Abstract: A reverse painting process includes the preheating of work prior to its powder coating. By the preheating of the work, it becomes possible to form a film having a sufficiently large thickness for maintaining a satisfactorily high level of rustproofness in the boundary area between a film of the powdery paint and a film formed by electrodeposition, thus achieving drastic shortening of the time required for heating it in the fusing oven.

Abstract: This invention describes methods of synthesis and applications of planarized photonic crystals. Provided are simple, quick, reproducible and inexpensive methods that combine self-assembly and lithography to achieve the first examples of vectorial control of thickness, structure, area, topology, orientation and registry of colloidal crystals that have been patterned in substrates for use in lab-on-chip and photonic chip technologies. 1-, 2 and 3-D colloidal crystals patterned either on or within substrates can be used for templating inverted colloidal crystal replica patterns made of materials like silicon as well as building micron scale structural defects in such colloidal crystals.

Abstract: Surface and thereafter applying a priming coating comprising a polytetrafluoroethylene solution containing a dispersed ceramic filler, wherein the priming coating is dried in two steps by first air-drying the coating, followed by force drying at elevated temperatures, wherein a second polytetrafluoroethylene coating is applied on the dried primer coating, and a third polytetrafluoroethylene coating is applied on the second coating while the second coating has not dried. The coated bond tool is baked to cure the second and third coatings. Prior to application of the priming coating, the metallic tool can be subjected to pretreatment such as pre-baking and grit blasting.

Abstract: A method for making a nonwoven reinforcing may for vinyl floor coverings is described. A base mat is formed from a mixture of glass fibers and polymeric binder fibers and/or powder, follows by treatment with a second water-based polymeric binder composition. The mat has been found to be highly satisfactory as a substrate for compressible vinyl floor covering.

Abstract: Low gloss appearance in a coating derived from UV curable powder coatings can be achieved by using UV curable powder containing crystalline components or blends of crystalline and amorphous components and after heat fusing the powders together, allowing the crystalline components in the coating time to flow out and recrystallize to form a matte low gloss finish at a temperature of about the melting point of the crystalline component before curing with UV radiation.

Abstract: The present invention aims at providing a material for a diamond sintered compact tool, which has a high strength and is available as a material for a cutting tool. Accordingly, the present invention is concerned with a diamond sintered compact comprising a WC-Co type cemented carbide substrate having slight undulation and a diamond sintered compact bonded to one surface of the substrate by sintering during a step of sintering at an ultra-high pressure and high temperature, which has a plate thickness is 0.5 mm to 5 mm and an outer diameter is at least 20 mm and whose diamond sintered compact layer has at least 50% of a thickness area within a range of 0.05 mm to 0.4 mm and contains Co diffusing from the cemented carbide substrate.

Abstract: Dip-coated ferrite stainless steel sheet usable in the automobile exhaust sector, characterized in that it comprises a steel core with the following composition by weight:

Abstract: There is disclosed a method and composition for cosmetically repairing a surface void in polyolefin objects. The method involves inserting a repair composition into the void and then applying heat thereto to fuse the repair composition with a surrounding portion of the polyolefin object. The repair composition is a physical mixture of a thermoplastic powder, a resin binder, and a solvent, having a paste-like consistency. The repair composition may be neutral in color, or may contain a colorant to closely match the underlying object. The heating step can be performed with an open flame or with a heat gun.

Abstract: An object of the invention is to provide a surface-treated copper foil capable of consistently attaining a percent loss in peel strength against hydrochloric acid degradation of 10% or less as measured on a copper pattern prepared from the copper foil and having a line width of 0.2 mm, by bringing out the maximum effect of the silane coupling agent employed in zinc-plated or zinc-alloy-plated anti-corrosive copper foil. Another object is to impart excellent moisture resistance, heat resistance, and long-term storage stability to the surface-treated copper foil.

Abstract: A powder coating method includes applying an antistatic material to the surface of an electrically nonconducting substrate. The antistatic material is preferably a fatty amine salt and is applied by spraying. A flow of electrostatically charged powder particles is directed toward the substrate to form a powder coating on the substrate, and the powder coating is thereafter cured.

Abstract: A pressure relief device comprises an unimpregnated graphite membrane having a gas impermeable coating.

Abstract: A metal article, in particular a component for a thermal cracking furnace, and a method of protecting the metal from exposure to carbon, the article having a protective coating that has a glass-ceramic surface and an interior having a CTE between that of the glass-ceramic and the metal.

Abstract: A structure having layers of controllable electrical properties is prepared by furnishing a sheet of a substrate material, patterning a pattern of recesses into a surface of the sheet of the substrate material, filling the pattern of recesses with a mixture of an active phase and a matrix, and laminating the sheet to a base structure. The filled recesses may be of any desired shape, depth, and orientation. The active phase is particles of a material such as an electrical conductor or semiconductor, or magnetic particles.

Abstract: A thermoplastic compound useful in filling pores and voids in wooden materials, particularly edge regions, wherein the thermoplastic compound comprises a blend of two copolyesters and optionally fillers, wherein the first copolyester has a melting point of 140° C. to 260° C. and a glass transition temperature of −10° C. to 80° C., and wherein the second copolyester has a melting point of 120° C. to 190° C. and a glass transition temperature of −70° C. to 10° C. Also, a method of filling pores in a wooden material comprising using a thermoplastic compound having a softening point of 140° C. to 200° C., an open time of 2 to 15 seconds, and a viscosity number of 30 to 150 ml/g, with the thermoplastic compound preferably being a blend of two different copolyesters, wherein the application of such thermoplastic compounds enable the surfaces of chipboard panels and the like to be smoothed in a continuous one-pass process.

Abstract: A light-reflective decorative glittered article is made by coating a light reflective foil with a powdered resin, fixing the resin, cutting the coated foil into glitter flakes, flocking the flakes onto a curable adhesive applied on areas of a base material to be decorated, and curing the adhesive while concomitantly causing the resin on contacting flakes to become tacky Scattering and fall-off of the flakes during manufacture are reduced.

Abstract: A ribbon for smoothing a print image is disclosed which is used in a method which comprises bringing the ribbon into contact with a print image formed on a receptor by thermal transfer and heating the print image from the opposite side of the ribbon with respect to the side contacting the print image under pressure by means of a thermal head, thereby smoothing the print image. The ribbon has a kinetic friction coefficient, &mgr;A, on the side A thereof contacting the thermal head and a kinetic friction coefficient, &mgr;B, on the side B thereof contacting the print image, the values &mgr;A and &mgr;B satisfying the following equations: &mgr;B>1.67 &mgr;A 0.10<&mgr;B<0.

Abstract: A porcelain enamel coating suitable for use on high-carbon content, heat-rolled sheet steel is provided. The coating includes a ground coat layer for coating directly onto the steel and a cover coat layer. The ground coat layer includes a soft ground coat frit having nickelous oxide dispersed substantially uniformly throughout. The resulting porcelain enamel coating provides good resistance to boiling defects, such as pinholes.

Abstract: A coating and method for reducing the tendency for coke and gum deposits of hydrocarbon fluids to form and adhere to a surface at an elevated temperature. The coating enhances surface flow conditions along the surface so as to reduce both surface reaction time and concentration of deposit precursors (radicals and atoms) that provide for polymer growth. The coating has a smooth surface that is free of microscopic pits and scratches, and preferably has a surface roughness not greater than about 16 microinches (about 4 micrometers) R.sub.a. The coating is also preferably resistant to chemical attack from contaminants in the fluid, and inhibits diffusion between the fluid and surface. In addition, the coating has a low surface wettability to hydrocarbons, meaning that the tendency for hydrogen in the fuel to bond with atoms at the coating surface (chemisorption) is reduced or eliminated.

Abstract: Fireproof panels, and methods for their construction are provided. The fireproof panels comprise at least one sheet including a layer of glass fibres impregnated with at least one fireproof resin free from solvent. The method for the construction includes the successive steps of distributing a fireproof resin in the form of a powder free from solvents on a layer of glass fibres, subjecting the latter to a first compression and heating step to soften the resin and, to a second compression and heating step to cross-link the resin and form the said panel. The panels find particular use in the production of partitions and furnishings.

Abstract: If hydrophobic substrates are coated--if appropriate under pressure--with an aqueous dispersion of a thermoplastic fluoropolymer having a number-average particle size of up to 100 nm and the fluoropolymer is fixed on the substrate thus impregnated by heat treatment, firmly adhering coatings are obtained.

Abstract: In a method for manufacturing a capacitor including a lower electrode, a ferroelectric layer formed on the lower electrode, and an upper electrode formed on the ferroelectric layer, at least one of the lower and upper electrodes is made of laminated metal and conductive oxide. The laminated metal and conductive oxide are deposited by a DC magnetron reactive sputtering process using one metal target and mixture gas including oxygen wherein a ratio of oxygen in the mixture gas and a substrate temperature are definite and a DC input power is changed depending on the metal and the conductive oxide.

Abstract: The invention relates to a method of manufacturing an anti-oxidation system for porous ceramics on the basis of SiC or Si.sub.3 N.sub.4. By means of infiltration into the pore inner spaces of a sol containing at least one metal component, conversion of the sol to a gel (sol-gel process) and a subsequent high-temperature treatment, it is possible successfully to provide a crystalline anti-oxidation layer, which is resistant to temperatures of up to at least 1650.degree. C. even under cyclic temperature stresses, and reveals a heat expansion behavior adapted to the SiC or Si.sub.3 N.sub.4 over the entire temperature range used.

Abstract: An epoxy coating powder composition and a method for controlling the denseness of cured wrinkle finish patterns are provided by the use of a curing agent mixture comprising a blocked Lewis acid, methylenedisalicylic acid and a ring-substituted homolog thereof having the formula ##STR1## wherein x and y are from 1 to 3, and R.sup.1 and R.sup.2 are, independently, hydrogen, alkyl groups having from 1 to 20 carbon atoms, aryl groups having from 6 to 10 carbon atoms, or aryl-substituted methylene groups; with the proviso that when x=y=3, R.sup.1 and R.sup.2 .noteq.hydrogen;wherein the ratio of methylene disalicylic acid and the ring-substituted homolog is from about 50:50 to about 2:98 by weight.

Abstract: Powder coating compositions are described containing a blend of ionomers and polyethylene copolymers which fuse at temperatures of about 150.degree. C. or below and are durable, weatherable, solvent-resistant, and thereby provide transparent protective coatings on substrates such as signs, particularly traffic signs and license plates.

Abstract: A method and apparatus are presented for encapsulating an article comprising, for example, a substantially circular turntable (12) having first and second opposed major surfaces (16 & 18), each major surface sharing an outer peripheral sidewall (20). First and second thermoplastic pre-forms (28 & 30) are fitted to sandwich the article and are sealed to encapsulate by rotating a thermoplastic band (32) onto and around the exposed seam (48) while applying pressure (70) and heat (74) to obtain a fused bonded reliable encapsulating joint (72). The method and apparatus presented are particularly well suited for encapsulating metal platens, holders, and internal parts of process equipment used in the semiconductor manufacturing industry to avoid contamination from the encapsulated metal.

Abstract: A method for priming an uneven surface of a blank uses a novel "thermally expansible spray putty". This spray putty is prepared by mixing a priming paint for the blank with thermally expansible micro-capsules in amount of 0.5 to 10 weight % of the solid matter of the priming paint. The thermally expansible spray putty is preferably conditioned with an exclusive thinner to a high viscous state enabling it to be air-sprayed. Shell walls of the micro-capsules soften at a temperature below the setting temperature of a thermosetting paint to be used in finish painting of the blank. After the blank being treated by degreasing, drying and the like, the uneven surface of the blank is coated with the thermally expansible spray putty by spraying. After suitably setting the coated spray putty, it is dried by heating so as to expand the micro-capsules to obtain a substantially smooth surface of the blank.

Abstract: The present invention provides a surface modification method that provides beneficial changes in surface properties, can modify a surface to a greater depth than previous methods, and that is suitable for industrial application. The present method comprises applying a thin-film coating to a surface of a substrate, then subjecting the coated surface to an ion beam. The ion beam power pulse heats the coated surface, leading to alloying between the material in the coating and the material of the substrate. Rapid cooling of the alloyed layer after an ion beam pulse can lead to formation of metastable alloys and microstructures not accessible by conventional alloying methods or intense ion beam treatment of the substrate alone.

Abstract: A heat resistant, mold releasing coating characterized in: (a) that it comprises a layer A formed to cover the surface of the base material to be coated, wherein the coating layer forming components thereof comprise 20 to 95% by weight of frit and 5 to 80% by weight of at least one heat resistant resin selected from the group consisting of fluoro resins, silicon based resins, aromatic polysulfone resins, poly(phenylenesulfide) resins, polyamideimide resins and polyimide resins, and (b) that it comprises a layer B formed to cover the surface of said layer A, wherein the coating layer forming components thereof comprise 20 to 100% by weight of one or more fluoro resins, 0 to 20% by weight of frit, and 0 to 80% by weight of at least one heat resistant resin selected from the group consisting of silicon based resins, aromatic polysulfone resins, poly(phenylenesulfide) resins, polyamideimide resins and polyimide resins.

Abstract: A process is proposed for producing a protective layer on workpieces made, for example, from carbon composite material, for use at temperatures above 1000.degree. C. In accordance with the invention, a comminuted solids mixture with refractory ceramic powder articles, e.g., of carbides, nitrides and/or silicides, preferably from groups III, IV and/or VIb of the periodic table, and with at least one compound of the general elemental composition Me.sub.x B.sub.z, where Me represents one of the elements Si, Al, Zr, Ti, Hf or Y, and x and z each represent a number from 1 to 6, and optionally, in addition, with at least one already formed glass with the following general oxidic composition: Al.sub.2 O.sub.3 --B.sub.2 O.sub.3 --SiO.sub.2 --RO, where RO represents MgO, CaO or BaO, is dispersed in a liquid carrier system, deposited on free surfaces of a workpiece, and heated together with the workpiece briefly with air access to a maximum temperature of 1200.degree. C.

Abstract: The present invention relates to a process for preparing a sheet of plastic coated with a hard varnish on at least part of at least one of its sides, including:1) preparing a sheet of plastic by injection molding,2) applying the varnish to the said sheet, and3) heating the combination at a temperature at least equal to the softening point of the plastic of which the sheet is made, the varnish of at least a central part of the said combination being free of any mechanical contact other than that with the said sheet; the flat or curved transparent sheet thus obtained; its application as a motor-vehicle component containing a transparent part forming glazing and as motor-vehicle glazing.

Abstract: This invention is based upon the unexpected discovery that aliphatic solvents and secondary plasticizers act to reduce the viscosity of plastisol compositions that contain a crosslinked nitrile rubber. It has been unexpectedly found that plastisol compositions having acceptable viscosities which contain more than 30 or even 40 percent crosslinked nitrile rubber can be made by incorporating an aliphatic solvent or an aliphatic plasticizer therein.

Abstract: A coating composition which encompasses an aqueous dispersion of from about 2 to about 40 percent by dry weight, based on the dry weight of the coating composition, of a cationic polymer; and from about 60 to about 98 percent by dry weight, based on the dry weight of the coating composition, of a nonionic or cationic binder. The coating composition is thermally fusible and adapted to be receptive to ink jet inks and to retain the ink jet inks after being thermally fused. Alternatively, the coating composition may encompass an aqueous dispersion of a powdered thermoplastic polymer and from about 10 to about 150 dry parts by weight of a binder, based on 100 dry parts by weight of the powdered thermoplastic polymer.

Abstract: An electrode is made by depositing a mixture of particulate carbon and very fine thermoplastic binder on the surface of a fluid permeable dielectric web. The coated web is then passed between a pair of rollers that apply heat to at least the Vicat softening point of the binder and simultaneously apply pressure to fuse the carbon and binder to the web. Two of such electrodes are employed to manufacture a flow-through capacitor suitable for use in water treatment.

Abstract: An apparatus for applying a coating to the head-shank junction of externally threaded fasteners in an automated fashion. The fasteners are positioned, head down, on rotating part holders positioned about the periphery of a rotating disc. The part holders may be magnetic or other forms, and are adapted to maintain the fasteners in a generally fixed position during their movement. The fasteners are pre-heated at a heating station during their rotational movement on the disc. A dispenser is then used to apply the coating to the articles, in timed sequence to the movement of the articles. In this fashion, a coating can be applied to selected portions of the entire periphery of the head-shank junction. A method for applying a coating to the head-shank junction of externally threaded fasteners in an automated fashion also forms part of the present invention.

Abstract: An improved method for producing low-cost carbon--carbon composites based on impregnating carbon fiber mat preforms with liquid dispersions or suspensions of fine carbon particles and subsequent mechanical consolidation is disclosed. A highly porous preform of carbon fibers is impregnated by a liquid suspension of colloidal graphite and dried in air at low temperatures. Multiple impregnation and drying densification cycles provide a soft, flexible carbon--carbon composite. Subsequent mechanical consolidation methods, such as pressing or rolling, combined with rigidization by resin or pitch impregnation and carbonization, render a thin carbon--carbon composite of high bulk density. Prior to rigidization, the composite may be sewn with carbon yarns for property enhancement.

Abstract: A method for preparing a transparency involves application of hot melt ink to a transparent substrate to form a three-dimensional pattern with subsequent heating of the hot melt image above its melting point to change the configuration of the upper surface. In the embodiment described in the specification, a hot melt ink image on a substrate is treated in a continuous manner by moving it along a platen having a heating zone to melt drops of hot melt ink and cause them to spread on the substrate. The platen has a flat central portion and curved portions at each end with curvatures sufficient to prevent formation of cockle. At the output end of the heating zone, the substrate is moved continuously into a quenching zone where a cooling platen cools the substrate by thermal contact at a rapid rate to prevent crystallization or frosting of the hot melt ink image.

Abstract: A continuous reinforced composite material, including a first sheet with at least two polymer layers and a first fabric layer operatively coupled therebetween. The first sheet having at least one border where at least some of the fibers of the first fabric layer are continuous thereby having no free ends at the border. The composite material further includes a second sheet with at least two polymer layers with a second fabric layer operatively coupled therebetween. The second sheet having at least one border where at least some of the fibers of the second fabric layer are continuous thereby having no free ends at the border. The composite material further includes a seam wherein the borders of the first sheet and second sheet overlap and are operatively coupled to one another.

Abstract: An adsorbent, supple, filter fabric composed of an air-permeable, supple, textile, carrier material having adsorbent particles fixed on it by means of a thermoplastic binding agent. The adsorbent particles are coated on their surface with binding-agent particles which are set apart from each other. The average diameter of the binding-agent particles is smaller than that of the adsorbent particles. The adsorbent particles are also bonded to each other by binding-agent particles. The coating of the carrier material with adsorbent material is over 200 g/m.sup.2. The fabric has a total thickness of 0.5 to 5 mm, and its suppleness permits a bending radius of not more than 5 mm able to be carried out free of destruction. The filter fabric is manufactured by first mixing absorbent and binding-agent particles while adding water.

Abstract: Compositions of fluoropolymer containing a first filler component such as mica and a second filler component such as talc are resistant to permeation by water and aqueous acid and provide useful coatings for such items as chemical equipment. The composition can be used as coatings which can be applied by electrostatic spray of dry powder.

Abstract: A process of bonding a plastic is provided. The process comprises applying to a plastic surface an aqueous dispersion of a hydroxyl-functional polyurethane prepolymer obtained by:(1) reaction of:a polyol component containing a polyester polyol,a compound selected from the group of compounds containing groups capable of salt formation and at least two isocyanate-reactive groups,an isocyanate component in a stoichiometric excess, at least 20% by weight of said component consisting of tetramethyl xylylene diisocyanate, and(2) subsequent dispersion in water and at least partial reaction of the remaining NCO groups with an aminoalcohol and, optionally, subsequent chain extension. The process further comprises drying said applied aqueous dispersion to form a primer and bonding said plastic surface having said primer to a part to be joined thereto. The process is particularly useful for priming plastics such as polyvinyl chloride.

Abstract: An article having a water-repellent fluororesin surface and a method for manufacturing the same, wherein the article has a water-repellent fluororesin surface composed of an irregularly porous material which has a maximum IPA diffusion diameter of at least 8 mm and is formed by irregularly stacking fluororesin particles with an average diameter of no more than 40 microns over one another and has a water droplet roll angle tangent of no more than 50/500. The obtained article has a fluororesin surface which exhibits excellent water-repellency, inhibits adhesion of water drops and soil entrained by the water drops and imparts a great bond strength to the substrate.

Abstract: A method of applying a layered structure on a host surface for hot-melt printing is provided. A print pattern layer is placed with a release layer and an upper cellophane sheet on a top surface of the print pattern layer, and a lower cellophane sheet on a bottom surface thereof. The print pattern layer is then seated on top of a host surface material and heat-pressed at a temperature within a temperature range of between 80.degree. to 150.degree. Celsius. Under those conditions, the upper cellophane sheet melts and permeates the print pattern layer to merge with the lower cellophane sheet and is attached onto the host surface material. After regenerative cooling, the release layer is able to be peeled off, forming a protective print pattern layer. The cellophane sheets are formed by applying synthetic resin directly onto the release layer, and by peeling off the release layer to form the upper cellophane sheet and the lower cellophane sheet.

Abstract: An epoxy coating powder composition and a method for controlling the denseness of cured wrinkle finish patterns are provided by the use of a curing agent mixture comprising a blocked Lewis acid, methylenedisalicylic acid and a ring-substituted homolog thereof having the formula ##STR1## wherein x and y are from 1 to 3, and R.sup.1 and R.sup.2 are, independently, hydrogen, alkyl groups having from 1 to 20 carbon atoms, aryl groups having from 6 to 10 carbon atoms, or aryl-substituted methylene groups; with the proviso that when x=y=3, R.sup.1 and R.sup.2 .noteq.hydrogen;wherein the ratio of methylene disalicylic acid and the ring-substituted homolog is from about 50:50 to about 2:98 by weight.

Abstract: Opaquely pigmented or thick filmed powder coatings for heat sensitive substrates, such as wood, wood composites, for example, medium density fiber board, and plastics, that can be fully cured, especially near the substrate, through the incorporation of a dual cure system in the powder comprising a thermal initiator, such as a peroxide, along with a UV initiator. The UV initiator cures the surface, while the thermal initiator cures at the substrate. Surprisingly, virtually no pregelation occurs during the heated melt and flow out step prior to UV curing. Consequently, the hardened film finish formed on the surface exhibits exceptional smoothness which is comparable to that of traditional UV curable powders. The hardened film finish is also fully cured throughout and exhibits exceptional adhesion to the substrate which cannot be achieved with traditional UV curable powders that have been pigmented.

Abstract: A membrane-coated substrate and method for forming the membrane coating on the substrate that involves providing a porous inorganic monolithic substrate having one or more through channels having inner surfaces, providing solid polymeric film fusible to the substrate, and joining the film to the substrate by applying the film in a softened state to those inner surfaces and applying pressure thereto, so that the film fuses to and coats the inner surfaces of the channels. A workstream is modified by passing it through the membrane-coated substrate to cause modification of the workstream by the membrane coating.

Abstract: A defogging article having a defogging coating formed on a substrate such as a glass plate, a mirror, a metal article, or a plastic article. The defogging coating includes titania, and at least one oxide selected from the group consisting of P.sub.2 O.sub.5, B.sub.2 O.sub.3, boehmite, .gamma.-Al.sub.2 O.sub.3, and SiO.sub.2 --Al.sub.2 O.sub.3 based oxide. The defogging coating contains the at least one oxide other than titania, in an amount ranging from 0.1 to 50% by weight.

Abstract: A fiber preform is partially infiltrated with a ceramic material.A porous solid polymer is formed by reaction forming the infiltrated preform which is then pyrolized. Microporous carbon in the composite matrix is converted into silicon carbide.

Abstract: Laboratory vessels are coated on an operational surface thereof with a hydrophobic coating polymer or reactive monomer to form a coating having an exposed surface populated with 30% by area or more terminal trifluoromethyl groups. Laboratory vessels coated with such coating solutions are provided having extremely low surface energies and high resistance to solvent attack. Methods of forming hydrophobic coatings on laboratory vessels are also provided and include methods of forming exposed coating surfaces having populations of from about 30% by area to 100% by area trifluoromethyl groups. The hydrophobic coatings may be prepared from solutions, suspensions or powdered materials containing a fluoroalkyl ethylenically unsaturated monomer substantially free of any crosslinking, having from about 3 to about 20 carbon atoms, and containing at least one terminal trifluoromethyl group, or containing a polymerization product of such a monomer.

Abstract: A method for producing a sensor which is used for sensing a temperature and/or a flow and which comprises a carrier and a structured resistance layer arranged on said carrier, comprises the steps of providing a mixture consisting of platinum resinate paste and a rhodium resinate paste, printing the mixed resinate paste by means of a screen printing process onto an aluminium oxide substrate, drying the paste which has been applied by printing, burning in the paste at such a temperature for such a period of time that a resinate component contained in the layer will be burnt out, repeating the last-mentioned three steps on the same substrate until a desired overall layer thickness has been obtained, and tempering the substrate with the whole layer so as to obtain a high and stable temperature coefficient.

Abstract: There is disclosed a method for the permanent application of indicia to the surface of the polyolefin object by applying pigmented material to the surface in an indica pattern, preferably from a transfer sheet. Preferably the pigmented material is a mixture of finely divided pigment, hydrocarbon wax and finely divided polyolefin. The polyolefin surface bearing the indicia is coated with a coating mixture comprising a mixture of polyolefin and a binder such as a rosin or wax. Thereafter, the coated, indicia-bearing polyolefin surface is surface-heated to a temperature sufficient to fuse the coating and incorporate the coating and indicia permanently into the polyolefin object. The heating can be performed by passing a heat source across the surface.