Powder Next To Solid Patents (Class 419/8)
  • Publication number: 20020057981
    Abstract: Disclosed are a method for manufacturing cutting blades with a shortened manufacturing process and an apparatus for manufacturing cutting blades with a single manufacturing facility, as well as a cutting blade having cutting segments in which diamond particles are uniformly distributed.
    Type: Application
    Filed: December 12, 2000
    Publication date: May 16, 2002
    Inventor: Rin Soon Park
  • Patent number: 6372362
    Abstract: A method for forming a composite vapor-deposited film one side of which suitable for vapor-deposition on a phosphor surface of a CRT, such as a color television picture tube, has high light reflectivity, and the other side of which has a property to absorb radiant heat, and a composite vapor-deposition material suitable for vacuum deposition are disclosed. The composite vapor-deposition material has a high vapor-pressure metal envelope and a low vapor-pressure metal in the core region of the envelope. Low vapor-pressure metal powder should preferably be dispersed and held by high vapor-pressure metal powder in the core region. Vacuum deposition using this composite vapor-deposition material yields a composite deposited film having a composition comprising almost 100% of the high vapor-pressure metal formed in the initial stage of evaporation, and a composition comprising 100% of the low vapor-pressure metal formed in the final stage of evaporation.
    Type: Grant
    Filed: March 24, 2000
    Date of Patent: April 16, 2002
    Assignee: Hitachi Metals, Ltd.
    Inventors: Shinji Furuichi, Shigetoshi Takashima
  • Publication number: 20020039000
    Abstract: The invention aims to provide a method for preparing a composite substrate which has minimized surface asperities on a dielectric layer, which are otherwise developed under the influence of an electrode layer, unevenness upon printing, and surface roughness inherent to thick-film dielectrics, which eliminates a need for a polishing step, which is easy to manufacture, and which is applicable to the fabrication of a thin-film light-emitting device of high display quality, as well as the resulting composite substrate and a thin-film EL device using the same.
    Type: Application
    Filed: May 30, 2001
    Publication date: April 4, 2002
    Applicant: TDK Corporation
    Inventors: Yukihiko Shirakawa, Taku Takeishi
  • Publication number: 20020015654
    Abstract: A method of fabricating a fully dense, three dimensional object by direct laser sintering is disclosed. In a chamber with a partial pressure atmosphere, a beam of directed energy melts metallic powder in order to form a solid layer cross section. Another layer of powder is deposited and melted, along with a portion of the previous layer. The energy beam typically is in the form of a laser, scanning along a path resembling a parametric curve or another, arbitrary piecewise parametric curve. In another embodiment, the previous layer is not remelted, thus creating an oxide film that acts as a clean stop to prevent unwanted downward growth.
    Type: Application
    Filed: June 1, 2001
    Publication date: February 7, 2002
    Inventors: Suman Das, Joseph J. Beaman
  • Publication number: 20020004141
    Abstract: The magnet has hard magnetic grains (K), with the hard magnetic grains (K) separated from one another in a surface layer of the magnet by a first phase (P1), while the hard magnetic grains (K) in the remaining part of the magnet are separated from one another through a nonmagnetic second phase (P2). The first phase (P1) is more corrosion resistant than the second phase (P2), so that the surface layer serves as corrosion protection. The first phase (P1) has, in addition to elements of which the second phase (P2) consists, at least one further element.
    Type: Application
    Filed: May 18, 2001
    Publication date: January 10, 2002
    Inventors: Peter Schrey, Wilhelm Fernengel, Lothar Zapf
  • Patent number: 6317946
    Abstract: A method for the manufacture of a projectile for small-bore weapons ammunition comprising the steps of producing a plurality of compacts from a mixture of a heavy metal powder and a light metal powder at room temperature, and without further treatment of the compacts, introducing the compacts into a metal jacket one at a time, including pressing each compact into the jacket with a pressure sufficient to ensure substantially complete filling of a respective portion of the jacket by each compact before introducing a further compact into the jacket. The compacts fill less that the entire volume of the jacket, leaving a portion of the jacket void of compacts. Prior to the pressing of the last of the compacts introduced into the jacket, a disc having an outer diameter substantially equal to the internal diameter of said jacket adjacent the open end thereof is introduced into the jacket.
    Type: Grant
    Filed: March 8, 1999
    Date of Patent: November 20, 2001
    Inventor: Harold F. Beal
  • Patent number: 6315945
    Abstract: A consolidated complex shaped article having a density of at least about 95 percent of theoretical density is prepared by placing a plurality of separate bodies in an arrangement, such that each separate body is in contact with at least one other separate body to form an aggregate body and wherein at least one of the separate bodies is essentially dense. The material of each separate body is comprised of a ceramic, a cermet or a metal. The aggregate body is then consolidated at a consolidating temperature, superatmospheric pressure and time at temperature and time at superatmospheric pressure sufficient to form a consolidated shaped article. In consolidating the aggregate body, the consolidating temperature is a temperature that fails to form a liquid within at least one separate body and the superatmospheric temperature is applied for at least a portion of the time at the consolidating temperature.
    Type: Grant
    Filed: January 20, 1998
    Date of Patent: November 13, 2001
    Assignee: The Dow Chemical Company
    Inventors: James M. Macki, Eric A Ness, Robert T. Nilsson, Ellen M. Dubensky, Walter J. Rozmus, Jr., Clifford A. Kelto, Edward E. Timm
  • Publication number: 20010033804
    Abstract: The present invention relates to an abrasive dressing tool used for mechanical and chemical planarization abrasion of the surface of the work pieces as can be used for semiconductor wafers or the like which require precise, planar and micro polishing, and a method for manufacturing the same dressing tool. Specifically, ultimately macro- and micro-scratches on wafers can be drastically reduced, the rate of inferior finished products or wafers can be decreased and abrasive life time of the tool can be prolonged, by sintering and brazing abrasive particles with a nickel based brazing metal on the abrasive tool, and then filling or covering the non-sintered parts and re-crystallized parts of sintered and brazed layers, apt to crack or fall-out from the surface, through electroplating process.
    Type: Application
    Filed: February 12, 2001
    Publication date: October 25, 2001
    Inventor: Jung Soo An
  • Patent number: 6306339
    Abstract: A hydrogen storage material is disclosed with no collapse due to pulverization of hydrogen storage alloy particles by repeated hydrogen absorption and desorption thereby permitting repeated use while manifesting excellent electric and thermal conductivities. Pressure molding of hydrogen storage alloy particles, each being covered with a plated metal film having microgranules of a thermoplastic resin, at a temperature higher than a glass transition temperature or a melting point of and below a thermal decomposition temperature of the thermoplastic resin can produce a porous hydrogen storage material of hydrogen storage alloy particles being bonded to each other via the thermoplastic resin. The hydrogen storage material can become firm and strong because the plated metal films covering the hydrogen storage alloy particles are clasped with each other complexly.
    Type: Grant
    Filed: October 10, 2000
    Date of Patent: October 23, 2001
    Assignee: Kiyokawa Plating Industries, Co., Ltd.
    Inventors: Tadashi Kiyokawa, Hajime Kiyokawa, Masayuki Takashima
  • Publication number: 20010014295
    Abstract: The electrode used in processing a surface of a mold is manufactured as follows. Material powder such as metal powder or metal compound powder is filled in a female mold of the mold. Then the material powder in the female mold is press-molded using a male mold. The surface of the mold is then treated using this electrode.
    Type: Application
    Filed: March 30, 2001
    Publication date: August 16, 2001
    Inventors: Akihiro Goto, Toshio Moro
  • Patent number: 6274082
    Abstract: A process for producing a shaped article, comprising: preparing a first powder having high strength and rigidity after completion of forming, and a second powder having abrasion resistance and surface hardness after completion of forming; compacting those powders to provide a forming material comprising a base part comprising the first powder and a supplemental part comprising the second powder; and forming the forming material into a shaped article by plastic processing, thereby producing a shaped article in which the base part and the supplemental part have different characteristics. The first powder preferably comprises a rapidly-solidified alloy powder and the second powder preferably comprises at least one member selected from among Al2O3, Si3N4, BN, SiC, Al4C3, Al8B2O15 and B2O or a mixture of the member and the first powder which may be the same one actually used as the first powder or another one having a different compositions from that of the actually used first powder.
    Type: Grant
    Filed: September 2, 1999
    Date of Patent: August 14, 2001
    Assignee: YKK Corporation
    Inventors: Junichi Nagahora, Koju Tachi, Koji Saito, Teruaki Onogi
  • Patent number: 6270718
    Abstract: A method of bonding a particle material to near theoretical density, includes placing a particle material in a die. In the first stage, a pulsed current of about 1 to 20,000 amps., is applied to the particle material for a predetermined time period, and substantially simultaneously therewith, a shear force of about 5-50 MPa is applied. In the second stage, an axial pressure of about less than 1 to 2,000 MPa is applied to the particle material for a predetermined time period, and substantially simultaneously therewith, a steady current of about 1 to 20,000 amps. is applied. The method can be used to bond metallic, ceramic, intermetallic and composite materials to near-net shape, directly from precursors or elemental particle material without the need for synthesizing the material. The method may also be applied to perform combustion synthesis of a reactive material, followed by consolidation or joining to near-net shaped articles or parts.
    Type: Grant
    Filed: October 5, 1999
    Date of Patent: August 7, 2001
    Assignee: Materials Modification, Inc.
    Inventors: Sang H. Yoo, Krupashankara M. Sethuram, Tirumalai S. Sudarshan
  • Patent number: 6264885
    Abstract: A metal/ferrite laminate magnet has perforations forming apertures in the magnet. The magnet is formed of outside metal plates surrounding a sandwich of two layers of ferrite material. The outside metal plates allow the perforations to be made in the magnet before sintering of the magnet and maintain the alignment of the holes during sintering. The metal plates also provide the magnet with mechanical robustness and rigidity and prevent cracking occurring between adjacent apertures.
    Type: Grant
    Filed: August 18, 1999
    Date of Patent: July 24, 2001
    Assignee: International Business Machines Corporation
    Inventors: John Ulrich Knickerbocker, Andrew Ramsay Knox, Robert Rosenberg
  • Publication number: 20010008703
    Abstract: A highly reliable sintered compact which can be readily and safely produced, and a method for producing such sintered compact are provided. The sintered compact is preferably formed into a heat sink 1 which comprises a heat sink main body 2. The heat sink main body 2 comprises a substrate 3, a plurality of projections 4 integrally formed with the substrate 3 on its heat dissipation surface, and a molded frame 5 integrally formed with the substrate 3 to surround the projections 4. On each corner of the substrate 3 is formed a circular molded hole 6. The opposite surface of the substrate 3 is formed into a contacting surface which is adapted to be in contact with the heat generating semiconductor chip, and this contacting surface is surface treated, for example, by plating. The sintered compact is produced from metal powders, and it comprises at least one metal selected from tungsten and molybdenum and 2 to 50% by weight of silver.
    Type: Application
    Filed: August 25, 1997
    Publication date: July 19, 2001
    Inventors: MASAAKI SAKATA, SHOJI TAKAHASHI, KENICHI SHIMODAIRA
  • Patent number: 6224816
    Abstract: Tool having a molding surface is formed from a flowable material (e.g., powder material) wherein the shape of molding surface is formed from a molding process using a master pattern having a surface with a shape substantially the same as the shape of the molding surface to be formed. The tool has at least one thermal control element located within it and spaced from the molding surface where a component used in forming the thermal control element is located within the flowable material prior to solidifying the material. The powder material is preferably a mixture of metals. The thermal control elements include fluid flow paths, heating elements, temperature sensors, and the like.
    Type: Grant
    Filed: September 17, 1998
    Date of Patent: May 1, 2001
    Assignee: 3D Systems, Inc.
    Inventors: Charles W. Hull, Michael S. Lockard, Thomas A. Almquist
  • Patent number: 6218025
    Abstract: A sintered electrode of high-melting metal (for example tungsten) is produced from spherical metal powder having a well defined particle size. The mean particle size is from 5 to 70 &mgr;m. The particle size distribution covers a range from at most 20% below to at most 20% above the mean particle size.
    Type: Grant
    Filed: August 18, 1998
    Date of Patent: April 17, 2001
    Assignee: Patent- Truchand-Gesellschaft fuer Elektrische Gluelampen mbH
    Inventors: Dietrich Fromm, Bernhard Altmann, Wolfram Graser, Peter Schade
  • Patent number: 6218026
    Abstract: A high performance hybrid member for use in applications where high stiffness, high temperature capacity and being lightweight are important. In one form of the present invention the hybrid member is formed of a titanium alloy outer portion with a gamma titanium aluminide alloy inner portion metallurgically bonded therin. The gamma titanium aluminide alloy material has a room temperature modulus of elasticity greater than the modulus of elasticity of the titanium alloy outer portion. The hybrid member has a modulus of elasticity greater than modulus of elasticity of the titanium alloy outer portion, and a density equivalent to that of the titanium outer portion. The wear resistant capability of the member can be increased at local regions by surface modification treatment such as plasma ion nitriding or by affixing at ends of the member hardened fittings.
    Type: Grant
    Filed: March 3, 1998
    Date of Patent: April 17, 2001
    Assignees: Allison Engine Company, Allison Advanced Development Company
    Inventors: Bruce Allan Ewing, Robert Anthony Ress, Jr., James Ronald Roessler
  • Patent number: 6200524
    Abstract: The present invention discloses a method of manufacturing a face seal wherein an annular groove on the face seal substrate is filled with a mixture of a metal binder and refractory metal carbide and pressed. A second metal binder layer is then placed upon the pressed mixture and a second pressing step is performed to form an integral green body of the first pressed mixture and the second metal binder layer. The integral green body is then heated to consolidate and adhere the green body to the substrate.
    Type: Grant
    Filed: April 29, 1999
    Date of Patent: March 13, 2001
    Assignee: Mech Coating Ltd.
    Inventors: Yefim Griskin, Natalya Griskin
  • Patent number: 6197431
    Abstract: A method for manufacturing machining tools out of composite powdered metal which is first formed to approximate the desired shape of the machining tool; then bonded metallurgically; and machined to the desired finished shape. Desirably, the forming step employs at least two distinct powdered metals, the first formed to the outer shape over the portion of the tool that interfaces with the work piece and selected to exhibit the desired hardness and wear-resistance properties. The second material supports the hollow form of the first material and includes a shank to interface with the machine that the tool will be employed with. The second material is chosen to exhibit the desired ductility, surface hardness, abrasion resistance and reduced cost. Additional materials can be used for different facets of the tool to obtain an optimum balance of long life, efficient operation and low cost.
    Type: Grant
    Filed: June 18, 1998
    Date of Patent: March 6, 2001
    Assignee: Siemens Westinghouse Power Corporation
    Inventors: Jimmy Arthur Cox, Herman Carter Denny
  • Patent number: 6183686
    Abstract: A method of producing a sputter target assembly including a metal target attached to a metal-matrix-composite backing plate and sputter target assemblies made thereby. The method includes hot isostatically pressing a silicon carbide-aluminum powder composition to form a backing plate while simultaneously bonding the powder composition to a metal target to form a diffusion-type bond between the target and the backing plate such that the target assembly possesses extremely high resistance to warpage at high operating temperatures. A second embodiment of the sputter target assembly includes an annular sealing member of machined aluminum disposed in the backing plate around the target.
    Type: Grant
    Filed: August 3, 1999
    Date of Patent: February 6, 2001
    Assignee: Tosoh SMD, Inc.
    Inventors: Steven L. Bardus, Sohail S. Qamar, Anurag Bansal
  • Patent number: 6171709
    Abstract: The invention provides a superabrasive containing composite product, comprising and/or prepared on the intense heating of an SHS process, self-propagating high-temperature synthesis. An effective method of such product is also provided. Said composite comprises a substrate of shaped metallic block and a functional layer of ceramic materials containing superabrasive particles, which is joined on a surface of the former, by means of and intermediated by molten metal which occurred during the SHS process.
    Type: Grant
    Filed: May 11, 1998
    Date of Patent: January 9, 2001
    Assignees: The Ishizuka Research Institute, Ltd., Mitsue Koizumi, Manshi Ohyanagi, Moscow Steel and Alloys Institute, SHS-Center
    Inventors: Mitsue Koizumi, Manshi Ohyanagi, Satoru Hosomi, Evgeny A. Levashov, Alexander V. Trotsue, Inna P. Borovinskaya
  • Patent number: 6120727
    Abstract: Disclosed is a method of manufacturing a machine component of sintered ferriferous composite comprising an outer part and an inner part which is fitted into a hole of the outer part. It has the steps of: preparing one of the outer part and the inner part as a green compact of ferriferous powdered metal and the other as one of a green compact of ferriferous powdered metal, a sintered compact of ferriferous powdered metal and a mass of ferriferous molten metal; inserting the inner part into the hole of the outer part; and sintering the outer part and the inner part to bond the outer part and the inner part. The outer part and the inner part are prepared to have a fitting clearance of approximately -100 to +5 .mu.m.
    Type: Grant
    Filed: September 15, 1999
    Date of Patent: September 19, 2000
    Assignee: Hitachi Powdered Metals Co., Ltd.
    Inventors: Kazuo Asaka, Tsuyoshi Kagaya, Masahiro Suzuki
  • Patent number: 6114048
    Abstract: The invention provides for a functionally-graded metal substrate that is made of at least two metal compositions, a functional insert and a surrounding body that surrounds the functional insert. In a preferred embodiment of the invention a functional insert powder composition of loose powder metal is placed in a compact of a surrounding body powder composition and both metal compositions are sintered in a sintering furnace to form a sintered part. The sintered part is infiltrated in part or in whole with a molten metal compound to produce a functionally graded metal substrate having a density of at least 90% of theoretical. A heat-generating component such as a chip can be attached to the metal substrate for use in microelectronic packaging. When the functionally-graded metal substrate has two discrete compositions of copper/tungsten the surrounding body which has a CTE that ranges from about 5.6ppm/.degree. C. to about 7 ppm/.degree. C.
    Type: Grant
    Filed: September 4, 1998
    Date of Patent: September 5, 2000
    Assignee: Brush Wellman, Inc.
    Inventors: David E. Jech, Jordan P. Frazier, Richard H. Sworden, Juan L. Sepulveda
  • Patent number: 6110418
    Abstract: A method for manufacturing cutting knives, in particular granulator knives in which a mass of highly wear resistant material is bonded along one edge of a main body of a tougher, more ductile material, the cutting edge machined into the mass of wear resistant material, to increase the service life of the knife between sharpenings without subjecting the tool to breakage during heavy use in a granulator.
    Type: Grant
    Filed: November 9, 1998
    Date of Patent: August 29, 2000
    Inventor: David A. Jablonski
  • Patent number: 6103186
    Abstract: Abradable coatings for turbine engine shrouds are formed from biscuits formed of silicon-diffused powdered alloy compositions which are processed with an HE precursor to strip oxides from the coating during processing, the alloy blends comprising MCrAl(Y).sub.n alloys in which n is 0, 1 or more.
    Type: Grant
    Filed: November 18, 1998
    Date of Patent: August 15, 2000
    Assignee: TMT Research Development, Inc.
    Inventors: George K. Sievers, Eugene V. Clark
  • Patent number: 6073518
    Abstract: A method of manufacturing a drill bit or other drilling-related structure used for drilling into subterranean formations is herein disclosed where a blank is formed by placing a ferrous metal powder such as steel into a mold, sintering the ferrous metal powder to form a preformed blank, packing an abrasion- and erosion-resistant material such as tungsten carbide powder around the preformed blank, and infiltrating the preformed blank and tungsten carbide with a common binder such as a copper-based binder. For some materials, during sintering, the preformed blank may shrink in size relative to the mold enough to provide space between the mold and the preformed blank for a layer of abrasion- and erosion-resistant material. With other materials, a separate blank mold may be used to form the sintered blank which can then be inserted into the mold for infiltration.
    Type: Grant
    Filed: September 24, 1996
    Date of Patent: June 13, 2000
    Assignee: Baker Hughes Incorporated
    Inventors: Jacob T. C. Chow, Sidney L. Findley, David P. Beacco, Lorenzo G. Lovato
  • Patent number: 6063333
    Abstract: This disclosure features a process of making a two part drill bit insert, namely, a body portion of hard particles such as tungsten carbide particles mixed in an alloy binding the particles. The alloy preferably comprises 6% cobalt with amounts up to about 10% permitted. The body is sintered into a solid member, and also joined to a PDC crown covering the end. The crown is essentially free of cobalt. The process sinters the crown and body while preserving the body and crown cobalt differences.
    Type: Grant
    Filed: May 1, 1998
    Date of Patent: May 16, 2000
    Assignees: Penn State Research Foundation, Dennis Tool Company
    Inventor: Mahlon Denton Dennis
  • Patent number: 6045601
    Abstract: A high density, non-magnetic alloy is described along with a process for manufacturing it. The preferred composition for the alloy is approximately 95% by weight of tungsten and 5% of austenitic stainless steel. The process for manufacturing the alloy begins with blending tungsten and stainless steel powders which are then mixed with an organic binder to form a feedstock. The latter is then molded into the form of compacted items, such as a hard drive counterweight balance, and then sintered in either vacuum or a hydrogen atmosphere. The tungsten heavy alloys of the present invention can be easily manufactured in large volume economically in many intricate shapes with excellent control of weight and dimensions.
    Type: Grant
    Filed: September 9, 1999
    Date of Patent: April 4, 2000
    Assignee: Advanced Materials Technologies, Pte, Ltd.
    Inventor: Lye King Tan
  • Patent number: 6042777
    Abstract: There is provided a method for fabricating intermetallic sputter targets of two or more elements in which a mixture of two or more elemental powders are blended and synthesized within a pressing apparatus at a temperature below the melting point of the lowest melting point element in the mixture, followed by heating the synthesized intermetallic powder in the pressing apparatus to a temperature below the melting point of the intermetallic structure while simultaneously applying pressure to the powder to achieve a final density greater than 90% of theoretical density. The powder metallurgy technique of the present invention provides a better microstructure than cast structures, and avoids contamination of the sputter target by eliminating the crushing step of synthesized intermetallic chunks necessitated by separate steps of synthesizing and pressing.
    Type: Grant
    Filed: August 3, 1999
    Date of Patent: March 28, 2000
    Assignees: Sony Corporation, Materials Research Corporation
    Inventors: Chi-Fung Lo, Darryl Draper, Hung-Lee Hoo, Paul S. Gilman
  • Patent number: 5993733
    Abstract: A synchronizing ring 10 having an annular structural part 11 and a frictional layer 12 is manufactured by filling a mold 20 with a material for the structural part or a material for the frictional layer and compacting the material filled in the mold 20, filling the mold with a material for the frictional layer or a material for the structural part and compacting the material filled into the mold to unify the structural part and the frictional layer, and sintering the unified structural part 11 and frictional layer 12 in a sintering furnace. The frictional layer 12 can be combined with the structural part 11 without forcibly mounting the frictional layer 12 on the structural part 11. The material for the frictional layer need not be presintered, and the frictional layer can be formed by a single sintering cycle.
    Type: Grant
    Filed: January 23, 1997
    Date of Patent: November 30, 1999
    Assignee: Dynax Corporation
    Inventor: Satoshi Kawai
  • Patent number: 5989489
    Abstract: The invention relates to a method for manufacturing a composite material wherein by dynamic densification of an amount of granular or powdered relatively brittle material or a mixture of one or more of such materials, a continuous porous product is obtained, whereafter, by infiltration thereof with a second material, the brittle material particles are embedded in a continuous network of the second material. The invention further relates to a composite comprising ceramic particles embedded in a continuous matrix of a second material, obtainable by a method according to the invention, and to products manufactured from such composite.
    Type: Grant
    Filed: November 25, 1997
    Date of Patent: November 23, 1999
    Assignee: Nederlandse Organisatie voor toegepast-natuurwetenschappelijk Onderzoek TNO
    Inventors: Marianne Euphemia Corry Stuivinga, Amanda Margaretha Maas, Erik Peter Carton
  • Patent number: 5985373
    Abstract: A method and apparatus for applying multi-layered coatings utilizing a detonation gun process. The present invention consists of multiple powder feeders (7, 8) attached to the barrel (13) of a detonation gun (2). The powder feeders (7, 8) are disposed at axially spaced locations along the barrel (13) and supply coating materials to the barrel (13) in advance of a detonation wave front (100) such that the powders are exhausted from the barrel (13) in serial fashion producing a multi-layered coating on the workpiece (1). The multi-layered coating system of the present invention substantially enhances the quality and productivity of the detonation coating process.
    Type: Grant
    Filed: October 16, 1998
    Date of Patent: November 16, 1999
    Assignee: Aerostar Coatings, S.L.
    Inventor: Alexandr Vladimirovich Chernyshov
  • Patent number: 5972521
    Abstract: The present invention provides a method of forming a continuous one-piece structural porous metal (SPM) structure having a predetermined geometry. The method the invention includes the steps of preparing a metal billet comprising a metal core formed of a metal and a gas, and solid metal face sheets bonded to opposite sides of the metal core; placing the metal billet in a mold cavity having a predetermined geometry defined by opposing inner surfaces of the mold with at least one of the opposing inner surfaces contacting at least a portion of the metal billet and spaced apart from at least a portion of the metal billet; and heating the metal billet to expand the metal core to form the expanded metal structure.
    Type: Grant
    Filed: October 1, 1998
    Date of Patent: October 26, 1999
    Assignee: McDonnell Douglas Corporation
    Inventors: Christopher S. Huskamp, Donald A. Deuser, Daniel S. Schwartz
  • Patent number: 5963778
    Abstract: A preferred method for producing a pair of sputter targets includes the step of machining fist and second backing plates to form surfaces having near net profiles characteristic of an ion source, the sputtering material and the target shape. A preform is constructed which includes the first backing plate, a first powder layer abutting against the first backing plate, a spacer abutting against the first powder layer, a second powder layer abutting against the spacer, and the second backing plate abutting against the second powder layer. In an especially preferred form, the spacer comprises a pair of metal plates separated by a layer of bond-resistant material such as boron nitride. The preform is heated and isostatically pressed to consolidate the powder layers to form the pair of sputter targets and to diffusion bond the targets to corresponding backing plates. The method promotes the formation of uniformly even sputtering surfaces on the targets.
    Type: Grant
    Filed: August 26, 1998
    Date of Patent: October 5, 1999
    Assignee: Tosoh SMD, Inc.
    Inventor: David E. Stellrecht
  • Patent number: 5960249
    Abstract: A method for forming an exterior surface of a high-temperature component, such as a blade or vane of a gas turbine engine. The method entails forming a shell by a powder metallurgy technique that yields an airfoil whose composition can be readily tailored for the particular service conditions of the component. The method generally entails providing a pair of inner and outer mold members that form a cavity therebetween. One or more powders and any desired reinforcement material are then placed in the cavity and then consolidated at an elevated temperature and pressure in a non-oxidizing atmosphere. Thereafter, at least the outer mold member is removed to expose the consolidated powder structure. By appropriately shaping the mold members to tailor the shape of the cavity, the consolidated powder structure has the desired shape for the exterior shell of a component, such that subsequent processing of the component does not require substantially altering the configuration of the exterior shell.
    Type: Grant
    Filed: March 6, 1998
    Date of Patent: September 28, 1999
    Assignee: General Electric Company
    Inventors: Ann Melinda Ritter, Paul Leonard Dupree, Melvin Robert Jackson, Donald Norman Wemple, Jr.
  • Patent number: 5954895
    Abstract: A method of making a deposit on a component made of a nickel or cobalt based superalloy is described wherein a deposit material consisting of reactive powders corresponding to an intermetallic material or of a superalloy powder is deposited on the component before placing it in a chamber and subjecting it to a neutral gas at a hydrostatic pressure of up to 1.5 GPa, the chamber being provided with heater means for producing a controlled temperature of up to 1200.degree. C. at a rate of increase of from 5.degree. C. to 120.degree. C. per minute and a thermal gradient of 200.degree. C. between the ends of the component, and the temperature and pressure conditions in the chamber are selected such that the deposit material undergoes a synthesis reaction by self-propagated combustion under high pressure so as to obtain densification of the deposit and a metallurgical bonding between the deposit and the component.
    Type: Grant
    Filed: August 21, 1997
    Date of Patent: September 21, 1999
    Assignee: Societe Sochata
    Inventors: Marie-Caroline Dumez, Jean-Pierre Huchin, Rose Marie Marin-Ayral, Didier Perraud, Jean-Claude Tedenac
  • Patent number: 5951791
    Abstract: This process provides a method of fabricating porous aluminide articles. First the process consists of plating a preform with nickel and aluminum to create a metal-plated structure. The plating of nickel consists of electrodeposition or gaseous plating. The plating of aluminum consists of gaseous deposition of an organometallic-aluminum compound. The preform has either an open felt, woven fabric or a reticulated foam shape. Reactive sintering the metal-plated structure leaves an open nickel-aluminum structure having porosity and excellent strength and oxidation properties above 400.degree. C.
    Type: Grant
    Filed: December 1, 1997
    Date of Patent: September 14, 1999
    Assignee: Inco Limited
    Inventors: James Alexander Evert Bell, Kirt Kenneth Cushnie, Anthony Edward Moline Warner, George Clayton Hansen, Raymond Augustus Bradford
  • Patent number: 5937268
    Abstract: A sintered sliding member having not only excellent in wear resistance but also low in attacking property against a mated member. To obtain the member, 0.1 to 3.5 wt. % h-BN and 0.1 to 3.5 wt. % graphite are mixed in a matrix material of iron-based powder containing chromium, and a resultant powder mixture is compacted to form a compact. The compact is sintered while bringing the compact into contact with copper or copper alloy so that the copper or copper alloy is infiltrated simultaneously with the sintering. In this way, the copper phase is filled in the iron-based matrix and the h-BN is distributed in the copper phase. Graphite reacts with chromium to be precipitated as chromium carbide in and/or near boundaries defined between the matrix and the copper phase.
    Type: Grant
    Filed: February 4, 1997
    Date of Patent: August 10, 1999
    Assignee: Daido Metal Company Ltd.
    Inventors: Kouki Ozaki, Koichi Yamamoto, Takayuki Shibayama
  • Patent number: 5937264
    Abstract: A composite oxygen electrode/electrolyte structure for a solid state electrochemical device having a porous composite electrode in contact with a dense electrolyte membrane, which electrode includes: (a) a porous structure having interpenetrating networks of an ionically-conductive material and an electronically-conductive material; and (b) an electrocatalyst different from the electronically-conductive material, dispersed within the pores of the porous structure. This electrode structure is relatively simple to manufacture, requiring relatively few steps to infiltrate an electrocatalyst precursor material to obtain an electrode structure which will perform advantageously in a solid oxide fuel cell, has a relatively low internal resistance, and permits the selection of an optimal electronically-conductive material and electrocatalyst.
    Type: Grant
    Filed: August 29, 1997
    Date of Patent: August 10, 1999
    Assignee: The Dow Chemical Company
    Inventor: Sten A. Wallin
  • Patent number: 5904993
    Abstract: A joint body in which aluminum and silicon nitride are strongly joined with each other is provided at a low cost, thereby providing a lightweight part which is excellent in sliding property as a mechanical part of an internal combustion engine of an automobile or the like. The joint body includes a base material which is mainly composed of aluminum, and a member consisting of a silicon nitride sintered body which is substantially directly joined to the base material. A powdery or bulky base material (2) mainly composed of aluminum, and a member (1) consisting of a silicon nitride sintered body are charged in a mold and heated under pressurization, thereby joining the same with each other.
    Type: Grant
    Filed: May 21, 1996
    Date of Patent: May 18, 1999
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Hisao Takeuchi, Koichi Sogabe, Takao Nishioka, Takashi Matsuura, Akira Yamakawa
  • Patent number: 5863398
    Abstract: Described is a hot pressed and sintered sputtering target assembly formed of hot pressed and sintered metal powder diffusion bonded together and to a backing plate by use of an intermediate adhesion layer of titanium or titanium alloy.
    Type: Grant
    Filed: October 11, 1996
    Date of Patent: January 26, 1999
    Assignee: Johnson Matthey Electonics, Inc.
    Inventors: Janine K. Kardokus, Diana Morales
  • Patent number: 5864744
    Abstract: The object of the invention is a reactive sintering method of forming intermetallic materials such as TiNi, TiAl which includes the preparation of a mixture of elemental metallic powders in desired proportions (1) (2), the compression (3) of the mixture of these elemental powders so as to obtain a tablet of powders, then the cladding (4) of this tablet of powders in a cladding resistant to pressure and heat, the clad product then being subjected to a reactive sintering (5) to obtain the intermetallic compound and to a final hot densification operation (6) . Generally, the cladding is removed (7).
    Type: Grant
    Filed: June 18, 1996
    Date of Patent: January 26, 1999
    Assignee: Commissariat A L'Energie Atomique
    Inventor: Yves Bigay
  • Patent number: 5853652
    Abstract: A method of manufacturing a lead having an electrode includes the steps of introducing a substrate into a mold, creating a negative pressure in the mold, injecting a slurry comprising a binder and a conductive particulate material into the mold cavity during the step of creating negative pressure in the mold cavity, heating the mold having the substrate and the particulate material in an oven to cojoin the particulates and thereby form an electrode, removing the mold from the oven, removing the electrode from the mold, and assembling the electrode into a lead. The produced lead may be used as a steroid eluting pacing cardiac lead.
    Type: Grant
    Filed: April 24, 1996
    Date of Patent: December 29, 1998
    Assignee: Medtronic, Inc.
    Inventors: Gary R. Schildgen, Charles R. Wait
  • Patent number: 5850591
    Abstract: A method of manufacturing a porous metal sheet having pores forming a pattern, comprising the steps of supplying metal powders to a peripheral surface, of at least one pattern roller of a pair of rollers, on which a pattern including a large number of concaves is formed; dropping metal powders to the concaves and accumulating metal powders on the peripheral surface of the pattern roller except the concaves; and rolling directly the metal powders accumulated on the peripheral surface of the pattern roller by rotating a pair of the rollers. It is preferable to laminate porous metal sheets or solid metal sheets manufactured by a method other than the above-described method on the metal sheet manufactured by the above-described method.
    Type: Grant
    Filed: April 18, 1997
    Date of Patent: December 15, 1998
    Assignee: Katayama Special Industries, Ltd.
    Inventor: Hirofumi Sugikawa
  • Patent number: 5842106
    Abstract: The present invention provides a method of forming a fluidtight electrical conduit through a high aspect ratio hole, the method comprising sintering a via ink to form the electrical conduit and to seal the hole.
    Type: Grant
    Filed: November 9, 1995
    Date of Patent: November 24, 1998
    Assignee: Sarnoff Corporation
    Inventors: Barry Jay Thaler, Robert Leon Quinn, Paul Leonard Braun, Peter J. Zanzucchi, Charlotte A. Burton, Sterling E. McBride, Robert R. Demers
  • Patent number: 5815791
    Abstract: A process for manufacturing a structural element with brazed-on, bent or folded metal foil components having a foil thickness of less than 500 .mu.m, made of an ODS sintered ferrous material. The sintered material is manufactured by mechanically alloying the basic powders, hot pressing and/or extruding, and subsequently hot-rolling, cold-rolling and final recrystalization annealing to form the sintered material into a foil having improved mechanical strength properties. After the cold-rolling step, the foil material is annealed so that the foil may be thereafter bent and folded at room temperature. The bent and/or folded foil is recrystallization-annealed at a temperature between 1100.degree. and 1300.degree. C. during 3-600 minutes, simultaneously with a brazing operation, in a single process step.
    Type: Grant
    Filed: March 20, 1996
    Date of Patent: September 29, 1998
    Assignee: Schwarzkopf Technologies Corporation
    Inventor: Dieter Sporer
  • Patent number: 5815790
    Abstract: The invention relates to a method for the manufacturing of a composite metal product. More particularly, the invention relates to a method for the manufacturing of a composite product consisting of at least two stainless steel materials having different chemical compositions, particularly a composite stainless product on which decorative patterns can or has been produced by etching.It is significant feature of the invention that at least two stainless steel materials having different chemical compositions are bonded together through hot isostatic compaction at a pressure exceeding 600 bar and a temperature exceeding 1000.degree. C., at least one of said materials consisting of powder, for the achievement of a consolidated body.
    Type: Grant
    Filed: December 4, 1996
    Date of Patent: September 29, 1998
    Assignee: Soderfors Powder Aktiebolag
    Inventors: Per Billgren, Kaj Embretsen
  • Patent number: 5812926
    Abstract: A hard facing alloy is applied to a surface of a substrate by making a mixture of at least two constituents whose net composition is the desired hard facing alloy composition. The constituents have different solidus temperatures, at least one of which is above a processing temperature of the substrate and another of which is below the processing temperature of the substrate. In one preferred approach, the mixture is prepared by pressing and lightly sintering the constituents in the form of powders, so that the mixture retains its shape and can be attached to the substrate surface. Then the substrate is heated to the processing temperature and maintained for a time sufficient to permit interdiffusion of the several different phases toward a homogeneous hard facing alloy composition uniformly through a major portion of the volume.
    Type: Grant
    Filed: September 3, 1991
    Date of Patent: September 22, 1998
    Assignee: General Electric Company
    Inventors: Joseph Carl Wukusick, Roger Johnson Perkins, deceased, Murray Sawyer Smith, Jr.
  • Patent number: 5812925
    Abstract: A method for joining a first metal surface to a second metal surface that includes providing powder metal particles substantially all of which have hardnesses lower than the hardnesses of the first and second metal surfaces, at normal temperatures; locating the particles in a layer between the first and second metallic surfaces, to form an assembly; heating the assembly to an elevated temperature or temperatures below the softening temperature of the first and second metallic surfaces; and effecting compression of the layer by and between the first and second surfaces at a pressure level or levels below the compressive yield strengths of the first and second surfaces, and above the compressive yield strengths of the particles, and for a time duration to effect a bond between the first and second metallic surfaces.
    Type: Grant
    Filed: October 23, 1996
    Date of Patent: September 22, 1998
    Inventor: Gunes M. Ecer
  • Patent number: 5805971
    Abstract: A method of producing a three-dimensional form includes the steps of spraying from at least one nozzle a gas including particles of materials having different properties onto a base surface to deposit a layer of particles, repeatedly spray-depositing layers of particles each on the upper surface of a deposition layer, thereby building up a three-dimensional object consisting of the accumulated deposition layers each having different properties in a two-dimensional plane, and utilizing the different properties in the accumulated deposition layers to remove part of the three-dimensional object, thereby producing a desired three-dimensional form.
    Type: Grant
    Filed: September 12, 1995
    Date of Patent: September 8, 1998
    Assignee: Agency of Industrial Science & Technology, Ministry of International Trade & Industry
    Inventor: Jun Akedo