With Water Patents (Class 427/353)
  • Patent number: 6715316
    Abstract: Removable coatings for protecting glass sheets and, in particular, for protecting LCD glass sheets during cutting, grinding, shipping, and/or storage are provided. The coatings comprise one or more polysaccharides, with the preferred polysaccharides being starches composed of a mixture of amylose and amylopectin molecules. The coatings can be removed from the glass sheets using water solutions, e.g., a mild detergent solution, in combination with, for example, ultrasonic cleaning and/or brush cleaning. After removal, the glass sheets have substantially the same surface characteristics and chemistry as untreated sheets and also have particle/contamination levels equivalent to those of control sheets held in a clean environment.
    Type: Grant
    Filed: August 27, 2001
    Date of Patent: April 6, 2004
    Assignee: Corning Incorporated
    Inventors: Lin He, Adrienne M. Powell-Johnson, Youchun Shi
  • Patent number: 6689418
    Abstract: An apparatus for and method of rinsing one side of a two-sided substrate and removing unwanted material from the substrate's edge and/or backside. One embodiment of the method is directed toward rinsing and cleaning a substrate having a front side upon which integrated circuits are to be formed and a backside. This embodiment includes dropping the substrate front side down onto a pool of rinsing liquid in a manner such that the front side of the substrate is in contact with the solution while the substrate is held in suspension by the surface tension of the solution liquid thereby preventing the backside of the substrate from sinking under an upper surface of the pool. Next, while the substrate is in suspension in said rinsing liquid, the substrate is secured by its edge with a first set of fingers and in some embodiments the substrate is subsequently spun. In another embodiment, a method of forming a copper layer on a front side of a substrate is disclosed.
    Type: Grant
    Filed: August 3, 2001
    Date of Patent: February 10, 2004
    Assignee: Applied Materials Inc.
    Inventors: Donald J. K. Olgado, Avi Tepman, Yeuk-Fai Edwin Mok, Arnold V. Kholodenko
  • Patent number: 6592929
    Abstract: A method is used to expose a fingerprint on the surface of a metallic object which is covered with a layer of a metallic oxide such as rust. The metallic oxide is dissolved with a reagent which reacts with the metallic oxide. The dissolved metallic oxide is removed from the surface of the metallic object by washing with water to expose the fingerprint and a permanent copy is made of the fingerprint. More specifically, rust from a ferrous object is dissolved with an aqueous acid, the acid and dissolved rust is washed away with water, and a photograph is taken of the exposed fingerprint. The rust can also be dissolved by spraying the rust with a Precision Brand Step #3 Aerosol Rust Inhibitor and Lubricant. The rust can be removed by contacting the rust with a reagent containing a complexing agent for Fe(III) ions.
    Type: Grant
    Filed: August 24, 2001
    Date of Patent: July 15, 2003
    Inventors: Ladislav H. Berka, Brian D. Elolampi
  • Patent number: 6582834
    Abstract: An anti-stick coating that inhibits the adhesion of contaminants that form deposits on the internal cooling passages of gas turbine engine components. The anti-stick coating is formed as an outer coating of the internal cooling passages, and preferably overlies an environmental coating such as a diffusion aluminide coating formed on the passage surfaces. The outer coating has a thickness of not greater than three micrometers, and is resistant to adhesion by dirt contaminants as a result of comprising at least one layer of tantala, titania, hafnia, niobium oxide, yttria, silica and/or alumina. The outer coating is preferably deposited directly on the environmental coating by chemical vapor deposition.
    Type: Grant
    Filed: June 12, 2001
    Date of Patent: June 24, 2003
    Assignee: General Electric Company
    Inventors: Bangalore Aswatha Nagaraj, Ching-Pang Lee, William Randolph Stowell, Aaron Dennis Gastrich
  • Patent number: 6560870
    Abstract: A method for applying diffusion aluminide coating on a selective area of a turbine engine component and the coating produced by that method is disclosed. A quartz infrared lamp heats only substantially the localized area of the component to be coated, rather than the complete part. Either halide activated or non-activated tape is applied on the area to be coated and is held in place during coating using a high temperature dimensionally stable tape holder manufactured from graphite or ceramic. The quartz infrared lamp is used to heat only the desired area to a coating temperature of about 1800° F. to about 2000° F. under an inert atmosphere for about 3 to about 8 hours to achieve the desired aluminide coating thickness. No powder masking of the machined surface area is required. Due to the localized heating, aluminum vapor generated from the tape will only deposit aluminide coating on the taped area.
    Type: Grant
    Filed: May 8, 2001
    Date of Patent: May 13, 2003
    Assignee: General Electric Company
    Inventors: Nripendra Nath Das, Raymond William Heidorn, Walter Michael Gmerek, Jr., David Andrew Jablonka
  • Patent number: 6531047
    Abstract: A surface modification method for an aluminum substrate, which comprises treating a Ni—P plated aluminum substrate with a functional water having a plus or minus oxidation-reduction potential for a predetermined period of time in a washing step after a polishing step of the Ni—P plated aluminum substrate.
    Type: Grant
    Filed: June 6, 2000
    Date of Patent: March 11, 2003
    Assignee: Mediken Inc.
    Inventors: Takamitsu Kato, Mitsugi Maekawa, Yuichi Hyakusoku, Tadao Tokushima, Masaaki Kato
  • Patent number: 6517401
    Abstract: The invention provides methods of forming a monomolecular chemisorption film having an excellent uniformity and liquid crystal alignment performance with a high production efficiency. The monomolecular chemisorption film of the invention can be suitably used for liquid crystal alignment layers.
    Type: Grant
    Filed: May 18, 2000
    Date of Patent: February 11, 2003
    Assignee: Matsushita Electric Industrial Co., Ltd.
    Inventors: Kazufumi Ogawa, Tadashi Ohtake, Takaiki Nomura
  • Patent number: 6495211
    Abstract: A process for producing a substrate 1 having a base-metal plating layer, which includes an immersion step for immersing the substrate 1 in a plating solution contained in a plating tank 33, to thereby form a base-metal plating layer; a washing step for removing the substrate 1 from the plating tank 33, transferring the substrate 1 to a washing tank, and washing the substrate 1; and a cooling step for applying a cooling liquid to the substrate 1 during at least a portion of the period during which the substrate is transferred to a position where the washing step is carried out after completing the immersion step, to thereby cool the substrate 1. An apparatus for carrying out the above process is also disclosed.
    Type: Grant
    Filed: June 18, 2001
    Date of Patent: December 17, 2002
    Assignee: NGK Spark Plug Co., Ltd.
    Inventors: Masahiro Iba, Hisashi Wakako, Kazuhisa Sato, Hiroyuki Hashimoto, Yasuo Doi
  • Patent number: 6475299
    Abstract: Disclosed are a conversion coating composition for use in the surface treatment of a PCB and a conversion coating method using the same. The composition comprises 0.1-30 vol % of sulfuric acid; 0.1-15 vol % of hydrogen peroxide; 0.01-10 wt % of an organic acid; 0.1-30 wt % of a nitrogen compound; 0.01-10 wt % of an organic silicate and/or organic titanate; and 0.1-20 wt % of a film forming auxiliary, 0.1-30 wt % of an etching rate controller, 0.1-20 wt % of a reaction promoter and/or 0.1-20 g/l of a stabilizer. This composition is applied to a PCB at 10-60° C. for 1-10 min. The conversion coating film is superb in adhesive strength, acid resistance, and adhesion and can be formed with ease.
    Type: Grant
    Filed: July 7, 2000
    Date of Patent: November 5, 2002
    Assignees: Samsung Electro-Mechanics Co., Ltd., SD Chemical Co., Ltd.
    Inventors: Byong Ho Lee, Dek Gin Yang, Yang Je Lee, Myong Gun Chong, Jae Ok Lim, Sung Wook Chun, Min Eui Hong, Kyu Hong An
  • Publication number: 20020147319
    Abstract: A method and apparatus for selectively applying a print material onto a substrate for the synthesis of an array of oligonucleotides at selected regions of a substrate. The print material includes a barrier material, a monomer sequence, a nucleoside, a deprotection agent, a carrier material, among other materials. The method and apparatus also relies upon standard DMT based chemistry, and a vapor phase deprotection agent such as solid TCA and the like.
    Type: Application
    Filed: April 24, 2001
    Publication date: October 10, 2002
    Applicant: Affymetrix, Inc.
    Inventors: R. Fabian Pease, Glenn McGall, Martin J. Goldberg, Richard P. Rava, Stephen P.A. Fodor, Virginia Goss, Lubert Stryer, James L. Winkler
  • Publication number: 20020127331
    Abstract: At least one monomolecule film is formed on a transparent substrate surface directly or via a protective film.
    Type: Application
    Filed: April 19, 2002
    Publication date: September 12, 2002
    Inventors: Kazufumi Ogawa, Norihisa Mino, Mamoru Soga
  • Patent number: 6448304
    Abstract: An optical material, particularly a plastic lens for spectacles, which absorbs almost all UV rays of up to around 400 nm or so and is not too yellow, is obtained by dipping a poly(thio)urethane material or a diethylene glycol bisallylcarbonate polymer material in a solution containing: (1) a dibenzoylmethane compound of a general formula (1): wherein R and R′ each represent a linear or branched alkyl or alkoxyl group having from 1 to 8 carbon atoms; and n and n′ are the same or different integers, each falling between 0 and 3, or (2) a benzotriazole compound of a general formula (2): wherein R″ represents a hydrogen atom, a chlorine atom or a bromine atom; and m and m′ each indicate 1 or 2.
    Type: Grant
    Filed: September 20, 2000
    Date of Patent: September 10, 2002
    Assignee: Hoya Corporation
    Inventors: Masahisa Kosaka, Shinsuke Itoh
  • Patent number: 6372160
    Abstract: A process for preparing a mold used for producing, for example, high resilience polyurethane foamed articles, comprises the step of spraying an aqueous release compound on the inner, article-contacting surface of the mold, the release compound including: an aqueous carrier; and a release agent which forms a release film on the article-contacting surface, wherein the release film is formed by evaporating a majority of the aqueous carrier. An aqueous rinse solution is gently sprayed on the inner mold surface after formation of the release film. The rinse solution, now carrying residual water, emulsifier(s) and/or contaminants, is mechanically removed via an air entrainment device before significant evaporation of the rinse solution has taken place.
    Type: Grant
    Filed: June 14, 1999
    Date of Patent: April 16, 2002
    Assignee: Genesee Polymers Corporation
    Inventor: Steven S. Kendall
  • Patent number: 6346295
    Abstract: Process for the alkaline passivation of galvanized and alloy-galvanized steel surfaces and of aluminum in strip lines, wherein the metal surfaces are brought into contact with an alkaline aqueous solution that contains complexing agents and iron, which has a free alkalinity in the range of 5 to 20 points and a total alkalinity in the range of 7 to 30 points and contains: 0.1 to 1 g/l magnesium ions, 0.1 to 1 g/l iron (III) ions and 0.5 to 5 g/l amino or hydroxy carboxylate ions. This may be followed by a chrome-containing or chrome-free secondary passivation.
    Type: Grant
    Filed: April 5, 2000
    Date of Patent: February 12, 2002
    Assignee: Henkel Kommanditgesellschaft auf Aktien
    Inventors: Joerg Riesop, Heike Krautbauer
  • Patent number: 6294222
    Abstract: A method of attaching a substantially uniform distribution of particulates to individual exposed surfaces of a matrix of fibrous material. The method includes the following steps: 1) electrically charging a matrix of fibrous material having individual exposed surfaces to create a substantially uniform distribution of charged sites at the exposed surfaces; 2) applying particulates to the charged matrix of fibrous material so that at least some particulates adhere at the charged sites; and 3) attaching particulates adhering to the fibrous material at charged sites by substantially non-transient bonding.
    Type: Grant
    Filed: June 10, 1996
    Date of Patent: September 25, 2001
    Assignee: Kimberly-Clark Worldwide, Inc.
    Inventors: Bernard Cohen, Judith Katherine Faass, Lamar Heath Gipson, Lee Kirby Jameson
  • Patent number: 6280796
    Abstract: A method for producing cylinder linings in an aluminum or magnesium engine block for an internal combustion engine utilizes plasma spraying of a mixture of powdered molybdenum and powdered steel containing from about 10 to about 70 wt. % molybdenum and from about 90 to about 30 wt. % steel. The resulting slide layer has good adhesion to the engine block and has high wear resistance.
    Type: Grant
    Filed: March 23, 2000
    Date of Patent: August 28, 2001
    Assignee: Volkswagen AG
    Inventors: Manfred Kloft, Reinhard Strich, Udo Schlegel
  • Patent number: 6255228
    Abstract: A method for removing contaminants from a semiconductor wafer having a spin on coating of material. Contaminants are removed by applying a cleaning solution to the periphery, and preferably, the exposed backside of the wafer after the edge bead has been dissolved and removed. The cleaning solution is formulated to react chemically with unwanted coating material residue to form a compound that may be ejected from the periphery of the spinning wafer. Any residual solution or precipitate that is not ejected from the wafer may be rinsed away with water, preferably deoinized water. One exemplary use of this method is the removal of metallic contaminants that may be left on the periphery and backside of a wafer after the formation of ferroelectric film coatings. A cleaning solution comprising a mixture of hydrochloric acid HCl and water H2O or ammonium hydroxide NH4OH and water H2O is applied to the periphery of the spinning wafer.
    Type: Grant
    Filed: May 30, 2000
    Date of Patent: July 3, 2001
    Assignee: Micron Technology, Inc.
    Inventor: J. Brett Rolfson
  • Patent number: 6231926
    Abstract: A process for producing poromeric synthetic leather comprises I. producing an essentially nonporous impregnate by impregnating a textile sheet material with an aqueous polyurethane dispersion and drying, and II. producing a poromeric synthetic leather from the impregnate by subjecting the impregnate to the action of an aqueous solution of a Brønsted base.
    Type: Grant
    Filed: June 4, 1999
    Date of Patent: May 15, 2001
    Assignee: BASF Aktiengesellschaft
    Inventors: Cesare Ronzani, Ralf Mossbach, Karl Häberle
  • Patent number: 6224945
    Abstract: The process consists in dissolving a photochromic agent in a solvent, in impregnating the polymeric material with the solution of photochromic agent and in rinsing the polymeric material with an aqueous solution in order to replace the solvent with the aqueous solution. Application: to contact lenses.
    Type: Grant
    Filed: September 7, 1999
    Date of Patent: May 1, 2001
    Assignee: Essilor International Compagnie Generale d'Optique
    Inventor: Isabelle Calderara
  • Patent number: 6224986
    Abstract: A neodymium/iron/boron permanent magnet is provided with high corrosion resistance by forming a coating layer of a vitrified sodium silicate on the surface. The vitreous coating layer of sodium silicate is formed by coating the surface of the permanent magnet with an aqueous coating solution of water glass followed by drying of the coating layer and vitrification of the dried coating layer by a heat treatment under specified conditions. Characteristically, the thus formed vitreous coating layer of sodium silicate is subjected to a leaching treatment with water at a specified temperature for a specified length of time in order to remove away residual sodium content leachable in water so that the troubles due to absorption of moisture by the alkali constituent in the sodium silicate coating layer can be largely dissolved.
    Type: Grant
    Filed: July 22, 1999
    Date of Patent: May 1, 2001
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Takehisa Minowa, Masao Yoshikawa, Ryuji Hamada
  • Patent number: 6190735
    Abstract: A process for treating a fibrous material which includes the steps of: 1) providing a liquid suspension composed of fibrous material; 2) intermixing the liquid suspension of fibrous material with a treatment over a time period T1—wherein the treatment requires a period of time TR sufficient to treat the fibrous material; 3) depositing the liquid suspension of fibrous material and intermixed treatment onto a forming surface to form a layer and removing a substantial portion of the liquid, over a perod of time T2; and 4) applying pressurized jets of a liquid to the layer of fibrous material to wash unused treatment from the fibrous material within a period of time T3. Periods of time T1, T2 and T3 are immediately consecutive and amount to a total period of time at least as great as TR.
    Type: Grant
    Filed: March 25, 1999
    Date of Patent: February 20, 2001
    Assignee: Kimberly-Clark Worldwide, Inc.
    Inventors: Fred Robert Radwanski, Henry Skoog
  • Patent number: 6168674
    Abstract: In a process of phosphatizing metal surfaces, which at least partly consist of iron or steel, in accordance with the low-zinc technology, the metal surfaces are brought in contact with aqueous acid phosphatizing solutions at a temperature of 30 to 65° C. for a period of 1 to 8 min, which solutions contain 0.4 to 2.0 g/l Zn 7 to 25 g/l P2O5 0.005 to 0.5 g/l peroxide (calc. as H2O2) 0.01 to 10 g/l formate (calc. as formate ion), are free from chlorate and added nitrite, and in which the weight ratio of free P2O5 to total P2O5 has been adjusted to a value in the range from 0.03 to 0.20, and the content of free acid has been adjusted to a value in the range from 0.5 to 2.5. After contact with the phosphatizing solution, the workpiece is rerinsed with water, which has been adjusted with mineral acid to a pH of from 3.6 to 5.0.
    Type: Grant
    Filed: December 20, 1999
    Date of Patent: January 2, 2001
    Assignee: Dynamit Nobel Aktiengesellscha
    Inventors: Horst Gehmecker, Thomas Kolberg, R{umlaut over (u)}diger Rein
  • Patent number: 6139831
    Abstract: Apparatus and method for immobilizing molecules, particularly biomolecules such as DNA, RNA, proteins, lipids, carbohydrates, or hormones onto a substrate such as glass or silica; patterns of immobilization can be made resulting in addressable, discrete arrays of molecules on a substrate, having applications in bioelectronics, DNA hybridization assays, drug assays, etc.
    Type: Grant
    Filed: May 28, 1998
    Date of Patent: October 31, 2000
    Assignee: The Rockfeller University
    Inventors: Ganaganor Visweswara Shivashankar, Albert J. Libchaber
  • Patent number: 6123994
    Abstract: An ink-jet recording head employed in an ink-jet recording apparatus is disclosed. A part of the channel is composed of resin material which comprises a base resin and a highly cationic resin attached on the surface of the base resin through reaction, the resulting surface being reacted with a hydrophilic organic material. A production method of the head, an ink-jet recording apparatus and production method of the ink-jet recording apparatus are also disclosed.
    Type: Grant
    Filed: April 21, 1999
    Date of Patent: September 26, 2000
    Assignee: Konica Corporation
    Inventors: Takeshi Ito, Hideo Watanabe, Hiroyuki Nomori
  • Patent number: 6120841
    Abstract: A fabric made of fibers of a carbon-precursor cellulose material is impregnated with a composition containing at least one inorganic ingredient having a function of promoting dehydration of cellulose, and the fabric is subjected to heat treatment. This treatment consists in raising temperature at a speed lying in the range 1.degree. C./min to 15.degree. C./min followed by keeping the temperature constant in the range 350.degree. C. to 500.degree. C., and it is followed by a step of washing the fabric. This produces directly an activated fabric of carbon fibers having a specific surface area of not less than 600 m.sup.2 /g, without subsequent activation treatment at a higher temperature.
    Type: Grant
    Filed: September 13, 1999
    Date of Patent: September 19, 2000
    Assignee: Messier-Bugatti
    Inventors: Philippe Parmentier, Veronique Fontarnou, Ludovic Ouvry
  • Patent number: 6117485
    Abstract: A vehicle masking material and method of use. The masking material in one embodiment includes a dextrin, a plasticizer, and water. The masking material may additionally include a surfactant. The masking material is applied to a surface which is to be protected from paint overspray or other coating processes, allowed to dry, and the surface is coated (e.g. with paint). After drying of the paint, or other coating, the masking material is removed by water washing.
    Type: Grant
    Filed: July 24, 1998
    Date of Patent: September 12, 2000
    Assignee: Cal-West Equipment Company, Inc.
    Inventors: Edward W. Woodhall, Ronald Swidler
  • Patent number: 6114254
    Abstract: A method for removing contaminants from a semiconductor wafer having a spin on coating of material. Contaminants are removed by applying a cleaning solution to the periphery, and preferably, the exposed backside of the wafer after the edge bead has been dissolved and removed. The cleaning solution is formulated to react chemically with unwanted coating material residue to form a compound that may be ejected from the periphery of the spinning wafer. Any residual solution or precipitate that is not ejected from the wafer may be rinsed away with water, preferably deionized water. One exemplary use of this method is the removal of metallic contaminants that may be left on the periphery and backside of a wafer after the formation of ferroelectric film coatings. A cleaning solution comprising a mixture of hydrochloric acid HCl and water H.sub.2 O or ammonium hydroxide NH.sub.4 OH and water H.sub.2 O is applied to the periphery of the spinning wafer.
    Type: Grant
    Filed: October 15, 1996
    Date of Patent: September 5, 2000
    Assignee: Micron Technology, Inc.
    Inventor: J. Brett Rolfson
  • Patent number: 6103301
    Abstract: A method of forming a mark on a substrate made of plastics material comprises the step of applying a basic solution to a surface portion having a prefixed pattern of the substrate. In a preferred embodiment, the basic solution is used in combination with at least one alkali-stable water-soluble polymer, to produce a viscous liquid composition, which is advantageously applicable to the substrate by means of pad-printing and silk-screen printing process.
    Type: Grant
    Filed: November 27, 1998
    Date of Patent: August 15, 2000
    Assignee: Intercast Europe S.p.A.
    Inventors: Giuseppe Iori, Giancarlo Albanesi, Paolo Baiocchi
  • Patent number: 6099897
    Abstract: A method of producing metal particles, including the steps of forming a membrane of a polymer or oligomer which has, at the terminals of its molecule and/or in the side chains thereof, at least one functional group selected from cyano, amino and thiol groups, and depositing a metal on the membrane through vapor deposition so that the membrane has particles of the metal and/or its oxide dispersed therein.
    Type: Grant
    Filed: January 27, 1998
    Date of Patent: August 8, 2000
    Assignee: Mitsuboshi Belting Ltd.
    Inventors: Koichi Sayo, Shigehiko Hayashi, Kazuo Goto, Shigehito Deki
  • Patent number: 6086764
    Abstract: A process for the preparation of semipermeable membranes with improved acid and base stability including: (a) coating a base and acid stable ultrafiltration (UF) membrane support polymer, with a high molecular weight amphoteric polyelectrolyte coating polymer optionally in solution, the amphoteric polyelectrolyte containing both cationic and anionic groups and in addition primary and secondary amine groups, the solution optionally containing a latent internal crosslinker compound that is a polyfunctional compound that crosslinks the coating polymer only during a curing step at elevated temperatures and basic pH; (b) draining or washing the coated support; and (c) reacting the coating with a solution of an external crosslinking compound that is a polyfuntional compound, not overly reactive so as not to be hydrolyzed prematurely in solution, the time of exposure to the external crosslinking compound being sufficient to ensure its diffusion into the bulk of the coating, so that the crosslinking is effected not o
    Type: Grant
    Filed: June 10, 1998
    Date of Patent: July 11, 2000
    Assignee: Crosswinds, Inc.
    Inventors: Charles Linder, Mara Nemes, Reuven Ketraro
  • Patent number: 6056993
    Abstract: A porous, tubular synthetic prosthesis, prosthesis precursor, and methods of producing the same are provided. Specifically the method involves co-spraying both a water soluble and water insoluble fibrous component onto a mold to form the prosthesis precursor. The water soluble fibrous component may then be at least partially removed so as to provide a porous, tubular synthetic prosthesis.
    Type: Grant
    Filed: April 17, 1998
    Date of Patent: May 2, 2000
    Assignee: Schneider (USA) Inc.
    Inventors: Jacob Leidner, Karim Amellal
  • Patent number: 6033730
    Abstract: Weathered reef-building coral is immersed in an aqueous alkali solution under reduced pressure to carry out alkali washing to make the aqueous alkali solution penetrate into the weathered reef-building coral throughout its fine structure inside the porous tissue, which is subsequently washed with water until a washing from the inside of the porous tissue is neutralized.As a result of this washing, various marine algae, various microorganisms including Vibrio bacteria inhabiting the ocean and other various organic substances held in the inner fine structure of weathered reef-building coral can be removed. Thus, a weathered reef-building coral material can be obtained whose safety has been ensured. This weathered reef-building coral material is suitable for food materials, filter mediums for water purifiers and so forth.
    Type: Grant
    Filed: June 12, 1998
    Date of Patent: March 7, 2000
    Assignee: Coral Biotech Kabushiki Kaisha
    Inventors: Satoshi Yoshizumi, Toshiharu Oda
  • Patent number: 6017582
    Abstract: A wiping strip for a motor vehicle screen wiper is in the form of a profiled element of vulcanised material consisting of rubber or an elastomeric material, having a surface layer for reducing the coefficient of friction between the wiping strip and a glass surface to be wiped. The surface layer is formed by immersion of the profiled element in a solution, or by exposing the profiled element to the solution in atomised form. The solution consists of a solvent with a powder, such as graphite, dispersed in it. The step of forming the surface layer is carried out during the step of vulcanising the material of the profiled element.
    Type: Grant
    Filed: June 13, 1997
    Date of Patent: January 25, 2000
    Assignee: Valeo Systemes D'Essuyage
    Inventors: Sophie Desormiere, Michel Oulie
  • Patent number: 6017583
    Abstract: In a process for the manufacture of a strip material (1) a plastics layer (5, 6) is formed at least on one side of a support (2) from a mixture of plastics materials and particulate soluble corpuscles wherein the soluble corpuscles are leachable by a solvent of a type against which the plastics material is stable. Thereafter the soluble corpuscles are leached out from the plastics layer (5, 6) with the formation of throughflow passages. According to the invention, a plastics powder is prepared as the plastics material, which is mixed with the soluble corpuscles and applied onto the support (2). By heat and pressure treatment a plastics layer (5, 6) including therein the soluble particles, is produced from the mixture of plastics powder and soluble corpuscles, prior to the soluble corpuscles being leached at least in part out of the plastics layer (5, 6).
    Type: Grant
    Filed: September 24, 1997
    Date of Patent: January 25, 2000
    Assignee: Conrad Munzinger & Cie AG
    Inventor: Michael Gass
  • Patent number: 5965200
    Abstract: A develop processing apparatus is provided for processing an object with a developing solution, comprising a retaining member for rotatably retaining the object, a developing solution supply nozzle for supplying the developing solution to the object, a developing solution sucking nozzle for sucking the developing solution supplied to the object, a developing solution supply nozzle moving mechanism for moving the developing solution supply nozzle above the object, a developing solution sucking nozzle moving mechanism for moving the developing solution sucking nozzle above the object. After the developing solution is supplied to the object subsequent to moving the developing solution supply nozzle, the developing solution sucking nozzle is moved and the developing solution on the object is sucked.
    Type: Grant
    Filed: September 25, 1997
    Date of Patent: October 12, 1999
    Assignees: Tokyo Electron Limited, Tokyo Electron Kyushu Limited
    Inventors: Kiyohisa Tateyama, Masafumi Nomura, Takayuki Tomoeda
  • Patent number: 5960251
    Abstract: Copper-containing surfaces of substrates such as laminated electronic circuit boards are protected by organometallic coatings comprising organic compounds selected from the group consisting of benzimidazoles, alkylimidazoles, benzotriazozles and alkyltriazoles, substituted or unsubstituted, and metal particles of solder-wettable metals or metal solders. The metal particles can be thermally formed in situ from metallic compounds such as noble metal acetates, acetylacetonates and carbonates.
    Type: Grant
    Filed: December 18, 1996
    Date of Patent: September 28, 1999
    Assignee: International Business Machines Corporation
    Inventors: Vista A. Brusic, Vijay S. Darekar, Michael A. Gaynes, Ravi F. Saraf
  • Patent number: 5952049
    Abstract: Processes for producing improved environmental protection, corrosion resistance and improved paint adhesion for metals; e.g., ferrous, aluminum, or magnesium alloys; and other surfaces upon contact is disclosed. The processes comprise use of one or more Group IV-A metals such as zirconium in an acidic solution with one or more oxyanions or other non-fluoanions to stabilize and solubilize the metal while fluorides are specifically excluded from the processes and compositions. The processes optionally contain pretreatment stages that serve to activate a surface and/or promote formation of a Group IV-A metal oxide matrices through use of an oxygen donor. The compositions are at a pH below about 5.0 and is preferably in a range between about 1.0 and about 4.0. The coatings may contain surfactants, sequestering agents, or organic additives for improved corrosion protection and paint adhesion. The substrate may be treated by immersion, spray, fogging or rollcoat.
    Type: Grant
    Filed: January 26, 1998
    Date of Patent: September 14, 1999
    Assignee: Natural Coating Systems, LLC
    Inventor: Charles E. Tomlinson
  • Patent number: 5948262
    Abstract: Particulate material for use in waste water treatment. The material comprises granules of a plastic material (e.g. poly-ethylene), each of which contains a plurality of grains of a substantially inert mineral (e.g. sand) coated thereon to provide a habitat for microorganisms effective in waste water treatment. The granules will have a predetermined particle size which is governed by the particle size range of the granules, e.g 3-10 mm and the grains will have a predetermined particle size range, e.g. 0.1-3.5 mm.
    Type: Grant
    Filed: August 12, 1997
    Date of Patent: September 7, 1999
    Assignees: Proceff Limited, John James Todd
    Inventors: John James Todd, Adrian Hopwood
  • Patent number: 5939208
    Abstract: In the present invention method, the surface of articles made of acrylic polymers and methacrylic polymers are converted into thin biomimetic layers by using the process involving at least the following two steps:(a) The polymer surface is contacted, in the presence of water and for a predetermined reaction time necessary to form a continuous surface layer thinner than about 500 microns, with a solution containing one or more tetraalkylammonium hydroxides of the general formula:R.sub.1 R.sub.2 R.sub.3 R.sub.4 N.sup.+ OH.sup.-where R.sub.1, R.sub.2, R.sub.3, R.sub.4 are the alkyl substituents, in which the sum of the number of carbon atoms is equal to or larger than 8 but smaller than 45; and,(b) The article is removed from the aqueous reaction solution and excess of tetraalkylammonium hydroxide is removed from the polymer surface by washing the polymer with a liquid miscible with the tetraalkylammonium hydroxide.
    Type: Grant
    Filed: November 7, 1997
    Date of Patent: August 17, 1999
    Assignee: Biomimetics, Inc.
    Inventor: Patrick Stoy
  • Patent number: 5935646
    Abstract: A process for producing a molecular sieve silica membrane comprising depositing a hybrid organic-inorganic polymer comprising at least one organic constituent and at least one inorganic constituent on a porous substrate material and removing at least a portion of the at least one organic constituent of the hybrid organic-inorganic polymer, forming a porous film.
    Type: Grant
    Filed: January 26, 1998
    Date of Patent: August 10, 1999
    Assignees: Gas Research Institute, Sandia National Laboratories
    Inventors: Narayan K. Raman, Charles Jeffrey Brinker
  • Patent number: 5897918
    Abstract: A faster and more efficient method for applying ultra thin films to substrate surfaces is disclosed. The method comprises heating a film forming composition comprising amphiphilic molecules to a liquid state, immersing the substrate surface in the heated liquid composition to heat the surface, and washing away the excess composition. For surfaces that ordinarily have insufficient or no chemical moieties reactive with the amphiphilic molecules, the immersion in the heated composition causes the substrate to become porous and expose previously unavailable chemically reactive moieties in the surface matrix. The amphiphilic molecules then self-assemble, chemically bond to the surface matrix and self-polymerize with each other and with other surface matrix-bound and/or surface-bound molecules to form the ultra thin surface film. The method is also faster and more efficient for coating non porous and metal surfaces.
    Type: Grant
    Filed: December 17, 1997
    Date of Patent: April 27, 1999
    Assignee: nanoFilm, Ltd.
    Inventors: Brij P. Singh, Pramod K. Arora
  • Patent number: 5897925
    Abstract: A fog-resistant microporous transparent film and the method of manufacturing the same are described. The fog-resistant film is made of SiOH which can absorb water molecules by both of a polar --Si--OH functional group and microporosity, and is hence provided with excellent and stable wettability. The SiOH film is coated on a PMMA or PC substrate by ion-assisted plasma-enhanced e-beam or thermal evaporation.
    Type: Grant
    Filed: March 28, 1996
    Date of Patent: April 27, 1999
    Assignee: Industrial Technology Research Institute
    Inventors: Daoyang Huang, Chao-Tsang Wei
  • Patent number: 5894039
    Abstract: A manufacturing method of water-covering type transparent keyboard comprises the steps of preparing the main body of silicone rubber keyboard, surface printing and coating, polyurethane layer coating, polyvinylalcohol thin film dipping, water rinsing, laser engraving text and graph forming, and polyurethane protective layer coating to form a water-covering keyboard. The water-covering type transparent keyboard according to the present invention can realize the effect of softness and good coherence.
    Type: Grant
    Filed: June 23, 1998
    Date of Patent: April 13, 1999
    Assignee: Silitek Corporation
    Inventors: Chi-Lung Tsai, Chui-Yu Chiu
  • Patent number: 5882731
    Abstract: A method is disclosed for applying a mildewcide compound laden film to surfaces by applying an aqueous, film-depositing composition onto said surfaces, allowing to stand momentarily, and rinsing with water. After rinsing, a residual, durable, virtually invisible film remains. This film is mildew resistant, paintable and its sheen closely mimics that of the surfaces prior to application of the aqueous composition. The aqueous composition comprises a mildewcide compound, a non-ionic surfactant, water, and at least one film-former.
    Type: Grant
    Filed: July 23, 1997
    Date of Patent: March 16, 1999
    Inventor: Richard L. Owens
  • Patent number: 5876806
    Abstract: An ultra thin, water and oil repelling and durable overcoat is easily formed on a substrate surface via covalent bonding by applying a finishing agent of the invention, comprising a chemically adsorptive compound with a chlorosilyl group and a nonaqueous viscous liquid or solid medium, on the substrate surface. A finishing agent, comprising a chemically adsorptive compound with a chlorosilyl group and a nonaqueous viscous liquid or solid medium, is applied on a substrate surface comprising hydrophilic groups. The substrate surface is then reacted with the chemically adsorptive compound at room temperature, and the agent containing unreacted chemically adsorptive compound is removed. The generation of hydrochloric acid gas can be prevented by adding tertiary amine or amide in the molar amount of one to three times more than the chemically adsorptive compound contained in the finishing agent.
    Type: Grant
    Filed: May 1, 1996
    Date of Patent: March 2, 1999
    Assignee: Matsushita Electric Industrial Co., Ltd.
    Inventor: Kazufumi Ogawa
  • Patent number: 5871815
    Abstract: An antistatic film comprising a chemically adsorbed film of straight chain molecules each containing a conductive group and provided on a chargeable substrate via covalent bonds each containing a Si group, said chemically adsorbed film having a conductivity of 10.sup.-10 S/cm or above. With the antistatic chemically adsorbed film according to the invention, conductive functional groups are secured via chemically adsorbed molecules and by siloxane bonds to the surface of a substrate material such as ceramics, glass, synthetic resins or synthetic fibers, a film, a plate, an display screen surface, a light-emitting tube. Thus, the film provides an antistatic effect and does not separate. In addition, this chemically adsorbed film has a thickness at the nanometer level and is thus excellently transparent, as well as capable of preventing contamination of the substrate surface due to charging thereof. The film is also excellently durable.
    Type: Grant
    Filed: July 14, 1997
    Date of Patent: February 16, 1999
    Assignee: Matsushita Electric Industrial Co., Ltd.
    Inventors: Kazufumi Ogawa, Norihisa Mino, Mamoru Soga
  • Patent number: 5869136
    Abstract: A chemically adsorbed multilayer film is formed through the process of replacing a halogen atom on the surface of a chemically adsorbed film with an alkaline metal or changing the halogen atom to a Grignard group by Grignard reaction. This manufacturing method does not disrupt the molecules of the chemically adsorbed film, is easy to perform, low in cost and is safe. After replacing the halogen (for example, Br) on the surface of the film with an alkaline metal such as Li, a condensation reaction including a dealkalihalide reaction is promoted by contacting the chemically adsorbed film with an adsorbent, such as a chemical adsorbent--containing a halosilane group at one end of a molecule--dissolved in a nonaqueous solvent. A chemically adsorbed multilayer film is then formed by reacting the chemically adsorbed film with chemical absorption composition and with water after removing unreacted adsorbents using a nonaqueous solution.
    Type: Grant
    Filed: February 3, 1993
    Date of Patent: February 9, 1999
    Assignee: Matsushita Electric Industrial Co., Ltd.
    Inventors: Tadashi Ohtake, Norihisa Mino, Kazufumi Ogawa
  • Patent number: 5851584
    Abstract: The present invention relates to a method for applying a protective layer to vessels or utensils used in the food industry, such as the milk and meat industries, wherein the vessels or utensils are contacted with an aqueous (natural) soap solution and then rinsed with water. The soap solution used is 2-10 ml, preferable 2-5 ml liquid soap per 100 l water, e.g. mains water. Furthermore, the relevant method is advantageously carried out at a temperature of the range of 10.degree.-40 .degree. C. By using a soap layer as protective layer, the use of disinfectants has become superfluous in the food industry so that the attendant problem of discharging or rendering harmless harmful disinfectants foreign to nature has also been solved.
    Type: Grant
    Filed: February 13, 1997
    Date of Patent: December 22, 1998
    Inventor: Petrus Johannes van Leeuwen
  • Patent number: 5814372
    Abstract: A composite porous membrane is provided which comprises a porous membrane substrate having an average pore size between 0.01 and 10 microns formed of a first polymer which is coated over its entire surface with a crosslinked second polymer. The second polymer is dissolved in a solvent with a free radical polymerization initiator in the absence of a crosslinking agent. The second polymer is crosslinked in situ and rendered insoluble by mild heating and/or exposure to ultraviolet light.
    Type: Grant
    Filed: September 26, 1996
    Date of Patent: September 29, 1998
    Assignee: Millipore Corporation
    Inventor: Wilson Moya
  • Patent number: H2077
    Abstract: Dispersions in water of “poly{vinyl alcohol}” (“PVA”), preferably those types resulting from about 90 mole % hydrolysis and/or ester interchange of polymers of vinyl carboxylates and having a molecular weight of about 155,000, are particularly effective for modifying the surfaces of plastic materials to cause water and/or other specified liquids to spread more readily over the treated surfaces than over the untreated surfaces. A biocide to repress the growth of micro-organisms in the dispersions is preferred.
    Type: Grant
    Filed: August 11, 2000
    Date of Patent: August 5, 2003
    Assignee: Henkel Corporation
    Inventor: Walter N. Opdycke