Alkali Metal Patents (Class 423/499.1)
  • Patent number: 11384288
    Abstract: A method for forming mesophase pitch can include applying a stimulus to a first amount of coal tar to form a first amount of mesophase pitch. The stimulus can include one or more of an electromagnetic field (“EMF”) or a magnetic field. The method can further include evaluating a characteristic of the first amount of mesophase pitch, changing a parameter of the stimulus in response to evaluating the characteristic of the first amount of mesophase pitch, and applying the stimulus exhibiting the changed parameters to a second amount of coal tar to form mesophase pitch.
    Type: Grant
    Filed: March 20, 2020
    Date of Patent: July 12, 2022
    Assignee: CARBON HOLDINGS INTELLECTUAL PROPERTIES, LLC
    Inventor: Charles Agee Atkins
  • Patent number: 11038198
    Abstract: Provided is a solid electrolyte having a high ion conductivity and excellent in battery performance not going through a step of removing water such as a drying step, while simplifying the production process and reducing the production cost. Specifically, provided is a method for producing a sulfide-based solid electrolyte, including causing a reaction of an alkali metal sulfide and a specific substance in a solvent.
    Type: Grant
    Filed: March 14, 2017
    Date of Patent: June 15, 2021
    Assignee: IDEMITSU KOSAN CO., LTD.
    Inventors: Takeshi Makino, Hiroaki Yamada
  • Patent number: 10050284
    Abstract: Disclosed is a process for one-step preparing electrolyte used for lithium-iron(II) disulfide batteries. The process includes the following steps of: adding iodine-containing precursors into an organic solvent in an inert atmosphere, homogeneously stirring, then adding lithium-containing precursors, stirring and reacting, separating solids to obtain an electrolyte used for lithium-iron(II) disulfide batteries. The process involves one-step synthesizing electrolyte used for lithium-iron(II) disulfide batteries. The whole procedures do not introduce water and have a lower cost. The lithium-iron(II) disulfide batteries prepared by using the electrolyte prepared by the process of the present invention have better properties.
    Type: Grant
    Filed: March 31, 2016
    Date of Patent: August 14, 2018
    Assignee: EVE ENERGY CO., LTD.
    Inventors: Yuan Zhu, Chen Cheng, Yanbin Wang, Jianhua Liu, Jincheng Liu
  • Patent number: 9566301
    Abstract: Methods and compositions for treating various indications by lessening oxidative stress in a patient are provided. A pharmaceutical composition comprises between about 0.001% to about 10.0%), or more specifically between about 0.015% to about 5%, sodium iodine or catalase by weight. The iodine ion or the catalase dissociates hydrogen peroxide into water and molecular oxygen to interrupt biological events that result in negative side effects. The pharmaceutical composition further comprises in some cases a reducing agent or various carrier materials. The pharmaceutical composition is in some cases formulated for a variety of delivery methods.
    Type: Grant
    Filed: March 28, 2013
    Date of Patent: February 14, 2017
    Assignee: CXL OPHTHALMICS, LLC
    Inventors: Roy S. Rubinfeld, Raymond A. Hartman, Sandy T. Feldman
  • Patent number: 9149434
    Abstract: The present invention provides a core particle for a pharmaceutical preparation which features the requisite properties of a core particle, and which has enough chemical stability, and in which reactivity with the drug (an active pharmaceutical ingredient) is limited or prevented. More specifically, the present invention relates to a core particle wherein a film containing an active pharmaceutical ingredient can be formed on the surface thereof, and (1) the core particle comprises a pharmaceutically acceptable inorganic material, (2) the inorganic material is poorly soluble in water, and (3) pH of a solution of the inorganic material is 5 to 8.
    Type: Grant
    Filed: September 8, 2008
    Date of Patent: October 6, 2015
    Assignee: TOMITA PHARMACEUTICAL CO., LTD.
    Inventors: Masashi Konishi, Shouichi Oonishi, Akira Ookubo, Masashi Yunoki, Ariumi Kawamoto, Kanako Hattori
  • Patent number: 8926861
    Abstract: The present invention relates to a hydrogen-storing composite material which is convertible essentially reversibly between a storing state and a non-storing state, wherein the reaction enthalpy in this conversion reaction can be set in a targeted manner to a value between 15 and 80 kJ/mol of H2, preferably 25 to 40 kJ/mol of H2.
    Type: Grant
    Filed: October 30, 2008
    Date of Patent: January 6, 2015
    Assignee: Helmholtz-Zentrum Geesthacht Zentrum für Material—und Küstenforschung GmbH
    Inventors: Nico Eigen, Martin Dornheim, Rüdiger Bormann
  • Publication number: 20140341798
    Abstract: A method of reacting amine compounds with halons and perhalogenated compounds, resulting in the conversion of these ozone-depleting species into non-volatile salts and a variety of other amine derivatives is disclosed.
    Type: Application
    Filed: March 18, 2014
    Publication date: November 20, 2014
    Inventor: Dru L. DeLaet
  • Patent number: 8784900
    Abstract: Methods and products are provided for treating a wound or infection in a mammal or disinfecting a surface with a hypochlorous acid solution that has been activated by a catalyst. Additionally provided is a process for preparing an antimicrobial product that produces an activated hypochlorous acid solution for use as an antimicrobial.
    Type: Grant
    Filed: March 13, 2008
    Date of Patent: July 22, 2014
    Assignee: Oculus Innovative Sciences, Inc.
    Inventor: Robert Northey
  • Patent number: 8784755
    Abstract: Aspects of the present invention relate to a process to obtain potassium chloride that includes submitting brine to concentration, separating brine after concentration, resulting in a first solid content and a first liquid content, cooling the first liquid content, separating the first liquid content after cooling, thus resulting in a second solid content and a second liquid content, enriching the second solid content, and separating the second solid content after enrichment, thus resulting in a third solid content and a third liquid content. Aspects of this process are environmentally safe, as the process includes stages using solvents and equipment which does not harm the environment. Moreover, aspects of this process present a significant energy consumption reduction.
    Type: Grant
    Filed: February 17, 2012
    Date of Patent: July 22, 2014
    Assignee: Vale S.A.
    Inventors: Flavio Marcio de Lima Faria, Marcus de Castro Carvalho Simoes, Antonio F. Pessoa
  • Patent number: 8764965
    Abstract: Electrochemical processes to convert alkali sulfates into useful chemical products, such as syngas, alkali hydroxide, and sulfur are disclosed. An alkali sulfate is reacted with carbon to form carbon monoxide and alkali sulfide. In one embodiment, the alkali sulfide is dissolved in water and subjected to electrochemical reaction to form alkali hydroxide, hydrogen, and sulfur. In another embodiment, the alkali sulfide is reacted with iodine to form alkali iodide sulfur in a non-aqueous solvent, such as methyl alcohol. The alkali iodide is electrochemically reacted to form alkali hydroxide, hydrogen, and iodine. The iodine may be recycled to react with additional alkali sulfide. The hydrogen and carbon monoxide from both embodiments may be combined to form syngas. The alkali hydroxide from both embodiments may be recovered as a useful industrial chemical.
    Type: Grant
    Filed: January 27, 2012
    Date of Patent: July 1, 2014
    Assignee: Ceramatec,Inc.
    Inventor: Ashok V. Joshi
  • Publication number: 20140170041
    Abstract: The invention generally relates to methods of removing potassium, rubidium, and/or cesium, selectively or in combination, from brines using tetrafluoroborates. Also disclosed are methods of producing potassium, rubidium, and/or cesium chlorides using ionic liquids and exchange media. This invention also generally relates to treated geothermal brine compositions containing reduced concentrations of silica, iron, and potassium compared to the untreated brines. Exemplary compositions of the treated brine contain a concentration of silica ranging from about 0 mg/kg to about 15 mg/kg, a concentration of iron ranging from about 0 mg/kg to about 10 mg/kg, and a concentration of potassium ranging from about 300 mg/kg to about 8500 mg/kg. Other exemplary compositions of the treated brines also contain reduced concentrations of elements like rubidium, cesium, and lithium.
    Type: Application
    Filed: February 24, 2014
    Publication date: June 19, 2014
    Applicant: Simbol Inc
    Inventors: Stephen Harrison, C.V. Krishnamohan Sharma, Raghu Bhakta, Pei-Yu Lan
  • Patent number: 8685135
    Abstract: A method forming a potassium chloride particle form potassium chloride powder having resistance to moisture absorption and shrinkage. The original feedstock comprises potassium chloride in a size distribution of 30 mesh and 100 mesh as well as a gluten based binder.
    Type: Grant
    Filed: December 3, 2012
    Date of Patent: April 1, 2014
    Assignee: Karnalyte Resources Inc.
    Inventor: Robin Phinney
  • Publication number: 20130266678
    Abstract: A thermal insulation layer for an HPHT cell, the thermal insulation layer including CsCl, CsBr, CsI, or a combination thereof, and the thermal insulation layer being electrically insulating; the thermal insulation layer including a thermal insulation sleeve and/or a thermal insulation button for an HPHT cell; a pressure transfer medium for an HPHT cell, the pressure transfer medium including CsBr, CsI or a combination thereof; and a pressure transfer medium for an HPHT cell, the pressure transfer medium including CsCl and additive, with the proviso that the additive does not include ZrO2 are disclosed. HPHT press systems that include a thermal insulation layer or a pressure transfer medium according to embodiments of the present disclosure are also disclosed.
    Type: Application
    Filed: March 14, 2013
    Publication date: October 10, 2013
    Inventors: YAHUA BAO, J. DANIEL BELNAP, STEWART N. MIDDLEMISS
  • Patent number: 8529155
    Abstract: The present invention relates to a method for making pure salt comprises recapturing post-drilling flowback water from hydro-fracturing; removing oil from the flowback water; filtering the flowback water using an ultra filter with a pore size of about 0.1 microns or less to remove solid particulates and large organic molecules, such as benzene, ethylbenzene, toluene, and xylene, from the water; concentrating the flowback water to produce a brine that contains from about 15 wt % to about 40 wt % of salt relative to the total weight of the flowback brine; performing one or more chemical precipitation process using an effective amount of reagents to precipitate out the desired high quality commercial products, such as, barium sulfate, strontium carbonate, calcium carbonate; and crystallizing the chemically treated and concentrated flowback brine to produce greater than 99.5% pure salt products, such as sodium and calcium chloride.
    Type: Grant
    Filed: March 15, 2012
    Date of Patent: September 10, 2013
    Assignee: FracPure Holdings LLC
    Inventors: Frank A. DiTommaso, Peter N. DiTommaso
  • Publication number: 20130149231
    Abstract: Aspects of the present invention relate to a process to obtain potassium chloride that includes submitting brine to concentration, separating brine after concentration, resulting in a first solid content and a first liquid content, cooling the first liquid content, separating the first liquid content after cooling, thus resulting in a second solid content and a second liquid content, enriching the second solid content, and separating the second solid content after enrichment, thus resulting in a third solid content and a third liquid content. Aspects of this process are environmentally safe, as the process includes stages using solvents and equipment which does not harm the environment. Moreover, aspects of this process present a significant energy consumption reduction.
    Type: Application
    Filed: February 17, 2012
    Publication date: June 13, 2013
    Applicant: VALE S.A.
    Inventors: Flavio Marcio de Lima FARIA, Marcus de Castro Carvalho Simoes, Antonio Francisco Cisne Pessoa
  • Patent number: 8367026
    Abstract: A method for converting depleted uranium tetrafluoride (UF4) to triuranium octaoxide (U3O8), and producing sulfur tetrafluoride, using a two step process. The first step uses heat and a mixture of the uranium tetrafluoride and an alkaline compound, either an alkaline oxide or an alkaline hydroxide, to produce U3O8 and a water-soluble metal halide. The second step uses heat, sulfur and a halogen to produce sulfur tetrafluoride and triuranium octaoxide.
    Type: Grant
    Filed: October 29, 2010
    Date of Patent: February 5, 2013
    Inventor: Bamidele A. Omotowa
  • Patent number: 8323371
    Abstract: A method forming a potassium chloride particle form potassium chloride powder having resistance to moisture absorption and shrinkage. The original feedstock comprises potassium chloride in a size distribution of 30 mesh and 100 mesh as well as a gluten based binder.
    Type: Grant
    Filed: August 12, 2009
    Date of Patent: December 4, 2012
    Assignee: Kamalyte Resources Inc.
    Inventor: Robin Phinney
  • Patent number: 8273320
    Abstract: The present invention relates to a method for making pure salt comprises recapturing post-drilling flowback water from hydro-fracturing; removing oil from the flowback water; filtering the flowback water using an ultra filter with a pore size of about 0.1 microns or less to remove solid particulates and large organic molecules, such as benzene, ethylbenzene, toluene, and xylene, from the water; concentrating the flowback water to produce a brine that contains from about 15 wt % to about 40 wt % of salt relative to the total weight of the flowback brine; performing one or more chemical precipitation process using an effective amount of reagents to precipitate out the desired high quality commercial products, such as, barium sulfate, strontium carbonate, calcium carbonate; and crystallizing the chemically treated and concentrated flowback brine to produce greater than 99.5% pure salt products, such as sodium and calcium chloride.
    Type: Grant
    Filed: March 15, 2012
    Date of Patent: September 25, 2012
    Assignee: FracPure Holdings LLC
    Inventors: Frank A. DiTommaso, Peter N. DiTommaso
  • Publication number: 20120141745
    Abstract: A chiral liquid crystal precursor composition which comprises at least one salt that changes a position of the selective reflection band exhibited by the composition in a cured state compared to the position of a selective reflection band exhibited by a composition in the cured state that does not contain the at least one salt. This abstract is neither intended to define the invention disclosed in this specification nor intended to limit the scope of the invention in any way.
    Type: Application
    Filed: December 7, 2011
    Publication date: June 7, 2012
    Applicant: SICPA HOLDING SA
    Inventors: Andrea CALLEGARI, Tristan JAUZEIN
  • Publication number: 20120104266
    Abstract: A method of producing a radiation detecting element with an improved resolution property, a radiation detecting element, a radiation detecting module, and a radiation image diagnostic apparatus are provided. The radiation detecting element includes a scintillator layer on a substrate. The scintillator layer includes a plurality of columnar crystals having substantially no irregularity on each side.
    Type: Application
    Filed: October 25, 2011
    Publication date: May 3, 2012
    Applicant: Sony Corporation
    Inventors: Nobuyuki Yokosawa, Mitsuhiro Kawanishi, Takahiro Igarashi, Ikumi Kusayama
  • Patent number: 8158098
    Abstract: Provided herein are processes for obtaining sylvinite and/or sylvite from sea water, sea bitterns and/or sea salts. The processes comprise reacting sea water, sea bitterns and/or sea salts with calcium hydroxide and/or calcium oxide.
    Type: Grant
    Filed: June 22, 2010
    Date of Patent: April 17, 2012
    Assignee: Exportadora de Sal, S.A. de C.V.
    Inventor: Abraham Sadan
  • Patent number: 8158097
    Abstract: The present invention relates to a method for making pure salt comprises recapturing post-drilling flowback water from hydro-fracturing; removing oil from the flowback water; filtering the flowback water using an ultra filter with a pore size of about 0.1 microns or less to remove solid particulates and large organic molecules, such as benzene, ethylbenzene, toluene, and xylene, from the water; concentrating the flowback water to produce a brine that contains from about 15 wt % to about 40 wt % of salt relative to the total weight of the flowback brine; performing one or more chemical precipitation process using an effective amount of reagents to precipitate out the desired high quality commercial products, such as, barium sulfate, strontium carbonate, calcium carbonate; and crystallizing the chemically treated and concentrated flowback brine to produce greater than 99.5% pure salt products, such as sodium and calcium chloride.
    Type: Grant
    Filed: June 25, 2010
    Date of Patent: April 17, 2012
    Assignee: FracPure Holdings LLC
    Inventors: Frank A. DiTommaso, Peter N. DiTommaso
  • Patent number: 8124046
    Abstract: A method for producing an alkali metal iodide salt solution including combusting a liquid for combustion so as to combust a combustible component of the liquid for combustion; and subsequently cooling a resultant gas containing a decomposition product. The method comprises the steps of (a) providing a liquid containing (i) an alkali metal iodide salt, (ii) an inorganic-salt-forming substance capable of forming, at combustion, an inorganic salt containing an alkali metal and (iii) an organic compound; (b) adding to the liquid a precipitation solvent capable of depositing the inorganic-salt-forming substance; (c) removing from the liquid the inorganic-salt-forming substance precipitated in the step (b) so as to obtain the liquid for combustion; and (d) combusting the liquid for combustion and subsequently cooling the resultant gas containing a decomposition product.
    Type: Grant
    Filed: March 11, 2008
    Date of Patent: February 28, 2012
    Assignee: Nippon Chemicals Co., Ltd.
    Inventors: Yuichiro Kinoshita, Sayaka Shiomitsu, Keisuke Takahashi
  • Publication number: 20110305905
    Abstract: To provide a low price industrial salt by reducing facility and operation costs without electro-deposition and crystallization and through reduction in quantity of chemicals used. An industrial salt S obtained by the steps of: extracting a part of combustion gas from a kiln exhaust gas passage running from an inlet end 12b of a cement kiln 12 to a bottom cyclone 13; recovering dust D from the extracted gas G2 and washing recovered dust; and drying a filtrate L1 after the washing in a gas stream. The industrial salt can be obtained by removing a calcium component from the filtrate and drying the filtrate from which the calcium component is removed in a gas stream. Further, from the filtrate can be removed sulfate radical, and drying the filtrate from which the calcium component is removed in a gas stream to obtain the industrial salt. For the drying can be used an exhaust gas discharged from a clinker cooler 12a and a spray drier 43 may be used for the drying.
    Type: Application
    Filed: April 15, 2009
    Publication date: December 15, 2011
    Inventors: Noritoshi Tamura, Shinichiro Saito, Yoshinobu Tatsumi
  • Patent number: 8038884
    Abstract: The present invention relates to process to prepare a chlorine-containing compound using an aqueous salt solution containing at least 100 g/l of sodium chloride and a contaminating amount of polyvalent cations comprising the steps of (i) preparing an aqueous salt solution containing at least 100 g/l of sodium chloride and at least 0.01 ppm of polyvalent cations by dissolving a sodium chloride source in water, (ii) adding an effective amount of at least one positive retention enhancing component to the aqueous solution, (iii) subsequently subjecting the solution to a nanofiltration step, thereby separating the solution into a retentate which is enriched for polyvalent cations and a permeate which is the purified aqueous salt solution, (iv) reacting the chloride anions in the permeate to a chlorine-containing compound by an electrolysis step, and (v) recycling at least part of the retentate to dissolution step (i).
    Type: Grant
    Filed: February 13, 2006
    Date of Patent: October 18, 2011
    Assignee: Akzo Nobel N.V.
    Inventors: Gerrald Bargeman, René Lodewijk Maria Demmer, Antoon Ten Kate, Boris Kuzmanovic, Cornelis Elizabeth Johannus Van Lare, Mateo Jozef Jacques Mayer, Maarten André Irène Schutyser, Jan Barend Westerink
  • Patent number: 8034316
    Abstract: Carbon blacks, such as rubber blacks, having a low PAH concentration are described. Furthermore, elastomeric or rubber compositions containing the carbon black of the present invention are further described, as well as methods of making carbon black having a low PAH concentration.
    Type: Grant
    Filed: November 6, 2007
    Date of Patent: October 11, 2011
    Assignee: Cabot Corporation
    Inventors: Irina S. Yurovskaya, William L. Sifleet, Steven J. List, Martin C. Green, Anand Prakash
  • Publication number: 20110198285
    Abstract: A desalination and minerals extraction process includes a desalination facility fluidly coupled to a minerals extraction facility. The desalination facility includes a nanofiltration membrane section producing a first tailings stream and a reverse osmosis membrane section producing a second tailings stream and a desalinated water outlet stream from an inlet feed stream. The extraction facility produces at least one mineral compound, an extraction tailings stream, and a second desalinated water outlet stream. At least one of the first tailings stream and the second tailings stream is fed into the extraction facility. In certain exemplary embodiments, a natural gas combined cycle power unit supplies power to at least one of the desalination facility and the extraction facility. In certain exemplary embodiments, the extraction tailings stream is recycled into the desalination facility and there are no extraction tailings streams or desalination tailings streams discharged into the environment.
    Type: Application
    Filed: June 18, 2010
    Publication date: August 18, 2011
    Applicant: KATANA Energy LLC
    Inventor: Paul Steven Wallace
  • Publication number: 20110190446
    Abstract: Provided is a three-dimensional modeling apparatus including a supply mechanism, a deposition area, a variable mechanism, a discharge mechanism, and a control means. The supply mechanism supplies a powder material. In the deposition area,, the supplied powder material is deposited. The variable mechanism varies a volume of the deposition area per a predetermined layer thickness, and thus the powder material is deposited per the predetermined layer thickness in the deposition area. The discharge mechanism discharges liquid for forming a three-dimensional object to the deposited powder material, the liquid being capable of hardening the powder material. The control means causes the discharge mechanism to discharge the liquid to the powder material, to thereby form a main body being an object being as a target to be modeled and a frame body being an object to be formed in a periphery of the main body, of the three-dimensional object.
    Type: Application
    Filed: January 11, 2011
    Publication date: August 4, 2011
    Applicant: Sony Corporation
    Inventors: Takeshi Matsui, Junichi Kazusako, Hiroyuki Yasukochi
  • Publication number: 20110008243
    Abstract: Provided herein are processes for obtaining sylvinite and/or sylvite from sea water, sea bitterns and/or sea salts. The processes comprise reacting sea water, sea bitterns and/or sea salts with calcium hydroxide and/or calcium oxide.
    Type: Application
    Filed: June 22, 2010
    Publication date: January 13, 2011
    Inventor: Abraham Sadan
  • Publication number: 20100303708
    Abstract: According to a method for producing an inorganic iodide in accordance with the present invention, it is possible to efficiently produce a highly pure inorganic iodide by reacting a hydrogen iodide gas with an inorganic base compound by bringing the hydrogen iodide gas into contact with the inorganic base compound. As such, it is possible to provide a simple and efficient method for producing an inorganic iodide.
    Type: Application
    Filed: January 29, 2009
    Publication date: December 2, 2010
    Applicant: Nippoh Chemicals Co., Ltd.
    Inventors: Satoshi Kanbe, Kazumi Hosono, Masahiro Wada
  • Patent number: 7815884
    Abstract: To provide a method for producing polycrystalline silicon at relatively low cost, wherein the amount of waste generated is reduced by decreasing the amount of waste generated in producing polycrystalline silicon from silicon chloride by a method of reduction and increasing the amount of reused auxiliary raw materials. In the production of polycrystalline silicon using a gas phase reaction of a silicon chloride gas and a reducing agent gas, a chlorine gas is blown into an exhaust gas discharged from a reaction device to initiate a reaction, an unreacted reducing agent and silicon particles contained in the exhaust gas are chlorinated, and then a reducing agent chloride contained in the exhaust gas is separated from the other impurities and recovered.
    Type: Grant
    Filed: March 19, 2008
    Date of Patent: October 19, 2010
    Assignee: Chisso Corporation
    Inventor: Satoshi Hayashida
  • Patent number: 7736617
    Abstract: An object of the present invention is to provide a method for recovering iodine, which can be carried out simply and economically without practicing mixing processing operation of iodine-containing material, an alkali metal compound and a solvent in advance before introducing to a combustion furnace. The object of the present invention can be attained by a method for recovering iodine which comprises feeding an iodine-containing solution containing iodine and/or iodine compound, a basic alkali metal compound solution and/or a basic alkaline earth metal compound solution separately to a roasting furnace, oxidatively decomposing a combustible material by heat treatment, and absorbing iodine and/or iodine salt contained in a component at heat treatment exit with water or an aqueous solution.
    Type: Grant
    Filed: April 28, 2006
    Date of Patent: June 15, 2010
    Assignee: Nippoh Chemicals Co., Ltd.
    Inventors: Shigenobu Shoji, Haruhisa Hujihira, Satoshi Kanbe
  • Publication number: 20100136122
    Abstract: The present invention provides an oral preparation sufficiently masking the bitter taste of pioglitazone and a salt thereof. The present invention provides an oral preparation containing pioglitazone or a salt thereof and alkali metal chloride.
    Type: Application
    Filed: May 22, 2007
    Publication date: June 3, 2010
    Inventors: Kazuhiro Okochi, Hiroyoshi Koyama, Arisa Maeda
  • Patent number: 7727501
    Abstract: Apparatus and method are disclosed for the production of compacted granular potassium chloride with improved handling qualities. A binding ingredient such as sodium hexametaphosphate is blended with the potassium chloride feed material in advance of compaction. The product of this apparatus and method has improved handling, storage, strength and other qualities over compacted granular potassium produced using prior art methods.
    Type: Grant
    Filed: May 3, 2004
    Date of Patent: June 1, 2010
    Assignee: The Mosaic Company
    Inventors: Del Ferguson, Rob Plosz, Annette Revet, Doug LaRocque, Peter Jackson, Carey Heinbigner, Dave Zirk, Scott St. Germaine
  • Publication number: 20100056362
    Abstract: A substrate, such as a glass, glass ceramic, ceramic or metal substrate, is provided with a thermocatalytically active coating on at least a part of the substrate surface. The thermocatalytic coating contains an inorganic lithium salt or organic lithium-containing compound in an amount that is equivalent to not less than 2 wt. % of lithium ions, based on total coating weight. The thermocatalytic coating has a glass, glass solder or sol-gel matrix in which the lithium salt or organic lithium-containing compound is introduced. Optional barrier and IR-reflecting layers are arranged between the substrate surface and the thermocatalytically active coating.
    Type: Application
    Filed: August 21, 2009
    Publication date: March 4, 2010
    Inventors: Inka Henze, Hrabanus Hack, Gerhard Weber, Hans-Joachim Schmitt, Wolfgang Schmidbauer, Torsten Gabelmann
  • Publication number: 20100021369
    Abstract: A method for producing an alkali metal iodide salt solution including combusting a liquid for combustion so as to combust a combustible component of the liquid for combustion; and subsequently cooling a resultant gas containing a decomposition product. The method comprises the steps of (a) providing a liquid containing (i) an alkali metal iodide salt, (ii) an inorganic-salt-forming substance capable of forming, at combustion, an inorganic salt containing an alkali metal and (iii) an organic compound; (b) adding to the liquid a precipitation solvent capable of depositing the inorganic-salt-forming substance; (c) removing from the liquid the inorganic-salt-forming substance precipitated in the step (b) so as to obtain the liquid for combustion; and (d) combusting the liquid for combustion and subsequently cooling the resultant gas containing a decomposition product.
    Type: Application
    Filed: March 11, 2008
    Publication date: January 28, 2010
    Inventors: Yuichiro Kinoshita, Sayaka Shiomitsu, Keisuke Takahashi
  • Publication number: 20090110629
    Abstract: The present invention contemplates for providing a producing method which can give highly pure caustic potash in a relatively simple process, in response to the above-described demand for increased high purity in caustic potash. A method to give highly pure caustic potash containing almost no impurities of sodium, chlorine, and heavy metals, such as iron, chromium and nickel, through crystallization, by bringing an aqueous caustic potash solution having a sodium content of 200 mg/kg or less and a chlorine content of 15 mg/kg or less when calculated in terms of a weight of potassium chloride, in which a caustic potash concentration of 48% is to be a standard, into a high temperature state.
    Type: Application
    Filed: August 8, 2006
    Publication date: April 30, 2009
    Inventors: Tsugiyoshi Osakabe, Sei Imayoshi, Mitsuharu Hamamori
  • Publication number: 20090011448
    Abstract: A pretreatment agent for a sample to be subjected to Limulus assay comprising an alkali metal sulfate and/or an alkaline earth metal sulfate wherein the sulfate(s) has a final concentration of 20 mM or more when the sulfate(s) is allowed to contact with the sample, or an alkali metal halide and/or an alkaline earth metal halide wherein the halide(s) has a final concentration of from 0.4 M to 1.2 M or less when the halide(s) is allowed to contact with the sample, or a kit for Limulus assay reagent comprising thereof as a composing article.
    Type: Application
    Filed: January 27, 2006
    Publication date: January 8, 2009
    Applicant: SEIKAGAKU CORPORATION
    Inventors: Toshio Oda, Jun Aketagawa
  • Patent number: 7465333
    Abstract: A precursor halide compound is reduced to a predetermined product at substantially ambient conditions. The halide is added to an anhydrous liquid reaction medium containing one or more alkali metals or alkaline earth metals as reductants. The metal reductants are dispersed as very small globules in the liquid by cavitation of the liquid, such as by application of high intensity ultrasonic vibrations or high-shear mixing to the reaction vessel. Continued cavitation of the liquid medium affects low temperature reduction of the precursor halide(s) to produce a metal, metal alloy, metal compound, ceramic material, metal matrix-ceramic composite material, or the like. The practice may be applied, for example, to titanium tetrachloride, alone or with other chlorides, to produce titanium metal, titanium alloys (for example Ti-6Al-4V), and titanium compounds (TiSi2).
    Type: Grant
    Filed: August 17, 2006
    Date of Patent: December 16, 2008
    Assignee: GM Global Technology Operations, Inc.
    Inventors: Ion C. Halalay, Michael P. Balogh, Michael K. Carpenter
  • Patent number: 7459139
    Abstract: A cost-effective process is described for the preparation of a stable and non-hazardous brominating reagent containing 2:1 stoichiometric ratio of alkali bromide to alkali bromate. The process comprises of reacting alkaline bromine intermediate mixture, obtained from bromine recovery plant, with chlorine gas in the presence of a strong alkali to oxidize the bromide ions to bromate ions. This brominating reagent is useful for the bromination of aromatic compounds by substitutions.
    Type: Grant
    Filed: May 30, 2003
    Date of Patent: December 2, 2008
    Assignee: Council of Scientific and Industrial Research
    Inventors: Ramachandraiah Gadde, Pushpito Kumar Ghosh, Adimurthy Subbarayappa, Ashutosh Bedekar, Dipak Balvantrai Shukla
  • Patent number: 7455713
    Abstract: A titanium halide and, optionally, other precursor halides compound are reduced to a predetermined titanium product, suitably at or near ambient conditions. Titanium tetrachloride, for example, is added to an anhydrous liquid reaction medium containing one or more alkali metals or alkaline earth metals as reductants. The metal reductants are dispersed as very small globules in the liquid by cavitation of the liquid reaction medium, such as by application of high intensity ultrasonic vibrations or high-shear mixing to the reaction vessel. Continued cavitation of the liquid medium affects relatively low temperature reduction of the precursor halide(s) to produce a titanium-containing product such as titanium metal, a titanium alloy or compound, or a titanium matrix-ceramic composite material, or the like.
    Type: Grant
    Filed: August 17, 2006
    Date of Patent: November 25, 2008
    Assignee: GM Global Technology Operations, Inc.
    Inventors: Ion C. Halalay, Michael P. Balogh
  • Publication number: 20080241040
    Abstract: Crystalline scintillator materials comprising nano-scale particles of metal halides are provided. The nano-scale particles are less than 100 nm in size. Methods are provided for preparing the particles. In these methods, ionic liquids are used in place of water to allow precipitation of the final product. In one method, the metal precursors and halide salts are dissolved in separate ionic liquids to form solutions, which are then combined to form the nano-crystalline end product. In the other methods, micro-emulsions are formed using ionic liquids to control particle size.
    Type: Application
    Filed: March 26, 2007
    Publication date: October 2, 2008
    Inventors: Brent Allen Clothier, Sergio Paulo Martins Loureiro, Alok Srivastava, Venkat Subramaniam Venkataramani
  • Patent number: 7361325
    Abstract: A substantially dried XF•nH2O2 product is produced by method(s) wherein a feed solution comprised of (i) a XF composition wherein X is K, Na+ or NH4+ and n is an integer from 1 to 3, (ii) hydrogen peroxide (H2O2), (iii) a fluid carrier component and (iv) a potassium bifluoride (KHF2) catalyst, is atomized as it enters a desiccation/evaporation chamber. The atomized feed solution coats fluidized particles passing through the desiccation/evaporation chamber. The coated fluidized particles are dried by a pre-heated gas stream and thereby creating fluid-bed particles that are coated with a layer of the XF•nH2O2 compound. The resulting XF•nH2O2 coated fluid-bed particles are then subjected to disintegration forces that serve to break substantial portions of the layer of dried XF•nH2O2 material from the outer surfaces of he individual fluid-bed particles. These dried XF•nH2O2 are then recovered as the product of these production methods.
    Type: Grant
    Filed: December 29, 2004
    Date of Patent: April 22, 2008
    Assignee: GeoStim Group LLC
    Inventor: Vladimir Marakov
  • Patent number: 7217402
    Abstract: A method of producing metal chlorides is disclosed in which chlorine gas is introduced into liquid Cd. CdCl2 salt is floating on the liquid Cd and as more liquid CdCl2 is formed it separates from the liquid Cd metal and dissolves in the salt. The salt with the CdCl2 dissolved therein contacts a metal which reacts with CdCl2 to form a metal chloride, forming a mixture of metal chloride and CdCl2. After separation of bulk Cd from the salt, by gravitational means, the metal chloride is obtained by distillation which removes CdCl2 and any Cd dissolved in the metal chloride.
    Type: Grant
    Filed: August 26, 2005
    Date of Patent: May 15, 2007
    Assignee: United States of America Department of Energy
    Inventors: William E. Miller, Zygmunt Tomczuk, Michael K. Richmann
  • Patent number: 7195740
    Abstract: A method and apparatus for removing BHP contaminants (alkali hydroxide and H2O2) from a recycled aqueous alkali chloride solution stream before the stream is fed to a chloralkali cell so that the contaminants do not impair the operation of a chloralkali cell. Unwanted alkali hydroxide within the recycled alkali chloride brine solution is reacted with chlorine gas and converted into an alkali chloride, which is useful in the operation of the chloralkali cell, and oxygen gas, which is outgassed from the system. Any H2O2 remaining in the recycled stream after elimination of the alkali hydroxide is reacted with chlorine to form HCl and oxygen gas. The HCl raises the pH of the brine solution, after which the pH may be adjusted by the addition of supplemental alkali hydroxide.
    Type: Grant
    Filed: March 29, 2004
    Date of Patent: March 27, 2007
    Assignee: The Boeing Company
    Inventors: Thomas L. Bunn, Stephen C. Hurlock, Alan Z. Ullman
  • Patent number: 7189327
    Abstract: A method of enhancing the recovery of useful coal or potassium chloride from screenbowl centrifuge separation operations comprising adding to the screenbowl centrifuge, from about 0.005 lbs active polymer/ton dry solids in centrifuge to about 0.70 lbs active polymer/ton dry solids in centrifuge, of an anionic copolymer, wherein said anionic copolymer is selected from the group comprising copolymers of acrylamide and acrylic acid and the known salts thereof.
    Type: Grant
    Filed: May 26, 2004
    Date of Patent: March 13, 2007
    Assignee: Nalco Company
    Inventors: Peter A. Dimas, Kenneth M. McGough
  • Patent number: 7175708
    Abstract: Methods and apparatus are provided for the removal and purification of the water and salt by-products from spent BHP emitted from a lasing process. The apparatus comprises a liquid processing system that freezes the water and salt by-products into a slurry, and then separates out the water (as ice) and salt components by filtering in a centrifuge. In order to remove as much residual BHP from the wet mixed ice-salt component as possible, a heat source is used to partially melt ice crystals, thereby generating an aqueous rinsing liquid on the surface of the wet mixed ice-salt crystals. The applied centrifugal force causes a continual displacement of the liquid film wetting the surface, so that it becomes progressively diluted. As such, the purification of the mixture of ice and salt crystals is implemented with an aqueous (water) rinse that is unaffected by the sub-freezing temperatures within the centrifuge.
    Type: Grant
    Filed: July 28, 2005
    Date of Patent: February 13, 2007
    Assignee: The Boeing Company
    Inventors: David Stelman, Steven M. Klee
  • Patent number: 7144568
    Abstract: Described is a process and a device for carrying out a reaction in liquid medium during which evolution of gas occurs. The process can be applied in particular to a reaction employing a peroxide such as hydrogen peroxide and, in particular, to the reduction of chlorine present in an aqueous effluent.
    Type: Grant
    Filed: December 21, 2001
    Date of Patent: December 5, 2006
    Assignee: Arkema France
    Inventors: Jean Philippe Ricard, Joel Choupeaux, Jean Michel Delassus
  • Patent number: 7087209
    Abstract: A method for producing halide brine wherein an alkali and a reducing agent are added to an aqueous fluid having a density greater than 8.30 lb/gal., (0.996 kg/L) water, waste water or sea water for example. The resulting fluid is then contacted with a halogen to form a halide brine. The reaction occurs in a conventional reactor such as a mixing tank.
    Type: Grant
    Filed: April 4, 2003
    Date of Patent: August 8, 2006
    Assignee: Tetra Technologies, Inc.
    Inventors: Raymond D. Symens, Lyle H. Howard, Surendra Kumar Mishra, Thomas William Polkinghorn
  • Patent number: 7087174
    Abstract: A method of enhancing the recovery of useful coal or potassium chloride or borax from screenbowl centrifuge separation operations comprising adding to the screenbowl centrifuge, from about 0.03 lbs active polymer/ton dry solids in centrifuge to about 0.70 lbs active polymer/ton dry solids in centrifuge, of a cationic terpolymer, wherein said cationic terpolymer is prepared by polymerizing from about 1 to about 99.1 mole percent of one or more cationic monomers, from about 0.1 to about 10 mole percent of one or more hydroxyalkyl(meth)acrylates and from one to about 98.1 mole percent of one or more nonionic monomers.
    Type: Grant
    Filed: April 8, 2004
    Date of Patent: August 8, 2006
    Assignee: Nalco Company
    Inventors: Peter A. Dimas, Kenneth M. McGough, Wesley L. Whipple