Abstract: Means are disclosed for rendering talcs such as Chinese talcs, Australian talcs, Italian talcs or like talcs which, when ground to an approximately 2.5-5.0 .mu.m median particle size, exhibit a wet powder brightness of at least about 30% and which have hitherto been considered acceptable as fillers for thermoplastic resinous compositions, and particularly polypropylene molding resins, even suitable for this use. Such talcs are beneficiated in accordance with this invention, generally at low cost, to further enhance brightness, heat stability or both these properties in thermoplastic molded articles filled with these beneficiated acceptable talcs, while also improving or at least not unacceptably diminishing other significant physical properties, particularly tensile properties, of the resulting molded article.

Abstract: A method for preventing the hydration/solubilization of the protective oxide coating of a phosphor is described. The method involves coating of the oxide coated phosphor particles with a continuous hydrophobic coating. After the phosphor particles are coated with the continuous hydrophobic coating and the continuous hydrophobic coating cured, they are added to a water-based suspension and subsequently processed into a lamp.

Abstract: A composite comprising: a substrate; and a polymeric coating adhered to at least one surface of said substrate, said polymer coating having a thickness of about 1 to about 100 micrometers, wherein said polymer coating comprises a neutralized carboxylated polymer having a carboxylate content of about 5 to about 300 meq. per 100 grams of said neutralized carboxylated polymer.

Abstract: A process for preparing an inorganic filler comprising treating a particulate inorganic material with a natural or synthetic latex composition and dewatering and drying the resultant mixture. The surface-treated inorganic filler can be used with advantage in a polymeric resin composition.

Abstract: A method is described in which a layered lattice silicate is surface modified with an organic material by reacting said layered lattice silicate in particulate form with a reactant system comprising gaseous NH.sub.3 at temperatures below about 1000.degree. C. and contacting the aminated silicate in particulate form with an organic compound selected from the group of monomers, co-monomers, prepolymers and compounds condensable with the amine group, such as a nylon precursor, in the presence of gaseous hydrogen. The surface modified silicates are useful as fillers in a filled polymer system comprising a matrix polymer and a filler.

Abstract: The process of the invention relates to the manufacture of hydrate salts-base thermal energy accumulators, designed to act as heat accumulators in plants for utilizing low temperature heat sources such as solar heat, domestic and industrial excess heat, and other heat sources currently not susceptible to economical utilization.The anhydrous salts are fed to an inclined rotary drum in which they are simultaneously hydrated and granulated to different diameters from 1.5 mm to about 2.5 cm and beyond. The granules are then cooled classified into classes of uniform size, and finally treated with a powdered inert filler and/or a resin so as to obtain a coating perfectly adhering to their surface and hermetic towards both gas and liquid.

Abstract: There is disclosed a process for coating particles, such as ceramic, metallic and organic cores, with fine powder, such as ceramic, metal, organic or carbon powder. The process comprises providing a mixture comprising the particles and a binder which is capable of slowly melting to viscous state. Then the mixture is tumbled while slowly heating it to enable the binder to reach the viscous state while allowing the particles to be substantially covered with the binder. The next step includes cooling the mixture to about room temperature and thereafter breaking up the particles that may have agglomerated during the tumbling and heating to give individual particles covered with the binder. As a final step, the fine powder is added to the individual binder covered particles and the mixture is tumbled and heated again to the viscous state under conditions effective to provide a coating of the fine powder on the particles.

Abstract: A filler for use in dental composites is made by the following process:(a) finely divided silica, such as fumed silica, is coated with a polymerizable monomeric material by (e.g., an acrylic monomer) by mixing the silica with an organic solvent solution of the monomer;(b) the solvent is removed by evaporation by any convenient means;(c) the coated silica particles are individualized, as by screening, to produce a powder of a predetermined particle size (e.g., 90 microns or smaller); and(d) the resin is then polymerized.Some individualization of the product of step (d) may be required. Light screening is usually sufficient.

Abstract: Sintering of metal particles at their normal sintering temperature is inhibited by coating the metal particles with an organic material such as polyvinyl butyral, polyvinyl formvar, polyvinyl alcohol, polyacrylonitrile epoxies, urethanes and cross-linked polyvinyl butyral. The organic coating serves as a barrier preventing physical contact between metal particles during the initial phase of the sintering cycle and degrades into a carbonaceous coating followed by volatilization during the intermediate phase of the cycle permitting coalescence of the metal particles into a dense mass along with the coalescence of the glass-ceramic particles. Co-sintering of the metal particles and the glass-ceramic particles with the aid of the organic coating results in a hermetic multi-layer glass ceramic substrate free of dimensional stability problems without deleteriously affecting the electrical conductivity of the metal conductor pattern.

Abstract: Ionomers in the salt form, such as the ammonium salts of sulfonated polystyrene, are precipitated from solution in a non-polar organic liquid by contact with a polar liquid in which the ionomer has only limited solubility (e.g., methanol) and a particulate solid such as a polyphenylene ether, followed by contact with a salt such as ammonium chloride, preferably in solution in the polar liquid. The resulting ionomer-coated polyphenylene ether particles are easily filtered and handled.

Abstract: The invention relates to a method for producing a water-permeable covering on granular, water-soluble substances by coating them with a synthetic resin. The method of the invention uses a coating composition which comprises a polyisocyanate and a polyol component of a condensation product from phenols and aldehydes, a softener containing hydroxyl groups and optionally a diluent containing hydroxyl groups. The coating composition is cured at room temperature with an amine as a catalyst.

Abstract: A process for preparing pigmented PVdF-based powder coating products is disclosed, which comprises the steps of (i) mixing PVdF resin with a compatible thermoplastic resin, preferably PMMA in a weight ratio of about 80:20 to 40:60, with pigments, and with a small amount of flow promoter, (ii) pelletizing the mixture of (i), and (iii) cryogenically grinding the pellets and sieving the large particles. Also disclosed is a process for coating a substrate, comprising the steps of (a) applying the above prepared powder coating product on a substrate, and (b) subjecting to a heat treatment.

Abstract: The invention relates to a process for the conditioning of radioactive or toxic waste in epoxy resins and a polymerizable mixture with two liquid constituents usable in this process.This process consists of incorporating the waste into a polymerizable mixture incorporating at least one epoxy resin, pitch and at least one epoxy resin hardener and allowing the thus obtained mixture to harden.Generally the mixture comprises at least 50% by pitch weight and can be used for treating radioactive waste constituted by large objects and organic liquids.

Abstract: A process is disclosed for coating particles comprising suspending the particles in a fluidized bed and introducing therein an encapsulating latex. During introduction of the latex, the fluid bed must be maintained at a temperature which is within 10.degree. C. lower to 20.degree. C. higher than the glass transition temperature of the polymer. Typical core materials include halogen and peroxygen bleaches, bleach precursors, enzymes, colorants and fabric softeners. Preferably, the latex comprises water as a carrier and a polymer with carboxyl functionality, the polymer being insoluble in water.

Abstract: A polyimide molding powder and a process for producing the same are disclosed, said powder comprising an aggregate of polyimide particles, in which the whole or a large portion of said powder comprises polyimide particles composed of a particulate filler coated with a polyimide resin and/or polyimide particles composed of a fibrous filler coated with a polyimide resin, and said process comprising reacting an aromatic tetracarboxylic acid dianhydride and an aromatic diamino compound in an organic solvent to synthesize a polyimide precursor and imidating the polyimide precursor to precipitate polyimide particles, wherein a particulate filler and/or a fibrous filler dispersed in a prescribed amount of an organic solvent is or are added to the reaction system at any stage before the imidation of the polyimide precursor. The molding powder produces polyimide molded products free from brittleness and excellent in appearance, as well as various performance characteristics due to the improving effects of the filler.

Abstract: An electroconductive core-sheath composite fiber comprising a core containing an electroconductive substance and a sheath formed of a fiber-forming polymer, which surrounds the core, wherein the core is completely covered with the sheath, the electric resistance of the surface of the fiber is lower than 10.sup.10 .OMEGA./cm, and the ratio of the electric resistance (.OMEGA./cm) of the surface to the internal electric resistance between the sections is lower than 10.sup.3.

Abstract: Encapsulated lithium including a shot shaped and sized body (10) of lithium metal encapsulated in a thin layer (12) of a predominantly fluorine substituted polyolefin based polymeric material, a method of making the same and a power plant utilizing the encapsulated lithium as fuel (FIG. 3).

Abstract: An improved laser markable material useful for encapsulation of electroic devices is obtained by adding TiO.sub.2 or TiO.sub.2 +CrO.sub.3 to common plastic encapsulants formed from a mixture of a resin+filler+carbon black+mold release agent. When irradiated by a laser, the originally grey material turns bright gold, providing a high contrast durable mark. The material has excellent marking contrast as well as better stability with time and temperature as compared to prior art laser markable encapsulants. Desirable concentrations, in weight percent of the compound, are 1-5% TiO.sub.2 and 0-3% CrO.sub.3, with 1-3%TiO.sub.2 and 0.5-2% CrO.sub.3 being preferred. Carbon black is optional but a concentration in the range 0.1-3% by weight is desirable with 0.5-1% preferred. Improved encapsulation and marking methods and improved devices using this material are described.

Abstract: Atmospheric contamination by residual hazardous particles remaining on a substrate following removal from the substrate of a layer of material containing such particles is substantially reduced by coating the substrate with certain aqueous coating compositions which produce tacky films on drying. For example, the health hazard from airborne asbestos fibers remaining attached to a substrate from which a layer of asbestos-containing material has been removed is substantially reduced by coating the substrate with an aqueous latex composition containing certain carboxylated butadiene styrene polymers.

Abstract: This invention relates to a combination of anionic and non-ionic polymers and surfactants useful for the control of dust emissions into the environment. More specifically, the invention relates to novel compositions and the use of said compositions in treating particulate matter which comprises an aqueous solution of water soluble polymers comprising a unique mixture of water soluble acrylic polymers in combination with water soluble non-ionic glycol polymers in an aqueous medium containing effective amounts of anionic surfactants such as sulfonates and nonionic cosurfactants.

Abstract: A packing material for liquid chromatography, comprising particles having a silicone polymer film coated on substantially the entire surface thereof, the packing material being produced by a process comprising the steps of:(a) bringing at least one silicone compound having the general formula (I):(R.sup.1 HSiO).sub.a (R.sup.2 R.sup.3 SiO).sub.b (R.sup.4 R.sup.5 R.sup.6 SiO.sub.1/2).sub.c (I)wherein R.sup.1, R.sup.2, and R.sup.3 represent, independently, a hydrocarbon residue having 1 to 10 carbon atoms, which may be substituted with at least one halogen atom, R.sup.4, R.sup.5, and R.sup.

Abstract: A plastic molded article excellent in transparency, antistatic property and abrasion resistance is produced by providing on the surface of a base material comprising a transparent plastic molded article an electrically conductive coat layer comprising 60-80% by weight of an electrically conductive powder mainly composed of tin oxide and 20-40% by weight of a resin component and further providing thereon a topcoat layer comprising 0-50% by weight of an electrically conductive powder mainly composed of tin oxide and 50-100% by weight of a resin component.

Abstract: Carbonyl iron powder (CIP) can be protected from extensive atmospheric oxidation by mixing and heating it with a silicon compound having one or more reactive groups. The resulting CIP is more readily accepted by a silicone binder when preparing mixtures thereof.

Abstract: Finely divided mineral ore is pelletized using a soluble synthetic polymer. Preferably the polymer is in the form of beads made by reverse phase polymerization and all having a size of below 300 .mu.m. When the ore gives a pH in water of below 8 the soluble polymer is preferably cationic.

Abstract: A particulate built nonionic synthetic organic detergent composition includes a detersive proportion of a nonionic synthetic organic detergent and a building proportion, in combination, of a polyacetal carboxylate builder for the nonionic detergent and a polyphosphate builder for such nonionic detergent. Such compositions are readily made by adding polyacetal carboxylate builder to the formula of a control detergent composition, with corresponding diminutions of other component(s), and have detersive powers superior to such control despite the decrease in detergent and other builders. Preferably, certain nonionic detergents, polyacetal carboxylate builders and polyphosphate, in certain proportions, are employed for better detergency and physical characteristics, e.g., flowability.

Abstract: A treatment for finely divided silica reinforcing fillers is provided which utilizes low temperature and hydroxy or alkoxy containing diorganopolysiloxane as the treating agent. The treatment of fillers in this manner facilitates the manufacture and incorporation into silicone rubbers.

Abstract: A solid substrate, which contains or consists of a biologically or chemically active substance, is coated with coating material containing at least one polymerizable crosslinkable polyfunctional acrylic or methacrylic compound whereafter the coating material is subjected to polymerization substantially in the absence of non-polymerizable components to form a network coating of polymer on the surface of the solid substrate. This coating permits either the controlled release of active substance from the coated substrate or the controlled access of material reacting with said active substance into the coated substrate and the controlled release of the resulting reaction products from the coated substrate.

Abstract: A particulate built nonionic synthetic organic detergent composition includes a detersive proportion of a nonionic synthetic organic detergent and a building proportion, in combination, of a polyacetal carboxylate builder for the nonionic detergent and carbonate and bicarbonate builders for such nonionic detergent. Such compositions are readily made by adding polyacetal carboxylate builder to the formula of a control detergent composition, with corresponding diminutions of other component(s), and have detersive powers superior to such control despite the decrease in proportions present of detergent and other builders. Preferably, certain nonionic detergents, polyacetal carboxylate builders, carbonate and bicarbonate, in certain proportions, are employed to make a product of better detergency and physical characteristics, e.g., flowability.

Abstract: A molded carbonaceous material which is a molded mixture comprising a carbonaceous powder and a binder, particles of said carbonaceous powder particles being bound together by means of said binder with the surface of said carbonaceous powder being not wholly covered with said binder.

Abstract: A high strength self-consolidating particle comprised of a particulate substrate, a substantially cured inner resin coating and a fusible curable outer resin coating.

Abstract: Stone chippings of the type used in the manufacture of road surfaces by hotmix and surface dressing techniques, are rendered water resistant, and less susceptible to binder adhesion failure, by treatment with wax, preferably with wax emulsion.

Abstract: Imaging systems employing photosensitive microcapsules having improved film speed are disclosed wherein the microcapsules contain a photosensitive composition in which the photoinitiator system includes a photobleachable sensitizer such as a 3-substituted coumarin compound; the invention is particularly useful in providing self-contained imaging systems which are sensitive at 390-500 nm but which can be photobleached to reduce background yellow; an imaging process including a photobleaching step following exposure and development is also disclosed.

Abstract: This invention relates to coating glass beads with a mixture of substances which mixture comprises a first substance which if used alone would tend to make the beads hydrophobic while leaving them oleophilic and as second substance which if used alone would tend to make the beads both hydrophobic and oleophobic. Said coated beads maybe used in a synthetic polymeric matrix, as a coating over paint and as a coating on a road surface.

Abstract: A foundry shell core and mold composition comprises particulate matter coated with a curable phenolic-furan resin. The process for making the resin coated particulate matter substantially eliminates the sue of hexamethylene tetramine.

Abstract: A composite comprising a substrate and an elastomeric coating adhered to at least one surface of said substrate, said elastomeric coating having a thickness of about 1 to about 100 micrometers, wherein said elastomeric coating comprises an interpolymeric complex of a neutralized sulfonated polymer and an amine containing polymer, said neutralized sulfonated polymer having a sulfonate content of about 4 to about 200 meq. per 100 grams of said neutralized sulfonated polymer and said amine containing polymer containing basic nitrogen atoms wherein the basic nitrogen content ranges from about 4 to about 500 meq. per 100 grams of polymer.

Abstract: Stabilized powder of red phosphorus, for use as flame-retardant agent, in particular for compositions on the basis of polymers, constituted by particles of red phosphorus enveloped by a thin capsule constituted by a first layer of Al(OH).sub.3 adhering on to the surface of red phosphorus individual particles, and by a second layer, superimposed onto said first layer, constituted by a crosslinked polyconsensation resin formed by urea-melamine-phenol-formaldehyde.

Abstract: A granule comprises an inner core, which is formed from a material which does not expand appreciably in the presence of organic compounds, and an outer shell formed from an organo-clay which is preferably held on the inner core with the aid of a binder.The granule can be prepared by tumbling a particle of the inner core material in admixture with a powdered organo-clay and a binder therefor. A particulate bed of the granules can be used for separating organic compounds from a mixture thereof with an aqueous medium.

Abstract: The present invention relates to coated particulate matter wherein the particles are individually coated with a cured combination of phenolic/furan resin or furan resin to form a precured resin coating on a proppant such as sand, thereby substantially improving the chemical resistance of the proppant over one having a straight phenolic precured coating.Another embodiment of this invention involves the use of multiple resin coatings on the particulate matter to form a final layered coating containing the desired amount of cured resin. This multiple coating of particulate material results in a final coated product that has a smoother and more uniform surface than particulate material having its entire resin coating applied in a single operation.

Abstract: A filler composition composed of metal particles present in the tightest possible packing which are individually coated with a cross-linked polymer layer is provided which has high thermal conductivity and high electrical insulation capacity. Such filler composition is usefull as an addition to resins employed in injection molding and extrusion. A high resistance to abrasion is achieved by the cross-linked coating layers (22,24). A filing degree of about 90 Vol. % is achievable with such a filler composition, and such displays a breakdown voltage greater than about 100 V.

Abstract: A granular expanded mineral material, e.g. vermiculite, is caused to move in the form of a free flow (28) through a mist (46) produced by an atomizer (29). A waterglass solution and a hardener therefor are supplied through conduits (32,43) and (33,42) respectively, to the intrior of the atomizer (29) for co-atomization to produce said mist (46). A small amount of hydrophobizing agent non-emulsifiable in the waterglass solution is introduced into the stream of waterglass solution in the conduit (32,43). An in-line mixer (53) is built into that conduit immediately ahead of its exit (45) to the atomizer. By passing through the atomized mist (46) the grains of the expanded mineral material are individually coated with a film of waterglass solution and hardener with hydrophobizing agent finely distributed therein. The film-coated granular material is immediately thereafter pneumatically conveyed to a place of deposition on a surface, e.g.

Abstract: Finely particulate iron ore is pelletized using finely particulate, free flowing, anionic water soluble synthetic polymer having intrinsic viscosity of from 3 to 16 as binder.

Abstract: Coated particulate materials comprise water-soluble particulate materials as cores and a coating deposited on the surface of the particulate materials and formed preponderantly of a copolymer of cyclopentadiene type oligomer and an unsaturated fatty acid oil. Said coated particulate materials are manufactured by coating the surface of water-soluble particulate materials with a copolymer composition of a cyclopentadiene type oligomer and an unsaturated fatty acid oil and subsequently curing the resultant coating.

Abstract: A solid phase can be coated superficially with a polymeric coating by substituting immobilized metal ions on the surface of the solid phase with a hydrophilic polymer or a derivative or aggregate thereof, through a chemisorption process. The solid phase may comprise a magnetic material, such as magnetite, and may have a particle form. The coating can be produced by bringing the solid phase into contact with a solution of a reagent which includes at least one metal chelating and one reactive group, and subsequently bringing the solid phase into contact with a solution of a compound which reacts with the chelater reagent adsorbed on the solid phase. The polymer layer may constitute a polyhydric alcohol, a polyamine, or a polyamide, for example a polysaccharide, such as agarose, a protein or a peptide, a polyacryl amide, etc. and the reactive group may be a vinylsulphone or an epoxide, an aminothiol or a hydroxyl.

Abstract: A denture cleansing composition of the hypochlorite type is rendered substantially free of hypochlorite chlorine odor by incorporating into the composition a hypochlorite deactivator. The deactivator is released into the cleansing solution at a controlled rate to optimize cleansing efficacy at a reduced hypochlorite/chlorine odor. The deactivators suitable for use in this invention include sodium perborate monohydrate and sodium nitrite. The preferred method of controlling deactivator release rate is by encapsulating the deactivator.

Abstract: A pre-cured proppant charge useful, for example, for propping a fracture in a subterranean formation is disclosed. The charge is made up of a large number of particles composed of a single substrate particle which can be silica sand, glass beads, or the like, coated with a thermoset resin. The thermoset resin is one which, when it is the resin coating on particles of a proppant charge, produces such a charge when the Conductivity Ratio, as defined herein, throughout a given closure stress range is greater than that of a charge of the uncoated particles. The proppant is produced by coating the particulate substrate with a suitable thermosettable resin, controlling the coating step to produce substrate particles coated with a fusible, thermosetting resin, and curing the resin by heating the coated particles, so that substantially all of the resin coated particles are composed of a single substrate particle with a thermoset resin coating thereon, prior to introduction into a subterranean well.

Abstract: A self-supporting structure comprising an inorganic sorbent and method for preparing is described in which the self-supporting structure is substantially free of sorbent fines and the sorption characteristics of the sorbent particles is retained. The process for immobilizing the sorbent particles in the self-supporting structure comprises the steps of:(a) preheating inorganic sorbent particles to an elevated temperature;(b) mixing the sorbent particles with particles of a polymeric binding material to form a mixture comprising the particles of polymeric binding material adhered to the sorbent particles; and(c) heating the mixture to about the solid-liquid transition temperature of the polymeric binding material with or without pressure to form a structure which upon cooling is self supporting.

Abstract: High strength, chemical resistant particulate solids are provided which are particularly suitable for use in treating subterranean zones penetrated by well bores such as for forming gravel packs, as fracture propping agents and as cement composition structural fillers. The high strength, chemical resistant particulate solids are formed by coating solids with the reaction product of an organofunctional silane and an aryl acid halide.

Abstract: Provided is a dielectric imaging sheet useful in electrographic imaging, wherein a particulate solid incorporated into the dielectric coating has been treated with an acyloxy or amino terminated polysiloxane. Short-chain polysiloxanes, e.g., 3 to 8 siloxane units, are preferred as the treating agent, with the amino group being preferably lower alkyl substituted and the acyloxy group being preferably lower acyloxy. Use of the specially treated particulate solid reduces moisture induced imaging defects upon using the dielectric sheet in electrographic imaging.

Abstract: An improved laser markable material useful for encapsulation of electronic devices is obtained by adding TiO.sub.2 or TiO.sub.2 +CrO.sub.3 to common plastic encapsulants formed from a mixture of a resin+filler+carbon black+mold release agent. When irradiated by a laser, the originally grey material turns bright gold, providing a high contrast durable mark. The material has excellent marking contrast as well as better stability with time and temperature as compared to prior art laser markable encapsulants. Desirable concentrations, in weight percent of the compound, are 1-5% TiO.sub.2 and 0-3% CrO.sub.3, with 1-3% TiO.sub.2 and 0.5-2% CrO.sub.3 being preferred. Carbon black is optional but a concentration in the range 0.1-3% by weight is desirable with 0.5-1% preferred. Improved encapsulation and marking methods and improved devices using this material are described.

Abstract: For use in trickle bed electrolytic cells, the preferred and illustrated embodiment sets forth an improved graphite composite chip. It is a chip characterized by having a much higher percentage with a more uniform coating thereon. The coating has the form of a mix of carbon and Teflon on graphite chips. It is more uniform and applied to both sides of the chips. This improves current flow and distribution in an electrolytic cell such as a hydrogen peroxide cell. One procedure taught herein is a method of making such composite chips on graphite wherein carbon in particulate form is mixed with water and particulate Teflon dispersion and is added to graphite chips of a selected mesh size; after mixing, the water is drained and all water is removed by a vacuum in a rotary evaporator whereupon the dried material is then sintered for a specified time and temperature.