Patents Assigned to Entegris, Inc.
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Patent number: 11764037Abstract: Disclosed herein are surface coatings for plasma components that have the benefit of being robust against chemical and plasma physical attack in aggressive (e.g., fluorine-based) plasma environments. The coatings also provide low plasma surface recombination rates for active oxygen, nitrogen, fluorine, and hydrogen species when compared with other known surface treatments. The coatings can be applied to any plasma system component not requiring etching or plasma cleaning including but not limited to materials like quartz, aluminum, or anodized aluminum. Additionally, the efficiency of the system is increased by applying a non-reactive coating to system components thereby increasing the flow of excited plasma species to the plasma chamber of the system.Type: GrantFiled: November 21, 2014Date of Patent: September 19, 2023Assignee: ENTEGRIS, INC.Inventor: Carlo Waldfried
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Patent number: 11761081Abstract: Described are vapor deposition methods for depositing metal films or layers onto a substrate, wherein the metal is molybdenum or tungsten; the methods involve organometallic precursor compounds that contain the metal and one or more carbon-containing ligands, and include depositing a metal layer formed from the metal of the precursor, onto a substrate, followed by introducing oxidizer to the formed metal layer.Type: GrantFiled: September 20, 2019Date of Patent: September 19, 2023Assignee: ENTEGRIS, INC.Inventors: Robert Wright, Jr., Thomas H. Baum, Bryan C. Hendrix, Shawn D. Nguyen, Han Wang, Philip S. H. Chen
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Patent number: 11761086Abstract: Cobalt precursors are described, having application for vapor deposition of cobalt on substrates, such as in atomic layer deposition (ALD) and chemical vapor deposition (CVD) processes for forming interconnects, capping structures, and bulk cobalt conductors, in the manufacture of integrated circuitry and thin film products.Type: GrantFiled: February 19, 2015Date of Patent: September 19, 2023Assignee: ENTEGRIS, INC.Inventors: Thomas H. Baum, Scott L. Battle, John M. Cleary, David W. Peters, Philip S.H. Chen
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Patent number: 11752471Abstract: Described are porous sintered bodies and methods of making porous sintered bodies by steps that include an injection molding step.Type: GrantFiled: July 9, 2020Date of Patent: September 12, 2023Assignee: ENTEGRIS, INC.Inventors: Virendra Warke, Devon N. Dion, David Smith, Christopher Reddy, Meghan Patrick
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Patent number: 11746413Abstract: A chemical delivery system includes a bulk container, a run/refill chamber, a first conduit and a second conduit. The bulk container stores a precursor. The run/refill chamber includes a plurality of spaced tubes having a plurality of surfaces for receiving the precursor in vapor form and storing the precursor in solid form. The first conduit connects the bulk container to the run/refill chamber for transporting the precursor from the bulk container to the run/refill chamber in vapor form. The second conduit connects the run/refill chamber to a deposition chamber for transporting the precursor from the run/refill chamber to the deposition chamber in vapor form.Type: GrantFiled: May 31, 2022Date of Patent: September 5, 2023Assignee: ENTEGRIS, INC.Inventors: David James Eldridge, David Peters, Robert Wright, Jr., Bryan C. Hendrix, Scott L. Battle, John Gregg
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Patent number: 11746912Abstract: Welded check valves include a poppet assembly, a spring, and a disc that contacts the spring. The disc may be held at a position away from a weld when forming the welded check valve. Embodiments may include retention features configured to allow one or more of the poppet assembly and disc to pass the retention features in an assembly orientation, and to retain those elements when they are in an operational orientation. Methods include inserting the poppet assembly, contacting the poppet assembly with a spring, inserting a disc, retaining the disc away from a weld side, and welding the check valve together. The poppet assembly and/or disc may pass one or more retaining features when inserted, and be retained by the retaining features when the check valve is operated. The weld may be a thermal weld.Type: GrantFiled: March 22, 2022Date of Patent: September 5, 2023Assignee: ENTEGRIS, INC.Inventor: John A. Leys
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Patent number: 11742781Abstract: An electrostatic chuck solves the problem of wafer sticking by providing conductive paths on raised embossments that are bridged together and are connected to ground that support the wafer substrate above the surface of the electrostatic chuck. Further, laterally spaced electrode patterns and electrode elements which are spaced laterally and longitudinally away from the raised embossments reduce or eliminate electrical coupling during wafer clamping between conductively coated embossments and the electrode elements, thereby creating a low resistance path for charges remaining on the wafer after declamping to promptly travel to ground. The conductive bridge and electrode pattern configuration also substantially reduces or eliminates any charge build up on the conductive bridge(s) during clamping in order that charge build up in “islands” (worn portions of the insulator layer of the main field area) do not affect the charge dissipation from the wafer substrate through the conductive bridges to ground.Type: GrantFiled: November 13, 2019Date of Patent: August 29, 2023Assignee: ENTEGRIS, INC.Inventors: Yan Liu, Jakub Rybczynski, Steven Donnell, Chun Wang Chan
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Patent number: 11731085Abstract: The present disclosure provides a porous polymeric membrane that is coated with a cross-linked polymerized monomer. The coating on the porous polymeric membrane has a charge when it is immersed in an organic liquid. The coated porous polymeric membrane, a filter utilizing the membrane, and a method for treating an organic liquid used for photoresist with the coated porous polymeric membrane to remove metal contaminants from the organic liquid are disclosed.Type: GrantFiled: November 9, 2021Date of Patent: August 22, 2023Assignee: ENTEGRIS, INC.Inventors: Jad Ali Jaber, Saksatha Ly, James Hamzik, Testu Kohyama
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Patent number: 11713252Abstract: A silicon carbide-graphite composite is described, including (i) interior bulk graphite material and (ii) exterior silicon carbide matrix material, wherein the interior bulk graphite material and exterior silicon carbide matrix material inter-penetrate one another at an interfacial region therebetween, and wherein graphite is present in inclusions in the exterior silicon carbide matrix material. Such material may be formed by contacting a precursor graphite article with silicon monoxide (SiO) gas under chemical reaction conditions that are effective to convert an exterior portion of the precursor graphite article to a silicon carbide matrix material in which graphite is present in inclusions therein, and wherein the silicon carbide matrix material and interior bulk graphite material interpenetrate one another at an interfacial region therebetween.Type: GrantFiled: August 6, 2021Date of Patent: August 1, 2023Assignee: ENTEGRIS, INC.Inventors: Troy Scoggins, Rex Gerald Sheppard, Abuagela H. Rashed, Jonathan Loyd Burr
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Patent number: 11713504Abstract: Described are multi-layer coatings, substrates (i.e., articles) coated with a multi-layer coating, and methods of preparing a multi-layer coating by atomic layer deposition, wherein the coating includes layers alumina and yttria.Type: GrantFiled: June 14, 2022Date of Patent: August 1, 2023Assignee: ENTEGRIS, INC.Inventors: I-Kuan Lin, Carlo Waldfried, Chandrasekaran Venkatraman
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Patent number: 11712653Abstract: Described are methods, devices, and systems useful for adsorbing organometallic vapor onto solid adsorbent material to remove the organometallic vapor from a gas mixture that contains the organometallic vapor and other vapor, particulate materials, or both.Type: GrantFiled: May 20, 2020Date of Patent: August 1, 2023Assignee: ENTEGRIS, INC.Inventors: Charles H. Applegarth, Rocky D. Gipson, Sarah Vogt, Joshua T. Cook, Matthew Browning, Marco Holzner
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Patent number: 11708380Abstract: Provided is a process for the mono-alkylation of cyclopentadiene, utilizing a cyclopentadiene magnesium halide and a metal salt of an alkyl or aryl sulfonate as co-reactant with an alkyl halide alkylating reactant. The process provides facile methodology for the mono-alkylation of cyclopentadiene, with conversions as high as about 96 percent and selectivity for mono-alkylation (over higher level alkylation, such as di- or tri-) as high as about 99%.Type: GrantFiled: October 21, 2021Date of Patent: July 25, 2023Assignee: ENTEGRIS, INC.Inventors: Paul Hinkle, Scott A. Laneman, Victoria Weidner
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Patent number: 11701623Abstract: The present disclosure relates to a composite membrane formed by lamination of two or more separate porous polymeric layers, as well as to a method and system for lamination. Advantageously, the resulting composite is a single layer, being difficult to separate into its component layers, yet effectively maintains the filtering capabilities of the component layers when not laminated.Type: GrantFiled: May 14, 2021Date of Patent: July 18, 2023Assignee: ENTEGRIS, INC.Inventors: Dongzhu Wu, Kwok Shun Cheng, Rajnikant B. Patel, Tony Yu, Puth Proeung, Maybelle Woo
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Patent number: 11697660Abstract: Provided is a facile process for preparing certain organotin compounds having alkyl and alkylamino substituents. The process provides organotin precursor compounds, for example tris(dimethylamido)isopropyl tin, in a highly pure form. As such, the products of the process are particularly useful in the deposition of high-purity tin oxide films in, for example, extreme ultraviolet light (EUV) lithography techniques used in microelectronic device manufacturing.Type: GrantFiled: January 27, 2022Date of Patent: July 11, 2023Assignee: ENTEGRIS, INC.Inventors: David Kuiper, David M. Ermert, Thomas Coyne
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Patent number: 11697767Abstract: Compositions useful for the selective removal of silicon nitride materials relative to polysilicon, silicon oxide materials and/or silicide materials from a microelectronic device having same thereon are provided. The compositions of the invention are particularly useful in the etching of 3D NAND structures.Type: GrantFiled: June 7, 2021Date of Patent: July 11, 2023Assignee: ENTEGRIS, INC.Inventors: Steven Michael Bilodeau, SeongJin Hong, Hsing-Chen Wu, Min-Chieh Yang, Emanuel I. Cooper
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Patent number: 11685752Abstract: Provided is a facile methodology for preparing certain organotin compounds having alkyl and alkylamino or alkyl and alkoxy substituents. The process provides the organotin compounds in a highly pure form which are particularly useful as precursors in the deposition of high-purity tin oxide films in, for example, extreme ultraviolet light (EUV) lithography techniques used in the manufacture of certain microelectronic devices.Type: GrantFiled: January 28, 2022Date of Patent: June 27, 2023Assignee: ENTEGRIS, INC.Inventors: David M. Ermert, Thomas H. Baum, Thomas M. Cameron
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Patent number: 11684898Abstract: Embodiments provide a filter with a generally rectangular, non-cylindrical profile. The filter may have multiple pleat packs positioned between pleat covers that define regions and flow channels in a cavity of the filter body. The pleat covers have openings that allow a fluid to flow through the multiple pleat packs via parallel flows or series flows. End caps bonded to the body define flow passages for directing the fluid from an inlet to an outlet via the pleat packs for series or parallel filtration. The pleat packs may be made of the same or different materials and may be configured with the same or different heights based on flow requirements. A cage or a separator may be positioned between the pleat packs. The pleat packs may be made of a continuous pleated membrane with bridges defining a space between the pleat packs to accommodate the cage or separator.Type: GrantFiled: September 24, 2015Date of Patent: June 27, 2023Assignee: ENTEGRIS, INC.Inventors: Kalyan Madhavaram, Bryan Carl Cochran, John Paul Puglia, J. Karl Niermeyer, Krishna Kamath, Christopher Paul Barck, Yoshikimi Douglas Hisano
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Patent number: 11682540Abstract: A system and method for ion implantation is described, which includes a gas or gas mixture including at least one ionizable gas used to generate ionic species and an arc chamber that includes two or more different arc chamber materials. Using the system ionic species are generated in the arc chamber with liner combination, and one or more desired ionic species display a higher beam current among the ionic species generated, which is facilitated by use of the different materials. In turn improved implantation of the desired ionic species into a substrate can be achieved. Further, the system can minimize formation of metal deposits during system operation, thereby extending source life and promoting improved system performance.Type: GrantFiled: September 3, 2021Date of Patent: June 20, 2023Assignee: ENTEGRIS, INC.Inventors: Ying Tang, Sharad N. Yedave, Joseph R. Despres, Joseph D. Sweeney, Oleg Byl
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Patent number: 11679385Abstract: A media sample holder includes a base and a plurality of retention assemblies including retaining tabs and opposing flexible release lever arms, configured to allow attachment of the base to an attachment adapter. The media sample holder can attach a media sample on or near a filter. The media sample holder held in the media sample holder can have a different removal efficiency curve than a removal efficiency curve of the filter. The media sample can be placed at or near the filter for a period of time, then tested to determine the status and/or life of the filter based on the relationship between the remaining life, exposure, or removal efficiency of the filter and the exposure or removal efficiency of the tested media sample.Type: GrantFiled: December 16, 2020Date of Patent: June 20, 2023Assignee: ENTEGRIS, INC.Inventors: John C. Gaudreau, Evan Warniers, Edward J. Washington
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Patent number: 11661249Abstract: This disclosure relates generally to a containment system for containing a fluid. More specifically, the disclosure relates to a fitment for attaching a liner within a container and providing a fluid path from the liner to an outside of the containment system. The liner and at least a part of the fitment provide the wetted surfaces for the containment system, while the fitment has a portion that can be joined to an outer container that, for example, provides rigidity and light protection. The fitment may be a two-piece fitment with a liner fitment to which the liner may be joined, and a retainer that may be joined to a container, where the liner fitment and the retainer are joined to one another, for example by a mechanical connection. The liner and liner fitment may be fluoropolymers or other non-reactive polymers. The container and retainer may be UV-blocking polymers.Type: GrantFiled: April 22, 2021Date of Patent: May 30, 2023Assignee: ENTEGRIS, INC.Inventors: Gregory W. Bores, Michael J. Schleicher, John A. Leys