Powder Next To Solid Patents (Class 419/8)
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Patent number: 5788142Abstract: A process for joining two parts of which at least one is made of an intermetallic material comprises:mixing elemental powders to form an intermetallic compound of the same type as that of the intermetallic part or parts;compacting and forming an intermediate part from the said compound at a temperature below that of the reaction sintering temperature of the compound;placing the intermediate part in position between the two parts to be joined;subjecting the assembly of parts to a first thermal cycle so as to effect a reaction sintering of the intermediate part and a consolidation of the assembly; and,subjecting the assembly to a second thermal cycle at a temperature above 0.8 of the fusion temperature of said intermetallic compound so as to effect a diffusion treatment and mechanical consolidation of the assembly.The process may also be adapted to form a coating or a repair of a part using an intermetallic material.Type: GrantFiled: October 3, 1996Date of Patent: August 4, 1998Assignees: Societe Nationale d'Etude et de Construction de Moteurs d'Aviation "Snecma", Commissariat a L'Energie AtomiqueInventors: Yves Bigay, Alain Lasalmonie
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Patent number: 5765095Abstract: A method for manufacturing a PCD bit by isostatically or mechanically press forming a green on a metallic blank. A metallic blank is vertically suspended into a flexible vessel. Powder metal is mixed with a binder and introduced into the flexible vessel surrounding the lower end of the suspended metallic blank. The vessel is then isostatically or mechanically pressed causing the powder mixture to stick together and to the blank, forming a green on the blank. The blank and green are removed from the vessel and the exposed end of the metallic blank is chucked onto a milling machine and turned for milling the green into the shape of a PCD bit head. After the milling is completed, the green and blank are sintered, hardening the bit head shaped green and strongly bonding it to the metallic blank, forming a PCD bit wherein the hardened green is the bit head while the metallic blank is the bit pin.Type: GrantFiled: August 19, 1996Date of Patent: June 9, 1998Assignee: Smith International, Inc.Inventors: Richard A. Flak, T. H. (Nick) Nichols, Thomas W. Oldham
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Patent number: 5759707Abstract: Metal structures, e.g. coolers or heat exchangers, can be produced by placing together metal components coated with solder, dipping them into a slurry of a flux, and soldering them by heating. Alternatively, components coated with solder can also be coated with flux, then placed together to form the metal structure and soldered by heating. In this case, however, the flux must be applied so as to adhere securely, and to this end in the prior art the flux has been "glued on" to the metal surface by organic or other binders, which when burned out during the soldering process can produce undesirable exhaust gases or emissions. The present invention discloses a metal component which is provided with a sintered flux coating which adheres without binder. The coating can optionally also contain solder metal or other auxiliaries dispersed therein.Type: GrantFiled: October 4, 1996Date of Patent: June 2, 1998Assignee: Solvay Fluor und Derivate GmbHInventors: Heinz-Joachim Belt, Ruediger Sander, Werner Rudolph
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Patent number: 5761592Abstract: A process for producing a sliding member employs a base material having a covering surface and pores, and a layer material comprising a constitutive component for reacting with a constitutive component of the base material. Initially, the layer material comes into contact with at least part of the covering surface of the base material. Next, the both are heated to the sintering temperature of the base material. Thus, a molten liquid occurs at the boundary between the base material and the layer material. Since the solidus temperature of the molten liquid increases with the reaction proceeding, the molten liquid can solidify early to seal the pores at the covering surface of the base material early. Therefore, the layer material remains on the covering surface of the base material, the remaining layer material comes to constitute a sliding surface.Type: GrantFiled: May 20, 1996Date of Patent: June 2, 1998Assignee: Toyota Jidosha Kabushiki KaishaInventors: Hiroshi Okajima, Akira Manabe
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Patent number: 5724643Abstract: A high performance hybrid shaft for use in applications where high stiffness, high temperature capacity and lightweight are important. In one form of the present invention the hybrid shaft is formed of a titanium alloy outer tube having in it's interior a gamma titanium aluminide alloy powder metal that is metallurgically bonded to the outer tube. The gamma titanium aluminide alloy powder metal has a room temperature modulus of elasticity greater than the modulus of elasticity of the titanium alloy tube. The hybrid shaft has a modulus of elasticity greater than modulus of elasticity of the titanium alloy tube, and a density equivalent to that of the titanium alloy tube. The wear resistant capability of the shaft is increased at local regions by surface modification treatment such as plasma ion nitrating or by affixing at the ends of the tube a hardened steel fitting.Type: GrantFiled: June 7, 1995Date of Patent: March 3, 1998Assignee: Allison Engine Company, Inc.Inventor: Bruce Ewing
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Patent number: 5722306Abstract: A method to produce a composite blank for a knife blade and, to produce knife blades from it. Each half of a pair of substrate halves has a groove filled with a powdered titanium carbide based metal matrix composite (Fe/TiC). It is placed in a metal container which is sealed, evacuated, and subjected to hot isostatic pressing (HIP) to cause the powder to sinter and bond to the halves. The container is cooled and removed from the contents. The metal halves are separated, and sliced to form the blanks, and the blanks are sharpened to form the knife blades.Type: GrantFiled: June 7, 1995Date of Patent: March 3, 1998Assignee: Alloy Technology International Inc.Inventors: Timothy M. Vela, David H. Atkinson
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Patent number: 5710969Abstract: A method of controlling chosen geometries in sintering operations uses an insert in the preform which is to be sintered, which insert can withstand sintering temperatures without distortion, and which will not bond to the preform and thus prevent removal subsequent to sintering. In powder metal sintering, inexpensive ceramic alumina inserts satisfy these criteria. A powdered metal preform is caused to shrink onto a precisely formed ceramic insert, thereby to determine final shape accurately. An insert larger in diameter than that of the uninserted undistorted preform final diameter may be used if potential impact on geometry density is factored into its selection. An insert shape other than that of the preform undistorted final shape may be used to create final geometries different by design than those of the preform.Type: GrantFiled: March 8, 1996Date of Patent: January 20, 1998Assignee: Camax Tool Co.Inventor: David P. Newman
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Patent number: 5708955Abstract: A method for manufacturing a component for use in an electromagnetically actuated clutch, such as an armature or a pole piece, having one or more flux breaks provided therein includes the initial step of providing a mold having an upstanding central post which defines an annular mold cavity. A quantity of powdered metal material is disposed within the mold cavity. The powdered metal material is formed from a magnetically permeable material, such as a ferromagnetic material. Next, one or more preforms of a non-magnetically permeable material are disposed within the mold cavity. The preform is placed on top of the quantity of powdered metal material axially above the desired location for the magnetically non-conductive region of the component to be formed. Then, a ram of a press machine is moved axially downwardly into engagement with the preform and the powdered metal material contained within the mold.Type: GrantFiled: November 16, 1995Date of Patent: January 13, 1998Assignee: Dana CorporationInventor: James R. Ungrue
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Patent number: 5678168Abstract: A system of two thick film pastes containing gold, in which the first paste is deposited directly onto a substrate, and the second is deposited directly onto the first, contain Cr.sub.2 O.sub.3 and Bi.sub.2 O.sub.3, which enhance the adhesion to the substrate of the first deposited paste and the solderability of the second deposited paste.Type: GrantFiled: November 13, 1995Date of Patent: October 14, 1997Assignee: National Starch and Chemical Investment Holding CorporationInventors: Orville W. Brown, David J. Nabatian
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Patent number: 5667903Abstract: A weld rod is prepared by placing a plurality of tungsten carbide/cobalt nuggets, preferably mixed with loose material, into a steel tube. The nuggets are previously sintered and have a generally ellipsoidal shape. A substrate is hard faced by progressively melting the weld rod onto the surface to be hard faced, and allowing the melted material to solidify on the surface.Type: GrantFiled: May 10, 1995Date of Patent: September 16, 1997Assignee: Dresser Industries, Inc.Inventor: James Edward Boyce
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Patent number: 5659876Abstract: A method for producing a washer having a boss comprises the following steps in the sequence set forth: (a) sprinkling powder of a bearing alloy onto a backing metal made of an iron-based alloy to form a composite material; (b) sintering the composite material to obtain a bimetal material so as to accomplish a primary sintering; (c) fabricating the bimetal material into a shape of the washer having the boss; and (d) simultaneously accomplishing a secondary sintering and carburizing of the washer having the boss. By virtue of simultaneously conducting the secondary sintering and the carburizing for the washer, the number of steps in producing method (particularly, during a heat treatment) is reduced thereby improving the productivity of the washer having the boss while reducing thermal energy required for the heat treatment.Type: GrantFiled: October 19, 1995Date of Patent: August 19, 1997Assignee: Jatco CorporationInventor: Muneo Mizuta
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Patent number: 5652877Abstract: The present invention relates to alloys in which the essential constituent is aluminum, metal deposits produced from these alloys, substrates coated with these alloys and the applications of these alloys. The alloys of the present invention are characterized in thatthey have the following atomic composition (I):Al.sub.a Cu.sub.b Co.sub.b' (B,C).sub.c M.sub.d N.sub.e I.sub.f(I)a+b+b'+c+d+e+f=100, expressed as number of atoms, a.gtoreq.50, 0.ltoreq.b<14, 0.ltoreq.b'.ltoreq.22, 0<b+b'.ltoreq.30, 0.ltoreq.c.ltoreq.5, 8.ltoreq.d.ltoreq.30, 0.ltoreq.e.ltoreq.4, f.ltoreq.2, where M represents one or more elements chosen from Fe, Cr, Mn, Ni, Ru, Os, Mo, V, Mg, Zn and Pd; N represents one or more elements chosen from W, Ti, Zr, Hf, Rh, Nb, Ta, Y, Si, Ge and the rare earths; I represents the inevitable production impurities;and they contain at least 30% by mass of one or more quasicrystalline phases.Type: GrantFiled: April 5, 1995Date of Patent: July 29, 1997Assignee: Centre National de la RechercheInventors: Jean-Marie Dubois, Antoine Pianelli
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Patent number: 5641921Abstract: This invention is directed toward a material which is used to coat or create a surface for machine cutting tools, all types of drill bit teeth, saw teeth, bearing surfaces valve seats, nozzles and the like, thereby producing surfaces which are highly abrasion and erosion resistant. Furthermore, this invention includes some of the possible methods for producing such a material given that the methods and apparatus required provide a significant cost reduction over those required for producing prior art surface materials with similar abrasion and erosion resistant properties. More specifically, the material set forth can be formed at relatively low temperatures and relatively low pressures by sintering mixtures for a relatively short period of time.Type: GrantFiled: August 22, 1995Date of Patent: June 24, 1997Assignee: Dennis Tool CompanyInventors: Mahlon Denton Dennis, Barton Hampshire
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Patent number: 5623724Abstract: A ceramic capacitor suitable for high energy density and high temperature application is disclosed. Such a capacitor is prepared by producing the selected ceramic powder via the sol-gel process forming the capacitor to the desired shape with the resulting powder using tape casting technology and firing the "green" form so produced.Type: GrantFiled: August 9, 1994Date of Patent: April 22, 1997Assignee: Northrop Grumman CorporationInventors: Stephen R. Gurkovich, Kenneth C. Radford, Deborah P. Partlow
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Patent number: 5620532Abstract: In a method for manufacturing Nb.sub.3 Al phase by a diffusion reaction of Nb.sub.2 Al phase and Nb phase, a part of the Nb.sub.2 Al phase is remained and dispersed in the Nb.sub.3 Al phase homogeneously as for magnetic flux pinning centers for a high magnetic field. As for a method for dispersing the Nb.sub.2 Al phase homogeneously, a Nb.sub.3 Al group superconducting precursory composition obtained by dispersing Nb particles and Nb.sub.2 Al ultrafine particles by a mechanical alloying method is used, and further, by a conventional method for generating Nb.sub.3 Al phase by a diffusion reaction of Nb and an aluminum alloy, A Nb.sub.3 Al group superconductor can be achieved.Type: GrantFiled: June 6, 1995Date of Patent: April 15, 1997Assignee: Hitachi, Ltd.Inventors: Naofumi Tada, Fumio Iida, Ryukichi Takahashi, Takaaki Suzuki
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Patent number: 5613181Abstract: A co-sintered ceramic substrate structure is formed through punching and screening of a plurality of ceramic green sheets with a plurality of composite metal pastes and/or inks and laminating the structure. The co-sintered surface metallization comprises dual screened composite metal pastes, one on top of the other and bonded to the sintered ceramic substrate to provide bonding of the surface metallization to the sintered ceramic substrate.Type: GrantFiled: December 21, 1994Date of Patent: March 18, 1997Assignee: International Business Machines CorporationInventors: Govindarajan Natarajan, Srinivasa S. N. Reddy
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Patent number: 5564064Abstract: A method for forming a gas-filled consolidated metal billet, involving preparing a metallic shell container, filling the shell with a metal core material and pressurized gas, and consolidating the shell and its contents to form the billet. The consolidated billet is further formed in the same manner as solid metal components by conventional wrought mill working technologies. After thus forming a shaped billet having a predetermined, desired geometry, it is subjected to a heat treatment that expands the gas trapped within the core, to produce in situ a metal body having an integral sandwich-type structure with a solid metal facing and a porous metal core.Type: GrantFiled: February 3, 1995Date of Patent: October 8, 1996Assignee: McDonnell Douglas CorporationInventor: Ricky L. Martin
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Patent number: 5564063Abstract: A method for manufacture of at least one micronozzle in an aerostatic bearing, wherein at least one hole is placed into a compacted bearing surface from porous sintered material by means of a laser beam and disposed so as to be distributed across the surface. The holes distributed across the compacted bearing surface constitute micronozzles of an aerostatic bearing.Type: GrantFiled: February 2, 1995Date of Patent: October 8, 1996Assignee: Joachim HeinzlInventors: Joachim Heinzl, Michael Muth, Bernd Schulz
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Patent number: 5561827Abstract: A nickel-base superalloy article has a coating having a composition, in weight percent, of from about 10 to about 20 percent cobalt, from about 14 to about 25 percent chromium, from about 2 to about 12 percent aluminum, from 0 to about 0.2 percent yttrium, from about 0.001 to about 3 percent boron, from about 1 to about 10 percent silicon, balance nickel and incidental impurities. The coating is preferably applied by mixing together two powders, one with a higher solidus temperature and one with a lower solidus temperature, whose net composition is that of the coating. The powder mixture is compacted with a binder, applied to a surface of the article, and heated to a temperature above the lower solidus temperature.Type: GrantFiled: December 28, 1994Date of Patent: October 1, 1996Assignee: General Electric CompanyInventors: Jim D. Reeves, David E. Budinger, Robert A. Anderson
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Patent number: 5553371Abstract: A friction plate in the shape of a disc is used in a clutch device to transfer a rotational torque from a driving member to a driven member and has frictional thin films on its side surface. These films are formed by spraying particulate materials on the side surfaces of the friction plate. According to the present invention the thin films are compressed by a compression roller arranged on the way of a path for feeding the metal strip having the thin film on its side surfaces.Type: GrantFiled: May 24, 1995Date of Patent: September 10, 1996Assignee: Aisin Seiki Kabushiki KaishaInventors: Ryuichi Uchino, Tadashi Higuchi, Takaaki Nakano, Shigenobu Tara
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Patent number: 5540882Abstract: The invention concerns a method relating to powder metallurgical manufacturing of a body having a through hole, for example a hollowed tool blank or thick-walled tube. The characteristic feature of the method is that in an outer capsule there is provided a tube (6) having substantially the same length as the capsule, so that the tube extends substantially through the entire length of the capsule, that in the tube there is provided a core (5) which also extends through the capsule and the entire length of the tube, that the space between the tube (6) and the inner side of the capsule (1) is filled with a metal powder (9) which shall form the desired body, that the space (10) in the tube (6) between the core (5) and the inner side of the tube is filled with a non-metallic powder (11), that the capsule is closed hermetically, and that the closed capsule and its content is subjected to hot isostatic compaction at a temperature exceeding 1000 C., so that the metal powder is compacted to complete density.Type: GrantFiled: April 7, 1995Date of Patent: July 30, 1996Assignee: Erasteel Kloster AktiebolagInventor: Per Billgren
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Patent number: 5534219Abstract: A method for producing a multifilamentary superconductor containing niobium-tin (Nb.sub.3 Sn). A fully bonded niobium/copper composite billet is formed having a plurality of longitudinally extending channels which are symmetrically distributed with reference to transverse cross-sections of the billet, each channel being filled with an inert removable filler material. The inert filler material is removed to open the longitudinally extending channels in the billet. Tin or a tin alloy is inserted into the channels, and the niobium/copper composite billet with the inserted tin or tin alloy is cold drawn to the desired final dimensions. The drawn composite is then heated to effect in situ formation of the niobium-tin.Type: GrantFiled: May 27, 1994Date of Patent: July 9, 1996Assignee: Oxford Instruments Inc.Inventors: William G. Marancik, Seungok Hong, Rouyi Zhou
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Patent number: 5531955Abstract: Process of imparting conductivity to a three-dimensional net-shaped porous sheet can be performed efficiently before carrying out electroplating process. Fine metallic powders are applied to the porous sheet made of a foamed sheet, a nonwoven sheet, a mesh sheet or a plurality of sheets layered one on the other, so that a conductive metallic layer is formed on the porous sheet. Then, an electroplated layer is formed on the surface of the conductive metallic layer. The conductive metallic layer remains when the porous sheet burned out. Consequently, a metallic layer of the conductive metallic layer and the electroplated layer forms the metallic framework of the metallic porous sheet.Type: GrantFiled: February 8, 1995Date of Patent: July 2, 1996Assignee: Katayama Special Industries, Ltd.Inventor: Hirofumi Sugikawa
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Patent number: 5531957Abstract: A mounting object comprises a combination of a mounting object body wherein engaging portions of fastener elements of a metallic heat-resistant two-dimensional fastener are projected outside from a mounting surface, and base portions are embedded and integrally molded, and a mating fastener element base object wherein mating fastener elements in detachably engagement with said fastener elements are projected and integrally molded. Said mounting object body is obtained as a heat-resistant material integral with a metallic two-dimensional fastener by covering and fixing part of the fastener elements of the metallic two-dimensional fastener with a carbon powder having a high melting temperature and covering bases thereof with a metallic powder, a ceramics powder or a mixed powder of them to mold and sinter it.Type: GrantFiled: April 12, 1995Date of Patent: July 2, 1996Assignee: National Aerospace Laboratory of Science & Technology AgencyInventors: Osamu Okamoto, Teruomi Nakaya
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Patent number: 5531956Abstract: A method for producing a ribbed electrode for a fuel cell including the steps of depositing a suspension of a powdered electrode metal onto the face of a substantially flat porous electrode metal substrate, forming a plurality of raised structures on the face of the electrode, and sintering the electrode.Type: GrantFiled: April 27, 1995Date of Patent: July 2, 1996Assignee: Institute of Gas TechnologyInventors: Estela T. Ong, Nellie Burton-Gorman
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Patent number: 5523170Abstract: An article with a high temperature superalloy body having a directionally oriented microsuucture and a structural discontinuity, such as a crack, or surface erosion or wear portion, is repaired, to provide a repaired article, using a mixture of Ni base ahoy powders. One powder includes a careful balance of the temperature depressants Si and B. In the one powder, Si is included in the range of about 0.05-2.2 wt. % to provide about 0.02-1.3 wt. % Si in a repaired portion as bonded with the article. In that same powder, B is include in the range of about 0.2-1.2 wt. % to provide about 0.08-0.7 wt. % in that repaired portion. In the repair method, the repaired portion can be provided, when shorter brazing times are used, with improved mechanical properties by diffusing the brazed alloy and aging the repaired structure in the range of about 1600.degree.-1700.degree. F. for a time in the range of about 1-16 hours.Type: GrantFiled: December 28, 1994Date of Patent: June 4, 1996Assignee: General Electric CompanyInventors: David E. Budinger, Jim D. Reeves, Robert A. Anderson
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Patent number: 5521016Abstract: Subject boron carbide to a passivation treatment at a temperature within a range of 1350.degree. C. to less than 1800.degree. C. prior to infiltration with a molten metal such as aluminum. This method allows control of kinetics of metal infiltration and chemical reactions, size of reaction products and connectivity of B.sub.4 C grains and results in cermets having desired mechanical properties.Type: GrantFiled: January 24, 1995Date of Patent: May 28, 1996Assignee: The Dow Chemical CompanyInventors: Aleksander J. Pyzik, Uday V. Deshmukh, Stephen D. Dunmead, Jack J. Ott, Timothy L. Allen, Harold E. Rossow
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Patent number: 5518383Abstract: To manufacture a reflector formed by a reflective metallic layer on a metallic matrix composite support, a metallic layer having a reflective surface whose shape is at least approximately identical to the required geometrical shape is disposed on a mold surface having a geometrical shape complementary to the required geometrical shape of the reflector. Fibers to constitute the composite support are draped on the metallic layer. They are metallized by the metallic or intermetallic material to form the metallic matrix. This layer and the metallized fibers are subjected to temperature and pressure conditions adapted to press the reflective surface strongly against the mold surface and to cause diffusion welding of the layer with the metallized fibers and of the metallized fibers with themselves so as to integrate the layer to the composite support during consolidation of the latter.Type: GrantFiled: May 9, 1994Date of Patent: May 21, 1996Assignee: Aerospatiale Societe Nationale IndustrielleInventor: Henri Abiven
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Patent number: 5518683Abstract: A metal alloy article is proved with an improved fretting wear resistant coating combination for use in the temperature range of about 650.degree.-1100.degree. F. on an article contact surface shaped to cooperate with an abutting member. An example is a gas turbine engine blade base carried by an abutting support slot. The coating combination includes an inner portion of a Ni base alloy having a room temperature annealed yield strength of greater than about 30 ksi to less than about 57 ksi and densely deposited from a powder, for example by the high velocity oxygen--fuel thermal spray process rather than by other processes such as air plasma spray. Cured on the inner portion is an outer portion of graphite particles mixed in an inorganic binder capable of stable use in the range of about 650.degree.-1100.degree. F., for example silicates or phosphates, such as of aluminum.Type: GrantFiled: February 10, 1995Date of Patent: May 21, 1996Assignee: General Electric CompanyInventors: Kevin P. Taylor, Jerry D. Schell
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Patent number: 5516483Abstract: A process of forming a sintered article for powder metal comprising blending carbon and ferro alloys and lubricant with compressible elemental iron powder, pressing said blended mixture to form sintering said article, and then high temperature sintering said article in a reducing atmosphere to produce a sintered article having a high density from a single compression.Type: GrantFiled: February 8, 1994Date of Patent: May 14, 1996Assignee: Stackpole LimitedInventors: Rohith Shivanath, Peter Jones, Danny T. D. Thieu
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Patent number: 5514326Abstract: In order to form internal conductors of a multilayer ceramic electronic component such as a multilayer ceramic capacitor, copper paste containing copper powder having a mean particle size of 0.3 to 2 .mu.m in a particle size range of 0.1 to 4 .mu.m and ceramic powder having a main component which is common to that of a ceramic material contained in the multilayer ceramic electronic component and being in a particle size range of 0.5 to 8 .mu.m, as well as an organic vehicle and a solvent with the contents of the copper powder and the ceramic powder and the total content of the organic vehicle and the solvent in ranges of 40 to 70 percent by weight, 1 to 15 percent by weight and 25 to 60 percent by weight respectively is applied onto ceramic green sheets. The ceramic green sheets provided with such copper paste films are stacked and fired so that occurrence of voids in the laminate and deformation of the laminate are suppressed in the as-obtained multilayer ceramic electronic component.Type: GrantFiled: November 14, 1994Date of Patent: May 7, 1996Assignee: Murata Manufacturing Co., Ltd.Inventors: Hiroji Tani, Kazuhito Ohshita, Mitsuyoshi Nishide
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Patent number: 5482671Abstract: A method is provided for manufacturing interlocking parts, in which at least one part is manufactured by powder injection molding. To compensate for the amount of contraction of one of the parts manufactured by powder injection molding and, if desired, to produce an additional clearance, a separation layer of plastic material is applied between the interlocking parts. After the injection process to form the separation layer, the separation layer and the binder are removed by a binder-removing and sintering process step. The method is also applicable to powdered metal extrusion for manufacture of double-layered metal parts.Type: GrantFiled: September 23, 1994Date of Patent: January 9, 1996Assignee: fischerwerke, Artur Fischer GmbH & Co. KGInventor: Wilfried Weber
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Patent number: 5476632Abstract: A process of forming a sintered article of powder metal comprising: selecting elemental iron powder; determining the desired properties of said sintered article and selecting, a quantity of carbon, and ferro alloy from the group of ferro manganese, ferro chromium, ferro molybdenum, ferro vanadium, ferro silicon and ferro boron; grinding said ferro alloy to a mean particle size of approximately 8 to 12 microns; introducing a lubricant while blending the carbon, ferro alloy, with said elemental iron powder; pressing the mixture to form the article; and then high temperature sintering the article at a temperature between 1,250.degree. C. and 1,350.degree. C. in a neutral or reducing atmosphere; so as to produce the sintered article of powdered metal; and includes the product formed thereby.Type: GrantFiled: January 14, 1994Date of Patent: December 19, 1995Assignee: Stackpole LimitedInventors: Rohith Shivanath, Peter Jones
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Patent number: 5474736Abstract: A method for manufacturing tubes filled with powdery and/or granular substances comprising the steps of forming a metal strip into a tube, feeding powdery and/or granular substances into the tube being formed as a core, joining together the edges of the tube filled with the core of the powdery and/or granular substances by high-frequency welding, and reducing the diameter of the welded tube filled with the core of the powdery and/or granular substances. At least the top layer of the core in the tube is composed of powdery and/or granular substances having low enough magnetic susceptibility to remain unattracted to the magnetized tube edges that is determined based on the welding heat input.Type: GrantFiled: September 23, 1993Date of Patent: December 12, 1995Assignee: Nippon Steel Welding Products & Engineering Co., Ltd.Inventors: Nobuo Araki, Takeji Kagami, Toru Ono, Iwao Yamada, Seiji Hashimoto
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Patent number: 5470524Abstract: A method is provided for manufacturing a bladed ring for drum-shaped rotors of turbomachinery, especially rotors for axial compressors of gas turbine engines. The bladed ring is to be manufactured by hot isostatic pressing (HIP) and the fiber rings are formed in a metallic powder material for the bladed ring arranged in a circumferential direction. The fiber rings are bonded with spacing therebetween. The fiber rings are reinforced by fibers embedded in a metal matrix. The bladed ring prefabricated in this fashion by HIP is machined down to its required dimensions.Type: GrantFiled: June 14, 1994Date of Patent: November 28, 1995Assignee: MTU Motoren- Und Turbinen-Union Muenchen GmbHInventors: Wolfgang Krueger, William Wei
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Patent number: 5455000Abstract: The invention provides a method for in-situ powder metallurgy processing of a functionally gradient material (FGM) which uses a preceramic polymer binder system with the metal and/or ceramic powders used to produce the intermediate layers of the composite. The invention also provides a method for controlling shrinkage of the functionally gradient material during processing while still preserving the desired density of the intermediate layers by controlling the preceramic polymer binder content within the functionally gradient material.Type: GrantFiled: July 1, 1994Date of Patent: October 3, 1995Assignee: Massachusetts Institute of TechnologyInventors: Dietmar Seyferth, Pawel Czubarow
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Patent number: 5447680Abstract: Microcracks in fiber-reinforced/titanium aluminide matrix composite materials are inhibited by employing a matrix comprising a titanium aluminide alloy having (1) from ten to twelve atomic percent niobium and (2) a critical admixture of from two to six atomic percent of a member selected from a group consisting of molybdenum, tungsten and vanadium. The tendency of the fiber/matrix interfacial reaction to increase the stability of the Alpha 2 phase in the matrix adjacent to the interface and the tendency to form a "beta phase depletion zone" are unexpectedly negated. Suppression of the beta depletion zone formation inhibits the formation and growth of interfacial microcracks, and allows the fabrication of crack-free titanium matrix composite materials. The need for an extraneous beta phase stabilization treatment at the fiber/matrix interface is eliminated.Type: GrantFiled: March 21, 1994Date of Patent: September 5, 1995Assignee: McDonnell Douglas CorporationInventor: David M. Bowden
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Patent number: 5435965Abstract: A sputtering target is disclosed which includes a backing member of a cylindrical shape and a target material bonded onto an outer peripheral surface of the backing member by hot isostatic pressing. A method for manufacturing a sputtering target is also disclosed. First, a cylindrical backing member is inserted into a mold such that a space is defined between the backing member and the mold. A target material is then filled into the space between the backing member and the mold, and the mold is sealed. Thereafter, the target material and the backing member are subjected to hot isostatic pressing.Type: GrantFiled: February 19, 1992Date of Patent: July 25, 1995Assignee: Mitsubishi Materials CorporationInventors: Munenori Mashima, Jun Tamura
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Patent number: 5429791Abstract: An article and method of manufacture of a (Bi,Pb)--Sr--Ca--Cu--O superconductor comprisingcalcinating powders of superconductor precursors of PbO, Bi.sub.2 O.sub.3, SrCO.sub.3 or SrO, CaCO.sub.3 or CaO in air to obtain a 2223 superconductor lump and second phases;crushing the lump into powder;molding the powder into a superconductor body;disposing the body within silver powder to form a composite;molding the composite;heat treating the composite to increase the bond strength of the silver powder; andworking the composite into a useable shape by rolling and drawing while applying intermediate and final heat treatments to obtain a final product.Type: GrantFiled: June 23, 1994Date of Patent: July 4, 1995Assignees: Korea Atomic Energy Research Institute, Korea Electric Power CorporationInventors: Hee-Gyun Lee, Seon-Chil Kweon, Dong-Yeon Won, Gye-Won Hong
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Patent number: 5429876Abstract: Disclosed is a copper-lead based bearing material having excellent corrosion resistance, comprising a steel back metal and a bearing layer of a copper-lead based bearing alloy, the latter consisting essentially, by weight, 0.5 to 10% Bi, 0.5 to 8% Sn, 15 to 30% Pb, 2 to 10% Ni, not greater than 0.2% P, the balance Cu and incidental impurities.By adding Bi in a copper-lead based bearing alloy it becomes possible to obtain excellent corrosion resistance without impairing the conformability and seizure resistance of the bearing material in comparison with the conventional copper-lead based bearing alloys.Type: GrantFiled: April 12, 1994Date of Patent: July 4, 1995Assignee: Daido Metal Company Ltd.Inventors: Tadashi Tanaka, Masaaki Sakamoto, Koichi Yamamoto, Tsukimitsu Higuchi
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Patent number: 5424138Abstract: A copper-alloy slide bearing for a low-rigidity housing having a three-layer structure of a steel back-metal, a copper-alloy layer and an overlay, the back metal containing 0.03 to 0.26% by weight of carbon. During the production of the slide bearing, a bimetal is prepared in such a manner that a back-metal portion is rolled at a total rolling reduction of 10 to 35%, and the resultant bimetal is heat-treated at a relatively low temperature, so that the slide bearing includes a back metal having a 0.01% elastic limit of not less than 300 N/mm.sup.2. When the copper-alloy slide bearing is used in a low-rigidity housing of an internal combustion engine, the slide bearing is capable of more excellently following the deformation of the housing, as well as capable of providing more excellent intimate contact and more excellent fretting resistance, than a conventional multi-layer slide bearing.Type: GrantFiled: October 26, 1993Date of Patent: June 13, 1995Assignee: Daido Metal Co., Ltd.Inventors: Tadashi Tanaka, Masaaki Sakamoto, Koichi Yamamoto, Tsukimitsu Higuchi
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Patent number: 5415833Abstract: A method for forming molten carbonate fuel cell (MCFC) anodes by adjusting the reaction condition of pack cementation is disclosed. The method includes the steps of embedding a base metal sheet containing at least Ni in a pack containing alloy metal powder, an activator and a filler, pre-heating the pack to remove the organic material included in the base metal sheet, and maintaining the pack under a H.sub.2 /N.sub.2 atmosphere at a temperature of 500.degree. C. to 800.degree. C. for one to eight hours to form a Ni alloy. The method has a simplified procedure and is very useful to manufacture MCFC anodes having a very low creep deformation rate while porosity is in an appropriate range.Type: GrantFiled: March 31, 1994Date of Patent: May 16, 1995Assignee: Samsung Electronics Co., Ltd.Inventors: Ho-jin Kweon, Hai-soo Chun, Ha-chull Chung, Je-hong Youn, Gwun-pil Park
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Patent number: 5415831Abstract: The method serves to produce a material based on a doped intermetallic compound. In carrying out the method, at least two differently doped powders each based on the intermetallic compound are selected. One of the two powders predominantly has coarse-grained particles. On the other hand, another powder is formed from comparatively fine-grained particles composed of a material having a lower creep strength but a higher ductility than the material of the coarse-grained powder. The at least two powders are mixed with one another in a ratio serving to establish a desired mixed microstructure and then hot-compacted and heat-treated to form the material.Material produced by this method is suitable for components which are exposed to high mechanical loads at high temperatures, such as, in particular, gas-turbine blades or turbine wheels of turbo chargers.Type: GrantFiled: December 13, 1993Date of Patent: May 16, 1995Assignee: ABB Research Ltd.Inventors: Robert Baumann, Joachim Rosler, Christoph Tonnes
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Patent number: 5405571Abstract: A fiber reinforced composite tape is made by casting a mixture comprising high temperature metal or intermetallic particles, substantially continuous ceramic fibers and a polymeric binder. The particles are preferably titanium alloy or titanium aluminide particles having a top size of greater than about 50 microns and the binder is preferably a polyisobutylene. The cast composite tape is combined with other tapes, heated in a vacuum to remove the binder and pressed at an elevated temperature and pressure to form a composite structure suitable for high temperature applications.Type: GrantFiled: November 8, 1993Date of Patent: April 11, 1995Assignee: Aluminum Company of AmericaInventors: William G. Truckner, Jon F. Edd
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Patent number: 5403670Abstract: The crack-resistant compound sleeve roll having a shell portion made of a sintered alloy and a core portion made of steel is produced by (a) charging an alloy powder consisting essentially, by weight, of 1.0-3.5% of C, 2% or less of Si, 2% or less of Mn, 10% or less of Cr, 3.0-15.0% of W, 2.0-10.0% of Mo and 1.0-15.0% of V, the balance being substantially Fe and inevitable impurities, into a metal capsule disposed around a roll core; (b) after evacuation and sealing, subjecting the alloy powder to a HIP (hot isostatic pressing) treatment at 1100.degree.-1300.degree. C. to form a shell portion; (c) after removing the metal capsule, subjecting the sintered shell portion to a heat treatment having hardening at 1140.degree.-1220.degree. C. and annealing at 540.degree.-620.degree. C.; and (d) chamfering edge portions of the roll on both axial ends thereof such that a boundary of the shell portion and the core portion exists in a chamfered surface.Type: GrantFiled: December 21, 1993Date of Patent: April 4, 1995Assignee: Hitachi Metals, Ltd.Inventors: Takuya Ohsue, Akira Noda, Hiroshi Fukuzawa, Itsuo Korenaga
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Patent number: 5399438Abstract: Disclosed is a stainless steel member with a high corrosion resistance suitable for a structural member used in highly corrosive environments, such as an edge seal plate of a molten carbonate fuel cell. This stainless steel member includes a base material consisting of stainless steel containing chromium, and a corrosion-protective layer formed on the surface of the base material. In this corrosion-protective layer, a granular heterophase containing chromium is precipitated in an ordered alloy consisting of aluminum and the constituent elements of the base material.Type: GrantFiled: September 14, 1993Date of Patent: March 21, 1995Assignee: Kabushiki Kaisha ToshibaInventors: Hiroshi Tateishi, Kiyoshi Imai, Hideyuki Ohzu, Kazuaki Nakagawa, Yoshihiro Akasaka
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Patent number: 5399312Abstract: A process for fabricating Thallium-based superconducting tapes comprising the steps of: (1) preparing a powder mixture having a nominal composition of (Tl.sub.1-x-y Bi.sub.y Pb.sub.z)(Ba.sub.2-z Sr.sub.z)Ca.sub.2 Cu.sub.3 O.sub.9 ; (2) placing the powder mixture into a silver tube and drawing and/or swaging the silver tube containing the powder mixture into a wire having a pre-determined diameter, wherein x and y are real numbers between 0.2 and 0.4, and z is a real number between 0 and 2; (3) rolling the wire into a tape having a pre-determined thickness; and (4) subjecting the tape to a two-stage single-sintering process at two respective sintering temperatures. The two-stage single-sintering process of the present invention allows Thallium-based superconducting tapes to be fabricated which exhibit substantially increased critical current density, without causing a substantially increased cost and complexity, as do other prior art processes, such as the double-sintering process.Type: GrantFiled: October 4, 1993Date of Patent: March 21, 1995Assignee: Industrial Technology Research InstituteInventors: Ru-Shi Liu, Sheng-Feng Wu, Chung-Ho Tai, Der-Shiuh Shy
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Patent number: 5397050Abstract: A method of producing a sputter target assembly including a tungsten-titanium target attached to a titanium backing plate. The method includes consolidating a tungsten-titanium powder composition to form a target while simultaneously bonding the powder composition to the titanium backing plate to form an interdiffusion-type bond between the target and the backing plate such that the target assembly possesses extremely high temperature operating capability.Type: GrantFiled: October 27, 1993Date of Patent: March 14, 1995Assignee: Tosoh SMD, Inc.Inventor: John J. Mueller
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Patent number: 5384088Abstract: Wire, bulk, film, etc. of a superconductive material is manufactured from a powdery precursor. The superconductive material has a superconductive crystal of 1223 phase and/or 1234 phase as a main component, and the powdery precursor comprises at least 1212 phase as a main component.Type: GrantFiled: October 23, 1992Date of Patent: January 24, 1995Assignees: Hitachi Cable, Ltd., Hitachi Ltd.Inventors: Junichi Sato, Masahiro Seido, Akira Nomoto, Tomoichi Kamo, Katsuzo Aihara
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Patent number: 5376462Abstract: A thixoformable material and a method for forming it are provided in which the material comprises a series of sequentially deposited layers of substantially metallic material, at least some of the layers having different properties. The layers may be of different materials or the layers may differ in that some are provided with reinforcing material whereas other are not. The reinforcing material may consist of particles of spherical, fiberous or other shapes and may be made of various carbides or other suitable reinforcing materials.The thixoformable material may be formed in sheets, cylindrical forms or any other shape and subsequently cut to the volume and/or shape required for the forming stage.A layered material of this sort offers the advantages of thixoformable materials but with enhanced toughness and damage resistance due to the layered 3-dimensional structure.Type: GrantFiled: May 18, 1993Date of Patent: December 27, 1994Assignee: Lucas Industries public limited companyInventor: Peter R. G. Anderson