The Material Primarily Contains Compound Containing Both Metal And Oxygen (e.g., Silver Nitrate) Patents (Class 516/88)
  • Patent number: 10850233
    Abstract: The present invention describes a fluid which is suitable for the decontamination of heat engines which can carry out both the catalytic reduction of oxides of nitrogen (NOx) contained in exhaust gases and assist in the regeneration of the particulate filter (PF), said fluid being in the form of a stable suspension of colloidal particles, these colloidal particles being dispersed in an aqueous solution containing at least one reducing agent or at least one precursor of a reducing agent for NOx. The invention also describes several embodiments for the preparation of said fluid.
    Type: Grant
    Filed: October 20, 2016
    Date of Patent: December 1, 2020
    Assignee: IFP ENERGIES NOUVELLES
    Inventors: Eric Lecolier, Patrick Gateau, Stephane Zinola, Nathalie Palazzo
  • Patent number: 9340738
    Abstract: A process for making cerium-containing oxide nanoparticles includes providing an aqueous reaction mixture containing a source of cerous ion and a source of one or more metal ions (M) other than cerium, a source of hydroxide ion, at least one monoether carboxylic acid nanoparticle stabilizer wherein the molar ratio of said monoether carboxylic acid nanoparticle stabilizers to total metal ions is greater than 0.2, and an oxidant. The cerous ion is oxidized to ceric ion, thereby forming a product dispersion of cerium-containing oxide nanoparticles containing one or more metal ions (M), Ce1-xMxO2-?, wherein x has a value from about 0.001 to about 0.95 and ? has a value of about 0.0 to about 0.5.
    Type: Grant
    Filed: November 10, 2014
    Date of Patent: May 17, 2016
    Assignee: Cerion, LLC
    Inventors: Albert Gary DiFrancesco, Richard K. Hailstone, Kenneth J. Reed, Gary R. Prok
  • Patent number: 9303223
    Abstract: A process for making cerium-containing oxide nanoparticles includes providing an aqueous reaction mixture containing a source of cerous ion, a source of hydroxide ion, at least one monoether carboxylic acid wherein the molar ratio of said monoether carboxylic acid to cerous ions is greater than 0.2, and an oxidant. The cerous ion is oxidized to ceric ion, thereby forming a product dispersion of cerium-containing oxide nanoparticles CeO2-?, wherein ? has a value of about 0.0 to about 0.5.
    Type: Grant
    Filed: November 11, 2014
    Date of Patent: April 5, 2016
    Assignee: Cerion, LLC
    Inventors: Albert Gary Difrancesco, Richard K. Hailstone, Kenneth J. Reed, Gary R. Prok
  • Patent number: 9162901
    Abstract: Disclosed is a method of producing metal oxides, comprising electrodepositing a metal oxide from an electrolyte solution onto a substrate to coat at least a portion of the substrate, whereby metal oxide seed particles are released into the solution, and precipitating metal oxide particles from the solution. The precipitated metal oxide particles have a maximum particle size of less than 1 micron.
    Type: Grant
    Filed: March 14, 2013
    Date of Patent: October 20, 2015
    Assignee: PPG Industries Ohio, Inc.
    Inventors: Robin Peffer, Michael J. Pawlik, Jane Valenta
  • Patent number: 9012349
    Abstract: A method for synthesizing catalyst beads of bulk transmission metal carbides, nitrides and phosphides is provided. The method includes providing an aqueous suspension of transition metal oxide particles in a gel forming base, dropping the suspension into an aqueous solution to form a gel bead matrix, heating the bead to remove the binder, and carburizing, nitriding or phosphiding the bead to form a transition metal carbide, nitride, or phosphide catalyst bead. The method can be tuned for control of porosity, mechanical strength, and dopant content of the beads. The produced catalyst beads are catalytically active, mechanically robust, and suitable for packed-bed reactor applications. The produced catalyst beads are suitable for biomass conversion, petrochemistry, petroleum refining, electrocatalysis, and other applications.
    Type: Grant
    Filed: November 1, 2013
    Date of Patent: April 21, 2015
    Assignee: UT-Battelle LLC
    Inventors: Jae Soon Choi, Beth L. Armstrong, Viviane Schwartz
  • Patent number: 8883865
    Abstract: A process for making cerium-containing oxide nanoparticles includes providing an aqueous reaction mixture containing a source of cerous ion, optionally a source of one or more metal ions (M) other than cerium, a source of hydroxide ion, at least one monoether carboxylic acid nanoparticle stabilizer wherein the molar ratio of said monoether carboxylic acid nanoparticle stabilizers to total metal ions is greater than 0.2, and an oxidant at an initial temperature in the range of about 20° C. to about 95° C. Temperature conditions are provided effective to enable oxidation of cerous ion to ceric ion, thereby forming a product dispersion of cerium-containing oxide nanoparticles, optionally containing one or more metal ions (M), Ce1-xMxO2-?, wherein “x” has a value from about 0.0 to about 0.95. The nanoparticles may have a mean hydrodynamic diameter from about 1 nm to about 50 nm, and a geometric diameter of less than about 45 nm.
    Type: Grant
    Filed: May 13, 2010
    Date of Patent: November 11, 2014
    Assignee: Cerion Technology, Inc.
    Inventors: Albert Gary DiFrancesco, Richard K. Hailstone, Kenneth J. Reed, Gary R. Prok
  • Patent number: 8664143
    Abstract: A metal oxide-carbon composite includes a carbon aerogel with an oxide overcoat. The metal oxide-carbon composite is made by providing a carbon aerogel, immersing the carbon aerogel in a metal oxide sol under a vacuum, raising the carbon aerogel with the metal oxide sol to atmospheric pressure, curing the carbon aerogel with the metal oxide sol at room temperature, and drying the carbon aerogel with the metal oxide sol to produce the metal oxide-carbon composite. The step of providing a carbon aerogel can provide an activated carbon aerogel or provide a carbon aerogel with carbon nanotubes that make the carbon aerogel mechanically robust.
    Type: Grant
    Filed: October 25, 2011
    Date of Patent: March 4, 2014
    Assignee: Lawrence Livermore National Security, LLC.
    Inventors: Marcus A. Worsley, Thomas Yong-Jin Han, Joshua D. Kuntz, Octavio Cervantes, Alexander E. Gash, Theodore F. Baumann, Joe H. Satcher, Jr.
  • Patent number: 8646612
    Abstract: Monodisperse metal oxide nanopowders are prepared by treating a dispersion of crude metal oxide nanopowder with ultrasonication, allowing the dispersion to settle, and subjecting the remaining suspended portion to centrifugation to obtain a supernatant comprising metal oxide nanopowder.
    Type: Grant
    Filed: March 19, 2012
    Date of Patent: February 11, 2014
    Assignee: The United States of America, as represented by the Secretary of the Navy
    Inventors: Woohong Kim, Guillermo R. Villalobos, Jasbinder S. Sanghera, Ishwar D. Aggarwal
  • Patent number: 8613799
    Abstract: The present invention relates to dispersants containing at least two lipophilic groups (e.g., alkenyl-substituted acylating agent, such as, dodecyl succinic anhydride), and the dispersants contain a hydrophilic component (e.g., alkylene glycol, polyalkylene glycol) present in an amount sufficient to at least partially disperse the amphiphilic compound in aqueous media (e.g., 30 wt % to 80 wt %). The invention further provides for dispersants as phosphate, sulphonate, and phosphite derivatives thereof. The invention further provides for the use of the dispersants in tinter compositions (e.g., universal tinter) and reduced shade paints.
    Type: Grant
    Filed: August 7, 2007
    Date of Patent: December 24, 2013
    Assignee: Lubrizol Limited
    Inventors: Dean Thetford, John J. Mullay, Christopher J. Kolp, Rita A. Sweet
  • Patent number: 8501825
    Abstract: Formulations useful for preparing hydrous hafnium oxide gels contain a metal salt including hafnium, an acid, an organic base, and a complexing agent. Methods for preparing gels containing hydrous hafnium oxide include heating a formulation to a temperature sufficient to induce gel formation, where the formulation contains a metal salt including hafnium, an acid, an organic base, and a complexing agent.
    Type: Grant
    Filed: January 7, 2010
    Date of Patent: August 6, 2013
    Inventors: Jack L. Collins, Rodney D. Hunt, Frederick C. Montgomery
  • Patent number: 8455554
    Abstract: A process for preparing a hydrosol of one or more metal oxides, e.g. titanium dioxide, comprising preparing a metal alkoxide solution in a water-miscible organic solvent, e.g. an alcohol; providing an aqueous solvent; mixing the metal alkoxide solution with the aqueous solvent in a volume or weight proportion to form a single-phase aqueous sol colloid (hydrosol) of hydrated metal oxide in absence of a non-ionic block polymer surfactant. Also disclosed is a corresponding hydrogel; water-insoluble particles encapsulated in hydrated metal oxide and a process for their encapsulation; uses of the encapsulation products.
    Type: Grant
    Filed: June 12, 2007
    Date of Patent: June 4, 2013
    Assignee: CaptiGel AB
    Inventors: Vadim G. Kessler, Gulaim A. Seisenbaeva, Sebastian Håkansson, Maria Unell
  • Patent number: 8362094
    Abstract: A simple, room-temperature method of producing zinc oxide nanoparticles was established by reacting zinc nitrate hexahydrate and cyclohexylamine (CHA) in either aqueous or ethanolic medium. Particles of polyhedra morphology were obtained for zinc oxide, prepared in EtOH (ZnOE) and zinc oxide prepared in water (ZnOW). The results indicate that there are significant morphological differences between ZnOE and ZnOW. ZnOE showed a regular polyhedral shape, while spherical and chunky particles were observed for ZnOW. The morphology was crucial in enhancing the cyanide ion photocatalytic degradation efficiency of ZnOE by a factor of 1.5 in comparison to the efficiency of ZnOW at equivalent loading of 0.0166 ZnO nanoparticles wt %.
    Type: Grant
    Filed: July 30, 2012
    Date of Patent: January 29, 2013
    Assignee: King Abdulaziz City for Science and Technology (KACST)
    Inventors: Abdulaziz A Bagabas, Reda M. Mohamed, Mohamed F. A. Aboud, Mohamed Mokhtar M. Mostafa, Ahmad S. Alshammari, Zeid A. Al-Othman
  • Patent number: 8252256
    Abstract: A simple, room-temperature method of producing zinc oxide nanoparticles was established by reacting zinc nitrate hexahydrate and cyclohexylamine (CHA) in either aqueous or EtOHic medium. Particles of polyhedra morphology were obtained for zinc oxide, prepared in EtOH (ZnOE), while an irregular spherical morphology, mixed with some chunky particles forzinc oxide prepared in water (ZnOW). The results indicate that there are significant morphological differences between ZnOE and ZnOW. ZnOE showed a regular polyhedral shape, while spherical and chunky particles were observed for ZnOW. The morphology was crucial in enhancing the cyanide ion photocatalytic degradation efficiency of ZnOE by a factor of 1.5 in comparison to the efficiency of ZnOW at equivalent loading of 0.02 ZnO nanoparticles wt %. Increasing the loading wt % of ZnOE from 0.01 to 0.07 led to an increase in the photocatalytic degradation efficiency from 67% to 90% after 45 minutes and a doubling of the first-order rate constant (k).
    Type: Grant
    Filed: January 1, 2012
    Date of Patent: August 28, 2012
    Assignee: King Abdulaziz City for Science and Technology (KACST)
    Inventors: Abdulaziz A Bagabas, Reda M. Mohamed, Mohamed F. A. Aboud, Mohamed Mokhtar M. Mostafa, Ahmad S. Alshammari, Zeid A. Al-Othman
  • Patent number: 8207085
    Abstract: A photocatalytic coating composition comprising photocatalytic titanium oxide, silver, copper and a quaternary ammonium hydroxide. The photocatalytic coating composition may include a photocatalytic titanium oxide sol dispersed in a binder. Furthermore, a photocatalytic member includes a substrate having a surface coated with the photocatalytic coating composition. The photocatalyst coating composition can contain highly antibacterial silver by skillfully utilizing copper and a quaternary ammonium hydroxide, and accordingly can show an antibacterial effect not only in a dark place simply due to silver, but also a higher antibacterial effect in a conventional application of employing ultraviolet sterilization by concomitantly using the photocatalyst titanium oxide sol according to the present invention and an ultraviolet sterilizer.
    Type: Grant
    Filed: December 20, 2010
    Date of Patent: June 26, 2012
    Assignees: Taki Chemical Co., Ltd., Toto Ltd.
    Inventors: Taketoshi Kuroda, Hiroyuki Izutsu, Isamu Yamaguchi, Yoshiyuki Nakanishi
  • Patent number: 8206680
    Abstract: Calco-magnesian aqueous suspension having particles of solid matter with, before being put into suspension, a specific surface area, calculated according to the BET method, which is less than or equal to 10 m2/g, and its method of preparation. Such an aqueous suspension of calco-magnesian solid matter can achieve a very low viscosity, making it possible to greatly increase the solid matter concentration of the suspension, or again to reduce the size of the particles in suspension, thus obtaining a concentrated and reactive milk of lime.
    Type: Grant
    Filed: July 27, 2004
    Date of Patent: June 26, 2012
    Assignee: S.A. Lhoist Recherche et Developpement
    Inventors: Luis Alfredo Diaz Chavez, Timothy L. Salter, Ziad Habib, Henri-René Langelin
  • Patent number: 8133616
    Abstract: A process for the production of nano-structured olivine lithium manganese phosphate (LiMnPO4) electrode material comprising of the following steps: sol gel preparation in a chelating environment; preparation of lithium manganese phosphate/carbon composite by ball-milling; and electrode preparation.
    Type: Grant
    Filed: February 14, 2006
    Date of Patent: March 13, 2012
    Assignee: Dow Global Technologies LLC
    Inventors: Ivan Exnar, Thierry Drezen, Nam Hee Kwon-Roth, Motoshi Isono
  • Patent number: 8133535
    Abstract: An antipenetrating agent is to be added to a solvent ink for preventing penetration of the solvent ink into a medium to be printed. The antipenetrating agent includes inorganic fine particles and a resin soluble in an organic solvent.
    Type: Grant
    Filed: March 20, 2008
    Date of Patent: March 13, 2012
    Assignee: Mimaki Engineering Co., Ltd.
    Inventors: Tomotaka Furuhata, Satoshi Takezawa, Isao Tabayashi
  • Patent number: 8026287
    Abstract: The invention provides colloidal dispersions of calcium phosphate platelets comprising at least one polymer which complexes the calcium and in which the length of the platelets, L, is between 5 and 500 nm and in which the thickness of the platelets is between 0.5 and 20 nm. Another subject-matter of the invention is the calcium phosphate platelets obtained by drying the colloidal dispersion according to the invention. The invention also provides a process for preparing these colloidal dispersions of calcium phosphate platelets according to the invention. Finally, another subject-matter of the invention is the use of the abovementioned colloidal dispersions of platelets as food additive, reinforcing filler, thermal insulation filler, pharmaceutical excipient, polishing agent, building materials, additive for oral formulations, in particular dentifrices, or encapsulating agent.
    Type: Grant
    Filed: October 4, 2010
    Date of Patent: September 27, 2011
    Assignee: Innophos, Inc.
    Inventor: Jean-Yves Chane-Ching
  • Patent number: 7879757
    Abstract: A photocatalytic titanium oxide sol presents antibacterial properties in a dark place, and, in particular, relates to a photocatalytic titanium oxide sol which is stable and causes no discoloration by light even though containing silver, and relates to a coating composition and a member using the same. The photocatalytic titanium oxide sol includes silver, copper and a quaternary ammonium hydroxide, may be dispersed in a binder, and may be coated on the surface of a substrate.
    Type: Grant
    Filed: September 27, 2007
    Date of Patent: February 1, 2011
    Assignees: Taki Chemical Co., Ltd., Toto Ltd.
    Inventors: Taketoshi Kuroda, Hiroyuki Izutsu, Isamu Yamaguchi, Yoshiyuki Nakanishi
  • Patent number: 7807724
    Abstract: The invention provides colloidal dispersions of calcium phosphate platelets comprising at least one polymer which complexes the calcium and in which the length of the platelets, L, is between 5 and 500 nm and in which the thickness of the platelets is between 0.5 and 20 nm. Another subject-matter of the invention is the calcium phosphate platelets obtained by drying the colloidal dispersion according to the invention. The invention also provides a process for preparing these colloidal dispersions of calcium phosphate platelets according to the invention. Finally, another subject-matter of the invention is the use of the abovementioned colloidal dispersions of platelets as food additive, reinforcing filler, thermal insulation filler, pharmaceutical excipient, polishing agent, building materials, additive for oral formulations, in particular dentifrices, or encapsulating agent.
    Type: Grant
    Filed: June 28, 2004
    Date of Patent: October 5, 2010
    Assignee: Innophos, Inc.
    Inventor: Jean-Yves Chane-Ching
  • Patent number: 7772288
    Abstract: The invention provides a composition that is a dispersion made from a Group III nitride, a solvent system, and a dispersant. The dispersion can be used to prepare Group III nitride thin films on a wide range of substrates, for example, glass, silicon, silicon dioxide, silicon nitride, silicon carbide, aluminum nitride, sapphire, and organic polymers. The particle size of the Group III nitride used for producing the thin films can be controlled by adjusting centrifugation of the dispersion and selecting a desired layer of supernatant. The dispersant can be removed from the thin films by calcination. The Group III nitride can contain a dopant. Doped Group III nitride thin films can emit visible light upon irradiation. Green, red, and yellow light emissions result from irradiating erbium-, europium-, and cerium-doped gallium nitride, respectively.
    Type: Grant
    Filed: June 1, 2007
    Date of Patent: August 10, 2010
    Assignee: Cornell Research Foundation, Inc.
    Inventors: Huaqiang Wu, Michael G. Spencer, Emmanuel Giannelis, Athanasios Bourlinos
  • Patent number: 7767721
    Abstract: A soft agglomerate of copper oxide ultrafine particles which has an average primary particle diameter of not more than 100 nm and an average secondary particle diameter of not less than 0.2 ?m and of producing the soft agglomerate by (1) forming ultrafine copper oxide by reducing a cuprous carboxyl compound in an aqueous solution, with hydrazine and/or a hydrazine derivative, optionally with a base and optionally with organic compounds, such as alcohol (e.g., ethylene glycol or ethanol), ether, ester or amide; and simultaneously or separately applying an agglomerating force, e.g., agglomerating agent; to produce copper oxide soft agglomerate. Alternatively (2), forming a colloidal dispersion of cuprous oxide ultrafine particles by heating and reducing at least one copper compound (e.g., copper carboxyl, copper alkoxy and copper diketonate compound) at a temperature of not lower than 160 ° C.
    Type: Grant
    Filed: December 2, 2003
    Date of Patent: August 3, 2010
    Assignee: Asahi Kasei Kabushiki Kaisha
    Inventors: Mutsuhiro Maruyama, En-Hai Sun
  • Patent number: 7722804
    Abstract: In a method of manufacturing a pressed scandate dispenser cathode, firstly, scandium nitrate, barium nitrate, calcium nitrate, aluminum nitrate and ammonium metatungstate (AMT) are dissolved in de-ionized water, respectively, and then mixed with a solution of a cross-link agent such as citric acid and H2O2. After water bathing, the mixed aqueous solution turns into gel, and the powders are obtained after the gel calcination. Secondly, the calcined powders are reduced by hydrogen. Finally, the reduced powders are pressed into shapes and then sintered in the furnace with the atmosphere of hydrogen or by Spark Plasma Sintering (SPS 3.202-MK-V) in vacuum.
    Type: Grant
    Filed: August 8, 2007
    Date of Patent: May 25, 2010
    Assignee: Beijing University of Technology
    Inventors: Jinshu Wang, Wei Liu, Meiling Zhou, Yiman Wang, Hongyi Li, Tieyong Zuo
  • Patent number: 7704414
    Abstract: A composition comprises a solvent, and an electroconductive substance and an amphiphilic block copolymers having a polyalkenyl ether repeating-unit structure, or a block copolymer enclosing an electroconductive substance. A black ink composition comprises a fine particulate metal having an average particle diameter of not more than 20 nm, an amphiphilic block copolymer, and a solvent. A method for forming an electroconductive pattern by applying the composition. A method for forming an electroconductive pattern by applying a composition comprises a block copolymer enclosing an electroconductive substance, system to form an electroconductive pattern on the substrate.
    Type: Grant
    Filed: May 2, 2005
    Date of Patent: April 27, 2010
    Assignee: Canon Kabushiki Kaisha
    Inventors: Koichi Sato, Tomoko Maruyama, Ikuo Nakazawa, Ryuji Higashi, Sakae Suda, Masayuki Ikegami, Keiichiro Tsubaki, Keiko Yamagishi
  • Patent number: 7666812
    Abstract: An improved gas diffusion electrode composed of a perovskite-type oxide dispersed in a mixture of carbon black and a hydrophobic binder polymer. An improved catalyst for use in the electrochemical reduction of oxygen comprising a perovskite-type compound having alpha and beta sites, and having a greater molar ratio of cations at the beta site. A particularly good reduction catalyst is a neodymium calcium manganite. An improved method of dispersing the catalysts with carbon in a reaction layer of the electrode improves performance of the electrode and the oxygen reduction process. This is provided by adding carbon black to an aqueous solution of metal salts before it is heated to a gel and then to a char and then calcined. Optionally, a quantity of the desired oxide catalyst can be premixed with a portion the carbon before adding the carbon to an aqueous solution of the metal salts to be heated.
    Type: Grant
    Filed: August 10, 2007
    Date of Patent: February 23, 2010
    Assignee: Ceramatec, Inc.
    Inventors: John Howard Gordon, Hachiya Toshinori, Shekar Balagopal, Sai Bhavaraju
  • Publication number: 20100041775
    Abstract: A method for producing an inorganic nanoparticle dispersion liquid, including: substituting a first dispersion medium serving to disperse inorganic nanoparticles in an inorganic nanoparticle dispersion liquid by a second dispersion medium with a third dispersion medium intervening between the first dispersion medium and the second dispersion medium, wherein an absolute value of the difference in solubility parameter values (SP values) between the third dispersion medium and the second dispersion medium is smaller than 3.
    Type: Application
    Filed: July 16, 2009
    Publication date: February 18, 2010
    Applicant: FUJIFILM Corporation
    Inventor: Koukichi Waki
  • Publication number: 20090170962
    Abstract: Methods for controlling dispersion of aqueous suspensions involving providing a solvent, and adding at least an additive, an ion source, and a particle source selected from a partially dissolving colloid or a non-dissolving colloid, to the solvent to produce the aqueous suspension where the additive is added to the solvent prior to the ion source and the particle source when the particle source is the partially dissolving colloid.
    Type: Application
    Filed: December 20, 2007
    Publication date: July 2, 2009
    Inventors: Glen Harold Kirby, Brett Allen Boutwell
  • Patent number: 7528177
    Abstract: An environmentally friendly method for preparing zinc oxide (zincite) nanoparticle sol having more than 90% visible light transmission at 20 wt % solid; comprises of the neutralizing, under specific pH, an inorganic zinc salt with an inorganic alkali, both dissolved in ethylene glycol, and thermally aging the precipitates afterward.
    Type: Grant
    Filed: September 29, 2005
    Date of Patent: May 5, 2009
    Assignee: Headway Advanced Materials Co., Ltd
    Inventors: Anthony Shiaw-Tseh Chiang, Chih-Tsung Hsu, Ching-Ping Yang
  • Publication number: 20090108233
    Abstract: A method for preparing a suspension of LDH particles comprises the steps of preparing LDH precipitates by coprecipitation to form a mixture of LDH precipitates and solution; separating the LDH precipitates from the solution; washing the LDH precipitates to remove residual ions; mixing the LDH precipitates with water; and subjecting the mixture of LDH particles and water from step (d) to a hydrothermal treatment step by heating to a temperature of from greater than 80° C. to 150° C. for a period of about 1 hour to about 144 hours to form a well dispersed suspension of LDH particles in water.
    Type: Application
    Filed: December 12, 2005
    Publication date: April 30, 2009
    Applicant: The Univeristy of Queensland
    Inventors: Gaoqing Lu, Zhiping Xu
  • Patent number: 7517915
    Abstract: A method for preparing a ceramic powder suspension is disclosed. A dispersant having a following structural formula is provided: wherein D is H or COOR1; R1 is a hydrogen atom, or an alkyl group, a cyclic aliphatic group, an aryl group, having 1 to 10 carbon atoms, or a cationic salt group; R2 is an alkyl group having 1 to 10 carbon atoms, a cyclic aliphatic having 1 to 10 carbon atoms or an aryl group having 1 to 10 carbon atoms; R3 is a hydrogen atom or a methyl group; Z is an oxygen atom or an NH group; A is —COO —SO3 or an acid form; a is an integer between 1 to 5000; and p and q are integers between 1 to 10. The dispersant is dissolved in a solvent. Ceramic powder is further added into the solvent with the dispersant.
    Type: Grant
    Filed: October 5, 2006
    Date of Patent: April 14, 2009
    Assignee: National Taiwan Normal University
    Inventors: Kung-Chung Hsu, Lung-Pin Chen, Dao-Shinn Hwung, Kuo-Liang Ying, Wen-Cheng Wei, Sea-Fue Wang
  • Patent number: 7514065
    Abstract: A layered ruthenic acid compound is converted to a protonic layered ruthenic acid hydrate, which is then converted to a layered alkylammonium-ruthenic acid intercalation compound to obtain a colloid containing ruthenic acid nanosheets having a thickness of 1 nm or smaller. Thereby, a ruthenic acid nanosheet is obtained.
    Type: Grant
    Filed: March 26, 2004
    Date of Patent: April 7, 2009
    Inventors: Yoshio Takasu, Yasushi Murakami, Wataru Sugimoto
  • Patent number: 7495032
    Abstract: A method for processing a ceramic powder suspension includes providing a dispersant having the following structure: wherein R1 is an H+ ion, an Na+ ion, an NH4+ ion or other cationic group; R2 is an H+ ion, an Na+ ion. an NH4+ ion or other cationic group; m is an integer from 10 to 5000 ; and n is an integer from 10 to 3000 . The dispersant is dissolved in a solvent. Ceramic powder is further added into the solvent with the dispersant.
    Type: Grant
    Filed: October 5, 2006
    Date of Patent: February 24, 2009
    Inventors: Kung-Chung Hsu, Lung-Pin Chen, Dao-Shinn Hwung, Kuo-Liang Ying, Wen-Cheng Wei, Sea-Fue Wang
  • Patent number: 7482384
    Abstract: Iron composite particles for purifying soil or ground water, comprise ?-Fe and magnetite, and having a ratio of a diffraction intensity D110 of (110) plane of ?-Fe to a sum of a diffraction intensity D311 of (311) plane of magnetite and the diffraction intensity D110 (D110/(D311+D110)) of 0.30 to 0.95 as measured from X-ray diffraction spectrum of the iron composite particles, an Al content of 0.10 to 1.50% by weight and an S content of 3500 to 7000 ppm; a process for producing the iron composite particles; a purifying agent containing the iron composite particles; a process for producing the purifying agent; and a method for purifying soil or ground water.
    Type: Grant
    Filed: June 8, 2004
    Date of Patent: January 27, 2009
    Assignee: Toda Kogyo Corporation
    Inventors: Masayuki Uegami, Junichi Kawano, Koji Kakuya, Tomoko Okita, Kenji Okinaka
  • Patent number: 7476695
    Abstract: There is provided a stable sol comprising modified stannic oxide-zirconium oxide complex colloidal particles, wherein the particles are formed by coating as nuclei stannic oxide-zirconium oxide complex colloidal particles in which stannic oxide colloidal particles obtained by a reaction of metal tin, an organic acid and hydrogen peroxide is bonded to zirconium oxide colloidal particles with tungsten oxide-stannic oxide-silicon dioxide complex colloidal particles. The sol has a high refractive index and is improved in water resistance, moisture resistance and weather resistance, and can be used by mixing with a hard coating paint as a component for improving properties of a hard coating film applied on a plastic lens surface.
    Type: Grant
    Filed: March 9, 2005
    Date of Patent: January 13, 2009
    Assignee: Nissan Chemical Industries, Ltd.
    Inventors: Yoshinari Koyama, Motoko Asada
  • Publication number: 20080255254
    Abstract: The invention includes a composition for stabilizing chlorinated water to sunlight decomposition, and methods of preparing compositions. The composition is a slurry composition of a monoalkali metal cyanurate, of low viscosity. Two methods of preparing the slurry are described, in which cyanuric acid or cyanuric acid wetcake is mixed with a monoalkali metal base. One method dry blends cyanuric acid or cyanuric acid wetcake with a monoalkali metal base. The invention also describes a method of preparing a dry, solid monoalkali metal cyanurate.
    Type: Application
    Filed: April 16, 2007
    Publication date: October 16, 2008
    Inventors: Michael S. Harvey, Jonathan N. Howarth
  • Patent number: 7435758
    Abstract: Described is an additive for producing the positive active material for lead-acid storage batteries on the basis of finely divided tetrabasic lead sulfate. The additive contains a tetrabasic lead sulfate of an average particle size smaller than about 3 ?m as well as finely divided silicic acid for preventing an agglomeration of the particles of the tetrabasic lead sulfate. During maturation, this additive ensures the formation of the structure of a tetrabasic lead sulfate crystal with a very narrow bandwidth of crystal sizes and a very homogeneous distribution. In a subsequent electrochemical formation to lead oxide, this leads to particularly efficient lead-acid storage batteries. Furthermore, the invention relates to a method of making the additive according to the invention as well as its advantageous use in the positive material for the maturation and drying of singled and not singled plates in the production of lead-acid storage batteries.
    Type: Grant
    Filed: December 23, 2003
    Date of Patent: October 14, 2008
    Assignee: Penarroya Oxide GmbH
    Inventors: Ian Klein, Werner Nitsche
  • Publication number: 20080242745
    Abstract: An aqueous dispersion of metal oxide fine particles, including metal oxide fine particles, a carboxylic compound and an acid compound containing a bulky anion having B value of ?0.01 or less in Equation (1), wherein the metal oxide fine particles, the carboxylic compound and the acid compound containing a bulky anion are dispersed in an aqueous solution, and the aqueous dispersion of metal oxide fine particles has a light transmittance at 800 nm wavelength of 90% or more: ?=?0(1+A?c+Bc) ??Equation (1) where ? represents a viscosity of a solution, ?0 represents a viscosity of a solvent, A and B respectively represent an inherent constant value of an acid, and c represents a concentration of the solution.
    Type: Application
    Filed: February 25, 2008
    Publication date: October 2, 2008
    Applicant: FUJIFILM Corporation
    Inventor: Kimiyasu Morimura
  • Publication number: 20080242746
    Abstract: A dispersion of metal oxide fine particles, containing metal oxide fine particles, a strong acid and an aqueous solution, wherein the metal oxide fine particles and the strong acid are dispersed in an aqueous solution containing alcohol, and the dispersion of metal oxide fine particles has a light transmittance at 800 nm wavelength of 90% or more.
    Type: Application
    Filed: March 25, 2008
    Publication date: October 2, 2008
    Applicant: FUJIFILM Corporation
    Inventors: Kimiyasu MORIMURA, Yoshio Tadakuma, Yoichi Maruyama
  • Publication number: 20080188574
    Abstract: This invention provides a disperse system having fine powder-typed inorganic metal oxide dispersed in water and preparing method for the same and more particularly, it provides a method for preparing a disperse system having fine powder-typed inorganic metal oxide dispersed in water characterized in that a) a hydrophobically treated fine powder-typed inorganic metal oxide; b) a sulfosuccinate or sulfosuccinamate or an alkoxylated alcohol dispersant; and c) water are mixed and dispersed by a high-speed bead mill and a disperse system having fine powder-typed inorganic metal oxide dispersed in water prepared by the same. The disperse system having fine powder-typed inorganic metal oxide dispersed in water of the present invention has excellent characteristics in that it has high transparency in the visible ray spectrum, it has excellent UV protection ability when applied to cosmetics, it provides better feelings than oil dispersions, and it has better water-proof property than existing water dispersions.
    Type: Application
    Filed: May 21, 2007
    Publication date: August 7, 2008
    Applicants: SUNJIN CHEMICAL Co., Ltd., RANCO CO., Ltd.
    Inventors: Sung-Ho Lee, Woo-Kyu Kang
  • Patent number: 7312252
    Abstract: A composition of matter comprising anionic clay having the general formula [M2+1-xM3+x(OH)2]x+(x/n)An?·yH2O??(I) or [M1+M3+2(OH)6]1+(1/n)An?·yH2O;??(II) where M1+ is a mono-valent metal; M2+ is a divalent metal; and M3+ is a trivalent metal; A is an inorganic or organic anion, chosen such that the rule of charge neutrality is obeyed; n is an integer; x is any rational number between 0 and 1; and y is any rational number between 0 and 10; where the anionic clay is in the form of particles having a volume weighted mean particle size diameter of less than 500 nm. Stable colloidal dispersions comprise such anionic clay particles having a volume weighted mean particle size diameter of less than 500 nm dispersed in a liquid medium.
    Type: Grant
    Filed: May 20, 2004
    Date of Patent: December 25, 2007
    Assignee: Eastman Kodak Company
    Inventors: Joseph F. Bringley, Craig A. Morris
  • Patent number: 7157024
    Abstract: The present invention relates to a metal oxide particle comprising tin atom, zinc atom, antimony atom and oxygen atom, having a molar ratio SnO2:ZnO:Sb2O5 of 0.01–1.00:0.80–1.20:1.00 and having a primary particle diameter of 5 to 500 nm; and a process for producing the metal oxide particle comprising the steps of: mixing a tin compound, a zinc compound and an antimony compound in a molar ratio SnO2:ZnO:Sb2O5 of 0.01–1.00:0.80–1.20:1.00; and calcining the mixture at a temperature of 300 to 900° C. The metal oxide particle is used for several purposes such as antistatic agents, UV light absorbers, heat radiation absorbers or sensors for plastics or glass, etc.
    Type: Grant
    Filed: May 24, 2004
    Date of Patent: January 2, 2007
    Assignee: Nissan Chemical Industries, Ltd.
    Inventors: Tadayuki Isaji, Osamu Fujimoto
  • Patent number: 7091250
    Abstract: The present invention is an additive for producing a positive active material for lead-acid storage batteries on the basis of finely divided tetrabasic lead sulfate. The additive contains a tetrabasic lead sulfate of an average particle size less than about 3 ?m as well as finely divided hydrophobic silicic acid for preventing agglomeration of the particles of the tetrabasic lead sulfate. During maturation, this additive ensures the formation of the structure of a tetrabasic lead sulfate crystal with a very narrow bandwidth of crystal sizes and a very homogeneous distribution. In the subsequent electrochemical formation to lead oxide, this leads to particularly efficient lead-acid storage batteries. Furthermore, the invention relates to a method of making the additive according to the invention as well as its advantageous use in the positive material for the maturation and drying of plates in the production of lead-acid storage batteries.
    Type: Grant
    Filed: April 3, 2003
    Date of Patent: August 15, 2006
    Assignee: PENOX GmbH
    Inventors: Ian Klein, Werner Nitsche
  • Patent number: 7053125
    Abstract: Comb polymers are used as dispersants to increase the stability of colloidal suspensions containing multivalent or high concentrations of monovalent ions. Stabilized colloidal suspensions and methods of forming stabilized colloidal suspensions are described, including suspensions containing ceramic precursors or bioactive agents useful in forming ceramic substrates or pharmaceutical compositions, respectively.
    Type: Grant
    Filed: January 3, 2003
    Date of Patent: May 30, 2006
    Assignees: The Board of Trustees of the University of Illinois, W.R. Grace & Co.-Conn.
    Inventors: Jennifer A. Lewis, Glen Kirby, Josephine Ho-Wah Cheung, Ara Avedis Jeknavorian
  • Patent number: 6955771
    Abstract: Disclosed are metal oxide sols made by mixing at least one metal alkoxide, wherein the metal is a transition metal, a post-transition metal, an alkali metal, or alkaline earth metal; at least one organosilane; at least one boron oxide compound selected from the group consisting of boric acid, alkoxy boron compounds, hydrocarbyl boric acids, hydrocarbyl hydroxy boron alkoxides, and hydroxy boron alkoxides; and a liquid. Also disclosed are composites containing a polymer and the metal oxide sols.
    Type: Grant
    Filed: January 7, 2003
    Date of Patent: October 18, 2005
    Assignee: APS Laboratory
    Inventor: Hong-Son Ryang
  • Patent number: 6884753
    Abstract: The present invention provides a method for producing a ceramic dispersion composition, the method comprising the step of heating a mixture of a ceramic powder having a photocatalytic activity, a dispersant and a solvent at a temperature of about 70° C. or higher without substantially letting the solvent out of the reaction system. The ceramic dispersion composition can be used for providing a film showing a high hydrophilicity by light irradiation.
    Type: Grant
    Filed: May 16, 2003
    Date of Patent: April 26, 2005
    Assignee: Sumitomo Chemical Company, Limited
    Inventors: Yoshiaki Sakatani, Kensen Okusako, Hironobu Koike
  • Patent number: 6838486
    Abstract: Disclosed are nanocomposites made of guest metal nanoparticles and metal oxide sols made by mixing at least one metal alkoxide, at least one organosilane, at least one boron oxide compound, and a liquid. Also disclosed are dielectric composites containing a dielectric material such as a polymer and the nanocomposites.
    Type: Grant
    Filed: April 30, 2003
    Date of Patent: January 4, 2005
    Assignee: APS Laboratory
    Inventor: Hong-Son Ryang
  • Publication number: 20040248997
    Abstract: A method of manufacturing a ceramic coating material which includes stirring a material including a complex oxide in the presence of a catalyst containing platinum group elements. The material is a sol-gel material which includes at least one of a hydrolysate and a polycondensate of the complex oxide.
    Type: Application
    Filed: March 25, 2004
    Publication date: December 9, 2004
    Applicant: SEIKO EPSON CORPORATION
    Inventors: Takeshi Kijima, Eiji Natori
  • Publication number: 20040159824
    Abstract: Disclosed are metal oxide sols made by mixing at least one metal alkoxide, wherein the metal is a transition metal, a post-transition metal, an alkali metal, or alkaline earth metal; at least one organosilane; at least one boron oxide compound selected from the group consisting of boric acid, alkoxy boron compounds, hydrocarbyl boric acids, hydrocarbyl hydroxy boron alkoxides, and hydroxy boron alkoxides; and a liquid. Also disclosed are composites containing a polymer and the metal oxide sols.
    Type: Application
    Filed: January 7, 2003
    Publication date: August 19, 2004
    Inventor: Hong-Son Ryang
  • Patent number: 6710091
    Abstract: A method for the preparation of nano size zinc oxide particles having an average primary particle diameter of less than or equal to 15 nm, which are redispersible in organic solvents and/or water, by basic hydrolysis of at least one zinc compound in alcohol or an alcohol/water mixture. The hydrolysis is carried out with substoichiometric amounts of base, based on the zinc compound. The precipitate which originally forms during hydrolysis is left to mature until the zinc oxide has completely flocculated. This precipitate is then thickened to give a gel and separated off from the supernatant phase.
    Type: Grant
    Filed: August 21, 2001
    Date of Patent: March 23, 2004
    Assignee: Bayer Aktiengesellschaft
    Inventors: Hermann-Jens Womelsdorf, Werner Hoheisel, Gerd Passing
  • Patent number: 6656976
    Abstract: A procedure for making well dispersed suspensions containing mixtures of powders displaying a low viscosity which remain stable over an extended period of time includes suspensions prepared in aqueous and/or ethanolic media using a cationic polyelectrolyte at the inherent pH of the mixture. The method is particularly useful for making robust slurries for subsequent spray drying of free flowing granules to be used in the fabrication of cemented carbide or cermet bodies.
    Type: Grant
    Filed: April 26, 2001
    Date of Patent: December 2, 2003
    Assignee: Sandvik Aktiebolag
    Inventors: Lennart Bergström, Eric Laarz