Metal Or Metal Oxide Patents (Class 51/309)
  • Patent number: 8470456
    Abstract: The invention relates to a layer system for the formation of a surface layer on a surface of a substrate, in particular on the surface of a tool, wherein the layer system includes at least one first hard layer of the composition (MoSipAYq)?(NrCsOt)? with (o+p+q)=?, (r+s+t)=?, and (?+?)=100, wherein 40???60 and wherein M is at least one metal of the group of the chemical elements consisting of Al and the elements of the secondary groups IVb, Vb, VIb of the periodic system of elements. In accordance with the invention the component AY is at least one element of the group of the chemical elements consisting of Mn, Fe, Co, Ni, Cu and the elements of the secondary group IIIB and the elements of the main group IA, IIA and IIIA and the elements of the group of the lanthanoids of the periodic system of chemical elements, with AY preferably additionally containing boron.
    Type: Grant
    Filed: June 24, 2008
    Date of Patent: June 25, 2013
    Assignee: Sulzer Metaplas GmbH
    Inventors: Jörg Vetter, Georg Erkens
  • Patent number: 8470060
    Abstract: A method of forming a thermally stable cutting element that includes disposing at least a portion of a polycrystalline abrasive body containing a catalyzing material to be leached into a leaching agent; and subjecting the polycrystalline abrasive object to an elevated temperature and pressure is disclosed. Thermally stable cutting elements and systems and other methods for forming thermally stable cutting elements are also disclosed.
    Type: Grant
    Filed: June 7, 2011
    Date of Patent: June 25, 2013
    Assignee: Smith International, Inc.
    Inventors: Anthony Griffo, Madapusi K. Keshavan
  • Publication number: 20130152483
    Abstract: A method for recovery of cerium oxide from the abrasive waste composed mainly of cerium oxide arising from the polishing of glass substrates, said method including the steps of (i) adding to the abrasive waste an aqueous solution of a basic substance; (ii) adding to the resulting solution a precipitant, thereby forming precipitates composed mainly of cerium oxide, and removing the supernatant liquid; (iii) adding to the resulting precipitates a solution of an acid substance, thereby making said precipitate slightly acid to neutral; (iv) washing the precipitates with an organic solvent; and (v) drying and crushing the precipitates. The method makes it possible to recycle abrasive waste into a pure abrasive composed mainly of cerium oxide which can be reused to polish synthetic quartz glass substrates for state-of-the-art semiconductor technology relating to photomasks and reticles.
    Type: Application
    Filed: December 18, 2012
    Publication date: June 20, 2013
    Applicant: SHIN-ETSU CHEMICAL CO., LTD.
    Inventor: SHIN-ETSU CHEMICAL CO., LTD.
  • Publication number: 20130152482
    Abstract: An abrasive article including a bonded abrasive body having a bond material present in an amount of not greater than about 15 vol % for the total volume of the body, abrasive particulate material contained in the bond material, the abrasive particulate material including abrasive agglomerates and unagglomerated abrasive particles, wherein the body comprises an abrasive particulate ratio (APp:APagg) within a range between 3:1 and about 1:3, wherein APp represents the amount (vol %) of unagglomerated abrasive particles present in the body and APagg represents the amount (vol %) of abrasive agglomerates present in the body, and a porosity of at least about 42 vol % of the total volume of the bonded abrasive body.
    Type: Application
    Filed: November 21, 2012
    Publication date: June 20, 2013
    Inventors: Nilanjan SARANGI, John CAMPANIELLO, James M. GAFFNEY, Stephen E. FOX, John R. BESSE, Stephen WOODS, Renaud FIX
  • Publication number: 20130153306
    Abstract: A method of manufacturing a fixed cutter drill bit may include loading a first matrix material of controlled thickness to at least a portion of a mold cavity corresponding to a heel surface of at least one blade; loading a second matrix material into the remaining portions of the mold cavity; heating the mold contents to form a matrix body of the fixed cutter drill bit; and disposing at least one back reaming element in at least one back reaming cutter pocket.
    Type: Application
    Filed: December 14, 2012
    Publication date: June 20, 2013
    Applicant: SMITH INTERNATIONAL, INC.
    Inventor: SMITH INTERNATIONAL, INC.
  • Publication number: 20130152480
    Abstract: Polycrystalline ultra-hard constructions are made by subjecting a sintered ultra-hard body, substantially free of a sintering catalyst material, to a further HPHT process. The process is controlled to initially melt and infiltrating a filler material into the sintered ultra-hard body to form a filler region having interstitial regions filled with the filler material. The filler region extends a partial depth into the sintered ultra-hard body and is formed at a temperature below the melting temperature of an infiltrant material. Next, the process is controlled to melt and infiltrate the infiltrant material into the sintered ultra-hard body to form an infiltrant region that extends a partial depth into the sintered ultra-hard body. A portion of the filler region and/or the infiltrant region may be removed to form a thermally stable region.
    Type: Application
    Filed: December 19, 2012
    Publication date: June 20, 2013
    Applicant: SMITH INTERNATIONAL, INC.
    Inventor: SMITH INTERNATIONAL, INC.
  • Publication number: 20130146369
    Abstract: Diamond bonded constructions comprise a polycrystalline diamond body having a matrix phase of bonded-together diamond grains and a plurality of interstitial regions between the diamond grains including a catalyst material used to form the diamond body disposed within the interstitial regions. A sintered thermally stable diamond element is disposed within and bonded to the diamond body, and is configured and positioned to form part of a working surface. The thermally stable diamond element is bonded to the polycrystalline diamond body, and a substrate is bonded to the polycrystalline diamond body. The thermally stable diamond element comprises a plurality of bonded-together diamond grains and interstitial regions, wherein the interstitial regions are substantially free of a catalyst material used to make or sinter the thermally stable diamond element. A barrier material may be disposed over or infiltrated into one or more surfaces of the thermally stable diamond element.
    Type: Application
    Filed: February 5, 2013
    Publication date: June 13, 2013
    Applicant: Smith International, Inc.
    Inventor: Smith International, Inc.
  • Publication number: 20130146368
    Abstract: Cutting elements include an ultrahard material body formed at high pressure and high temperature conditions in the absence of catalyzing material to provide a material microstructure comprising a matrix phase of bonded together ultrahard material particles and interstitial regions disposed throughout the matrix phase providing porosity of less than about 6 volume percent. The body may include a substrate attached thereto, and may include an infiltrant material disposed in a population of the interstitial regions. The body may have regions with different porosities, e.g., with a higher porosity region located adjacent a substrate interface and/or along a central region. The body may include more than one infiltrant, each located in different regions. The infiltrant may be introduced into the body during a separate high pressure/high temperature process. The body may include a region which extends a depth from a working surface that is substantially free of any infiltrant.
    Type: Application
    Filed: December 6, 2012
    Publication date: June 13, 2013
    Applicant: SMITH INTERNATIONAL, INC.
    Inventor: Smith International, Inc.
  • Publication number: 20130139447
    Abstract: In the production method for abrasive grains according to the invention, an aqueous solution of a salt of a tetravalent metal element is mixed with an alkali solution, under conditions such that a prescribed parameter is 5.00 or greater, to obtain abrasive grains including a hydroxide of the tetravalent metal element.
    Type: Application
    Filed: January 31, 2013
    Publication date: June 6, 2013
    Inventors: Tomohiro IWANO, Hisataka MINAMI, Hirotaka AKIMOTO
  • Publication number: 20130143476
    Abstract: The invention discloses a metal-bonded diamond grinding wheel prepared by self-propagating pressure-less sintering and a preparation method thereof. The metal bonded diamond grinding wheel mainly comprises a working layer and a non-working layer, wherein the working layer comprises metal bond and grinded diamond, the non-working layer is metal bond, and the metal bond in the working layer and non-working layer have the same components that comprise metal powders of Cu, Al, Ni, Ti, Sn, and Co. To prepare the metal-bonded diamond grinding wheel prepared by self-propagating pressure-less sintering solves the problems of high energy consumption and low manufacture efficiency in the current sintering processes of the metal bonded diamond grinding wheel, and improves the binding force of the metal bond to the grinded diamond by forming carbides between the bond and the grinded diamond.
    Type: Application
    Filed: March 28, 2011
    Publication date: June 6, 2013
    Applicant: ZHENGZHOU SHINE MORE SUPERRABRASIVES CO., LTD.
    Inventors: Mingyao Liu, Junyong Shao, Juxue Xia
  • Publication number: 20130139446
    Abstract: A sintered compact for use in making a cutting tool, the sintered compact including about 10 vol. % to about 90 vol. % cubic boron nitride, and a binder phase including about 0.1 vol. % to about 10 vol. % graphene. A method for a sintered compact including mixing a powder blend having about 10 vol. % to about 90 vol. % cubic boron nitride and about 0.1 vol. % to about 10 vol. % graphene, pressing the powder blend into a pill, and sintering the pill at high pressure and high temperature. A sintered cutting tool including about 10 vol. % to about 90 vol. % cubic boron nitride, and a binder phase including about 0.1 vol. % to about 10 vol. % graphene, wherein the sintering is performed at a pressure of about 45 kBar and a temperature of about 1500° C. for about 30 minutes.
    Type: Application
    Filed: December 5, 2012
    Publication date: June 6, 2013
    Applicant: DIAMOND INNOVATIONS, INC.
    Inventor: Abds-Sami Malik
  • Publication number: 20130140095
    Abstract: A drill bit matrix is provided that contains a powdered abrasive material and a refractory metal powder in which the refractory metal powder is a coated powder in which each granule of the refractory metal powder is coated by a coating material. A core drill bit is further provided, containing a powdered abrasive material, a refractory metal powder and a steel tube onto which the powdered abrasive material and refractory metal powder are alloyed. The refractory metal powder is a coated powder in which each granule of the refractory metal powder is coated by one or more coating materials. A method is finally provided for manufacturing a core drill bit. First a matrix is formed by mixing together a powdered abrasive material and a coated refractory metal powder. The matrix is placed in a mould and a steel tube is placed on top of the mould to form a drill bit assembly. The drill bit assembly is then heated under atmospheric conditions.
    Type: Application
    Filed: August 6, 2010
    Publication date: June 6, 2013
    Inventor: Robert Kenneth Miller
  • Patent number: 8455116
    Abstract: The present invention relates to PVD coated cemented carbide cutting tool inserts semifinishing and finishing metal cutting operations. The cemented carbide cutting tool insert comprises a substrate and a wear resistant coating. The substrate comprises in addition to WC, from about 5.5 to about 8.5 wt-% Co and Cr such that the Cr/Co weight ratio is from about 0.08 to about 0.12 and also small amounts of Ti and Ta. The wear resistant coating is a homogeneous AlxTi1?xN-layer with x equals from about 0.6 to about 0.67. The thickness of this layer is from about 1 to about 3.8 ?m.
    Type: Grant
    Filed: May 29, 2008
    Date of Patent: June 4, 2013
    Assignee: Sandvik Intellectual Property AB
    Inventors: Pierre Donnadieu, Susanne Norgren
  • Publication number: 20130133951
    Abstract: A hard composite composition comprises a binder, and a polymodal blend of matrix powder In an embodiment, the polymodal blend of matrix powder has at least one local maxima at a particle size of 30 ?m or less, at least one local maxima at a particle size of 200 ?m or more, and at least one local minima between a particle size of about 30 ?m to about 200 ?m that has a value that is less than the local maxima at a particle size of 30 ?m or less.
    Type: Application
    Filed: June 25, 2010
    Publication date: May 30, 2013
    Applicant: Halliburton Energy Services, Inc.
    Inventor: Garrett T. Olsen
  • Publication number: 20130133269
    Abstract: An abrasive compact may include an ultra-hard phase that may include ultra-hard particles having a Knoop hardness of 5000 KHN or greater, a sinter catalyst, and a reaction phase that may include a catalyst-ceramic compound having a Knoop hardness lower than that of the ultra-hard phase.
    Type: Application
    Filed: January 24, 2013
    Publication date: May 30, 2013
    Applicant: DIAMOND INNOVATIONS, INC.
    Inventor: DIAMOND INNOVATIONS, INC.
  • Publication number: 20130133957
    Abstract: A cutting element having a substrate, an abrasive layer mounted to the substrate at an interface, and a longitudinal axis extending through the abrasive layer and the substrate is disclosed, wherein the substrate has a binder material, a plurality of metal carbide grains bonded together by an amount of the binder material, and at least one binder gradient, and wherein the amount of binder material decreases along at least one direction to form the at least one binder gradient.
    Type: Application
    Filed: November 26, 2012
    Publication date: May 30, 2013
    Applicant: SMITH INTERNATIONAL, INC.
    Inventor: SMITH INTERNATIONAL, INC.
  • Patent number: 8449854
    Abstract: According to some embodiments, a method of preparing a superhard material involves using mixtures of boron with carbon nitride of C3N4 stoichiometry as precursors. The C3N4 may be nanospherical. The result of chemical interaction of these components is the formation of new ternary compound B—C—N compound with a cubic structure. According to some embodiments, the composition is BCxN, where x is about 0.5. According to some embodiments, the composition is BCxN, where x is about 0.2. According to some embodiments, the compound has a unit cell parameter a=3.645±0.005 ?. According to some embodiments, the unit cell parameter a is about 3.655 ?. Synthesis is carried out under the conditions of thermodynamic stability of diamond at pressures higher that 6.0 GPa and temperatures above 1000° C. The starting components are taken according to the following ratio: boron—20-60 wt. %, C3N4—40-80 wt. %.
    Type: Grant
    Filed: January 29, 2008
    Date of Patent: May 28, 2013
    Assignee: William Marsh Rice University
    Inventors: Valery N. Khabashesku, Vladimir P. Filonenko, Valeri A. Davydov
  • Patent number: 8449636
    Abstract: A polishing composition and method for polishing polymer-based surfaces that can be rinsed from the polished polymer-based surface using water so as to leave substantially less polishing residue behind as compared to conventional polishing compositions. Polishing compositions according to the invention include abrasive particles and a rinsing agent dispersed in water. Polishing compositions according to the invention can be used to polish all types of polymer-based surfaces including, for example, organic polymer-based ophthalmic substrates and clear-coat automotive finishes.
    Type: Grant
    Filed: August 9, 2010
    Date of Patent: May 28, 2013
    Assignee: Ferro Corporation
    Inventor: Jon Jun Song
  • Patent number: 8449992
    Abstract: Disclosed is a surface coated member having excellent adhesion resistance and fracture resistance. A surface coated member (1) comprises a coating layer (3) on the surface of a base (2). The coating layer (3) is composed of a multilayer body wherein a titanium carbonitride (TiCN) layer (4), a continuously existing intermediate layer (5) containing titanium, aluminum, carbon and oxygen and having an average film thickness of 5-30 nm, and an ?-aluminum oxide (Al2O3) layer (9) composed of aluminum oxide (Al2O3) having an ? crystal structure are sequentially formed by deposition.
    Type: Grant
    Filed: February 25, 2009
    Date of Patent: May 28, 2013
    Assignee: KYOCERA Corporation
    Inventors: Takahito Tanibuchi, Yoshikazu Kodama, Tsuyoshi Fukano
  • Publication number: 20130125476
    Abstract: The present invention provides a cerium oxide slurry, a cerium oxide polishing slurry, and a method of polishing a substrate by using the same, wherein decrease of scratches and polish at high speed can be realized by reducing the content of coarse grains by improving in the disperse state of cerium oxide particles. The invention relates to a cerium oxide slurry containing cerium oxide particles, dispersant and water, in which the ratio of weight of cerium oxide/weight of dispersant is in a range of 20 to 80 and relates a cerium oxide polishing slurry comprising the cerium oxide slurry and additives such as a water-soluble polymer.
    Type: Application
    Filed: January 15, 2013
    Publication date: May 23, 2013
    Applicant: HITACHI CHEMICAL CO., LTD.
    Inventor: Hitachi Chemical Co., Ltd.
  • Publication number: 20130125477
    Abstract: Shaped abrasive particles comprising a ceramic and comprising a first plate integrally joined to a second plate at a predetermined angle?.
    Type: Application
    Filed: August 3, 2011
    Publication date: May 23, 2013
    Applicant: 3M INNOVATIVE PROPERTIES COMPANY
    Inventor: Negus B. Adefris
  • Publication number: 20130125475
    Abstract: The present invention relates to tungsten rhenium compounds and composites and to methods of forming the same. Tungsten and rhenium powders are mixed together and sintered at high temperature and high pressure to form a unique compound. An ultra hard material may also be added. The tungsten, rhenium, and ultra hard material are mixed together and then sintered at high temperature and high pressure.
    Type: Application
    Filed: January 14, 2013
    Publication date: May 23, 2013
    Applicant: SMITH INTERNATIONAL, INC.
    Inventor: Smith International, Inc.
  • Patent number: 8444728
    Abstract: A chemical mechanical polishing composition, comprising, as initial components: water; 0.1 to 20 wt % abrasive having an average particle size of 5 to 50 nm; and, 0.001 to 1 wt % of an adamantyl substance according to formula (II): wherein A is selected from N and P; wherein each R8 is independently selected from hydrogen, a saturated or unsaturated C1-15 alkyl group, C6-15 aryl group, C6-15 aralkyl group, C6-15 alkaryl group; and, wherein the anion in formula (II) can be any anion that balances the positive charge on the cation in formula (II).
    Type: Grant
    Filed: June 12, 2012
    Date of Patent: May 21, 2013
    Assignee: Rohm and Haas Electronic Materials CMP Holdings, Inc.
    Inventors: Yi Guo, Zhendong Liu, Kancharla-Arun Kumar Reddy, Guangyun Zhang
  • Patent number: 8440314
    Abstract: The present disclosure is directed to cutting tools. The disclosed cutting tools may have a wear resistant coating on a substrate. The substrate may have hard particles cemented in a binder phase. The binder may have a near-surface concentration gradient of at least one platinum group element and/or rhenium. Processes for producing cutting tools are also disclosed.
    Type: Grant
    Filed: August 25, 2009
    Date of Patent: May 14, 2013
    Assignee: TDY Industries, LLC
    Inventors: Craig W. Morton, Dewitt Dortch, John Bost, David J. Wills
  • Patent number: 8440328
    Abstract: In one aspect, coated cutting tools are described herein which, in some embodiments, can demonstrate improved wear resistance in one or more cutting applications. In some embodiments, a coated cutting tool described herein comprises a substrate and a coating adhered to the substrate, the coating comprising an inner layer deposited by physical vapor deposition and an outer deposited by physical vapor deposition over the inner layer.
    Type: Grant
    Filed: March 18, 2011
    Date of Patent: May 14, 2013
    Assignee: Kennametal Inc.
    Inventors: Aharon Inspektor, Nicholas F Waggle, Jr., Michael F Beblo, Mark J Rowe, Zhigang Ban
  • Patent number: 8435316
    Abstract: A method of forming an abrasive article includes forming a mixture comprising a liquid carrier and a glass precursor material, wherein the glass precursor material comprises a material selected from the group of materials consisting of a hydrated metal compound, an organic silicate compound, or a combination thereof. The method further includes providing abrasive grains within the mixture, forming the mixture into a green ceramic body, and heating the green ceramic body to form a bonded abrasive article comprising the abrasive grains contained within a bond matrix, wherein the bond matrix comprises an amorphous phase formed from the glass precursor material.
    Type: Grant
    Filed: December 15, 2009
    Date of Patent: May 7, 2013
    Assignees: Saint-Gobain Abrasives, Inc., Saint-Gobain Abrasifs
    Inventors: Jianhui Wu, Srinivasan Ramanath, Richard W. J. Hall, Gilles Querel
  • Patent number: 8435896
    Abstract: A chemical mechanical polishing composition useful for chemical mechanical polishing a semiconductor wafer containing an interconnect metal is provided, comprising, as initial components: water; an azole inhibitor; an alkali metal organic surfactant; a hydrotrope; a phosphorus containing agent; a water soluble cellulose; optionally, a non-saccharide water soluble polymer; optionally, a water soluble acid compound of formula I, wherein R is selected from a hydrogen and a C1-5 alkyl group, and wherein x is 1 or 2; optionally, a complexing agent; optionally, an oxidizer; optionally, an organic solvent; and, optionally, an abrasive.
    Type: Grant
    Filed: March 3, 2011
    Date of Patent: May 7, 2013
    Assignee: Rohm and Haas Electronic Materials CMP Holdings, Inc.
    Inventors: Hamed Lakrout, Jinjie Shi, Joseph Letizia, Xu Li, Thomas H. Kalantar, Francis Kelley, J. Keith Harris, Christopher J. Tucker
  • Patent number: 8435317
    Abstract: Polycrystalline diamond abrasive elements having a fine grained microstructure are produced from fine grained diamond particles and a catalyst solvent material, at least a portion of which is in the form of nanosized particles. The abrasive elements exhibit high homogeneity and exhibit significant increases in toughness and improved wear resistance.
    Type: Grant
    Filed: August 16, 2006
    Date of Patent: May 7, 2013
    Inventors: Anthony Roy Burgess, Cornelius Johannes Pretorius, Gerrard Soobramoney Peters, Peter Michael Harden
  • Patent number: 8435651
    Abstract: Provided is a wood cutting tool with improved wear resistance and corrosion resistance. A hard fundamental layer (18) of chromium nitride (CrN) is subjected to PVD to be coated on a rake face (16) of a substrate (12) formed of a cemented carbide alloy or a tool steel. The hard fundamental layer (18) has a five-layer structure having a first layer (18a) to a fifth layer (18e) disposed in order from the substrate (12) side. A hard main layer (20) of chromium oxide (Cr2O3) is coated on the outer surface of the fifth layer (18e) of the hard fundamental layer (18). The hard main layer (20), like the hard fundamental layer (18), is formed by PVD. The hard fundamental layer (18) is coated with the hard main layer (20) to suppress corrosion, thereby improving the wear resistance and corrosion resistance of a cemented carbide replaceable knife (10).
    Type: Grant
    Filed: April 22, 2009
    Date of Patent: May 7, 2013
    Assignee: Kanefusa Kabushiki Kaisha
    Inventors: Toru Minami, Satoru Nishio
  • Publication number: 20130097942
    Abstract: A process for control melting a mixture of coal ash, electric arc furnace dust, recycled glass and additives to create a feedstock. The feedstock is quenched or air dried in a mold to create useful products, such as fracking compounds, abrasives, construction products, building materials, landscaping materials, and the like.
    Type: Application
    Filed: June 21, 2011
    Publication date: April 25, 2013
    Inventors: James Morano, John Buddemeyer
  • Publication number: 20130098691
    Abstract: Implementations of the present invention include a binder with high hardness and tensile strength that allows for the creation of drilling tools with increased wear resistance. In particular, one or more implementations include a binder having about 5 to about 50 weight % of nickel, about 35 to about 60 weight % of zinc, and about 0.5 to about 35 weight % of tin. Implementations of the present invention also include drilling tools, such as reamers and drill bits, formed from such binders.
    Type: Application
    Filed: October 25, 2011
    Publication date: April 25, 2013
    Applicant: LONGYEAR TM, INC.
    Inventors: Cody A. Pearce, Christian M. Lambert
  • Publication number: 20130098692
    Abstract: The present invention provides a drill bit (1), and a method for its manufacture, that is suitable for use within a casing drilling process. The drill bit (1) comprises a monolithic body (5, 6, 8) made from bronze, e.g. aluminium bronze or nickel aluminium bronze, and a relatively hard material mounted thereon. The hard material may comprise polycrystalline diamond (PDC), tungsten carbide or cubic boron nitride. In one embodiment the monolithic body comprises a crown (6) and a plurality of cutting members (5). The hard material may be mounted directly on the crown or, alternatively, on the cutting members (5). The described drill bit (1) facilitates the drilling of hard rock formations while still being capable of being drilled through by a standard oilfield drill bit.
    Type: Application
    Filed: March 18, 2011
    Publication date: April 25, 2013
    Applicant: TESCO Corporation
    Inventors: Michael Wardley, Mitch Bavidge
  • Patent number: 8425640
    Abstract: An abrasive article comprising an elongated body, a bonding layer overlying a surface of the elongated body, and abrasive grains contained within the bonding layer at an average abrasive grain concentration within a range between about 0.02 ct/m and about 0.30 ct/m.
    Type: Grant
    Filed: August 16, 2010
    Date of Patent: April 23, 2013
    Assignees: Saint-Gobain Abrasives, Inc., Saint-Gobain Abrasifs
    Inventors: Susanne Liebelt, Vincent Tesi, Theodor von Bennigsen-Mackiewicz
  • Publication number: 20130092450
    Abstract: Composite materials for use with a drill bit for drilling a borehole in earthen formations. The composite material comprises a first pre-infiltrated hardphase constituent and a second pre-infiltrated hardphase constituent. The second pre-infiltrated hardphase constituent is a carbide which comprises at least 0.5 weight % of a binder and at least about 1% porosity. The composite material further comprises an infiltrant.
    Type: Application
    Filed: October 12, 2011
    Publication date: April 18, 2013
    Applicant: NATIONAL OILWELL DHT, L.P.
    Inventor: Harold A. SRESHTA
  • Publication number: 20130092454
    Abstract: Polycrystalline compacts include a polycrystalline superabrasive material comprising a first plurality of grains of superabrasive material having a first average grain size and a second plurality of grains of superabrasive material having a second average grain size smaller than the first average grain size. The first plurality of grains is dispersed within a substantially continuous matrix of the second plurality of grains. Earth-boring tools may include a body and at least one polycrystalline compact attached thereto. Methods of forming polycrystalline compacts may include coating relatively larger grains of superabrasive material with relatively smaller grains of superabrasive material, forming a green structure comprising the coated grains, and sintering the green structure. Other methods include mixing diamond grains with a catalyst and subjecting the mixture to a pressure greater than about five gigapascals (5.0 GPa) and a temperature greater than about 1,300° C.
    Type: Application
    Filed: October 12, 2012
    Publication date: April 18, 2013
    Applicant: BAKER HUGHES INCORPORATED
    Inventor: Baker Hughes Incorporated
  • Publication number: 20130086848
    Abstract: The present invention relates to polycrystalline Al2O3 bodies based on melted aluminum oxide having a mean crystallite size of the primary crystals between 20 ?m and 100 ?m and a closed macroporosity between 10% by volume and 30% by volume. The polycrystalline Al2O3 bodies may be obtained by tapping out and quenching a liquid aluminum oxide melt and simultaneous seeding of the pouring stream with seed crystals and can be used advantageously for the production of abrasive materials and refractory products.
    Type: Application
    Filed: August 15, 2011
    Publication date: April 11, 2013
    Applicant: Center for Abrasives and Refractories Research & Development C.A.R.R.D. GMBH
    Inventor: Sebastian Sachse
  • Patent number: 8415033
    Abstract: A cutting tool is disclosed. The cutting tool comprises a substrate and a coating layer on the substrate. The coating layer consists of nitride or carbonitride containing Ti and Al, and has a thickness of 3 to 9 ?m on a flank face. A first intensity ratio I(400)/I(311) of the coating layer on an outer surface is larger than the first intensity ratio of the coating layer on the substrate side.
    Type: Grant
    Filed: January 29, 2009
    Date of Patent: April 9, 2013
    Assignee: KYOCERA Corporation
    Inventor: Masahito Matsuzawa
  • Publication number: 20130081335
    Abstract: A method of forming polycrystalline diamond includes forming metal nanoparticles having a carbon coating from an organometallic material; combining a diamond material with the metal nanoparticles having the carbon coating; and processing the diamond material and the metal nanoparticles having the carbon coating to form the polycrystalline diamond. Processing includes catalyzing formation of the polycrystalline diamond by the metal nanoparticles; and forming interparticle bonds that bridge the diamond material by carbon from the carbon coating.
    Type: Application
    Filed: October 4, 2011
    Publication date: April 4, 2013
    Applicant: BAKER HUGHES INCORPORATED
    Inventors: Oleg A. Mazyar, Michael H. Johnson, Anthony A. DiGiovanni, Dan E. Scott
  • Publication number: 20130084786
    Abstract: An abrasive article including a substrate in the form of an elongated member having a core and a barrier layer in direct contact with an peripheral surface of the core. The barrier layer consists essentially of tin.
    Type: Application
    Filed: September 26, 2012
    Publication date: April 4, 2013
    Applicants: SAINT-GOBAIN ABRASIFS, SAINT-GOBAIN ABRASIVES, INC.
    Inventors: SAINT-GOBAIN ABRASIVES, INC., SAINT-GOBAIN ABRASIFS
  • Patent number: 8409990
    Abstract: The present invention provides an aqueous CMP slurry composition that includes abrasive particles and from about 0.01% to the limit of solubility in water of a compound according to Formula (I): wherein only one of R1, R2, R3, R4 and R5 is a hydroxyl group (—OH), only one of R1, R2, R3, R4 and R5 is a methoxy group (—OCH3), and the three of R1, R2, R3, R4 and R5 that are not either a hydroxyl group (—OH) or a methoxy group (—OCH3) are hydrogen atoms (—H).
    Type: Grant
    Filed: August 25, 2009
    Date of Patent: April 2, 2013
    Assignee: Ferro Corporation
    Inventor: Bradley M. Kraft
  • Patent number: 8409695
    Abstract: A wear resistant multilayer nitride hard coating for substrates. The hard coating includes a first layer of titanium aluminum nitride and a second layer comprising a plurality of sublayer groups. Each sublayer group includes a first sublayer of titanium silicon nitride and a second sublayer of titanium aluminum nitride. The composition of the titanium aluminum nitride, both in the first layer and in the sublayer groups, is (TixAl1-x)N, wherein 0.4?x?0.6. The composition of the titanium silicon nitride sublayers is (TiySi1-y)N, wherein 0.85?y?0.98, and all of the silicon is in solid solution in the titanium silicon nitride such that no silicon phase or silicon nitride phase exists in this sublayer. The combined amount of aluminum and silicon present in the sublayer groups being narrowly controlled such that the sum of x and y is in the range of 1.38 to 1.46.
    Type: Grant
    Filed: May 28, 2010
    Date of Patent: April 2, 2013
    Assignee: Kennametal Inc.
    Inventors: Wangyang Ni, Yixiong Liu, Mark S. Greenfield, Ronald M. Penich
  • Patent number: 8409732
    Abstract: A cutting tool insert includes a body of a hard alloy of cemented carbide, cermet, ceramics, cubic boron nitride based material or high speed steel and a hard and wear resistant coating, including one or several layers, at least one of which is an (Al,Cr)2O3 layer. The coating, with a total thickness of 2-20 ?m includes one or several layers, at least one of which is an (Al,Cr)2O3 layer with a thickness of 1-5 ?m having a corundum phase crystalline structure and a composition (Al1-yCry)2O3 with 0.5?y?0.7. The (Al,Cr)2O3 layer has a fiber texture with rotational symmetry in the direction of the coated surface normal with an inclination angle, ?, of the basal planes relative to the coated surface normal or the inclination angle, ?, for the highest peak in the pole plot with 20°<?<55°.
    Type: Grant
    Filed: March 3, 2009
    Date of Patent: April 2, 2013
    Assignee: Seco Tools AB
    Inventors: Mats Johansson, Tommy Larsson
  • Patent number: 8409702
    Abstract: Coated cutting tools are disclosed which have a hard coating that includes at least one aluminum titanium nitride layer having a single phase structure of B1 cubic phase and a composition of (AlxTi1-x)N, where x is in the range of about 0.46 to about 0.52 moles. The hard coatings also have a residual stress in the range of from about ?0.4 to about ?3 GPa as measured by the XRD Sin2 ? method, and a crystallographic orientation characterized by an x-ray diffraction (200) to (111) peak intensity ratio in the range of about 1 to about 14. Preferably the aluminum titanium nitride layer has an average crystallite size in the range of about 15 to about 50 nanometers. Methods of making such coated cutting tools are also disclosed.
    Type: Grant
    Filed: February 7, 2011
    Date of Patent: April 2, 2013
    Assignee: Kennametal Inc.
    Inventors: Wangyang Ni, Zhigang Ban, Ronald M. Penich, Yixiong Liu
  • Patent number: 8409696
    Abstract: A cutting tool includes a body of a hard alloy of cemented carbide, cermet, ceramics, cubic boron nitride based material or high speed steel and on which at least one of the functioning parts of the surface thereof, a hard and wear resistant coating is applied. The coating includes a polycrystalline laminar, multilayered structure of metal nitride compounds, in a repetitive form . . . MeN/(Ti1-xAlx)N/MeN/(Ti1-xAlx)N/MeN/(Ti1-xAlx)N/MeN/(Ti1-xAlx)N . . . of cubic structured (Ti1-xAlx)N layers where 0.3<x<0.95 and cubic structured MeN layers where Me is one or more of the metal element Ti, Zr, Hf, V, Nb, Ta, Mo and Al. The laminated structure has a repeat period, ?, of 5 nm??<20 nm, a layer thickness relation of 1/10<(dMeN/d(Ti,Al)N)<1/3 and a thickness dMeN?1 nm that is essentially constant throughout its total thickness up to 20 ?m.
    Type: Grant
    Filed: February 19, 2009
    Date of Patent: April 2, 2013
    Assignee: Seco Tools AB
    Inventors: Mats Johansson, Jacob Sjölén, Magnus Odén, Axel Knutsson
  • Patent number: 8409731
    Abstract: A cutting tool insert includes a body of a hard alloy of cemented carbide, cermet, ceramics, cubic boron nitride based material or high speed steel. A hard and wear resistant coating, having at least one layer, to which an (Al,Cr)2O3 layer is applied. This insert is particularly useful for machining of steel and stainless steel. The coating with a total thickness of 2-20 ?m has one or several layers, at least one of which is an (Al,Cr)2O3 layer with a thickness of 1-5 ?m having a corundum phase crystalline structure and a composition (Al1-yCry)2O3 with 0.4?y?0.6. The (Al,Cr)2O3 layer has a fiber texture with rotational symmetry in the direction of the coated surface normal to an inclination angle, ?, of the basal planes relative to the coated surface normal or the inclination angle, ?, for the highest peak in the pole plot with 70° <?<90° .
    Type: Grant
    Filed: March 3, 2009
    Date of Patent: April 2, 2013
    Assignee: Seco Tools AB
    Inventors: Mats Johansson, Tommy Larsson
  • Patent number: 8409734
    Abstract: Coated substrates having high wear resistant coatings are disclosed. The coatings include at least one layer of either titanium oxycarbonitride or titanium aluminum oxycarbonitride, such that the layer has an oxygen to titanium atomic percent ratio in the range of about 0.01 to about 0.09 and an aluminum to titanium atomic percent ratio in the range of about 0 to about 0.1. The coatings have a hardness to Young's modulus ratio of at least 0.06. The substrate may be a cutting insert. Methods of making such coated substrates are also disclosed in which layers comprising titanium oxycarbonitride or titanium aluminum oxycarbonitride are deposited by medium temperature chemical vapor deposition (MT-CVD) on substrates in the temperature range of about 750 to about 950° C. using a mixture of gases wherein the ratio of the hydrogen gas to the nitrogen gas is greater than 5.
    Type: Grant
    Filed: March 4, 2011
    Date of Patent: April 2, 2013
    Assignee: Kennametal Inc.
    Inventors: Zhigang Ban, Yixong Liu, Mark S. Greenfield
  • Publication number: 20130074418
    Abstract: An abrasive article includes an abrasive particulate material made of alumina crystals and a primary additive composition impregnated within the abrasive particulate material, the primary additive composition including a combination of Mg and Ca, wherein Mg and Ca are present in an additive ratio [Mg:Ca] within a range between about 1:1 and about 10:1, and further comprising at least about 0.2 wt % Ca for the total weight of the abrasive particulate material.
    Type: Application
    Filed: September 26, 2012
    Publication date: March 28, 2013
    Inventors: Tracy H. Panzarella, Doruk O. Yener
  • Publication number: 20130074420
    Abstract: A method for forming a thermally stable cutting element that includes forming at least one acid infusion pathway in a polycrystalline abrasive body containing a catalyzing material to be leached; and contacting at least a portion of the at least one acid infusion pathway in the polycrystalline abrasive body with a leaching agent is disclosed.
    Type: Application
    Filed: November 7, 2012
    Publication date: March 28, 2013
    Inventors: Youhe Zhang, Yuelin Shen
  • Patent number: 8404366
    Abstract: In a cutting tool, if the outermost ceramic coating layer is a ?-Al2O3 coating layer, then certain microns of the ?-Al2O3 layer will be transformed into an ?-Al2O3 by instantaneous melting, vaporization and solidification. Further, if the outermost coating layer of the ceramic coating layers is an ?-Al2O3 coating layer, then the surface roughness will be enhanced since at least a portion of it will be melted, wherein the melted surface will be solidified with its surface flattened by the surface tension provided in a melted state.
    Type: Grant
    Filed: January 2, 2007
    Date of Patent: March 26, 2013
    Assignee: TaeguTec, Ltd.
    Inventors: Dong Gil Ahn, Joo Wan Lee
  • Patent number: 8404010
    Abstract: An abrasive compact may include an ultra-hard phase that may include ultra-hard particles having a Knoop hardness of 5000 KHN or greater, a sinter catalyst, and a reaction phase that may include a catalyst-ceramic compound having a Knoop hardness lower than that of the ultra-hard phase.
    Type: Grant
    Filed: December 13, 2007
    Date of Patent: March 26, 2013
    Assignee: Diamond Innovations, Inc.
    Inventor: Steven W. Webb