Inorganic Coating Patents (Class 427/343)
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Publication number: 20130155822Abstract: A method of manufacturing a decorative article, including a first coating formation step of forming a first coating of primarily TiN on a substrate; a second coating formation step of forming a second coating on the first coating by means of a dry plating method using a target containing 70.0 wt %?85.0 wt % Au and 15.0 wt %?30.0 wt % Cu; a heat treatment step of promoting formation of a solid solution of the constituents of the second coating by applying a heating process that heats the substrate on which the first coating and the second coating are disposed to 300° C.?395° C. and then applying a cooling process; and an acid treatment step that, of the constituents of the second coating to which the heating process was applied, removes the constituents not forming a solid solution by applying an acid treatment.Type: ApplicationFiled: November 27, 2012Publication date: June 20, 2013Applicant: SEIKO EPSON CORPORATIONInventor: SEIKO EPSON CORPORATION
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Publication number: 20130143036Abstract: A new roofing tile with enhanced surface durability and processes for manufacturing the same. The abstract of the disclosure is submitted herewith as required by 37 C.F.R. §1.72(b). As stated in 37 C.F.R. §1.72(b): A brief abstract of the technical disclosure in the specification must commence on a separate sheet, preferably following the claims, under the heading “Abstract of the Disclosure.” The purpose of the abstract is to enable the Patent and Trademark Office and the public generally to determine quickly from a cursory inspection the nature and gist of the technical disclosure. The abstract shall not be used for interpreting the scope of the claims. Therefore, any statements made relating to the abstract are not intended to limit the claims in any manner and should not be interpreted as limiting the claims in any manner.Type: ApplicationFiled: June 1, 2012Publication date: June 6, 2013Inventors: Andreas DRECHSLER, Jürgen KLEIN, Florence YZIQUEL, Jeffrey CHEN, Emmanuel FOURDRIN
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Patent number: 8404307Abstract: The present invention provides a hydrophilic film, which displays excellent hydrophilicity, and also displays excellent durability with respect to acidic, neutral, and alkaline detergents and chemicals. A hydrophilic film of the present invention comprises a double oxide of silicon and zirconium, an alkali metal, and water. Furthermore, the film may also comprise aluminum or a bivalent metal, and may also contain at least one of a silane coupling agent and an acrylic resin.Type: GrantFiled: March 17, 2009Date of Patent: March 26, 2013Assignee: Sumitomo Osaka Cement Co., Ltd.Inventors: Keijiro Shigeru, Daisaku Maeda
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Publication number: 20130065076Abstract: A method for applying a protective coating to gas turbine engine components using a saturated solution of nickel acetate tetrahydrate, applying a uniform thickness of the coating onto the thermal barrier coating of selected components, and heat treating the coated component in air at a temperature sufficient to form a protective layer of NiO. The saturated NiO solution has sufficient solubility to penetrate into the microscopic cracks of the thermal barrier coating to form a “sacrificial mitigation layer” of NiO that substantially inhibits the reaction between vanadium pentoxide and yttria-stabilized compounds present in the thermal barrier coating.Type: ApplicationFiled: September 12, 2011Publication date: March 14, 2013Inventor: Richard Todd Everhart
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Publication number: 20130052445Abstract: Onto a substrate, a first material containing one of elements A and B is supplied, and an oxidant is supplied to form a first layer containing an oxide of the one of the elements A and B. Then, a second material containing the other of the elements A and B is supplied, and an oxidant is supplied to form a second layer containing an oxide of the other of the elements A and B. The steps are repeated to prepare a stack of a plurality of the first layers and a plurality of the second layers. Furthermore, the substrate and the stack are subjected to a heat treatment to produce a composite oxide film containing AXB6O.—.5X+12 (6?X?30).Type: ApplicationFiled: August 22, 2012Publication date: February 28, 2013Applicant: HONDA MOTOR CO., LTD.Inventors: Satoshi NAKADA, Masayuki SUGAWARA
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Patent number: 8367207Abstract: The invention relates to a hydrogenated amorphous carbon coating and to a method for the production thereof. It also relates to devices having such a coating. The method of the invention consists in producing a hydrogenated amorphous carbon coating comprising at least two layers of hydrogenated amorphous carbon, each of said layers having chemical compositions and physical and mechanical properties that are identical, and with thicknesses that are identical or different. The coating of the invention finds many applications, in particular in the mechanical field for parts subject to considerable wear and rubbing problems. It may also be applicable, in particular, in the field of surgical implants and in the MEMS (microelectromechanical systems) field.Type: GrantFiled: October 20, 2008Date of Patent: February 5, 2013Assignees: Commissariat a l'Energie Atomique et aux Energies Alternative, Centre National de la Recherche ScientifiqueInventors: Caroline Chouquet, Cédric Ducros, Frédéric Sanchette
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Publication number: 20130022756Abstract: The adhesion of metal thin films onto polymeric substrates can be significantly enhanced by contacting the surface of the polymeric substrate with a non-complexing solvent before or after depositing the metal film.Type: ApplicationFiled: July 19, 2012Publication date: January 24, 2013Inventors: BRIAN HOWARD AUGUSTINE, WILLIAM CHRISTOPHER HUGHES, ALAN KOON-KEE MO, THOMAS CARROLL DEVORE
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Patent number: 8349517Abstract: A method of coating a surface of a fuel cell plate is disclosed herein, and involves forming a sol gel mixture by mixing a weak acid and a composition including at least two metal oxide precursors. One of the metal oxide precursors is configured to be hydrolyzed by the weak acid to form a mixed metal oxide framework with an other of the metal oxide precursors having at least one organic functional group that is not hydrolyzed by the weak acid. The mixture is applied to the surface, and is condensed by exposure to air at least one predetermined temperature and for a predetermined time. The sol gel mixture is immersed in water at a predetermined temperature and for a predetermined time to form a porous, hydrophilic, and conductive film on the surface.Type: GrantFiled: April 23, 2009Date of Patent: January 8, 2013Assignee: GM Global Technology Operations LLCInventors: Wen Li, Ping Liu, Jennifer J. Zinck, Tina T. Salguero, Richard H. Blunk
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Patent number: 8343584Abstract: A method of manufacturing a decorative article, including a first coating formation step of forming a first coating of primarily TiN on a substrate; a second coating formation step of forming a second coating on the first coating by means of a dry plating method using a target containing 70.0 wt %?85.0 wt % Au and 15.0 wt %?30.0 wt % Cu; a heat treatment step of promoting formation of a solid solution of the constituents of the second coating by applying a heating process that heats the substrate on which the first coating and the second coating are disposed to 300° C.?395° C. and then applying a cooling process; and an acid treatment step that, of the constituents of the second coating to which the heating process was applied, removes the constituents not forming a solid solution by applying an acid treatment.Type: GrantFiled: November 19, 2010Date of Patent: January 1, 2013Assignee: Seiko Epson CorporationInventors: Atsushi Kawakami, Yuzuru Tsukamoto
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Publication number: 20120308728Abstract: A magnetoresistive element includes a magnetoresistive film including a magnetization pinned layer, a magnetization free layer, an intermediate layer arranged between the magnetization pinned layer and the magnetization free layer, a cap layer arranged on the magnetization pinned layer or on the magnetization free layer, and a functional layer arranged in the magnetization pinned layer, in the magnetization free layer, in the interface between the magnetization pinned layer and the intermediate layer, in the interface between the intermediate layer and the magnetization free layer, or in the interface between the magnetization pinned layer or the magnetization free layer and the cap layer, and a pair of electrodes which pass a current perpendicularly to a plane of the magnetoresistive film, in which the functional layer is formed of a layer including nitrogen and a metal material containing 5 atomic % or more of Fe.Type: ApplicationFiled: August 13, 2012Publication date: December 6, 2012Applicant: KABUSHIKI KAISHA TOSHIBAInventors: Hideaki FUKUZAWA, Shuichi Murakami, Hiromi Yuasa, Yoshihiko Fuji
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Patent number: 8313802Abstract: Provided here is a method of producing a monolithic body from a porous matrix, comprising: (i) providing a porous matrix having interstitial spaces and comprising at least a first reactant; (ii) contacting the porous matrix with an infiltrating medium that carries at least a second reactant; (iii) allowing the infiltrating medium to infiltrate at least a portion of the interstitial spaces of the porous matrix under conditions that promote a reaction between the at least first reactant and the at least second reactant to provide at least a first product; and (iv) allowing the at least first product to form and fill at least a portion of the interstitial spaces of the porous matrix, thereby producing a monolithic body, wherein the monolithic body does not comprise barium titanate.Type: GrantFiled: November 14, 2008Date of Patent: November 20, 2012Assignee: Rutgers, The State University of New JerseyInventors: Richard E. Riman, Vahit Atakan
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Publication number: 20120288479Abstract: A hydrogel material composition includes: (1) an alginate (or other cross-linking polymer) material; (2) an optional ?-hydroxy carboxylate material; and (3) an iron cation material. The hydrogel material composition with or without the ?-hydroxy-carboxylate material may be used in a photolithographic imaging application or a photorelease application within the context of a photoirradiation induced reduction/oxidation reaction of an iron (III) cation material to form an iron (II) cation material.Type: ApplicationFiled: May 14, 2012Publication date: November 15, 2012Applicant: CLARKSON UNIVERSITYInventor: Artem Melman
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Patent number: 8303853Abstract: A method using a chemical synthesis method to produce a metallic nanoparticle inorganic composite having fine metallic nanoparticles that are uniformly dispersed at a high density in a solidified matrix, a metallic nanoparticle inorganic composite, and a plasmon waveguide using this composite are provided. Thus, a method including: preparing a precursor solution, applying the precursor solution onto a substrate, and then hydrolyzing the precursor solution to form an oxide film having fine pores, bringing the oxide film into contact with an acidic aqueous solution of tin chloride to chemically adsorb Sn2+ ions in the fine pores, removing an excess of the Sn2+ ions, bringing the oxide film into contact with an aqueous metal chelate solution to precipitate metallic nanoparticles in the fine pores, and removing an excess of ions of the metal is provided.Type: GrantFiled: July 10, 2009Date of Patent: November 6, 2012Assignee: Kabushiki Kaisha ToshibaInventors: Miho Maruyama, Kenji Todori, Tsukasa Tada, Reiko Yoshimura, Yasuyuki Hotta, Ko Yamada, Masakazu Yamagiwa
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Publication number: 20120251794Abstract: The present invention provides a method for making a sheet of a carbon nanotube (CNT) layer. First, a CNT solution is provided. A substrate is also provided. The substrate is then covered by the CNT solution, and a CNT layer is formed on the substrate through vacuum filtration. The CNT layer is cleaned with an organic chemical solution, and the CNT layer is cleaned with water. Finally, water is removed from the CNT layer. Additionally, in the step of vacuum filtration, a whirlpool is created in the CNT solution.Type: ApplicationFiled: March 30, 2011Publication date: October 4, 2012Inventor: Hsin Yuan MIAO
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Publication number: 20120243370Abstract: System and method for providing an anti-fouling function to a streamer to be towed under water for seismic survey data collection. The method includes mixing a thermoplastic material with a biocide material to form an external sheath material; and forming an external sheath over a main sheath of the streamer to provide the anti-fouling function. The external sheath is formed from the external sheath material such that the biocide material is distributed throughout the external sheath.Type: ApplicationFiled: June 7, 2012Publication date: September 27, 2012Applicant: SERCELInventor: Jean-Jacques VIGNAUX
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Patent number: 8273411Abstract: The various embodiments herein provide a method and composition to produce an anti-corrosive layer. According to one embodiment herein, a titanium based sol is synthesized and deposited on a substrate, dried for 120° C. for 1 hour, calcinated upto 400° C. for 1 hour, doped with a corrosion inhibitor, dried and deposited a layer of hybrid silica sol and cured to obtain the anticorrosive layer. According to another embodiment, a surface pre-treatment coating has a composition comprising a titanium dioxide layer, a corrosion inhibitor doped on the titanium dioxide layer, a hybrid silicate layer deposited on the doped titanium layer to form a coating to provide an improved corrosion resistance and self-healing effect.Type: GrantFiled: July 3, 2010Date of Patent: September 25, 2012Inventors: Sayed Morteza Madani, Maryam Ehteshamzadeh, Hassan Hashemipour Rafsanjani
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Publication number: 20120213933Abstract: A method of forming a metal-coated substrate having a CuInGaR2 film on a surface of the metal coating is performed in such a manner that reaction of the metal with Se is substantially prevented, wherein R is Se or a combination of Se and S and wherein the metal is selected from the group consisting of Mo, W, Cr, Ta, Nb, V and Ti. The method includes the steps of: providing a precursor film on the surface of the metal coating, wherein the metal coating contains oxygen in an amount sufficient to inhibit reaction of the metal with Se; and selenizing the precursor film; wherein said selenizing is limited to providing only that amount of Se required to form the CuInGaR2 film.Type: ApplicationFiled: April 30, 2012Publication date: August 23, 2012Inventors: Erten Eser, Shannon Fields
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Patent number: 8227040Abstract: A method for forming an inorganic or hybrid organic/inorganic layer on a substrate, which method comprises applying a metal alkoxide to form a layer atop the substrate and exposing the metal alkoxide layer to heat from a catalytic combustion heater in the presence of water to cure the layer is provided.Type: GrantFiled: December 28, 2007Date of Patent: July 24, 2012Assignee: 3M Innovative Properties CompanyInventors: Mark A. Strobel, Michael J. Ulsh, Christopher S. Lyons, Judith M. Invie
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Patent number: 8221842Abstract: The present invention provides a metallic laminate and a method for preparing the same. The metallic laminate includes a metal layer, and at least one polyimide resin layer. The polyimide resin layer has a modulus of elasticity of 70 Mpa at 400° C.Type: GrantFiled: March 6, 2007Date of Patent: July 17, 2012Assignee: LG Chem, Ltd.Inventors: Byung-Nam Kim, Heon-Sik Song, Joo-Eun Ko, Soon-Yong Park, Jung-Jin Shim
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Patent number: 8206788Abstract: In the manufacture of electronic devices that use porous dielectric materials, the properties of the dielectric in a pristine state can be altered by various processing steps. In a method for restoring and preserving the pristine properties of a porous dielectric layer, a substrate is provided with a layer of processed porous dielectric on top, whereby the processed porous dielectric is at least partially exposed. A thin aqueous film is formed at least on the exposed parts of the processed porous dielectric. The exposed porous dielectric with the aqueous film is exposed to an ambient containing a mixture comprising at least one silylation agent and dense CO2, resulting in the restoration and preservation of the pristine properties of the porous dielectric.Type: GrantFiled: July 3, 2007Date of Patent: June 26, 2012Assignee: IMECInventors: Fabrice Sinapi, Jan Alfons B. Van Hoeymissen
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Patent number: 8158204Abstract: For making ceramic or oxidic layers (CL/OL) on substrates (S), the method according to the invention therefore provides that following application (I) and drying (II) of a suitable precursor (P) the formed precursor layer (PLD) is gassed (III) with a moist reactant gas (RG) for conversion into a corresponding hydroxide or complex layer (HL) and then thermally treated (IV) for forming a ceramic or oxidic layer (CL/OL). For the alternative production of other chalcogenidic layers of increased material conversion additional gassing is carried out with a reactant gas containing chalcogen hydrogen. Metallic layers may alternatively be made by use of a reducing reactant gas. The methods in accordance with the invention may be used wherever surfaces, even those of shaded structures, must be protected or modified or provided with functional layers, particularly in solar and materials technology.Type: GrantFiled: April 6, 2000Date of Patent: April 17, 2012Assignee: Helmholtz-Zentrum Berlin Fuer Materialien und Energie GmbHInventors: Christian-Herbert Fischer, Martha Christina Lux-Steiner, Hans-Juergen Baecker
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Publication number: 20120082793Abstract: Dispersoids having metal-oxygen groups that are suitable for the production of metal oxide thin-films at a low temperature of 200° C. or below and for the production of homogeneous organic-inorganic hybrid materials. The dispersoid having metal-oxygen bonds may be obtained by mixing a metal compound having at least three hydrolyzable groups with at least 0.5 mole but less than 2 moles of water per mole of the metal compound in an organic solvent, in the absence of an acid, a base, and/or a dispersion stabilizer, and at a temperature at or below the temperature at which the metal compound begins to hydrolyze, then raising the temperature to at least the temperature at which hydrolysis begins.Type: ApplicationFiled: December 14, 2011Publication date: April 5, 2012Applicant: NIPPON SODA CO., LTD.Inventors: Nobuo KIMURA, Yoshitaka FUJITA, Norifumi NAKAMOTO, Motoyuki TOKI, Akiji HIGUCHI, Kazuo ONO, Tomoya HIDAKA, Hiroyuki TAKEDA
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Publication number: 20120073439Abstract: Synthesis of a support material impregnated with silver sulfide provides a sorbent composition. Generating the silver sulfide relies on reaction of sulfur dioxide and one of hydrogen gas and hydrogen sulfide in presence of the support material following silver loading of the support material. Contacting a fluid stream with the sorbent composition removes heavy metal from the fluid stream.Type: ApplicationFiled: September 23, 2011Publication date: March 29, 2012Applicant: CONOCOPHILLIPS COMPANYInventors: Roland SCHMIDT, Mark A. HUGHES, John Michael HAYS, Robert William MORTON, Jon M. NELSON
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Publication number: 20120070667Abstract: Processes for growing carbon nanotubes on carbon fiber substrates are described herein. The processes can include depositing a catalyst precursor on a carbon fiber substrate, optionally depositing a non-catalytic material on the carbon fiber substrate, and after depositing the catalyst precursor and the optional non-catalytic material, exposing the carbon fiber substrate to carbon nanotube growth conditions so as to grow carbon nanotubes thereon. The carbon nanotube growth conditions can convert the catalyst precursor into a catalyst that is operable for growing carbon nanotubes. The carbon fiber substrate can remain stationary or be transported while the carbon nanotubes are being grown. Optionally, the carbon fiber substrates can include a barrier coating and/or be free of a sizing agent. Carbon fiber substrates having carbon nanotubes grown thereon are also described.Type: ApplicationFiled: September 13, 2011Publication date: March 22, 2012Applicant: APPLIED NANOSTRUCTURED SOLUTIONS, LLCInventors: Brandon K. Malet, Tushar K. Shah
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Publication number: 20120064332Abstract: Methods for growing carbon nanotubes on glass substrates, particularly glass fiber substrates, are described herein. The methods can include depositing a catalytic material or a catalyst precursor on a glass substrate; depositing a non-catalytic material on the glass substrate prior to, after, or concurrently with the catalytic material or catalyst precursor; and exposing the glass substrate to carbon nanotube growth conditions so as to grow carbon nanotubes thereon. The glass substrate, particularly a glass fiber substrate, can be transported while the carbon nanotubes are being grown thereon. Catalyst precursors can be converted into a catalyst when exposed to carbon nanotube growth conditions. The catalytic material or catalyst precursor and the non-catalytic material can be deposited from a solution containing water as a solvent. Illustrative deposition techniques include, for example, spray coating and dip coating.Type: ApplicationFiled: September 12, 2011Publication date: March 15, 2012Applicant: APPLIED NANOSTRUCTURED SOLUTIONS, LLCInventors: Brandon MALET, Tushar Shah
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Publication number: 20120040099Abstract: The present invention relates to a sedimentation-stable sol which, in addition to a copper(II) salt, also comprises at least one further metallic salt, an additive which is contained ensuring that the metallic salts contained in the sol remain dissolved or in dispersion. Furthermore, the sol is suitable in the method according to the invention for producing a metallic mixed oxide layer on a substrate, the metallic mixed oxide layer having a delafossite structure. Likewise, a substrate which has a metallic mixed oxide layer with a delafossite structure and also possibilities of use thereof are indicated according to the invention.Type: ApplicationFiled: July 6, 2009Publication date: February 16, 2012Applicant: Fraunhofer-Gesellschaft Zur Förderung Der Angewandten Forschung E.V.Inventors: Stefan Götzendörfer, Peer Löbmann, Martina Kapuschinski
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Publication number: 20120028011Abstract: A hermetic thin film includes a first inorganic layer and a second inorganic layer contiguous with the first inorganic layer, wherein the second inorganic layer is formed as a reaction product of the first inorganic layer with oxygen and has a molar volume that is about ?1% to 15% greater than a molar volume of the first inorganic layer. An equilibrium thickness of the second inorganic layer is at least 10% of but less than an as-deposited thickness of the first inorganic layer.Type: ApplicationFiled: September 10, 2010Publication date: February 2, 2012Inventors: CHONG Pyung An, Mark Alejandro Quesada
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Publication number: 20120028123Abstract: Provided are a substrate on which carbon nanotubes each having one end connected to the substrate can be formed at a high synthetic rate and from which the carbon nanotubes are less likely to be peeled off. The substrate is a substrate for forming the carbon nanotubes and includes a buffer layer 13 formed on at least one of surfaces of a substrate main body 14 and containing aluminum atoms and fluorine atoms. The carbon nanotube complex includes the substrate and a plurality of carbon nanotubes 11 each having one end connected to a surface of the buffer layer 13.Type: ApplicationFiled: February 14, 2011Publication date: February 2, 2012Inventors: Takuma Asari, Hironori Kumagai, Shigeo Hayashi, Yasuhiro Hashimoto, Naoki Yoshikawa, Takashi Okada
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Publication number: 20120021224Abstract: Methods for making composite membranes (graphene/graphene oxide platelet composite membranes) and methods of aligned transfer of such composite membranes to substrates are shown. Compositions and devices that include such composite membranes are further shown.Type: ApplicationFiled: June 2, 2011Publication date: January 26, 2012Applicant: CLEAN ENERGY LABS, LLCInventors: William Neil Everett, William Martin Lackowski, Joseph F. Pinkerton
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Publication number: 20120012004Abstract: The invention relates to thin, hydrogen-permeable, sulfur-resistant membranes formed from multi-layers of palladium or palladium-alloy coatings on porous, ceramic or metal supports, methods of making these membranes, methods of repairing layers of these membranes and devices that incorporate these membranes.Type: ApplicationFiled: July 15, 2011Publication date: January 19, 2012Inventors: J. Douglas Way, Oyvind Hatlevik
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Patent number: 8088443Abstract: A process to coat a shear thickening fluid onto a material which comprises emulsifying dispersions of a shear thickening fluid (STF) dissolved in a miscible carrier fluid or a partially miscible carrier fluid to form an emulsion and applying said emulsion to the material. The invention also relates to a suspoemulsion containing a shear thickening fluid which has been emulsified in a volatile solvent. The invention further relates to a method coating a material. The invention further relates to a method of a coating a material with the suspoemulsion.Type: GrantFiled: September 30, 2009Date of Patent: January 3, 2012Assignee: University of DelawareInventors: Norman J. Wagner, Caroline H. Nam
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Patent number: 8066805Abstract: Printable metal formulations, methods of making the formulations, and methods of coating or printing thin films from metal ink precursors are disclosed. The metal formulation generally includes one or more Group 4, 5, 6, 7, 8, 9, 10, 11, or 12 metal salts or metal complexes, one or more solvents adapted to facilitate coating and/or printing of the formulation, and one or more optional additives that form (only) gaseous or volatile byproducts upon reduction of the metal salt or metal complex to an elemental metal and/or alloy thereof. The formulation may be made by combining the metal salt(s) or metal complex(es) and the solvent(s), and dissolving the metal salt(s) or metal complex(es) in the solvent(s) to form the formulation. Thin films may be made by coating or printing the metal formulation on a substrate; removing the solvents to form a metal-containing precursor film; and reducing the metal-containing precursor film.Type: GrantFiled: May 30, 2008Date of Patent: November 29, 2011Assignee: Kovio, Inc.Inventors: Fabio Zürcher, Aditi Chandra, Wenzhuo Guo, Erik Scher, Mao Takashima, Joerg Rockenberger
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Publication number: 20110262646Abstract: Natural biopolymers in the form of cellulose nanocrystals (CNC) are shown to have the required characteristics to serve as chemically reactive biotemplates for metallic and semiconductor nanomaterial synthesis. Silver (Ag), gold (Au), copper (Cu) and platinum (Pt), cadmium sulfide (CdS), zinc sulfide (ZnS) and lead sulfide (PbS) nanoparticles, nanoparticle chains and nanowires may be synthesized on CNCs by exposing metallic precursor salts to a cationic surfactant, cetyltrimethylammonium bromide (CTAB), and a reducing agent. The nanoparticle density and particle size may be controlled by varying the concentration of CTAB, pH of the salt solution, as well as the reduction time or reaction time between the reducing agent and the metal precursor.Type: ApplicationFiled: February 9, 2011Publication date: October 27, 2011Applicant: PURDUE RESEARCH FOUNDATIONInventors: Lia Antoaneta Stanciu, Sonal Padalkar, Robert John Moon
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Publication number: 20110236703Abstract: Provided is a method of preparing a film including the steps of providing a polymer substrate, depositing a metal layer on the polymer substrate in a metallization chamber, removing the metallized film from the metallization chamber, and applying a topcoat to said metal layer within 1 week of depositing the metal layer on the polymer substrate. A film produced by such a method exhibits improved barrier properties, such as improved water-vapor transmission rates.Type: ApplicationFiled: September 9, 2009Publication date: September 29, 2011Inventor: Dennis E. McGee
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Patent number: 8021720Abstract: A process for extending the cyclic service life of thermal barrier coatings made of yttrium-stabilized zirconium oxide (YSZ) or the like which have been applied to a substrate with an oxidizing bond coat in between includes increasing or long-term stabilizing the strain tolerance of the thermal barrier coating.Type: GrantFiled: January 16, 2008Date of Patent: September 20, 2011Assignee: Alstom Technology LtdInventors: Frigyes Szuecs, Alexander Stankowski
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Publication number: 20110206578Abstract: Methods for activating and/or reactivating a metal oxide surface for deposition, immobilizing, and/or growing a biological sample (e.g., an oligonucleotide, a polynucleotide, functionalized particle, a polymer, etc.) thereon are disclosed. The metal oxide surface (e.g., zirconium oxide) can be activated and/or reactivated by exposing the metal oxide surface to various activation and/or treatment protocols capable of enhancing a slide's activity relative to the activity of an untreated slide. The activation and/or treatment protocol can include subjecting the slide (or at least the metal oxide layer) to an oxygen plasma treatment and/or a peroxide solution for an amount of time sufficient to activate and/or reactivate the metal oxide surface. Activated sequencing slides capable of incorporation, for example, into various embodiments of a flow cell for use in NGS platforms are also disclosed herein.Type: ApplicationFiled: February 23, 2011Publication date: August 25, 2011Applicant: LIFE TECHNOLOGIES CORPORATIONInventors: Evan Foster, Jessica Reed, Heather Shepherd, Christina Inman, Scott Benson
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Patent number: 7972655Abstract: A method is disclosed for enhancing the corrosion resistance of a surface of a copper or copper alloy substrate. The method comprises depositing a metallic surface layer comprising a precious metal on a surface of the copper or copper alloy substrate by immersion displacement plating and exposing the electronic device to an aqueous composition comprising a first organic molecule comprising at least one functional group that interacts with and protects precious metal surfaces and a second organic molecule comprising at least one functional group that interacts with and protects copper surfaces.Type: GrantFiled: November 21, 2007Date of Patent: July 5, 2011Assignee: Enthone Inc.Inventors: Joseph A. Abys, Shenliang Sun, Theodore Antonellis
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Patent number: 7972539Abstract: A process for producing a metallic-nanoparticle inorganic composite 10 includes an oxide film formation step in which an oxide film 14 having micropores is formed on a substrate by a sol-gel method in which a metal alkoxide is partly hydrolyzed by the action of an acid catalyst, a tin deposition step in which the oxide film 14 is brought into contact with an acidic aqueous solution of tin chloride, an excess Sn2+ ion removal step in which Sn2+ ions are removed from the micropores, a metallic-nanoparticle deposition step in which the oxide film 14 is brought into contact with an aqueous solution of a metal chelate to deposit metallic nanoparticles 12 in the micropores, and an excess metal ion removal step in which metal ions are removed from the micropores; and a metallic-nanoparticle inorganic composite 10 is produced by this process.Type: GrantFiled: September 25, 2008Date of Patent: July 5, 2011Assignee: Kabushiki Kaisha ToshibaInventors: Miho Maruyama, Kenji Todori, Tsukasa Tada, Reiko Yoshimura, Yasuyuki Hotta, Ko Yamada, Masakazu Yamagiwa
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Patent number: 7968149Abstract: A regeneration apparatus for an electroless plating solution, which includes a sensor for measuring the formation rate of phosphorous acid formed in a plating tank in response to a plating treatment, a split device for taking out a plating solution in the plating tank to transfer the plating solution to a first processing tank, a sensor for measuring the concentration of the phosphorous acid contained in the plating solution taken out, an addition device for supplying calcium carbonate or calcium hydroxide, an amount of which is required for producing a calcium phosphite from the phosphorous acid contained in the plating solution, to the first processing tank, a separation device for separating and removing the calcium phosphite produced in the first processing tank from the plating solution, and a return pump for transferring the plating solution from which the calcium phosphite has been separated and removed to the plating tank.Type: GrantFiled: December 30, 2010Date of Patent: June 28, 2011Assignee: Murata Co., Ltd.Inventors: Hidenori Takagami, Hiroshi Kawakami, Kazuhiko Kato
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Publication number: 20110123815Abstract: A method of manufacturing a decorative article, including a first coating formation step of forming a first coating of primarily TiN on a substrate; a second coating formation step of forming a second coating on the first coating by means of a dry plating method using a target containing 70.0 wt %?85.0 wt % Au and 15.0 wt %?30.0 wt % Cu; a heat treatment step of promoting formation of a solid solution of the constituents of the second coating by applying a heating process that heats the substrate on which the first coating and the second coating are disposed to 300° C.?395° C. and then applying a cooling process; and an acid treatment step that, of the constituents of the second coating to which the heating process was applied, removes the constituents not forming a solid solution by applying an acid treatment.Type: ApplicationFiled: November 19, 2010Publication date: May 26, 2011Applicant: SEIKO EPSON CORPORATIONInventors: Atsushi KAWAKAMI, Yuzuru TSUKAMOTO
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Patent number: 7931940Abstract: A method for producing a silica aerogel film by hydrolyzing and polymerizing alkoxysilane in the presence of a base catalyst to prepare an alkaline sol, adding an acid catalyst to the alkaline sol to carry out further hydrolysis and polymerization to prepare a first acidic sol, hydrolyzing and polymerizing alkoxysilane in the presence of an acid catalyst to prepare a second acidic sol, applying a mixture of the first and second acidic sols to a substrate, and drying it.Type: GrantFiled: August 27, 2008Date of Patent: April 26, 2011Assignee: Hoya CorporationInventors: Mineta Suzuki, Takanobu Shiokawa, Kazuhiro Yamada, Hiroyuki Nakayama, Hideki Yamaguchi, Ayako Maruta
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Publication number: 20110081542Abstract: A process for the production of a substrate having antimicrobial properties is described. It comprises a step consisting of the déposition of a métal non-gelling layer comprising an inorganic antimicrobial agent, starting from a precursor, in métal, colloid, chelate or ion form on at least one of the surfaces of the glass substrate; and a step consisting of the diffusion of the agent into said at least one surface of the substrate by thermal treatment. Alternatively, the substrate may be coated with an underlayer or a topcoat and the diffusion occurs either in the underlayer or in the topcoat. Glass and metallic substrates having antimicrobial properties are also described. In particular, a substrate exhibiting a bactericidal activity measured in accordance with standard JIS Z 2801 of higher than log 2.Type: ApplicationFiled: December 16, 2005Publication date: April 7, 2011Applicant: AGC FLAT GLASS EUROPE S.A.Inventors: Georges Pilloy, Christophe Ego, Jean-Pierre Poels, Muriel Tournay, Andre Hecq, Kadosa Hevesi, Nadia Jacobs
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Patent number: 7892603Abstract: A regeneration apparatus for an electroless plating solution includes a sensor for measuring the formation rate of phosphorous acid formed in a plating tank in response to a plating treatment, a split device for taking out a plating solution in the plating tank to transfer the plating solution to a first processing tank, a sensor for measuring the concentration of the phosphorous acid contained in the plating solution taken out, an addition device for supplying calcium carbonate or calcium hydroxide, an amount of which is required for producing a calcium phosphite from the phosphorous acid contained in the plating solution, to the first processing tank, a separation device for separating and removing the calcium phosphite produced in the first processing tank from the plating solution, and a return pump for transferring the plating solution from which the calcium phosphite has been separated and removed to the plating tank.Type: GrantFiled: July 7, 2006Date of Patent: February 22, 2011Assignee: Murata Co., Ltd.Inventors: Hidenori Takagami, Hiroshi Kawakami, Kazuhiko Kato
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Publication number: 20110036478Abstract: The invention relates to a method for producing coated spring-loaded steel rails especially for windshield wipers comprising a rubber or elastomer wiper blade, wherein a cold-rolled steel rail blank is provided with a zinc layer, whereafter a zinc-containing anchor layer is produced, and a coating made of a polymerizable coating powder is deposited on the anchor layer and partially cured.Type: ApplicationFiled: February 18, 2009Publication date: February 17, 2011Applicant: Stahlwerk Ergste Westig GmbHInventors: Victor Castro, Oskar Pacher
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Patent number: 7858184Abstract: A method for producing fine, coated metal particles comprising the steps of mixing Ti-containing powder except for Ti oxide powder with oxide powder of a metal M, an M oxide having a standard free energy of formation meeting the relation of ?GM-O>?GTiO2; and heat-treating the resultant mixed powder at a temperature of 650-900° C. in a non-oxidizing atmosphere, thereby reducing the oxide of the metal M with Ti to provide the resultant fine particles of the metal M with TiO2-based titanium oxide coating.Type: GrantFiled: March 15, 2006Date of Patent: December 28, 2010Assignee: Hitachi Metals, Ltd.Inventors: Hisato Tokoro, Shigeo Fujii
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Publication number: 20100310795Abstract: An ink jet recording medium having a gas-permeable substrate, and an ink receiving layer and a surface layer provided in that order on the gas-permeable substrate, wherein the surface layer is formed through the steps of (1) applying a coating liquid comprising a first inorganic pigment and a binder onto the ink receiving layer, and (2) applying a coagulating liquid comprising a coagulant and a second inorganic pigment having a refractive index higher by 0.30 or more than that of the above first inorganic pigment and an average particle size of 100 nm or less onto the applied coating liquid to subject the coating liquid to a coagulating treatment followed by pressing a coating layer including the coating liquid and the coagulating liquid against a heated casting drum while the coating layer is in a wet condition to subject the coating layer to a cast treatment.Type: ApplicationFiled: April 28, 2010Publication date: December 9, 2010Applicant: CANON KABUSHIKI KAISHAInventors: Takatoshi Tanaka, Hiroshi Asakawa, Hitoshi Nagashima, Takeshi Tsurusaki, Saki Suzuki
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Publication number: 20100304158Abstract: The various embodiments herein provide a method and composition to produce an anti-corrosive layer. According to one embodiment herein, a titanium based sol is synthesized and deposited on a substrate, dried for 120° C. for 1 hour, calcinated upto 400° C. for 1 hour, doped with a corrosion inhibitor, dried and deposited a layer of hybrid silica sol and cured to obtain the anticorrosive layer. According to another embodiment, a surface pre-treatment coating has a composition comprising a titanium dioxide layer, a corrosion inhibitor doped on the titanium dioxide layer, a hybrid silicate layer deposited on the doped titanium layer to form a coating to provide an improved corrosion resistance and self-healing effect.Type: ApplicationFiled: July 3, 2010Publication date: December 2, 2010Applicant: SHAHID BAHONAR UNIVERSITY OF KERMANInventors: Sayed Morteza Madani, Maryam Ehteshamzadeh, Hassan Hashemipour Rafsanjani
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Publication number: 20100291302Abstract: A protected article is prepared by providing the article, depositing a bond coat onto an exposed surface of the article, and producing a thermal barrier coating on an exposed surface of the bond coat. The step of producing the thermal barrier coating includes the steps of depositing a primary ceramic coating onto an exposed surface of the bond coat, and depositing a stabilization composition onto an exposed surface of the primary ceramic coating. The stabilization composition includes a first element selected from Group 2 or Group 3 of the periodic table, and a second element selected from Group 5 of the periodic table. The atomic ratio of the amount of the first element to the amount of the second element is at least 1.3, more preferably at least 1:1.Type: ApplicationFiled: March 12, 2007Publication date: November 18, 2010Applicant: GENERAL ELECTRIC COMPANYInventors: John Frederick Ackerman, Venkat Subramanian Venkataramani, Irene T. Spitsberg, Brett Allen Rohrer Boutwell, Ramgopal Darolia
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Publication number: 20100291303Abstract: A method is disclosed for enhancing the corrosion resistance of a surface of a copper or copper alloy substrate. The method comprises depositing a metallic surface layer comprising a precious metal on a surface of the copper or copper alloy substrate by immersion displacement plating and exposing the electronic device to an aqueous composition comprising a first organic molecule comprising at least one functional group that interacts with and protects precious metal surfaces and a second organic molecule comprising at least one functional group that interacts with and protects copper surfaces.Type: ApplicationFiled: November 21, 2007Publication date: November 18, 2010Applicant: Enthone Inc.Inventors: Joseph A. Abys, Shenliang Sun, Theodore Antonellis
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Publication number: 20100285224Abstract: The use of pervious concrete has been rapidly growing as a means to meet burgeoning stormwater regulations. A difficulty in placement of pervious concrete has been the need to rapidly cover the material after placement and leave it covered for seven days to ensure moisture is not lost and the cement paste fully cures. Surface unraveling is a common cause of failure of pervious concrete installations due to rapid moisture loss from the cement paste of the freshly placed pervious concrete mixture. By adding to the pervious concrete mixture an internal curing agent which holds and releases moisture in a controlled manner to the cement paste as it cures, the likelihood of under-cured cement paste and surface raveling of the pervious concrete is greatly reduced. This invention comprises materials and methods for their use which provide a source of moisture with controlled release for curing of the cement portion of pervious concrete.Type: ApplicationFiled: May 11, 2009Publication date: November 11, 2010Inventor: Dale Fisher