Abstract: Briefly described, embodiments of this disclosure include chemicals, modified pigments, and methods of preparing a modified pigment.

Abstract: The method for producing a propellant powder (TLP) with a layered grain structure starts with a green powder, which is impregnated in a watery emulsion with an energetic plasticizer and a polymeric deterrent. Propellant powders (TLP) can be produced in industrial quantities by avoiding the dangerous direct introduction of a blasting oil. The propellant powders (TLP) produced in this way have similar characteristics and a similar structure as the known propellant powders (TLP).

Abstract: The present invention relates to a coarse-particled microcapsule preparation comprising microencapsulated latent heat accumulators and one or more polymeric binders, the ratio of surface area to volume of the particles obeying the following relationship: Surface ? ? area 2 Volume 3 ? 2.5 , and to processes for its production and its use in heat exchangers and building materials.

Abstract: Microcapsules comprising one or more lipophilic substances as core material and a polymer as capsule shell, which are obtainable by free-radical polymerization of an oil-in-water emulsion comprising from 30 to 100% by weight, based on the total weight of the monomers, of one or more C1-C24-alkyl esters of acrylic and/or methacrylic acid (monomer I), from 0 to 80% by weight, based on the total weight of the monomers, of a bifunctional or polyfunctional monomer (monomers II) which is insoluble or sparingly soluble in water and from 0 to 40% by weight, based on the total weight of the monomers, of other monomers (monomers III), the lipophilic substance and solid inorganic particles having a mean particle size of from 45 to 1000 nm, and a process for producing them are described. They can be used in binding building materials, textiles and gypsum plasterboard.

Abstract: Disclosed herein is a method of doping nanosized nickel (Ni) on the surface of carbon nanotubes to improve the hydrogen storage capacity of the carbon nanotubes. The method comprises: sonicating carbon nanotube samples produced by vapor deposition, in sulfuric acid solution, followed by filtration to remove a metal catalyst from the carbon nanotube samples; and doping the carbon nanotube samples in liquid phase solution, followed by drying and reduction, so as to dope nanosized nickel on the surface of the carbon nanotubes.

Abstract: Optically coherent multilayered film-coated powder having weather resistance and a clear intended color, and processes for designing and producing the same are provided. A substance of the base particles providing an intended function and an intended color are selected; a spectral intensity curve and values in CIELAB color system of the intended color are measured; and with substances capable of being used as the coated layers and refractive indexes thereof being included in factors, substances and thicknesses of the coated layers and an order of formation of the layers are obtained that provide optically coherent multilayered film-coated powder having such values in CIELAB color system that minimizes a color difference and makes a hue ratio proximate to 1, by solving numerical solutions of the recurring formula for film multiple coherence.

Abstract: The present invention relates to a method of preparing a nanoparticle film having metal ions incorporated and to a film prepared by said method. The invention furthermore relates to uses of such a film.

Abstract: In various aspects provided are methods for producing a nanoparticle within a cross-linked, collapsed polymeric material. In various embodiments, the methods comprise (a) providing a polymeric solution comprising a polymeric material; (b) collapsing at least a portion of the polymeric material about one or more precursor moieties; (c) cross-linking the polymeric material; (d) modifying at least a portion of said precursor moieties to form one or more nanoparticles and thereby forming a composite nanoparticle.

Abstract: Composites and methods associated with the same are provided. The composite structures are formed of quantum dots and magnetic nanoparticles. The structures may be coated, for example, with a non-organic shell such as silica. In some cases, the shell may be functionalized or derivatized to include compounds, atoms, or materials that can alter or improve properties such as water solubility, water stability, photo-stability and biocompatibility. A reverse microemulsion process can be used to form the coated composites. The composition and other characteristics of the composites may be controlled to provide desired magnetic and optical properties. The structures may be used in a variety of applications including biological labeling, magnetic resonance imagine (MRI) and drug targeting, amongst others.

Abstract: A method for avoiding the agglomeration of pellets of several kinds of materials when treated at high temperatures, which comprises: covering the pellets with a long term stabilized magnesium hydroxide suspension which can be stored for at least three months without substantial agitation and without experiencing substantial settlement and solid hard substrate formation, comprising a solid content of about 51% to 61%; a water content of about 39% to 49%; a viscosity of about 500 to 1,500 cp.; an average particle size of about 1 to 2.5 microns; a Mg(OH).sub.2 content of about 50% to 60%; an equivalent magnesium oxide content of 34% to 42%; including a compound that improves the adhesion of the suspension to the pellets at a concentration of at least 30% in an amount of 0.

Abstract: Resin particles comprised of an acrylic resin. Not only is the maximum compression deformation ratio thereof as great as 60% or more but also the load required for 60% compression deformation is as small as 60 mN or less. Wiring boards are therefore coupled in using an anisotropic conductive adhesive obtained by first manufacturing conductive particles having a conductive coating formed on a resin particle surface of the resin particles by adhering a conductive material to the surface of the above resin particles as a core. On dispersing the conductive particles in an adhesive material, the conductive particles sandwiched between metallic wires of the wiring boards are greatly deformed by a small load, so that the electrical devices having a high conduction reliability can be obtained.

Abstract: The present invention relates to magnetic beads in the form of composite beads with an inner core of metal particles, which are coated with an inert synthetic polymer and thereafter a hydrophilic porous polymer, preferably dextran. This provides porous biocompatible beads without metal leakage. This construction also allows for simple and convenient handling of cell expansion media by magnetism.

Abstract: The invention relates to process for coating a solid, water-insoluble particulate matter, with a metal oxide comprising: (a) contacting the solid water-insoluble particulate matter with a cationic additive in an aqueous medium to obtain a dispersion of said particulate matter having a positive zeta potential; (b) coating the solid water-insoluble particulate matter by precipitation of a metal oxide salt onto the surface of the particulate matter, forming a metal oxide layer thereon; and (c) aging said coating layer The invention further relates to coated particulate matter obtained by the process and to compositions comprising solid, water-insoluble particulate matter, coated by a metal oxide layer, the particulate matter being a dermatological active agent or a pesticide. The invention additionally relates to methods of treating a surface condition in a subject using compositions comprising solid, water insoluble dermatologically active agent, coated by a metal oxide layer.

Abstract: Implementations of the present invention relate to systems, methods, and apparatus for manufacturing aesthetically pleasing, post-formable, reparable decorative architectural resin panels having a thin or brittle veneer layer such as thinly sliced natural wood or stone. In particular, at least one implementation includes a flat or curved decorative resin panel made with a natural wood veneer layer whose structural integrity has been maintained despite being subject to various heats and pressures. The resulting resin panel is at least partially translucent, and allows for a unique display both of the resin sheets used to form the panel and of the thin wood materials encapsulated therein. Additional implementations relate to the use of other brittle veneer layers, such as translucent stone, translucent metals, or the like, which also provide unique, decorative architectural, aesthetic features.

Abstract: A method for preparing composite nanoparticles comprised of a nickel ferrite core having a photocatalytic shell comprised of titania. The method is a combined reverse micelle plus chemical precipitation method that can be controlled to produce nanoparticles having a substantially uniform size and spherical shape.

Abstract: A method for making a doped magnesium diboride powder is provided. The method includes coating a polymeric precursor on at least one of a plurality of particles of a first phase, where the first phase includes a magnesium diboride powder, where the polymeric precursor includes chemical elements yielding a second phase. The second phase includes one or more of a boride, a nitride, a carbide, an oxide, an oxy-boride, an oxy-nitride, an oxy-carbide, or combinations thereof. The method further includes forming a second phase coating onto at least one of the plurality of particles of the magnesium diboride powder.

Abstract: A method for manufacturing a resin-coated carbon nanomaterial whereby an ultrasonic stirring method can be applied even for polycarbonate. A poly-carbonate resin is dissolved in a first organic solvent primarily composed of tetrahydrofuran, and an additive and a carbon nanomaterial are added to the solution, whereby a carbon nanomaterial coated by the polycarbonate resin is obtained. The polycarbonate resin alone cannot withstand ultrasonic stirring, but accompanying the polycarbonate resin with the carbon nanomaterial enables ultrasonic stirring to be applied.

Abstract: This invention provides a method for manufacturing a solid plating material which has excellent electrical conductivity and durability, and the solid plating materials manufactured by this method, wherein a suspension liquid is made by mixing a fluid for coating that includes an organic binder, with a powder for plating having electrical conductivity and a metal powder to be used for binding, wherein then layers having the plating powder and the metal powder, and bound to the surfaces of core particles with the organic binder, are formed by means of injecting the suspension liquid on the surfaces of the core particles while the core particles are being agitated by centrifugal fluidization, and wherein then the core particles are heated until their temperature is above the melting temperature of the metal powder to be used for binding so as to remove the organic binder and to form deposited layers of the plating powder by melting the metal powder to be used for binding.

Abstract: A display device including: a first substrate having a pixel electrode; a second substrate having a common electrode; a microcapsule sandwiched between the first substrate and the second substrate; and a display material changing its optical characteristic in response to an electrical stimulation, the display material being encapsulated in the microcapsule, the microcapsule being selectively disposed on a display area formed by the pixel electrode in between the first substrate and the second substrate, and a background area of one of the first substrate and the second substrate being colored with a background color, the background area serving as a background with respect to the display area.

Abstract: To provide a process of treating particulates such as an inorganic powder or resin beads to impart water repellency, to effectively impart water repellency particularly to a porous inorganic powder or the like, without use of an organic solvent as a dispersion medium of a silicone oil. Water repellent particulates are produced by a first step of adding, to particulates, an aqueous emulsion of a silicon compound such as a silicone oil to apply surface treatment to the particulates with mixing and stirring in a dry state, and a second step of heating the treated particulates to bake the silicon compound on the surface of the particulates and to separate the aqueous medium in the emulsion. The aqueous emulsion of the silicon compound is preferably an aqueous emulsion of any one of methyl hydrogen silicone oil, dimethyl silicone oil, epoxy-modified silicone oil, amino-modified silicone oil, polyether-modified silicone oil and carboxyl-modified silicone oil.

Abstract: A coating of an encapsulated electrophoretic medium is formed on a substrate (106) by dispersing in a fluid (104) a plurality of electrophoretic capsules (102), contacting at least a portion of a substrate (106) with the fluid (104); and applying a potential difference between at least a part of the portion of the substrate (106) contacting the fluid (104) and a counter-electrode (110) in electrical contact with the fluid (104), thereby causing capsules (102) to be deposited upon at least part of the portion of the substrate (106) contacting the fluid (102). Patterned coatings of capsules containing different colors may be deposited in registration with electrodes using multiple capsule deposition steps. Alternatively, a patterned coating may be deposited upon a substrate containing a conductive layer by varying the conductivity of the conductive layer by radiation exposure or by coating portions of the conductive layer with an insulating layer, typically a photoresist.

Abstract: A cost-effective, scalable technique for producing microspheres loaded with biologically active solid proteins is provided. The microspheres degrade over time and release biologically active VEGF, as demonstrated by the proliferation of HUVECs in vitro compared to negative controls. A defined concentration of microspheres can deliver a quantifiable level of VEGF with known release kinetics. The invention can be used with other growth factors and applied to tissue engineering applications such as the regeneration of peripheral nerve, bone, adipose tissue, and solid organs.

Abstract: The present invention relates to core-shell polymers having a hydrophilic copolymer shell, and a high level of core material of from 75 to 95 weight percent. The hydrophilic shell provides better coverage of the core resulting in better powder properties such as anti-blocking. The hydrophilic shell also allows for a thinner shell and a larger elastomeric core. Core-shell polymers of the invention are especially useful as impact modifiers for plastic materials.

Abstract: The present invention relates to a hollow sphere polymer composition suitable for absorbing active ingredients including oily substances and hydrophobic materials. A process for encapsulating one or more active ingredients using hollow sphere polymers is described.

Abstract: The invention concerns a method for producing nanocapsules and microcapsules comprising a polyelectrolyte shell by surface precipitation from the solution, by applying a shell to template particles comprising the steps (a) providing a dispersion of template particles of suitable size in a salt-containing liquid phase which contains the components required to form the shell in a dissolved form and (b) precipitating the components from the liquid phase onto the template particles under conditions which enable the formation of a shell around the template particles that has a thickness of from 1 to 100 nm.

Abstract: In color printing, and in the fine arts, cholesteric liquid crystal (CLC) color inks are known to possess much higher color saturation and brightness than conventional pigment and dyed based inks. However, prior art CLC ink formulations are inconvenient because in the liquid phase they have to be confined in cells, and in the solid phase, they have to be applied at high temperature, and have to be aligned by some means to produce the optimum color. This invention solves the problem encountered in the CLC prior art, by making pre-aligned CLC platelets or flakes of appropriate thickness and size and mixing them in appropriate host fluids producing a novel CLC ink which can be applied at room temperature and without the need for alignment. The new pre-aligned room temperature CLC ink can be used as a substitute for conventional inks in almost all printing and plotting, and manual drawing and painting. Using the notch filter CLC platelets, the brightness is further enhanced.

Abstract: In order to provide a method by means of which the surface of substrates can be protected from corrosive attack and which, in particular, avoids the necessity for oxidative treatment to form oxide layers on surfaces or for phosphatizing or chromatizing treatment steps and is, in addition, simple to apply, it is proposed that the substrate be brought into contact with a solution of a polymer which exhibits UCST properties and which is caused to be deposited onto the surface of the substrate as a layer by decreasing the temperature of the polymer solution.

Abstract: Volatile organic compound or other materials are produced in the thermoplastic manufacture of thermoplastic polyester beverage containers. Such materials can be eluted into beverages such as carbonated beverages, sparkling or still water from the polyester. Such thermoplastic polyester resins can be manufactured with a substituted cyclodextrin material that can prevent the formation of, or react with, and absorb volatile by-products during the formation of thermoplastic preforms or containers from the thermoplastic pellet or chip. Further, as the preform is blown into a polyester container, the active materials of the invention prevent the generation of additional undesirable volatile materials. Lastly, the scavenger material can act as a barrier that prevents transport of materials from the exterior of the container into the container contents.

Abstract: A cost-effective, scalable technique for producing microspheres loaded with biologically active solid proteins is provided. The microspheres degrade over time and release biologically active VEGF, as demonstrated by the proliferation of HUVECs in vitro compared to negative controls. A defined concentration of microspheres can deliver a quantifiable level of VEGF with known release kinetics. The invention can be used with other growth factors and applied to tissue engineering applications such as the regeneration of peripheral nerve, bone, adipose tissue, and solid organs.

Abstract: Nanoparticles, nanocomposites, and methods for making the nanoparticles and nanocomposites are disclosed. Illustrated methods include preparing a nanocomposite particle by binding a silicate compound to the surface of a core particle in an aqueous suspension, adding a silicate source and an organic surfactant template, and stirring the aqueous suspension to obtain silicate growth.

Abstract: A method for continuously introducing a substance in liquid phase into plastics granules comprising: a) feeding a substantially continuous flow of the plastics granules to at least one substantially static spraying chamber, b) spraying the substance in liquid phase onto the plastics granules, c) passing the granules partially or totally coated by the substance in liquid phase by a substantially static mixing means supported in at leas one mixing chamber provided downstream of the spraying chamber, d) submitting the mixed granules to drying for a time sufficient to allow a substantially complete absorption of the substance in liquid phase by the granules.

Abstract: The present invention relates to high quality composite materials from fibrous materials, in which the composite incorporates a polymer matrix embedding individual fibers. The matrix is derived from polymer particles which penetrate into a strand and substantially fill gaps between individual fibers. Such penetration can occur by exposing the strand to a stable emulsion of the polymer particles. The invention also relates to novel composite structures which incorporation of various types of fibrous segments. These composite structures allow the use of inexpensive and readily available scrap materials. The composites of the present invention are lightweight materials displaying enhanced strength and durability.

Abstract: An improved coated phosphor filler for an optical device includes a plurality of individual phosphor filler particles, and a coating layer having a plastic substance coated on each of the phosphor filler particles.

Abstract: A method for the production of a robust, chemically stable, crystalline, passivated nanoparticle and composition containing the same, that emit light with high efficiencies and size-tunable and excitation energy tunable color. The methods include the thermal degradation of a precursor molecule in the presence of a capping agent at high temperature and elevated pressure. A particular composition prepared by the methods is a passivated silicon nanoparticle composition displaying discrete optical transitions.

Abstract: A coated ferromagnetic particle comprises a ferromagnetic core and a coating. The coating comprises a residue resulting from a thermal treatment of a coating material comprising a polymer selected from the group consisting of polyorganosiloxanes, polyorganosilanes, and mixtures thereof. A composite magnetic article comprises a compacted and annealed article of a desired shape. The composite magnetic article comprises a plurality of coated ferromagnetic articles. Each coated ferromagnetic particle comprises a ferromagnetic core and a coating. The coating comprises a residue resulting from a thermal treatment of a coating material comprising a polymer selected from the group consisting of polyorganosiloxanes, polyorganosilanes, and mixtures thereof.

Abstract: Apparatus and method for preparing microparticles. An emulsion is formed by combining two phases in a static mixing assembly. The static mixing assembly preferably includes a preblending static mixer and a manifold. The emulsion flows out of the static mixing assembly into a quench liquid whereby droplets of the emulsion form microparticles. The residence time of the emulsion in the static mixing assembly is controlled to obtain a predetermined particle size distribution of the resulting microparticles.

Abstract: A particulate composition comprising particles having a core comprising a hydrophobic polymer within a shell, characterised in that the shell comprises a semi-permeable membrane. Particulate composition can be used for making a stable dispersion of particles uniformly distributed throughout a first hydrophobic liquid, wherein the particles comprise a core within a shell and the core comprises a hydrophobic polymer into has been imbibed a second hydrophobic liquid, Compositions can be used to encapsulate active substances and may be used in sustained release mechanisms.

Abstract: This invention relates to novel fluorinated dendrons and to a universal strategy for producing functional fluorinated dendrons programmed to self-assemble into supramolecular nanocylinder compositions containing p-stacks of high electron or hole mobility donors (D), acceptors (A), or D-A complexes in the core. Such nanocylinder compositions are uniquely applicable to devices spanning from single supramolecule to nanoscopic and to macroscopic scales including transistors, photovoltaics, photoconductors, photorefractives, light emissives, and optoelectronics.

Abstract: A process for the production of encased, spherical granular grains comprising spraying grains which consist of a prostane derivative and a cyclodextrin vehicle, forming together a prostane-cyclodextrine-clathrate, with an aqueous polymer dispersion of ethyl cellulose and/or poly(methyl)acrylic acid ester in a fluidized or boiling bed is disclosed. The polymer dispersion is applied in a thickness equivalent to 1-5% (w/w) of the total mass of the encased grains. The coated grains are cured for at least 24 hours. Grains produced according to this method have a pharmaceutical active ingredient release profile which remains unchanged over the storage time.

Abstract: Described is a process for preparing a dispersion of microcapsules by condensing a partially methylated melamine-formaldehyde resin having a molar ratio of melamine:formaldehyde:methanol of from 1:3.0:2.0 to 1:6.0:4.0 in water in which the essentially water-insoluble material forming the capsule core is present in dispersion in the presence of an alkali metal salt of a homopolymer or copolymer of 2-acrylamido-2-methylpropanesulfonic acid as protective colloid at a pH of from 3 to 6.5 by preforming the microcapsules at a temperature of from 20 to 50° C. and then curing the capsule wall of the preformed microcapsules at >50 to 100° C., which comprises adding from 5 to 100% by weight of melamine, based on the melamine-formaldehyde resin, in the course of curing. The microcapsule dispersions are formaldehyde-reduced and of low viscosity.

Abstract: In order to make it possible to treat particles in such a manner that they are stabilized as disperse particles in liquid media, such as varnishes, a method of coating particles with LCST polymers is proposed which is characterized by the following steps: a) dissolution of an LCST polymers in a solvent at a temperature below the LCST; b) mixing the solution obtained in step a) with the particles to be coated; and c) increasing the temperature of the mixture obtained in step b) to or beyond the point at which the LCST polymer deposits onto the particle surfaces.

Abstract: A structural dielectrically tailored prepreg panel includes structural materials having desired electrical qualities in one or more desired areas without loss of structural integrity or the addition of parasitic weight. In one method of manufacture an applicator such as a spray nozzle applies a first dielectric material to a first area not covered by a mask. In another method, the dielectric material includes a dry material, which is sprinkled upon a tacky impregnating resin in a controlled volume percentage to provide a dielectric gradient. In yet another embodiment an applicator arrangement includes a plurality of applicators arranged to form a multiple of applicator sets which communicates with a controller to selectively activate a particular applicator and dispense a desired dielectric resin in a desired location.

Abstract: The invention generally provides a method of coating a material, the method including the following steps: (a) forming a generally elongate coating structure (15), the coating structure having an internal cavity (17) extending at least substantially along its length, and wherein the internal cavity of the coating structure is capable of receiving a core material (21); (b) inserting a core material (21) into the internal cavity (17) of the coating structure (15); (c) compressing the coating structure at a first location (44) along its length so as generally to form a seal at that location; and (d) compressing the coating structure at a second location along its length (45).

Abstract: The invention concerns a method for making coated granules with masked taste and instant release of the active principle which consists in: first, mixing the constituents of a powder comprising at least the active principle and a granular disintegrating agent; then, granulating the resulting powder, in the presence of a mixture of carriers comprising at least a binding agent capable of binding the particles together to obtain grains; coating the grains formed by spraying a suspension comprising at least a coating agent and a membrane disintegrating agent; finally drying the resulting coated granules.

Abstract: A process is provided for producing a polymeric layer having a desired image thereon or a three dimensional article comprising a number of such layers in which a layer of a liquid photocurable composition which comprises photo colorable particles is cured by light and selected areas thereof are irradiated with light of a different dose, thereby forming the desired image which composition comprises particles dispersed in it which are micro-capsules containing a photosensitive color changing composition within a barrier layer which is substantially impermeable to the components of the color changing composition or are solid particles comprising an immobilized photosensitive color changing composition. The process permits the use of the same initiating mechanism to cure the resin and to change the color of the particles.

Abstract: A method for treating substrates including the steps of: providing a substrate; exposing said substrate to a plasma glow discharge in the presence of a fluorocarbon gas; maintaining said gas at a pressure between about 50 mTorr and about 400 mTorr; generating said plasma as a modulated glow discharge; pulsing said discharge at an on time of 1-500 milliseconds; pulsing said glow at an off time of 1-1000 milliseconds; maintaining said plasma glow discharge at a power density of 0.02-10 watts/cm2; and applying a hydrophobic coating to said substrate.

Abstract: Methods of making and using annealable insulated metal-based powder particles are provided. The insulated metal-based powder particles are formed from metal-based core particles that are coated with an annealable insulating material. The annealable insulating material has at least one inorganic compound and at least one organic polymeric resin. The inorganic compound in the insulating material forms a nonporous insulating layer surrounding the metal-based core particles upon heating. The organic polymeric resin preferably aids in dispersing or binding the inorganic compound to the metal-based core particles prior to annealing. The insulated metal-based powder particles produced can be formed into core components that can be annealed to improve the magnetic performance of the core component. The core components produced are particularly useful under AC operating conditions of 500 Hz or lower.

Abstract: The present invention relates to a particle comprising an active dispersed in a visco-elastic liquid matrix having a &eegr;′ and a &eegr;″ between 103 to 1014 Pa measured in a cone-and-plate rheometer at 25° C. and a sinusoidal frequencies &ohgr; of 1 Hz.

Abstract: The present invention provides a method for preparing submicron sized particles of an organic compound, the solubility of which is greater in a water-miscible first solvent than in a second solvent which is aqueous, the process including the steps of (i) dissolving the organic compound in the water-miscible first solvent to form a solution, (ii) mixing the solution with the second solvent to define a pre-suspension; and (iii) adding energy to the pre-suspension to form particles having an average effective particle size of 400 nm to 2 microns.

Abstract: Bioactive agent is encapsulated in a polymer microparticle in a (water-in-oil)-in-water emulsion-based method, and using a solvent that comprises ethyl acetate. Also described are microparticles comprising low inherent viscosity (i.v.) PLG, some with i.v. less than 0.5 dl/g, and methods for their preparation. DNA release is modified through use of low i.v. PLG. A particle production method for scale-up uses a blender that avoids excessive shear damage to DNA being encapsulated.