Abstract: A device for collecting particles and microorganisms present in ambient air, the device comprising means for sucking air into a small volume enclosure in which the particles and microorganisms are separated from the sucked-in air by centrifuging, the device being portable, self-contained, and capable of being handled in one hand only, e.g. by means of a handle associated with the air suction means.

Abstract: An apparatus for concentrating a vaporous substance, which comprises: a sorbent material capable of capturing a vaporous substance; a first housing in which the sorbent material is located, a heating element proximate the exterior of the housing; a second housing defining a chamber within which the first housing resides, the first housing being located in said chamber such that there is a space permitting gas flow between the outside of the first housing and the inside of the second housing; and a pump capable of causing an exhaust gas to flow through the space in contact with the outside of the first housing; and methods for making and utilizing such apparatus.

Abstract: An apparatus and method are disclosed for pre-concentrating gaseous vapors for analysis. The invention finds application in conjunction with, e.g., analytical instruments where low detection limits for gaseous vapors are desirable. Vapors sorbed and concentrated within the bed of the apparatus can be thermally desorbed achieving at least partial separation of vapor mixtures. The apparatus is suitable, e.g., for preconcentration and sample injection, and provides greater resolution of peaks for vapors within vapor mixtures, yielding detection levels that are 10-10,000 times better than for direct sampling and analysis systems. Features are particularly useful for continuous unattended monitoring applications.

Abstract: The present invention is an electrostatic collector for low cost, high throughput, high efficiency sampling and concentration of bioaerosols. The device is small enough to be portable and can be contained within or placed on the wall of a typical office or hospital building. The collector comprises one or more collector modules, each having an ionizing electrode, a conical outer electrode, a wet collection electrode, and a liquid collection system. Airflow through a collector module may be partially blocked to enhance the collection of smaller particles and the collection electrode may comprise multiple, programmable electrodes to focus particle deposition onto a smaller area. Particles are collected into a small volume of liquid to facilitate subsequent analysis by an attached analyzer or at a remote site.

Abstract: Volatile suspended particles are eliminated from an aerosol by heating the aerosol to a temperature at which the volatile suspended particles evaporate and diluting the aerosol with a dilution gas. The sequence heating and diluting may be performed in any order. According to another aspect of the invention, dilution of the raw gas takes place such that raw gas is led to a measurement gas channel through which measurement gas flows, wherein the quantity of raw gas transferred per unit of time is dependent on the volume flow in the raw gas channel. According to a further aspect of the invention, in a condensation nucleus counter the number and intensity of scattered light pulses is evaluated in order to be able to draw conclusions on the reliability of the measurement.

Abstract: A cytocentrifuge sample chamber includes a sample receiving well to receive and hold a sample to be centrifuged and a sedimentation chamber adjacent a microscope slide upon which cells and/or other sediment material in the sample is to be deposited. A passage, such as a spillway, connects the sample receiving well and the sedimentation chamber, so that sample flows from the sample well under the influence of centrifugal force as centifugation begins into the sedimentation chamber where the sample is forced by centrifugal force against the microscope slide leaving a vacant space at the inner end of the sedimentation chamber. Sedimentation of the sample takes place against the microscope slide. When centrifugation ends, the liquid components of the sample flow back into the vacant space in the sedimentation chamber and can be removed from the vacant space at the inner end of the sedimentation chamber through a removal chamber.

Abstract: The present invention relates to an apparatus for characterizing particles suspended in a liquid, especially a self-contained disposable cartridge for single-use analysis, such as for single-use analysis of a small quantity of whole blood. Furthermore, the present invention relates to a method for characterizing particles in liquid and a device for sampling a small and accurate volume of liquid. The apparatus comprises a housing having a mixing chamber and a collection chamber separated by a wall containing an opening, a first bore in the outer surface of the housing for entrance of a liquid sample, a first cavity for receiving and holding a first liquid sample, and a second cavity for receiving and holding a second liquid sample.

Abstract: A non-contact, extractive sampling system and method is provided for measuring the exhaust gas composition and fine particle composition of exhaust emissions of various types of vehicles under actual operating conditions. A portion (or sample) of an exhaust plume of a vehicle is pulled or extracted through an extraction sampling tube, via a vacuum pump, to a remote trace gas detection system where the concentration of one or more constituents present in the sample of exhaust plume may be measured. In this regard, the invention enables vehicle emissions measurements to be made at a location remote from roadway, rather than using known, “cross-path” remote emissions sensing systems.

Abstract: An apparatus for airborne particle sorting is provided comprising a charging system adapted for applying an electrostatic charge to the particles, such that particles of at least a first group are deflected to a greater extent than particles of a second group are deflected. A focusing system is adapted for electrostatically focusing substantially at least the particles of the first group into a focused stream that is narrower than the input air stream. A deposition system is adapted for substantially depositing the particles of the first group from the focused stream upon a target surface, where the target surface may be transported to an analysis system capable of analyzing the particles deposited thereon.

Abstract: The present disclosure relates to methods and devices that may be used to separate components from one or more samples.

Abstract: A detector system that can analyze multiple samples with a single detector. The detector may contain a portal with a first opening and a second opening. A first sample is obtained from the first opening and a second sample is obtained from the second opening. The openings are coupled to a single detector that can analyze both samples.

Abstract: Systems and methods are provided through which in some embodiments for controlling intermolecular forces between a contact surface and a fabricated microstructure having a base and at least one or more nano-structures. The contact surface and the fabricated microstructure are joined by the interplay of electrostatic and van der Waals forces. The contact surface can be planetary dust with surfaces involved in planetary exploration, as well as synthetic gecko hairs that would allow small robots to climb walls and traverse ceilings. The system and method allow intense electrostatic forces to be applied at variable levels in order to modulate the effectiveness of van der Waals forces as well as external electrostatic forces. This device enables advanced small robot mobility, planetary dust control at all possible ambient pressures, as well as dust sample collection for exploration analysis.

Abstract: A liquid sampler which provides a receptacle and a releasably sealable receptacle cover having at least two apertures each of which can be configured to adjust the flow rate of an amount of liquid into the liquid sampler upon submersion into a liquid.

Abstract: A dilution device includes an inlet port and an outlet port. The dilution device also includes a first porous conduit defining an internal flow passage. The first porous conduit has a plurality of pores that communicate between an outside region external of the first porous conduit and the internal flow passage. The dilution device also includes a second porous conduit disposed around the first porous conduit. The second porous conduit defines a first chamber peripherally about the first porous conduit. The second porous conduit has a plurality of pores that communicate between an outside region external of the second pours conduit and the first chamber. The dilution device further includes a housing disposed around the second porous conduit. The housing defines a second chamber peripherally about the second porous conduit. The housing has an inlet port in communication with the second chamber.

Abstract: The object of the present invention is to provide a particle counter which can accurately count the number of particles contained in fluid where the number concentration of particles is high. The particle counter includes a particle removing portion for removing particles contained in fluid at a predetermined rate, a sensor portion for counting the particles passing through the particle removing portion, and a particle number correcting means comprising a characteristic data memory and a digital signal processor for performing correction processing to the number of the particles counted in the sensor portion by using removal characteristics of the particle removing portion with respect to the particle diameter.

Abstract: A vessel with retention features for the retention of pellets for use in laboratory processes, manufacturing, and producing packaged foods, chemicals, and medicines.

Abstract: A container system for a liquid has an open-topped receptacle for receiving a liquid and a cover. The cover has an interior surface fitting on or within the open top of the receptacle and an exterior surface that it exposed when the cover is fitted to the open top of the receptacle. The cover also has an aspirating nipple formed therein. The aspirating nipple has a tube with an internal channel extending from the exterior of the cover into the receptacle for transferring liquid out of the receptacle and a gasket disposed on the exterior surface of the cover and surrounding the channel.

Abstract: Vials used for obtaining an aliquot of a biological sample are provided. Also provided are method of using the vials and instruments to obtain an aliquot of a biological sample.

Abstract: The present disclosure concerns embodiments of a sampling apparatus that utilizes one or more cyclone separators to collect airborne particles from the atmosphere. In one representative embodiment, the sampling apparatus includes a collection-vessel retaining member that is adapted to be removably coupled to a collection vessel. The retaining member has an air-inlet conduit for permitting air to flow through the open end of the collection vessel and an air-outlet conduit for permitting air to exit the open end of the collection vessel. The airinlet conduit and the air-outlet conduit are configured to cause air flowing into the collection vessel to establishes a cyclonic flow path, which causes airborne particles to separate out from the air stream and collect in the collection vessel.

Abstract: A biological sample processing apparatus and method of use thereof. The biological sample processing apparatus includes a rod-shaped magnet having a north pole, a south pole, a length and a width, and a plunger covering the magnet. The north pole and the south pole of the rod-shaped magnet are substantially orthogonal to the length of the rod-shaped magnet. The apparatus separates magnetic particles from a solution containing, for example, a biological sample.

Abstract: A method and apparatus enables testing of sifting segregation of a particulate solid mixture in a storage bin or hopper. The apparatus makes use of a convergently and divergently angled hopper for collecting the mixture. The apparatus further makes use of a minimally-shearing feeder mechanism supplying a desired flow of mixture, with minimal to no sifting segregation, to the angled hopper. A collection mechanism removes samples of the mixture from the angled hopper for analysis with minimal disruption of the particles of the mixture relative to each other. Thus, samples resulting from the testing apparatus, and corresponding method, are highly representative of mixture conditions within a larger storage hopper.

Abstract: A system for sampling emission products from an emissions source, for example combustion engines including gasoline, diesel and natural gas engines, for subsequent measurement and analysis of the emission products. The system includes a dilution apparatus, a residence time chamber, a plurality of sampling probes within the residence time chamber, and a plurality of sampling trains connected to the sampling probes to take simultaneous representative emission samples for subsequent analysis. The system has particular use in quantifying chemical and toxic trace species from emissions sources. The results of the analysis can be used to formulate decisions on changes in engine design strategy, and can be used to determine the effectiveness of aftertreatment systems on the emissions source.

Abstract: The present invention provides a device for continuous real-time monitoring of ambient air. The device includes a receptacle, a liquid supply, and a pressure balancing system. The receptacle includes a gas inlet slit located such that the gas inlet slit is covered by liquid within the receptacle during use. The pressure balancing portion of the present device includes communication between a point within the receptacle above the liquid level in the receptacle, as well as a liquid inlet portion at the lowermost end of the receptacle, and an air space above a liquid supply portion and the liquid supply portion itself, respectively.

Abstract: A system and method for using a spray/liquid particle count (LPC) to measure particulate contamination is disclosed. Initially, a component for particulate extraction is received. A sprayer is provided for spraying a liquid on the component. In addition, a container is provided for catching the liquid spraying on the component. The container is clean prior to receiving the liquid and the liquid is collected for later analysis of a number of particles extracted from the component.

Abstract: The invention is directed to a system and method for detecting substances, such as high boiling and low vapor pressure materials, using high energy radiation imparted by a suitable radiation source, such as a strobe or laser over a short time period. The radiation source causes the materials to vaporize. A system handling system is used in conjunction with a detector to detect the presence of the materials including explosives, explosive-related compounds, chemical warfare agents, drugs, toxic industrial compounds, and derivatives thereof.

Abstract: A method and apparatus for sampling potential biohazard particles in an air flow tests for biological particles in the air flow; collects a sample of particulate matter from a specific portion of the air flow in response to an indication in the step of sensing of the presence of biological particles in the specific portion of the air flow, and delays particle movement between the steps of sensing and collecting to coordinate the steps of sensing and collecting to the specific portion of the air flow.

Abstract: The present application relates to a surface-coated SPME with an extracting tip that resists breaking during analysis. Rather than utilizing a hollow fiber tip, a resilient surface coated rod is utilized. Specifically, several grooves are machined into the tip of the SPME device, allowing an adsorbent material to be retained thereon. The resulting surface coated SPME device is more rugged in laboratory use and allows for testing of analytes in chemical environments that result in failures when using fiber tipped SPME devices.

Abstract: In various embodiments, the present disclosure provides an automated seed sampler system that includes a milling station for removing at least a portion of seed coat material from a seed and a sampling station for extracting a sample of seed material from the seed where the seed coat has been removed. A seed transport subsystem conveys the seed between the milling station and the sampling station and a seed deposit subsystem conveys the seed from the seed transport subsystem to a selected well in a seed tray after the seed has been sampled.

Abstract: A circumferential slot virtual impactor includes a disk-shaped housing with an endless circumferential slot for receiving aerosols. The slot forms an acceleration nozzle, and a receiver nozzle spaced apart radially inwardly from the acceleration nozzle exit. In an annular gap between the two nozzles, negative pressure is selectively applied to draw a major flow of the aerosol axially away from the nozzles, while a minor flow of the aerosol is drawn radially inward and enters the receiver nozzle. A portion of the larger particles leaves the major flow and merges with the minor flow due to particle momentum, thus increasing the large-particle concentration of the minor flow. The acceleration nozzle incorporates convex curvature along its opposed interior surfaces, for a smoother aerosol flow and reduced large-particle deposition.

Abstract: Sample preparation device and method particularly useful for large volume capture and small volume elution. The device comprising a manifold, a sample holder or reservoir, and a filter unit containing chromatography media such that a filtration path is established between the sample holder, the filter unit and the manifold. Upon subjecting the sample in the sample holder to a driving force such as vacuum, the sample flows through the chromatography media in the filter unit. Molecules of interest bind to the media and any unwanted molecules can be washed under vacuum mode. Elution can then be carried out by removing the filter unit and subjecting the media to a driving force such as vacuum or centrifugation. In another embodiment, molecules of interest can be eluted into a low volume centrifugal spinner directly in the manifold.

Abstract: A method for determining the characteristic properties of soot particles originating from combustion processes utilizes the determination of the blackening of a filter paper. In order to allow for achieving a quick and relatively accurate determination of the particle sizes, possibly of further characteristics as well, a method of this kind provides that the pressure conditions on the filter paper are established as well. It is advantageous for this purpose to determine the differential pressure on the filter and/or filter paper caused by the deposition of the particles.

Abstract: A method for characterizing contaminants within sediment comprising positioning a sampler in a continuous manner within the sediment, exposing the sampler to the sediment for a dwell time, retrieving the sampler, and analyzing the sampler. The sampler is exposed to the sediment for a sufficient period of time to allow at least one analyte of interest to permeate the sampler. The sampler may be analyzed using fluorescence and/or gas chromatography/mass spectrometry to determine contamination versus sampler length. The contamination versus sampler length may be converted to contamination versus depth or contamination versus horizontal position.

Abstract: The present invention includes a system and method for detecting contaminated objects, for example mail pieces, through use of a pinching device that compresses the objects, thereby possibly releasing potential contaminant-containing particles into the air in a closed chamber. Whatever particles are in the closed chamber mix with the air in the closed chamber and form cavity air, which is captured by a detection and alert mechanism.

Abstract: A fluid sampling device is provided comprising an elongated housing having a longitudinal axis, a plurality of alternating sorbent units and spacer units disposed longitudinally through the housing and slidably movable therethrough along the longitudinal direction, and means for individually and sequentially exposing the sorbent units to a fluid. The adsorbed components can then be desorbed and analyzed to provide composition data of target compounds in a fluid, e.g., a gas, over a period of time.

Abstract: The present invention is embodied in a system for collecting biological samples from air including a collection assembly to store at least one biological sample and a separator to remove selected particles from the air prior to entry into the collection assembly. In one embodiment, the selected particles are magnetic and the separator includes at least one magnet to attract the particles from the air.

Abstract: An apparatus for collecting particles or vapor from air or surfaces comprising: a housing comprising an inlet open to the air to be sampled and an outlet; and a fan having one or more open areas within the housing capable of being driven at a speed effective to cause collection on the surface of the fan of particles or vapor in the air. A method of collecting a particulate sample from air comprising the step of driving a fan having one or more open areas within a housing comprising an inlet open to the air to be sampled and an outlet, at a speed effective to cause collection on the surface of the fan of particles in the air.

Abstract: Sample collection assemblies and methods that use a collection wand having a working end and an operating end, a collection tube having a barrel portion, an assay chamber, and a partition member, with the working end of the collection wand having a scoop configured for collecting a predetermined sample volume, and with the partition member having an orifice with a boundary complementary to a cross-section of the scoop, whereby an excess of sample material can be excluded from entering the assay chamber.

Abstract: Disclosed is a compact, non-contacting device for collecting samples, and particularly minute quantities of bio-agents or particulates, from a surface. The device vibrates a region of a target surface containing the sample and collects the sample on an electrically charged pin array. The sample can be later released to a detector or other instrumentation for subsequent analysis.

Abstract: A lightweight, economical, mass-producible, reusable airfoil can be deployed in an airspace while in or attached to any moving vehicle for the purpose of collecting air samples. A frame has an airfoil shape that provides pressure differentials that preferentially direct particulates and contaminants of differing size and mass to different areas of an absorbent media attached or integral to the frame. The absorbent media are readily detachable from the frame for sanitary and efficient transfer to facilities where the samples can be analyzed.

Abstract: An apparatus (10) and a method for concentrating and transferring volatile compounds contained in a sample on a detachable solid support (12) into a liquid for subsequent detection and/or analysis of the volatile compounds, are described. The apparatus comprises a holder (14) for the solid support (12), means (16) for transporting the holder (14) to a heating position on a heatable plate (18), an enclosed space-creating arrangement comprising the heatable plate (18) attached to a movable housing (30), the holder (14), the solid support (12), a funnel (20) on the solid support (12), and inside the funnel (20) a chilled member (22), means inside the housing (30) for heating the heatable plate (18) to evaporate the volatile compounds which then are condensed on the chilled member (22), means (24) for transporting the chilled member (22) from a cooler (26) to the inside of the funnel (20) and from there to a position (28) where condensed compounds are removed from the chilled member (22) into a liquid.

Abstract: A liquid measuring device is described for carrying out the assay using a gas or vapor permeable but liquid impermeable membrane barrier to control the volume of liquid to be measured or transferred. The membrane may be used in any instance where a fixed volume of liquid needs to be measured.

Abstract: The invention relates to a method of sampling a fluid phase in a multiphase fluid mixture flowing in a pipe (7) under given pressure conditions (P), said method comprising the following steps; admitting the multiphase fluid mixture into a phase separator (9); separating the multiphase fluid mixture so as to isolate the fluid phase for sampling; pressurizing a sampling device (10) to the given pressure in the pipe (7); and recovering a sample of said fluid phase in said sampling device. According to the invention, the method further comprises a step of increasing the pressure in the phase separator (9) in successive stage until said pressure in the separator reaches the give pressure (P) in the pipe (7).

Abstract: An automated method for suppressing fugitive dust dissemination is disclosed. The method provides for automated measurement of dust levels at remote locations, transmission of the measurements to a centralized monitoring and control system which sends a signal to remote dust suppression treatment application apparatus which apply the appropriate dust suppression treatment chemicals.

Abstract: A vapor trap for detecting VOCs includes a housing, having a first end portion, a second end portion and at least one opening for receiving gas vapor. The housing is at least partially buried in ground with a vapor containment mechanism detachably connected to the first end portion of the housing. The vapor containment mechanism can be removed and replaced with a vapor sampling mechanism. An organic vapor analyzer can be connected in fluid relationship to the vapor sampling mechanism to measure VOCs. Optionally, a vacuum pump can be utilized to draw vapor into the vapor trap and then subsequently into the organic vapor analyzer. There can be a first selector valve located between the vapor sampling mechanism and the vacuum pump and a second selector valve located between the vapor sampling mechanism and the organic vapor analyzer. A preferred organic vapor analyzer is a photo-ionization detector.

Abstract: A method of sampling reservoir fluid includes establishing communication between a reservoir and an entry port of a flow line disposed in a borehole penetrating the reservoir. The method includes separating fluid received in the entry port into individual fluid components and sequentially flowing slugs of each individual fluid component along the flow line, observing the slugs as they move along the flow line in order to determine the composition of the slugs, estimating when a desired slug containing a desired fluid component would be in the vicinity of a sample chamber in the flow line, and opening the sample chamber to capture the desired slug when the desired slug is in the vicinity of the sample chamber. The method also includes checking that the sample chambers open and close successfully. Finally, the method further includes creating an accurate record of events, which can then be used to audit the sampling process.

Abstract: The invention comprises a vessel for solid phase micro-extraction chemical sampling. The vessel includes a container having an open end and a cap used to close the open end. The cap has a holder to hold a solid phase coated fiber within an interior of the container. There also is an inlet at a first location of the vessel and an outlet at a second location of the vessel. The inlet and the outlet are adapted to fill the vessel with a material to be exposed to the solid phase coated fiber. The vessel also includes a diffuser plate attached to the container. The plate is adapted to reduce fluid forces exerted on the solid phase coated fiber as material flows from the inlet to the outlet. The purpose of the diffuser plate is both to assure that forces are reduced and to provide laminar flow to assure rapid and complete exchange of the fluid in the vessel.

Abstract: A method and device for determining the concentration of analytes in a sample. The device has a surface with an extraction coating thereon. The method is carried out while the sample is highly agitated to maintain a substantially constant boundary layer. The sample is brought into contact with the coating for a limited time so that all the analytes that pass through the boundary layer are adsorbed by the coating. The amount of analytes in the coating is determined and the concentration of those same analytes in the sample is then calculated from the diffusion coefficient of the analytes. The device is first calibrated using analytes of known concentration.

Abstract: A tank contains both Zeolite and a hydrate in a gas chamber formed beneath a piston in the sample tank. Out of safety considerations, we avoid using source cylinders of nitrogen whose pressures exceed 4000 psi. Thus, the gas chamber of the sample tank is initially pressurized by the source cylinder to no more than 4000 psi of nitrogen at room temperature at the surface. Nitrogen gas is sorbed onto the zeolite at room temperature. As the tank is heated by being lowered downhole, nitrogen desorbs from the zeolite and the gas pressure increases. However, once this tank reaches a temperature high enough to release the hydrate's water of hydration, the released water is preferentially sorbed by zeolite, displacing sorbed nitrogen, and causing the pressure in the gas volume to increase even further. Because well temperatures are not high enough to desorb water from zeolite, any water sorbed onto a Zeolite sorption site will permanently block released nitrogen from resorbing at that site.

Abstract: The invention is directed to a system and method for detecting substances, such as high boiling and low vapor pressure materials, using high energy radiation imparted by a suitable radiation source, such as a strobe or laser over a short time period. The radiation source causes the materials to vaporize. A system handling system is used in conjunction with a detector to detect the presence of the materials including explosives, explosive-related compounds, chemical warfare agents, drugs, toxic industrial compounds, and derivatives thereof.

Abstract: In one embodiment, the present method includes the steps of introducing a volume of a sample into a vapor delivery line and volatilizing at least a portion of the volume as it is carried through the vapor delivery line. At least a portion of the volatilized volume contacts a sensor element, which produces a signal that is monitored to reveal information about the sample. All components upstream of the sensor element are substantially free of sorbent materials so that the sample volume does not contact a substantially sorbent material before contacting the sensor element.