Abstract: Certain aspects of the present disclosure relate to methods and apparatus for microbial sampling of foods. For example, a method may include providing at least one aggregating sampler at one or more sampling locations, and sampling a production lot of produce or other food items such as meat using the at least one aggregating sampler to create one or more samples that makes up a microbial sampling. Certain aspects of the present disclosure relate to methods and apparatus for microbial sampling of foods. For example, an apparatus, such as a microbial aggregating sampler, may include a covering having a microbial sampling material with a pocket formed in the covering to receive an appendage or a tool for handling of the covering.

Abstract: To provide a method with which it is possible to ascertain a gas concentration in a furnace rapidly, and to charge an amount of fuel and/or oxygen corresponding to the state within the furnace, and with which it is possible to reduce the device maintenance load. In order to solve the abovementioned problem, this method for analyzing components contained in flue exhaust gas of a furnace includes: a sampling step of collecting a portion of the flue exhaust gas from a flue; a dust removal step of using a centrifugal dust collecting device to separate out dust in the flue exhaust gas collected in the sampling step, to yield an analysis gas; a measuring step of measuring components in the analysis gas to obtain the concentration of carbon monoxide in the analysis gas; and an analysis gas discharging step of causing the analysis gas to be sucked by an ejector.

Abstract: A detection method includes calibration mode of calibrating sensor with low-concentration gas being caused to flow along direction from the sensor toward an adsorption part, first detection mode of, after the calibration mode, detecting chemical substance with sample gas being caused to flow along the direction from the sensor toward the adsorption part, first adsorption mode of adsorbing, by the adsorption part, the chemical substance during an execution time period including time period overlapping at least part of an execution time period of the first detection mode, second adsorption mode of, after the first adsorption mode, adsorbing, by the adsorption part, the chemical substance with the sample gas being caused to flow along direction from the adsorption part toward the sensor, and second detection mode of desorbing, from the adsorption part, the chemical substance adsorbed in the first and second adsorption modes and detecting the chemical substance by the sensor.

Abstract: A detector inlet for providing a sample to an analytical apparatus for detecting an aerosol, the detector inlet comprising; an intake for inhaling a flow of gaseous fluid to be sampled by the analytical apparatus; a mixing region; a first conduit for carrying a first part of the flow of gaseous fluid from the intake to the mixing region; a second conduit for carrying a second part of the flow of gaseous fluid from the intake to the mixing region; and a heater configured to heat the first part more than the second part, and wherein the detector inlet is configured to combine the first part with the second part in the mixing region.

Abstract: The invention relates to a probe arranged for subsurface penetration of a soil for measuring properties of the soil. The probe comprising a probe body and at least one fiber optical sensor. The at least one fiber optical sensor is arranged for measuring at least one of a cone resistance, sleeve friction, pore water pressure or inclination.

Abstract: Provided are particle analyzers and related methods for verifying calibration status of the particle analyzer. The method includes the steps of providing an optical particle analyzer and modulating a power applied to a source of EMR. The method includes the steps of, in response to the modulating step, inducing a detector signal waveform and analyzing the detector signal waveform to determine a value of at least one diagnostic parameter associated with one or more of the source of EMR, an optical assembly, a chamber, a detector, and an optical collection system of the optical particle analyzer. The method includes the step of determining a calibration status of the optical particle analyzer based on the one or more determined values of the at least one diagnostic parameter.

Abstract: Apparatuses are disclosed including an apparatus for machine fluid monitoring or sampling comprising a transparent sight glass attachable to a machine such that machine fluid is transferable to the sight glass. The sight glass is at least partially constructed of one or more materials that is transparent to light in a visible region. The sight glass has an open first end, a closed second end, an inside surface and an outside surface extending from the open first end to the closed second end and across the closed second end, the sight glass at least partially surrounds a cavity within the sight glass, the inside surface and the outside surface of the closed second end being parallel. The closed second end is constructed of the one or more materials that are transparent to light in the visible region to allow inspection of machine fluid through the closed second end.

Abstract: A particle detecting module is disclosed and includes a main body, which is consist of an air guiding part and a detecting part, by driving a plurality of heating elements disposed within a plurality of storage chambers of the air guiding part, air inside these storage chambers is heated and the moisture of the air is removed, and then the air is transported to the detecting part, so that a sensor of the detecting part could detect the sizes and the concentrations of the suspended particles, and the interference of the humidity is reduced.

Abstract: The present invention is directed to a method and device to generate a chemical signature for a mixture of analytes. The present invention involves using a SPME surface to one or both absorb and adsorb the mixture of analytes. In an embodiment of the invention, the surface is then exposed to different temperature ionizing species chosen with appropriate spatial resolution to desorb a chemical signature for the mixture of analytes.

Abstract: The present invention relates to a method of detecting one or more metals in as liquid sample. The method includes the step of extracting the metal from the liquid sample and retaining the metal on a binding material. The detection of the extracted metal can be performed with the metal retained on the binding material or after the elution of the metal off the binding material.

Abstract: The present invention is directed to a method and device to generate a chemical signature for a mixture of analytes. The present invention involves using a SPME surface to one or both absorb and adsorb the mixture of analytes. In an embodiment of the invention, the surface is then exposed to different temperature ionizing species chosen with appropriate spatial resolution to desorb a chemical signature for the mixture of analytes.

Abstract: The present invention is directed to a method and device to generate a chemical signature for a mixture of analytes. The present invention involves using a SPME surface to one or both absorb and adsorb the mixture of analytes. In an embodiment of the invention, the surface is then exposed to different temperature ionizing species chosen with appropriate spatial resolution to desorb a chemical signature for the mixture of analytes.

Abstract: A sample extraction device and a desorption device for use in gas chromatography (GC), gas chromatography-mass spectrometry (GCMS), liquid chromatography (LC), and/or liquid chromatography-mass spectrometry (LCMS) are disclosed. In some examples, the sample extraction device includes a lower chamber holding a sorbent. The sample extraction device can extract sample headspace gas from a sample vial by placing the sorbent inside the vial and creating a vacuum to increase recovery of low volatility compounds, for example. Once the sample has been collected, the sample extraction device can be inserted into a desorption device. The desorption device can control the flow of a carrier fluid (e.g., a liquid or a gas) through the sorbent containing the sample and into a pre-column and/or a primary column of a chemical analysis device for performing GC, GCMS, LC, LCMS, and/or some other chemical analysis process.

Abstract: A method for indoor air analysis, and a sampling arrangement are disclosed. The method includes taking a sample from indoor air in such a way that a surface is cooled to be so cold that water molecules of the indoor air undergo deposition on the surface, whereby frost is generated on the surface; defrosting the frost into water; and analysing the quality of the indoor air from the water.

Abstract: A desorber for a trace detection system. The desorber includes an inlet configured to receive a sample, a heating element configured to generate a vapor from the sample, and an active cooling element configured to cool the desorber.

Abstract: A system for on-stream sampling of pressurized process gas such as natural gas or the like, said system optimized for use with pressurized process gas having liquid entrained therein, or otherwise referenced as “wet”. In the preferred embodiment, a probe and method of sampling is contemplated to provide linear sample of fluids from a predetermined of said fluid stream. Further taught is the method of preventing compositional disassociation of a gas sample having entrained liquid utilizing a probe having a passage formed to facilitate capillary action in fluid(s) passing therethrough. The present system further contemplates a heated pressure regulator or adapter formed to thermally engage a heat trace via conducting plates and heat pipes, in order to dispense with the need for an external power source for heating.

Abstract: It is aimed to analyze a gas component of a to-be-analyzed gas with a reduced influence of a liquid component contained in the to-be-analyzed gas. Provided is an analyzing apparatus for analyzing a gas component of an exhaust gas that has passed through a scrubber apparatus and the like. The analyzing apparatus includes a collecting nozzle configured to collect a to-be-analyzed gas, a liquid collecting unit configured to collect a liquid component contained in the to-be-analyzed gas collected by the collecting nozzle and to allow the to-be-analyzed gas to pass therethrough, a liquid discharging unit configured to discharge the liquid component collected by the liquid collecting unit, and an analyzing unit configured to analyze a gas component of the to-be-analyzed gas that has passed through the liquid collecting unit.

Abstract: A sampling point assembly for an aspirating particle detection system includes a sampling point body having a bore running from an inlet at a first end of the bore to an outlet at a second end of the bore, the inlet being configured to be maintained in fluid communication with a volume being sampled to receive an air sample therethrough, and the outlet being configured to be coupled to a conduit such that the air sample can pass through the central bore to the conduit. A fastening mechanism includes at least one surface adjacent the inlet and arranged in use to support the sampling point assembly on a first side of a mounting structure, and at least one fastening actuator for holding the surface against the mounting structure from the first side. A cap conceals the fastening mechanism and inlet from view from the first side of the mounting structure.

Abstract: The present invention is directed to a method and device to generate a chemical signature for a mixture of analytes. The present invention involves using a SPME surface to one or both absorb and adsorb the mixture of analytes. In an embodiment of the invention, the surface is then exposed to different temperature ionizing species chosen with appropriate spatial resolution to desorb a chemical signature for the mixture of analytes.

Abstract: There is described a duct detector (1) and components (2, 3, 6) for duct detectors. In one form the duct detector (1) includes: a port unit (3) and detector unit (2). The port unit (3) is mountable to a duct in use so as to position one or more ports in the duct. The detector unit (2) includes a detection region. The port unit (3) and detector unit (2) are reconfigurable between a close coupled configuration and a separated configuration in which the units (2,3) are mountable with a variable separation between them and coupled by one or more elongate conduits (12A, 12B) to provide fluid communication between the units (2,3).

Abstract: A method for detecting a volatile analyte to class and sort cork stoppers depending on the concentration of the analyte, detection being preformed of concentrations in the order of ng/L (parts per trillion), in a concentrated gas applied to the cork stoppers in close containment. Cork stoppers are conveyed individually or groups to an incubation chamber; air/nitrogen is injected into the incubation chamber, the gas enriched with cork volatile compounds is entrained and carried to the concentration system containing a trap heated by desorption of entraining gas to a detection system recording a signal associated with presence of the analyte, the signal being used for classing the stopper/groups of stoppers; a software receives and compares the signal with a minimum limit, deciding to approve or reject the stopper. A system for implementing this method is described.

Abstract: A sample injection device for sample collection and thermal desorption includes: a sample collection structure; a piston type adsorber having an adsorption cavity communicating with the sample collection structure; a piston cylinder defining a piston chamber accommodating the adsorber and communicating with the adsorption cavity; a thermal desorption chamber communicating with the adsorption cavity and the piston chamber; and a pump configured to pump a sample diffused in an ambient gas into the adsorption cavity through the sample collection structure and the piston chamber; the adsorber is movable between a sample collecting position where the adsorption cavity is outside the thermal desorption chamber and adsorbs the sample collected by the sample collection structure and a sample desorbing position where the adsorption cavity is inside the thermal desorption chamber so that the adsorbed sample is thermally desorbed in the thermal desorption chamber.

Abstract: Provided is a gas-spouting liquid-sample injector, for supplying a mist of liquid sample into a container, including: a sample introduction tube having an outer tube for a nebulizer gas and an inner tube for a liquid, the inner tube having a projecting section protruding from the lower end of the outer tube; a branch tube provided in the container, having a main line allowing an insertion of the sample introduction tube and a bypass line branched from the main line; an inlet portion provided at the upper end of the main line, for making gas-tight contact with the lower end of the outer tube; an outlet portion provided at the lower end of the main line, for making gas-tight contact with the outer circumferential surface of the inner tube; and a blower tube extending from the lower end of the bypass line toward an area below the outlet portion.

Abstract: We disclose a device that both extracts and preconcentrates volatile analytes in preparation for separation by gas chromatography. The device includes a conduit that may include two, and sometimes three, separate sections that are connected end-to-end, but which may be separated prior to inserting into a gas chromatograph port. The inner surface of each section is coated with one or more sorbents, each with a different affinity for volatile analytes. The sorbents may be positioned along the sections of the column in order of relative affinity for volatile analytes. The sections may be heated independently of each other to release the volatile analytes from the sorbents more quickly. This device reduces the time and the temperature required to achieve separation by gas chromatography. The device may be used to perform gas chromatography in ubiquitous environments such as the home or a mobile situation.

Abstract: The present invention is directed to a method and device to generate a chemical signature for a mixture of analytes. The present invention involves using a SPME surface to one or both absorb and adsorb the mixture of analytes. In an embodiment of the invention, the surface is then exposed to different temperature ionizing species chosen with appropriate spatial resolution to desorb a chemical signature for the mixture of analytes.

Abstract: A sample introduction device comprises a sampling unit, a gas suction pump, adsorption units, a piston cylinder and a desorption cylinder that comprises a desorption chamber, a carrier-gas inlet, a split/purge vent and an analyzer nozzle communicating with the desorption chamber. A heating film and a temperature sensor are provided on outer wall of the desorption cylinder. The piston cylinder above the desorption cylinder comprises two piston chambers, each of which is provided with the adsorption unit and in communication with the desorption chamber. The piston cylinder comprises a sample-gas inlet connected to the sampling unit and a gas-suction-pump orifice connected to the gas suction pump, each of which can communicate with both piston chambers. Each adsorption unit comprises an adsorption cylinder-like screen for holding adsorbents and a piston rod slidably mounted in the piston chamber.

Abstract: A reactor system including an enclosed pressure relief system and/or a control system. The enclosed pressure relief system including a slurry separation system communicatively coupled with a pressure relief valve coupled to a loop reactor such that activation of the pressure relief valve results in discharge of a slurry from the loop reactor to the slurry separation system, wherein the slurry separation system is capable of separating solid and liquid components from gas components of the slurry and transmitting the gas components to a flare via a flare header.

Abstract: An inlet apparatus is disclosed. The apparatus may include a first conduit for sampling, and a second and third conduit for directing flow throughout the inlet apparatus. Flow may be induced in two opposite directions through the second conduit, which affect the flow of gas through the first conduit for sampling. The various conduits of the apparatus may be connected to a device for inducing flow in different directions. The duration of the flow in a particular direction affects the amount of sample gas that enters a detection device.

Abstract: A method and system for taking a sample of ballast water. The method includes withdrawing a sample of ballast water via a tube inserted in a ballast water pipe, wherein the tube includes a sample inlet, and isokinetic flow is achieved via a pump that controls the flow of the sample ballast water through the tube inlet by comparing a flow of the ballast water pipe with a flow of the sample ballast water through the tube; and controlling the flow of water through the sample tube inlet when a flow of the ballast water pipe is sensed to be different; withdrawing a portion of the sample ballast water for testing; and returning remaining sample ballast water to the ballast water pipe.

Abstract: An apparatus for heating a flowing fluid includes a tubing assembly, a heater block made of thermally conductive material, and a heater cartridge in thermal communication with the heater block. The heater cartridge is configured to provide heat to the heater block for transfer to fluid flowing through the tubing assembly. The apparatus also includes circuitry in electrical communication with the heater cartridge to control a temperature of the heater block by controlling operation of the heater cartridge. The heater block is die-cast about the tubing assembly.

Abstract: A thermophoretic sampler includes a sample assembly into which a removable sample cartridge can be inserted. The sample cartridge holds a substrate that, upon insertion, is exposed to a sample chamber. Thermophoresis is induced in the sample chamber, causing nanoparticles to be deposited on the substrate.

Abstract: A system for preparing samples for chemical analysis comprises at least one sample container, and a container receptacle apparatus for receiving the sample container. The sample container comprises an elongate tubular body having a crucible portion proximal to a closed end for receiving a sample therein, and an expansion portion proximal to an open end. The container receptacle apparatus comprising a housing having a heating compartment, a cooling compartment spaced apart from the heating compartment, and an insulating region located between the heating compartment and the cooling compartment. The heating compartment is shaped to receive the crucible portion of the sample container, and the cooling compartment is shaped to receive the expansion portion of the sample container. The apparatus also includes a heating mechanism for heating the sample within the crucible portion of the sample container, and a cooling mechanism for cooling the expansion portion of the sample container.

Abstract: A sampling system that contains filter components for collecting and concentrating vapor and particles in high-volume flows. The sample is then vaporized and delivered to a detector at a low-volume flow. The invention also has a sampling probe that contains an air-jet to help dislodge particles from surfaces and a heating lamp to help vaporize compounds on surfaces or objects. The sampling system is especially useful for screening for explosives and other illicit chemicals and toxins on people, baggage, cargo, and other objects.

Abstract: A fabric phase sorptive extractor (FPSE) is a sampling device where a flexible fabric is coated with at least one sol-gel derived film that includes at least two of a metal oxide portion, a siloxy portion, and an organic portion, where the gel has at least some amorphous portions. The FPSE is flexible such that it can be used in an extended form or draped over a solid surface to contact a gaseous, liquid, or solid environment and can be manipulated for placement in a container where the absorbed analyte can be removed from the FPSE for instrumental analysis. The FPSE can have specific functionalities that bind to specific analytes or can provide a general sorbent medium for extraction of a wide range of analytes, such that the sampling device can be employed for sampling analytes with biological, environmental, food, pharmaceutical, bio-analytical, clinical, forensic, toxicological, national security, public health, and/or safety implications.

Abstract: Analytes are rapidly desorbed from a carbonaceous sorbent powder with improved quantitation and reduced analyte re-adsorption, thermal degradation, and rearrangement. The sample is distributed in a thin layer onto a desorption surface within a chamber. The layer can be a monolayer. Heating light irradiates the sample through a window, directly and rapidly heating the sample while the desorbed analytes diffuse into a vacuum or are removed by a carrier gas. Finally, the sorbent is flushed from the chamber by a transport gas. The desorption surface can be an inner surface of the window, or a surface of a porous frit that divides the chamber into two sections. The frit can be stainless steel or glass. The carrier gas can be helium, argon, or carbon dioxide. The light source can be a tungsten halogen lamp. A heater can control the chamber temperature according to a heating profile.

Abstract: A device for detecting volatile substances has a containment box with at least one inlet opening for introduction of gas flow, one or more outlet openings of the gas flow, at least one analysis opening, one or more detection sensors arranged in the containment box, and at least one probe insertable in the containment box through at least one analysis opening. When the probe is initially treated by a sample of a substance to be examined and is inserted in the containment box, the gas flow uniformly carries the volatile substances from the sample to one or more sensors. A detection apparatus and a detection method for volatile substances are also described.

Abstract: An integrated apparatus and method for screening an object for a target material is provided. The integrated apparatus comprises a housing and an integrated screener. The housing is positionable adjacent the object, and has a channel therethrough. The integrated screener is positionable in the housing, and comprises a fan, at least one filter, a heater and an analyzer. The fan is for drawing air carrying particles and vapor through the channel of the housing. The filter(s) is/are positionable in the channel of the housing for passage of the air therethrough. The filter(s) comprise(s) at least one metal foam having a plurality of pores therein for collecting and adsorbing a sample from the particles and vapor passing therethrough. The heater is for applying heat to the at least one metal foam whereby the collected sample is desorbed from the metal foam. The analyzer detects the target material from the desorbed sample.

Abstract: A fluid transfer device transfers a fluid from a first fluid channel with a first cross-sectional area into a second fluid channel with a second cross-sectional area, larger than the first cross-sectional area. The fluid transfer device includes a fluid inlet interface at which the fluid is transferable from the first fluid channel into the fluid transfer device; an inlet branch configured to split the fluid from the first fluid channel into multiple inlet branch channels; multiple outlet branches, each of which is configured to split the fluid from the inlet branch channels into respective outlet branch channels; and a fluid outlet interface configured to transfer the fluid in the outlet branch channels into the second fluid channel. The inlet and output branches and branch channels are disposed such that the fluid exits from the fluid outlet interface, distributed in a two-dimensional manner across the second cross-sectional area.

Abstract: A system and a method is described herein for the collection of small particles in a concentrated manner, whereby particles are deposited onto a solid surface or collected into a volume of liquid. The collected samples readily interface to any of a number of different elemental, chemical, or biological or other analysis techniques.

Abstract: A method of extracting an analyte from a sample is described. The sample is added to a sample container. A liquid solvent and a gas are added into the sample container. The addition of the gas is controlled to establish an elevated pressure within the sample container. The liquid solvent is heated to an elevated temperature that is below the boiling temperature of the liquid solvent at the elevated pressure. A type of gas is used that does not transition to a supercritical fluid at the elevated temperature and pressure used in the extraction process. The analyte can dissolve from the solid sample into the liquid solvent. Next, at least a portion of the liquid solvent containing the dissolved analyte can be removed from the sample container for subsequent analysis.

Abstract: A sample introduction system configured for introducing analytes of a solid phase micro extraction (SPME) sample into an analytical instrument system (e.g., mass spectrometer) is described. The sample introduction system includes a pressure vessel configured with an inlet port via which a probe portion (e.g., SPME fiber) of a SPME assembly is received into a sealed volume of the pressure vessel. The probe portion of the SPME assembly is coated with an extracting phase material, the analytes being absorbed into and/or adsorbed onto the extracting phase material. The pressure vessel is configured for providing an environment in which desorption of the analytes from the extracting phase material occurs at a gaseous pressure which is substantially less than atmospheric pressure (e.g., less than 100 mTorr). The desorbed analytes are then directed to the vacuum chamber of the analytical instrument system via an outlet port of the pressure vessel.

Abstract: A method for determining the styrene microblock content of a copolymer sample, the method comprising: (i) pyrolyzing the copolymer sample to form polymer fragments of the polymer sample; (ii) analyzing the fragments to determine the relative amounts of styrene monomer fragments, styrene dimer fragments, and styrene trimer fragments, where the relative amounts of the fragments include the amount of any given fragment relative to the total of the monomer fragments, dimer fragments, and trimer fragments; and (iii) using the relative amounts of the styrene monomer fragments, styrene dimer fragments, and styrene trimer fragments to predict the polystyrene microblock content from a mathematical model that is based upon the relative styrene monomer fragments, relative styrene dimer fragments, relative styrene trimer fragments, and microblock content of a copolymer having known microblock content.

Abstract: A liquid natural gas sample conditioning cabinet structure with a covered vent disposed proximate to the cabinet floor for preventing pooling of and venting heavier-than-air hydrocarbon gases.

Abstract: A device for sampling surfaces for the presence of compounds is provided, including a housing having a proximal end adapted to receive it negative pressure gradient and a distal end adapted to contact the surfaces; a heating element spaced from the distal end; a primary filter spaced from the heating element; and a secondary filter spaced from the primary filter, the secondary filter removably received by the housing. Also provided is as method for sampling a surface for the presence of compounds, the method including contacting the surface to dislodge the compounds from the surface; capturing first fractions of the compounds with a primary filter while allowing second fractions of the compounds to pass through the primary filter; heating the primary filter to volatilize the first fractions; capturing the volatized first fractions and the second fractions with a secondary filter; and analyzing the secondary filter to identify the compounds.

Abstract: The present invention relates to an adsorbed gas content measuring instrument and its testing method. The instrument comprises sealed cylinders, gas collecting graduated canisters and a test box, wherein the sealed cylinders are provided with valves, the gas collecting graduated canisters are equipped with drain hole adjustment valves and vent hole switching valves fit for the valve ports, and there is a heating element and a temperature controller in the test box. The method is mainly as follows: put gas-contained samples and saturated brine into the sealed cylinder, seal the cylinder, feed water in the test box and heat the box, place the sealed cylinder into the water bath of the test box, introduce saturated brine into the gas collecting graduated canister, connect the canister and cylinder, open the drain hole of the gas collecting graduated canister, record the liquid level of the graduated canister and cut off the connection after the test.

Abstract: Certain aspects and examples are directed to sorbent devices and methods of using them. In certain embodiments, a sorbent device comprising a body comprising a sampling inlet, a base and a longitudinal diffusion path between the inlet and the base is provided. In some embodiments, the sorbent device can include at least two sorbent materials fluidically coupled to the longitudinal diffusion path, in which the sorbent materials are arranged from a material with a weakest sorbent strength to a material with a strongest sorbent strength with the weakest sorbent strength material adjacent to the sampling inlet.

Abstract: Apparatus and method for collecting particles of both high and low vapor pressure target materials entrained in a large volume sample gas stream. Large volume active cooling provides a cold air supply which is mixed with the sample gas stream to reduce the vapor pressure of the particles. In embodiments, a chiller cools air from ambient conditions to 0-15° C. with the volumetric flow rate of the cold air supply being at least equal to the volumetric flow rate of the sample gas stream. In further embodiments an adsorption media is heated in at least two stages, a first of which is below a threshold temperature at which decomposition products of the high vapor pressure particle are generated.

Abstract: The device for sampling and vaporizing liquefied natural gas includes a circuit provided at one end with a device for collecting a sample of liquefied gas and conveying the sample to a measurement device. The circuit includes and passes through a device for vaporizing the sample. The device for vaporizing includes at least one vaporization chamber having a first convergent section portion and a second divergent section portion being consecutive along the circuit and shaped so as to vaporize all of the sample under supercritical conditions at a pressure of greater than 80 bar without fractionating. The vaporization chamber includes, at the entrance of the first convergent section portion, a port with a variable opening. The port is sized so as to limit the vaporization pressure to a maximum of 90 bar in conjunction with a fixed opening at the outlet of the second divergent section portion.

Abstract: A sampling system that contains filter components for collecting and concentrating vapor and particles in high-volume flows. The sample is then vaporized and delivered to a detector at a low-volume flow. The invention also has a sampling probe that contains an air-jet to help dislodge particles from surfaces and a heating lamp to help vaporize compounds on surfaces or objects. The sampling system is especially useful for screening for explosives and other illicit chemicals and toxins on people, baggage, cargo, and other objects.

Abstract: A method for attaching a frozen specimen to a manipulator probe tip typically inside a charged-particle beam microscope. The method comprises cooling the probe tip to a temperature at or below that of the frozen specimen, where the temperature of the frozen specimen is preferably at or below the vitrification temperature of water; bringing the probe tip into contact with the frozen specimen, and bonding the probe tip to the frozen specimen by flowing water vapor onto the region of contact between the probe tip and the frozen specimen. The bonded probe tip and specimen may be moved to a support structure such as a TEM grid and bonded to it by similar means. The probe tip can then be disconnected by heating the probe tip or applying a charged-particle beam.