the dried particles are heated to a temperature of about 400.degree. C. to effect a pyrolysis of the polymer core, and the particles are subsequently sintered at a temperature from 900.degree. to 1400.degree. C.Type: GrantFiled: November 25, 1987Date of Patent: October 4, 1988Assignee: Norddeutsche Affinerie AkitiengesellschaftInventor: Manfred Jaeckel
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Patent number: 4770718Abstract: Copper-dendritic composite alloys are prepared for mechanical reduction to increase tensile strength by dispersing molten droplets of the composite alloy into an inert gas; solidifying the droplets in the form of minute spheres or platelets; and compacting a mass of the spheres or platelets into an integrated body. The spheres preferably have diameters of from 50 to 2000 .mu.m, and the platelets thicknesses of 100 to 2000 .mu.m. The resulting spheres or platelets will contain ultra-fine dendrites which produce higher strengths on mechanical reduction of the bodies formed therefrom, or comparable strengths at lower reduction values. The method is applicable to alloys of copper with vanadium, niobium, tantalum, chromium, molybdenum, tungsten, iron and cobalt.Type: GrantFiled: October 23, 1987Date of Patent: September 13, 1988Assignee: Iowa State University Research Foundation, Inc.Inventors: John D. Verhoeven, Edwin D. Gibson, Frederick A. Schmidt, William A. Spitzig
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Patent number: 4770849Abstract: Solid materials are dynamically loaded by impact with a piston (10) fired at the material (11) in a suitable support (12) wherein a "punch", (22) a body of material introducing an impedance mismatch, is inserted between the piston (10) and the material (11).Type: GrantFiled: October 22, 1986Date of Patent: September 13, 1988Assignee: University of QueenslandInventor: Neil W. Page
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Patent number: 4765837Abstract: A pellet or bolus for administration to a ruminant by deposition in its rumeno-reticular sac where it is eroded away by rumen juices and releases active agent(s) and/or components, either continuously or in pulsed doses, comprises or incorporates a magnesium-based alloy which comprises at least 40% of magnesium, at least 30% zinc and up to 20% aluminium and, optionally, copper up to 5%, and trace elements, selected from cobalt, manganese, nickel and selenium up to 1%, the percentages being by weight. A paste can be made by heating the alloy to between its solidus and liquidus points, when it can be admixed with lead shot for weighting the bolus.In the illustrated case, the bolus comprises tubular sheath 14 which contains alloy/iron shot filling 16. However, the alloy can be used for any appropriate component of the bolus.Type: GrantFiled: February 2, 1987Date of Patent: August 23, 1988Inventor: Derek J. Whitehead
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Patent number: 4764212Abstract: This invention relates to a method of manufacturing thermoelectric material which has the steps of quenching a thermoelectric alloy in a molten state at a quenching rate higher than 10.sup.3 .degree. C./sec into a membrane or powdery form and subjecting the membrane or powder to cold-forming or sintering. The thermoelectric alloy is a Bi--Sb series alloy having a composition represented by{(Bi.sub.100-x .multidot.Sb.sub.x).sub.100-y .multidot.E.sup.II.sub.y }.sub.100-z .multidot.E.sup.I.sub.zwhere E.sup.I represents a group III or group IV element, E.sup.II represents a group IV or group VI element, x represents a number of 5-20, y represents an integer of 0-20 and z represents a number of 0.05-10, respectively.Type: GrantFiled: February 19, 1987Date of Patent: August 16, 1988Assignee: Kabushiki Kaisha Komatsu SeisakushoInventor: Takuji Okumura
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Patent number: 4762754Abstract: Shock wave formation of superconductive ceramic oxide electric and magnetic circuit elements with improved microstructures and mechanical properties.Type: GrantFiled: October 23, 1987Date of Patent: August 9, 1988Assignee: The United States of America as represented by the United States Department of EnergyInventors: William J. Nellis, M. Brian Maple, Theodore H. Geballe
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Patent number: 4762678Abstract: The present invention provides a method of producing a bulk amorphous metal alloy article. The method involves mechanically alloying a matrix metal and a fast diffuser element into a powder mixture consisting of particles having a modulated structure and whereby the powder is at least 50% but less than 100% amorphous. The resultant powder mixture is formed into a bulk amorphous metal alloy article by standard forming methods such as cold or hot-pressing. This bulk article can be further processed into a bulk crystalline metal alloy article by heating at a temperature above the glass transition temperature of the amorphous metal alloy article.Type: GrantFiled: November 3, 1987Date of Patent: August 9, 1988Assignee: Allied-Signal Inc.Inventor: Benjamin P. Dolgin
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Patent number: 4761264Abstract: A method for molding powders which comprises introducing a thin-wall resilient mold inside a ventilative mold support, reducing the outside pressure of the ventilative mold support to less than the atmospheric pressure (760 Torr), putting a thin-wall resilient mold exactly close to the inside wall of the ventilative mold support, supplying powder material into the thin-wall resilient mold, exhausting air existing in the voids formed in the powder material, and taking the ventilative mold support apart to apply cold isostatic press treatment to the thin-wall resilient mold. The shape of the thin-wall resilient mold is similar to the shape of the ventilative mold support.Type: GrantFiled: June 12, 1987Date of Patent: August 2, 1988Assignee: Nippon Kokan Kabushiki KaishaInventors: Hiroaki Nishio, Jun Harada
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Patent number: 4759905Abstract: Apparatus is provided for the production of ultrafine powder. The powder is produced by spark erosion within an electric discharge cell. The starting material for production of the powder is a body in chunk form of the material to be pulverized. The material is contained in an electric discharge cell having a fine mesh screen bottom. The cell and its contents are immersed in a dielectric fluid such as water, liquified gas or an organic base liquid. The cell and its contents are vibrated to cause the chunks to separate repeatedly and momentarily. A sparking voltage is impressed repeatedly through the body to develop sparks between confronting portions of separated chunk surfaces. Small particles produced as a result of the sparking fall through the screen of the cell and are collected as product.Type: GrantFiled: April 3, 1987Date of Patent: July 26, 1988Assignee: General Electric CompanyInventors: John L. Walter, Ami E. Berkowitz
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Patent number: 4752335Abstract: A process for forming a metallic sputter target and a metallic sputter target product are provided. The process provides a dense homogenious bulk material of high strength comprising ductile metal components which forms a brittle composition when alloying. The process employs a mixture of individual components at least one of which being ductile at room temperatures. The individual components can be all metals, or a mixture of metals and non-metals. The individual components are formed into a powder mixture in a first step. Unlike hot pressing or other melting techniques which can cause ductile components to alloy into brittle materials, the powder mixture is cold pressed to form a shaped body which is thereafter densified by repeated working at temperatures below the lowest of the melting points of the individual components. This treatment occurs under conditions of material flow and cold welding.Type: GrantFiled: April 30, 1987Date of Patent: June 21, 1988Assignee: Schwarzkopf Development CorporationInventor: Georg Korb
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Patent number: 4743185Abstract: An electrochemical cell comprising a zinc electrode in an electrolyte solution wherein the electrode is formed from a zinc powder compacted to a density of at least about 6.5 g/cc to substantially reduce the corrosion of the zinc electrode and the consequent evolution of hydrogen gas without resorting to the addition of mercury to the electrode.Type: GrantFiled: February 27, 1987Date of Patent: May 10, 1988Assignee: Sab Nife Inc.Inventors: Viet Vu, Paul F. Hettwer
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Patent number: 4743317Abstract: The invention provides an aluminum based alloy consisting essentially of the formula Al.sub.bal Fe.sub.a X.sub.b, wherein X is at least one element selected from the group consisting of Zn, Co, Ni, Cr, Mo, V, Zr, Ti, Y, Si and Ce, "a" ranges from about 7-15 wt %, "b" ranges from about 1.5-10 wt % and the balance is aluminum. The alloy has a predominately microeutectic microstructure.The invention also provides a method and apparatus for forming rapidly solidified metal, such as the metal alloys of the invention, within an ambient atmosphere. Generally stated, the apparatus includes a moving casting surface which has a quenching region for solidifying molten metal thereon. A reservoir holds molten metal and has orifice means for depositing a stream of molten metal onto the casting surface quenching region. A heating mechanism heats the molten metal contained within the reservoir, and a gas source provides a non-reactive gas atmosphere at the quenching region to minimize oxidation of the deposited metal.Type: GrantFiled: July 19, 1984Date of Patent: May 10, 1988Assignee: Allied CorporationInventors: David J. Skinner, Paul A. Chipko, Kenji Okazaki
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Patent number: 4734253Abstract: A sintered magnet of Fe-B-rare earth alloy having an axis of easy magnetization oriented at an angle to a major axis can be directly produced from the alloy material by (a) press molding the material in an applied magnetic field into a compact of the dimensions determined by taking into account factors of shrinkage expected in X, Y and Z directions, and (b) sintering the compact.Type: GrantFiled: March 25, 1987Date of Patent: March 29, 1988Assignee: TDK CorporationInventors: Kazuo Sato, Shinichi Yamashita
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Patent number: 4731133Abstract: The invention is directed to microcrystalline Al-based alloys produced by annealing an alloy formed initially in a substantially amorphous state by rapid solidification (about 10.sup.4 K/sec) and having a composition consisting essentially of, in atomic %:from 5 to 30% Sifrom 11 to 22% Niwherein the Ni may be partially substituted by Fe up to 10%, by V or B up to 5 atomic % each, or totally substituted by Mn up to 22 atomic %, and wherein Fe+Ni+Si.ltoreq.42%. In the microcrystalline state, in the vicinity of the first crystallization peak, there is a metastable hexagonal phase whose crystalline parameters are about a=0.661 nm and c=0.378 nm.Type: GrantFiled: February 13, 1986Date of Patent: March 15, 1988Assignee: Cegedur PechineyInventor: Salim Dermarkar
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Patent number: 4731116Abstract: Sputter targets and a process for producing sputter targets are provided, comprised of carbides and/or nitrides and/or borides of refractory metals. In a first step, a dense composite body is produced comprised of one or more carbides and/or nitrides and/or borides of the metals of Groups IV A-VI A of the periodic table and a metallic binding agent comprised of one or more metals of the iron group of the periodic table. This composite body in the form of a shaped blank is machined, if necessary, and the binding agent is removed by chemical or electrochemical treatment. The sputter target as so produced has excellent mechanical strength and high thermal shock resistance. Levels of contaminating elements and the residual metallic binding agent are extremely low, meeting the requirements typically placed on sputter targets.Type: GrantFiled: December 18, 1986Date of Patent: March 15, 1988Assignee: Schwarzkopf Development CorporationInventor: Erich Kny
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Patent number: 4726843Abstract: Aluminum alloy, suitable for rapid quenching from a melt supersaturated with alloy components, which contains 2 to 5.5% by weight of Cr and 2 to 5.5% by weight of V, the remainder being Al, and may contain further added amounts of Mo, Zr, Ti or Fe, individually or in combination, up to a total content of not more than 1% by weight, the total content of all alloy elements being no more than 10% by weight. The simultaneous occurrence of the phases Al.sub.13 Cr.sub.2 and Al.sub.10 V in silid solution and as hardness-imparting dispersoids having a particle diameter of not more than 0.1 .mu.m results in good high-temperature strength and thermal stability coupled with good ductility and toughness of the material. The comparatively Low Vickers hardness of, on average, only about 130 (HV) for the rapidly solidified alloys initially obtained make the powders readily processable. After the heat treatment, the Vickers hardness of the workpiece reaches values up to about 200 (HV).Type: GrantFiled: June 18, 1986Date of Patent: February 23, 1988Assignee: BBC Brown, Boveri & Company LimitedInventor: Malcolm J. Couper
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Patent number: 4717627Abstract: Shock wave formation of thin layers of materials with improved superconducting and permanent magnetic properties and improved microstructures.Type: GrantFiled: December 4, 1986Date of Patent: January 5, 1988Assignee: The United States of America as represented by the United States Department of EnergyInventors: William J. Nellis, Theodore H. Geballe, M. Brian Maple
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Patent number: 4710344Abstract: Getter assembly having an annular channel for containing getter material, the bottom of the channel being provided with an annular, integral, groove of bulb-shaped cross-section extending into said channel to lock with said getter material.Type: GrantFiled: December 22, 1986Date of Patent: December 1, 1987Assignee: Union Carbide CorporationInventors: Thomas H. Ward, Phillip A. Costanzo, Vincent Pietrasz, Edmund J. Soeder