Abstract: The invention relates to the extraction of a frozen hydrated sample for TEM (Transmission Electron Microscope) inspection, such as a vitrified biological sample, from a substrate and the attaching of said sample to a manipulator. Such a hydrated sample should be held at a cryogenic temperature to avoid ice formation. By melting or sublimating a part of the sample material outside the area to be studied in the TEM and freezing the material to the manipulator (10), a bond is formed between sample (1) and manipulator. This makes it possible to transport the sample from the substrate to e.g. a TEM grid. In a preferred embodiment a part (2) of the manipulator (10) is held at a cryogenic temperature, and the melting or sublimation is caused by heating the tip (3) of the manipulator by electric heating of the tip and then cooling the tip of the manipulator to a cryogenic temperature, thereby freezing the sample (1) to the manipulator.

Abstract: A CTD and method of using a CTD for automatic sampling and analysis of target analytes, such as explosive materials, chemical warfare agents, and narcotics present on documents or other articles is provided. The CTD comprises an article processing mechanism, a swabbing medium, a thermal desorber, and a spectrometer.

Abstract: An apparatus for concentrating a vaporous substance, which comprises: a sorbent material capable of capturing a vaporous substance; a first housing in which the sorbent material is located, a heating element proximate the exterior of the housing; a second housing defining a chamber within which the first housing resides, the first housing being located in said chamber such that there is a space permitting gas flow between the outside of the first housing and the inside of the second housing; and a pump capable of causing an exhaust gas to flow through the space in contact with the outside of the first housing; and methods for making and utilizing such apparatus.

Abstract: A CTD and method of using a CTD for automatic sampling and analysis of target analytes, such as explosive materials, chemical warfare agents, and narcotics present on documents or other articles is provided. The CTD comprises an article processing mechanism, a swabbing medium, a thermal desorber, and a spectrometer.

Abstract: Volatile suspended particles are eliminated from an aerosol by heating the aerosol to a temperature at which the volatile suspended particles evaporate and diluting the aerosol with a dilution gas. The sequence heating and diluting may be performed in any order. According to another aspect of the invention, dilution of the raw gas takes place such that raw gas is led to a measurement gas channel through which measurement gas flows, wherein the quantity of raw gas transferred per unit of time is dependent on the volume flow in the raw gas channel. According to a further aspect of the invention, in a condensation nucleus counter the number and intensity of scattered light pulses is evaluated in order to be able to draw conclusions on the reliability of the measurement.

Abstract: A monitoring device for use in monitoring the life of a filter used in the operating unit of an air conditioning system. The monitoring device has a support for use in attaching the device to the housing of the operational unit in the air conditioning system, the unit having a least one air conditioning filter holding filter material. At least one tubular arm attached to the support, each arm having an air inlet and an air outlet. The support is mounted in a manner to have a portion of the air passing through the air conditioning unit pass through the arm on the support as well. A sample filter is provided along with mounting means for removably mounting the sample filter on the arm to have air passing through the arm also pass through the sample filter. The sample filter holds the same filter material as the air conditioning filter.

Abstract: There is provided a sample treatment apparatus which can, continuously and stably for a long time, treat a sample containing an easily precipitating substance such as sulfur and a measuring apparatus providing it. The sample treatment apparatus includes: a path for introducing a fluid for an aspirator, at least two sample flow paths A connected in one side to the path for introducing a fluid for an aspirator and connected in the other side to a sample collecting part, a sample flow path B connected in one side to one sample flow path A passing a fluid for an aspirator and connected in the other side to the other sample flow path A, a cooling part for cooling a part of the sample flow paths A, and a controller for selecting and switching the sample flow paths A into which a fluid for an aspirator is introduced.

Abstract: A method includes the phases of measuring the quantity of a given gas in the gases extracted from a calibration sample of a calibration mud, in at least two stages for extraction under predetermined conditions. A family of curves representing the extraction, under the predetermined conditions, of the given gas from the drilling mud, is established on the basis of the measurements carried out. The method also includes the phases of measuring the quantity of given gas in the gases extracted from an analysis sample of the drilling mud in an extraction stage, under the predetermined conditions; and computing the given gas content of the drilling mud on the basis of the measured quantity of given gas and of a curve of the family.

Abstract: A heated sampling hose assembly includes a sampling hose having an inlet and an outlet for passage of a sample gas. An outer sleeve surrounds the sampling hose with an annular purge gas passage radially therebetween. The outer sleeve is closed at opposite ends by first and second fittings having a purge gas inlet and purge gas outlet, respectively, and a heater is arranged to heat the purge gas in the annular purge gas passage to a temperature of the sample gas.

Abstract: A sample collection device for use with a chemical analyzer, the device comprising a sample collecting assembly having at least one sampling medium and a sample desorbing assembly arranged to receive the sampling medium therein, the sample collecting assembly and sample desorbing assembly being movable with respect to one another between a sample collecting configuration in which the sampling medium is substantially exposed and a sample desorbing configuration in which the sampling medium is substantially housed within the sample desorbing assembly.

Abstract: A vessel is provided for collecting a process stream and fractionating the process stream into a liquid and gas phase in the vessel. Cooling may be provided by an internal bath and/or an external bath. The liquid phase retained in the vessel and the gas phase collected in lots from the vessel may be delivered to a lab for analysis.

Abstract: A method and system for sampling high vapor pressure substances is provided. In one embodiment, a sample is pre-concentrated by compression and condensation, water is removed by a condensing gas dryer, particulates are removed from the sample with an electrostatic precipitator; and the sample is shuttled through a sintered core at high vapor pressure so that molecules are condensed on the surface of the sintered core. In another embodiment, a system for sampling high vapor pressure substances includes a shuttle having a first piston and second piston for shuttling a sample through a sintered core at high vapor pressure and a condensing heat exchanger between the first piston and the second piston, the condensing heat exchanger including the sintered core.

Abstract: A sampling system that contains filter components for collecting and concentrating vapor and particles in high-volume flows. The sample is then vaporized and delivered to a detector at a low-volume flow. The invention also has a sampling probe that contains an air-jet to help dislodge particles from surfaces and a heating lamp to help vaporize compounds on surfaces or objects. The sampling system is especially useful for screening for explosives and other illicit chemicals and toxins on people, baggage, cargo, and other objects.

Abstract: The invention is directed to a system and method for detecting substances, such as high boiling and low vapor pressure materials, using high energy radiation imparted by a suitable radiation source, such as a strobe or laser over a short time period. The radiation source causes the materials to vaporize. A system handling system is used in conjunction with a detector to detect the presence of the materials including explosives, explosive-related compounds, chemical warfare agents, drugs, toxic industrial compounds, and derivatives thereof.

Abstract: An apparatus is provided for identifying trace amounts of substances of interest in an air flow. The apparatus includes an inlet for receiving the air flow and an outlet for exhausting major portions of the air flow. The outlet is offset from the inlet. A porous impactor is disposed in alignment with the inlet and is impacted by particles entrained in the air flow. The porous impactor is heated sufficiently to vaporize particles impinging thereon. A detector communicates with the porous impactor and is operative for identifying substances of interest in the vaporized particles.

Abstract: A fluid analyzer having a concentrator and separator for concentrating and separating fluid samples at pressures up to about 10,000 psi (˜700 bar). The concentrator and separator may consist of a solid-state thin-film heater-adsorber and a channel supported by a solid substrate. The concentrator may have numerous heated interactive elements for adsorbing and desorbing constituents of a sample fluid. The interactive elements may be heated in a time phased sequential manner by heaters. The separator may separate the sample fluid by compound. There may be thermal conductivity detectors, a flow sensor and electrical conductivity detectors proximate to the channels. This system of concentrator, separator, heaters and sensor may provide information about the sample fluid composition. A pump may be connected to the channel to move the sample fluid through it.

Abstract: A system for the collection and initial conditioning of sample gas for “on-line” analyzers, or filling of gas sample cylinders. The preferred embodiment of the present invention contemplates a system configured to obtain a representative gas phase sample from a process gas containing entrained liquid, or a process gas which generally is susceptible to partial condensation of some gas phase components. The preferred embodiment of the present invention teaches a sample probe assembly including a heat pipe configured for maintaining sample gas drawn through said sample probe at or near the source gas temperature and pressure. Accuracy of the analysis of source gas stream is enhanced and compositional changes of the gas phase are avoided by preventing the partial condensation of gas components or vaporization of entrained liquid.

Abstract: An apparatus is provided for detecting whether a person has handled explosives, narcotics or other substances of interest. The apparatus includes a metallic sample collection surface on which a person may place a finger. Upon removal of the finger, the metallic sample collection surface is moved to a desorber. The desorber heats the metallic surface sufficiently to vaporize residue transferred from the person. The vaporized residue then is transmitted to a detector for analysis. The detector also may include a fingerprint reading apparatus for reading the fingerprint of the person and comparing the fingerprint to known fingerprint data.

Abstract: A sample heater assembly which permits the detection of low volatility agents by existing chemical agent detectors is described. Existing chemical agent detectors often lack the capability to accurately detect low volatility agents, such as the chemical warfare agent VX. The sample heater assembly provides this capability by heating low volatility agents to vaporization and interfacing with the existing chemical agent detector. The sample heater assembly comprises a sample containment reservoir for holding the low volatility agent sample, which can be attached to the chemical agent detector, and a heating element which attaches to the sample containment reservoir for heating the sample.

Abstract: A system for the retrieval and initial conditioning of sample gas for “on line” analyzers or filling of gas sample cylinders. The preferred embodiment of the present invention contemplates a system configured to obtain a representative gas phase sample from a process gas containing entrained liquid, or a process gas which generally is highly susceptible to partial condensation of some gas phase components. The preferred embodiment of the present invention teaches an assembly including a phase separation membrane and housing configured to facilitate the removal of entrained liquid from a sample gas stream. Accuracy of the sample is enhanced, and compositional changes are avoided by first extracting a sample from the process gas followed by removal of entrained liquid it may contain, with the entrained liquid removal being conducted at the prevailing process gas pressure and temperature. Thereafter the liquid free sample may be desaturated by lowering its pressure to reduce its susceptibility to condensation.

Abstract: A water trap system based on a thermoelectric cooling device is employed to remove a major fraction of the water from air samples, prior to analysis of these samples for chemical composition, by a variety of analytical techniques where water vapor interferes with the measurement process. These analytical techniques include infrared spectroscopy, mass spectrometry, ion mobility spectrometry and gas chromatography. The thermoelectric system for trapping water present in air samples can substantially improve detection sensitivity in these analytical techniques when it is necessary to measure trace analytes with concentrations in the ppm (parts per million) or ppb (parts per billion) partial pressure range. The thermoelectric trap design is compact and amenable to use in a portable gas monitoring instrumentation.

Abstract: A micro fluid analyzer having a concentrator and separator. A strip continuous through a channel in the concentrator may provide a hot zone that may move with the flow of fluid through the channel of the concentrator to provide a concentration of heat in the flow. A pump may provide a flow to the fluid through the analyzer. Detectors may be positioned at places where the fluid may flow. A processor or controller may be connected to the strip, separator, pump and detectors. The concentrator, separator, detectors and processor may be integrated on one chip.

Abstract: An apparatus and method for generating ions from an aerosol and transferring the ions into a mass analyzer. In the apparatus and method, an aerosol beam is generated, the aerosol beam is directed to a spatial volume outside the mass analyzer, particles in the aerosol beam are ionized to produce the ions, and the ions are collected into the mass analyzer. As such the apparatus includes respectively an aerosol beam generator, an ion source generator, and an ion collector.

Abstract: A tank contains both Zeolite and a hydrate in a gas chamber formed beneath a piston in the sample tank. Out of safety considerations, we avoid using source cylinders of nitrogen whose pressures exceed 4000 psi. Thus, the gas chamber of the sample tank is initially pressurized by the source cylinder to no more than 4000 psi of nitrogen at room temperature at the surface. Nitrogen gas is sorbed onto the zeolite at room temperature. As the tank is heated by being lowered downhole, nitrogen desorbs from the zeolite and the gas pressure increases. However, once this tank reaches a temperature high enough to release the hydrate's water of hydration, the released water is preferentially sorbed by zeolite, displacing sorbed nitrogen, and causing the pressure in the gas volume to increase even further. Because well temperatures are not high enough to desorb water from zeolite, any water sorbed onto a Zeolite sorption site will permanently block released nitrogen from resorbing at that site.

Abstract: A system for the retrieval and initial conditioning of sample gas for “on line” analyzers or filling of gas sample cylinders. The preferred embodiment of the present invention contemplates a system configured to obtain a representative gas phase sample from a process gas containing entrained liquid, or a process gas which generally is highly susceptible to partial condensation of some gas phase components. The preferred embodiment of the present invention teaches an assembly including a phase separation membrane and housing configured to facilitate the removal of entrained liquid from a sample gas stream. Accuracy of the sample is enhanced, and compositional changes are avoided by first extracting a sample from the process gas followed by removal of entrained liquid it may contain, with the entrained liquid removal being conducted at the prevailing process gas pressure and temperature. Thereafter the liquid free sample may be desaturated by lowering its pressure to reduce its susceptibility to condensation.

Abstract: The invention is directed to a system and method for detecting substances, such as high boiling and low vapor pressure materials, using high energy radiation imparted by a suitable radiation source, such as a strobe or laser over a short time period. The radiation source causes the materials to vaporize. A system handling system is used in conjunction with a detector to detect the presence of the materials including explosives, explosive-related compounds, chemical warfare agents, drugs, toxic industrial compounds, and derivatives thereof.

Abstract: An explosive detection system including a sample injection region, an ion source region for generating ions of a sample injected by the ion injection region, a mass analysis region for analyzing mass of the ions, a heater for heating the sample injection region and the ion source region, a plurality of pumps for exhausting a chamber in which the mass analysis region is disposed, and a controller for controlling the regions and the plurality of pumps. The controller conducts control so as to heat the sample injection region and the ion source region with the heaters, then reduce heating electric power supplied to the heaters in order to prevent a predetermined electric power value from being exceeded, and drive the plurality of pumps successively to exhaust the chamber.

Abstract: An equipment or environment health monitor having a micro gas apparatus incorporating a phased heater array, concentrator, separator and detector for achieving the sensitivity needed for detection of extremely small amounts of fluids. The apparatus is capable of detecting trace gases, and may be utilized to detect “fault” gas of operating equipment so as to determine, for example, the prospects of imminent failure of the equipment. Also, the micro gas apparatus is capable of detecting miniscule amounts of pollutants in ambient environment of a conditioned or tested space. The output of the apparatus may go to a microcontroller and/or processor for prompt analysis. The output from the microcontroller or processor may go to either a transmitter/receiver for wireless communication or a modem for utility line, cable or optical communication with a station for data and results observation and review.

Abstract: A sample plate structure is provided including a retainer plate having a central recess with a trough along its periphery, a sample insert plate which fits into and rests on contact surface of the recess, and a magnet that is held below the contact surface. A portion of the bottom surface of the insert is formed of a magnetic material. The magnet provides sufficient force to retain the insert plate in the retainer plate during MALDI MS analysis. The sample insert plate is provided with a peripheral configuration, which assures that the sample insert plate is properly oriented within the sample plate support structure and is held flat. A hole for a protrusion allows easy insert installation and alignment against the orientation feature in the recess as well as easy removal of the insert simply by pushing up from underneath the retainer plate. While the insert sample plate can be a consumable, the remaining portion of the apparatus can be reused.

Abstract: A detector requires a stream of dry air for transporting particles to the detector. The detector then operates to determine whether the dry air has transported any particles of interest. Continuous operation of the detector is permitted by providing first and second dryers that can be operated alternately for drying air that is to be directed to the detector. The dryer that is not being operated is recharged. Air is directed alternately between the first and second dryer to ensure that neither dryer is operated after reaching saturation.

Abstract: A hazardous material detection system that can suppress occurrence of contamination due to ionization. When a sensor detects that a test sample has entered an inspection region of an X-ray inspection device as a belt conveyor moves, a corona discharge power supply in a hazardous material detection device is turned on for a constant time, to introduce a gaseous sample containing a substance stuck to the test sample into the hazardous material detection device via a sucking section and gaseous sample introduction piping, in order to ionize the gaseous sample and analyze it at an analyzer, based on a result of which analysis, a data processor decides whether the gaseous sample contains a hazardous material, to display a decision result on a screen. When the test sample is detected by an exit side sensor, the corona discharge power supply is turned off.

Abstract: An apparatus for capturing, from gases such as soil gas, target analytes. Target analytes may include emanations from explosive materials or from residues of explosive materials. The apparatus employs principles of sorption common to solid phase microextraction, and is best used in conjunction with analysis means such as a gas chromatograph. To sorb target analytes, the apparatus functions using various sorptive structures to capture target analyte. Depending upon the embodiment, those structures may include a capillary tube including an interior surface on which sorptive material (similar to that on the surface of a SPME fiber) is supported (along with means for moving gases through the capillary tube so that the gases come into close proximity to the sorptive material).

Abstract: A system for the retrieval and initial conditioning of sample gas for “on line” analyzers or filling of gas sample cylinders. The preferred embodiment of the present invention contemplates a system configured to obtain a representative gas phase sample from a process gas containing entrained liquid, or a process gas which generally is highly susceptible to partial condensation of some gas phase components. The preferred embodiment of the present invention teaches an assembly including a phase separation membrane and housing configured to facilitate the removal of entrained liquid from a sample gas stream. Accuracy of the sample is enhanced, and compositional changes are avoided by first extracting a sample from the process gas followed by removal of entrained liquid it may contain, with the entrained liquid removal being conducted at the prevailing process gas pressure and temperature.

Abstract: A gas sampler (1) for a portable gas analyser, having a cooler or chiller (8) through which cooler or chiller (8) the gas sample is passed prior to being conveyed to a gas analyser, has the cooler or chiller (8) operable by means other than electrical power. The invention also includes a portable gas analyser provided with such a sampler (1).

Abstract: A system and methods of the present invention advantageously provide efficient mail processing and handling that, as compared to existing procedures, enhances detection within the mail being processed or handled of biological, germ, chemical, or other harmful agents. A system and methods provide additionally a higher level of quality and consistency for processing and handling mail so that concerns over contamination of postal workers and potential mail recipients are reduced. A system and methods further provide enhanced disabling of contaminated mail contents, mail, mail equipment, mail containers, and mail personnel due to exposure or contact with harmful agents associated with mail.

Abstract: A gas sampling separator 29 for the separation of liquid or other contaminants from gas received from a pipeline may be easily inspected visually and cleaned. A cylindrical body 62 forming a separation chamber 64 is threaded onto a base 40. A tube 68 within the separation chamber receives gas from a port in the base and directs the gas into the separation chamber for separation of the gas from the contaminants. The separated contaminants collect in a sump 58 formed by the base and may be vented upon actuation of a manually actuated valve 76.

Abstract: An apparatus and method for producing a diffusive, continuous laminar flow for particle growth via condensation of vapors with a mass diffusivity near or higher than the thermal diffusivity of the surrounding gas. In an exemplary embodiment, the method uses the condensation of water vapor onto particles suspended in air.

Abstract: A system for the retrieval and initial conditioning of sample gas for “on line” analyzers or filling of gas sample cylinders. The preferred embodiment of the present invention contemplates a system configured to obtain a representative gas phase sample from a process gas containing entrained liquid, or a process gas which generally is highly susceptible to partial condensation of some gas phase components. The preferred embodiment of the present invention teaches an assembly including a phase separation membrane and housing configured to facilitate the removal of entrained liquid from a sample gas stream. Accuracy of the sample is enhanced, and compositional changes are avoided by first extracting a sample from the process gas followed by removal of entrained liquid it may contain, with the entrained liquid removal being conducted at the prevailing process gas pressure and temperature.

Abstract: Rapid characterization and screening of polymer samples to determine average molecular weight, molecular weight distribution and other properties is disclosed. Rapid flow characterization systems and methods, including liquid chromatography and flow-injection analysis systems and methods are preferably employed. High throughput, automated sampling systems and methods, high-temperature characterization systems and methods, and rapid, indirect calibration compositions and methods are also disclosed. The described methods, systems, and devices have primary applications in combinatorial polymer research and in industrial process control.

Abstract: An explosive detection system includes an X-ray inspection apparatus, a mover for moving an object to be inspected to the X-ray inspection apparatus, a sample introduction probe for sampling a gas sample from the object to be inspected, a pipe for introducing the sampled gas into a corona discharge region and for subjecting the sampled gas to negative corona discharge to ionize the sampled gas and to generate negative ions. A mass spectrometer is provided to analyze the mass of the negative ions of the sampled gas and to provide results thereof. Inspection by the X-ray inspection apparatus is performed in relation to sampling of the gas sample, and explosive detection system inspects whether or not an explosive is present in the object to be inspected, from the analysis results of the sampled gas.

Abstract: A system for the retrieval and initial conditioning of sample gas for “on line” analyzers or filling of gas sample cylinders. The preferred embodiment of the present invention contemplates a system configured to obtain a representative gas phase sample from a process gas containing entrained liquid, or a process gas which generally is highly susceptible to partial condensation of some gas phase components. The preferred embodiment of the present invention teaches an assembly including a phase separation membrane and housing configured to facilitate the removal of entrained liquid from a sample gas stream. Accuracy of the sample is enhanced, and compositional changes are avoided by first extracting a sample from the process gas followed by removal of entrained liquid it may contain, with the entrained liquid removal being conducted at the prevailing process gas pressure and temperature.

Abstract: A gas sample extraction apparatus to recover sample gases from fluids such as the return flow drilling mud of an oil and gas well has a sample canister forming a sample chamber with a fluid inlet port and a fluid outlet port. The gas sample extraction apparatus is disposed in a flow of fluid to be sampled, and the fluid sample flows through the sample chamber via the fluid inlet and outlet ports. A bubbler enclosure is in fixed relationship to the sample canister and has an exit bubbler port at the desired fluid level of the sample chamber. Compressed air is supplied to the gas sample extraction apparatus to maintain the fluid sample level within the sample canister at the desired fluid level.

Abstract: An apparatus for collecting particles or vapor from air or surfaces comprising: a housing comprising an inlet open to the air to be sampled and an outlet; and a fan having one or more open areas within the housing capable of being driven at a speed effective to cause collection on the surface of the fan of particles or vapor in the air. A method of collecting a particulate sample from air comprising the step of driving a fan having one or more open areas within a housing comprising an inlet open to the air to be sampled and an outlet, at a speed effective to cause collection on the surface of the fan of particles in the air.

Abstract: A sampling system for providing a sample plug 70 from a fluid sample, comprising: a flow channel through which a flow of a fluid sample is passed; plasma generators 12 and 14; and a control unit configured to drive the plasma generator 12 at a power level at which the fluid sample is modified by the plasma P1 and interrupt busy the plasma P1 for a period of time such as to allow a plug of the fluid sample to pass downstream thereof. The volume of the plug 70 is determined by the time period during which the plasma P1 is interrupted. With the plasma P1 being maintained, the components of the plug 70 separate on transit through a separation channel 10. These components pass through the second plasma P2, and the emissions generated are detected by an optical detector 16.

Abstract: A passive air sampler is designed to facilitate emptying granular or particulate adsorbent from it directly into a thermal desorption tube or other vessel for use in an analytical instrument. The preferred form has an adsorbent container in a conical or funnel-like shape.

Abstract: An inlet system is used in conjunction with a standard gas chromatograph/mass spectrometer to facilitate the analysis of volatile components of substances fired from inkjet pens. The system allows for the investigation of changes in the ink resulting from resistor firing. In addition, the system can be used as a diagnostic tool to detect failures in individual firing chamber. After a block is cooled with liquid nitrogen, an analyte sample of ink is deposited on a stage in a chamber in the block and the chamber is then sealed. The stage is then heated vaporizing a portion of the analyte sample. A transfer gas passes over the stage and mixes with vaporized analyte. The mixture then enters a gas chromatography mass spectrometer which determines the analyte sample's components and relative amounts thereof.

Abstract: An apparatus for, and a method of, sampling and analyzing thermally-labile chemical species, comprises a quartz tube having a filter member positioned in the bore of the tube. The filter member comprises a plug of quartz beads having a layer of quartz frits on either side. A fluid (gas or liquid) carrying one or more chemical substances associated with particulate matter is passed through the tube, the particulate material being collected by the quartz beads. After sample collection, the material remaining/retained from the original sample is removed, as for example by thermal desorption, and the material is then analyzed.

Abstract: Fluid sampling device comprising a sampling cell (1) provided with a thermal control valve having a plug (21) made from a solid low-melting temperature material that is made permeable to the fluid by temporary heating. The device comprises an intermediate cell (6) with a central channel (7) provided with a plug made from the solid material, which communicates an inlet with a first end and an outlet with the opposite end, and suited to tightly fit into the inlet hole of the sampling cell, a device (12, 13) for connecting the two cells (1, 6) to each other and an element (14) associated with a seal (20) for connecting, at the inlet of intermediate cell (6), a linking tube (15) to a reactor (17) producing the fluid to be sampled.

Abstract: A gas sample extraction apparatus to recover sample gases from fluids such as the return flow drilling mud of an oil and gas well has a sample canister forming a sample chamber with a fluid inlet port and a fluid outlet port. The gas sample extraction apparatus is disposed in a flow of fluid to be sampled, and the fluid sample flows through the sample chamber via the fluid inlet and outlet ports. A bubbler enclosure is in fixed relationship to the sample canister and has an exit bubbler port at the desired fluid level of the sample chamber. Compressed air is supplied to the gas sample extraction apparatus to maintain the fluid sample level within the sample canister at the desired fluid level.

Abstract: An apparatus and method for preconcentrating particles and vapors. The preconcentrator apparatus permits detection of highly diluted amounts of particles in a main gas stream, such as a stream of ambient air. A main gas stream having airborne particles entrained therein is passed through a pervious screen. The particles accumulate upon the screen, as the screen acts as a sort of selective particle filter. The flow of the main gas stream is then interrupted by diaphragm shutter valves, whereupon a cross-flow of carrier gas stream is blown parallel past the faces of the screen to dislodge the accumulated particles and carry them to a particle or vapor detector, such as an ion mobility spectrometer. The screen may be heated, such as by passing an electrical current there through, to promote desorption of particles therefrom during the flow of the carrier gas. Various types of screens are disclosed.