Patents Assigned to Rigaku Corporation
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Publication number: 20230160840Abstract: There is provided a technique for non-destructively and relatively easily acquiring orientation information of an anisotropic material even for a large-sized object. An object is irradiated with X-rays in a tangential direction of a curved anisotropic material from a radiation source of a phase-contrast X-ray optical system. A scattering image is then obtained using a detection signal of X-rays having penetrated through the object. Structure information of the anisotropic material is acquired based on the scattering image.Type: ApplicationFiled: November 18, 2022Publication date: May 25, 2023Applicants: RIGAKU CORPORATION, TOYOTA JIDOSHA KABUSHIKI KAISHAInventors: Masashi KAGEYAMA, Kenichi OKAJIMA, Masaru KURIBAYASHI, Yuzo MIURA, Yuichi NAGAMATSU
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Patent number: 11656190Abstract: An X-ray fluorescence spectrometer of the present invention includes: a determination module (21) configured to determine, with respect to every one of measurement lines that correspond to secondary X-rays having intensities to be measured, whether or not a ratio of a theoretical intensity in thin film calculated on the basis of an assumed thickness and known contents of respective components to a theoretical intensity in bulk calculated on the basis of the known contents of the respective components exceeds a predetermined threshold; and a saturation thickness quantification module (23) configured to, according to a positive determination by the determination module (21), calculate a saturation thickness with respect to each of the measurement lines, at which the theoretical intensity saturates, on the basis of the known contents of the respective components and to adopt a largest saturation thickness as a quantitative value of a thickness.Type: GrantFiled: September 10, 2021Date of Patent: May 23, 2023Assignee: Rigaku CorporationInventors: Shinya Hara, Yasujiro Yamada, Hisashi Homma
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Publication number: 20230152248Abstract: A correction amount specifying apparatus comprises circuitry for storing diffraction data including a combination of the diffraction angle of the irradiation X-rays with respect to the sample rotation angle and the sample surface height, the diffraction data being acquired by irradiating X-rays to a standard sample that is an aggregate of isotropic and stress free crystal particles, determining a first correspondence relationship based on the diffraction data, and specifying a correction amount of the sample surface height with respect to a desired sample rotation angle and a desired diffraction angle based on the first correspondence relationship.Type: ApplicationFiled: November 17, 2022Publication date: May 18, 2023Applicant: Rigaku CorporationInventors: Takuya KIKUCHI, Tetsuya OZAWA, Ryuji MATSUO
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Patent number: 11636995Abstract: An X-ray generation device includes: a sealed X-ray tube including a cathode and an anode; a magnetic field generation portion applying a magnetic field to the electron beam, the magnetic field extending in a first direction, which crosses a traveling direction of the electron beam; and a rotary drive system configured to rotate the sealed X-ray tube, the anode having a surface including a first region and a second region arranged on one side and another side, with respect to a straight division line, the first region having a first metal arranged therein, and the second region having a second metal arranged therein, the second metal being different from the first metal, and by means of the rotary drive system rotating the sealed X-ray tube, the sealed X-ray tube being arranged with respect to the magnetic field generation portion so that the straight division line lies along the first direction.Type: GrantFiled: March 26, 2021Date of Patent: April 25, 2023Assignee: RIGAKU CORPORATIONInventors: Masahiro Nonoguchi, Masashi Kageyama
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Publication number: 20230115151Abstract: A control apparatus, system, method and program that enable simultaneous measurement of counts of multiple energy ranges in an efficient configuration are provided. A control apparatus 200 for controlling an X-ray detector 100 and outputting a measurement result comprises a setting section 220 configured to set the energy range of X-rays to be detected for each unit region of the X-ray detector 100, a data management section 250 configured to acquire a count value of the set energy range for each unit region as measurement data by a result of the X-ray measurement, and an outputting section 270 configured to output the measurement data. Thus, counting of multiple energy ranges can simultaneously be measured.Type: ApplicationFiled: December 22, 2020Publication date: April 13, 2023Applicant: Rigaku CorporationInventors: Takuto SAKUMURA, Yasukazu NAKAYE, Tetsuya OZAWA, Kazuyuki MATSUSHITA
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Publication number: 20230097836Abstract: Correcting artifacts by motion according to reconstruction of a CT image includes circuitry configured to acquire a projection image of 360-degree scanning; calculate a motion amount using parameters by setting a motion model including the parameters; calculate a relative motion amount of a projection data from the projection data of the projection image and opposite data thereto; prepare a fixed-point equation including the motion amount and the relative motion amount; determine the parameters in the motion model by self-consistently solving the fixed-point equation; and correct the projection image using the motion amount.Type: ApplicationFiled: September 19, 2022Publication date: March 30, 2023Applicant: Rigaku CorporationInventor: Takumi OTA
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Patent number: 11609192Abstract: Provided is an energy-dispersive X-ray fluorescence spectrometer capable of easily determining reliability of a result of quantitative analysis and quickly recognizing an abnormality in measurement conditions, an X-ray fluorescence spectrometer, a sample, preprocessing for the sample, or the like. The energy-dispersive X-ray fluorescence spectrometer includes: a spectrum acquisition unit configured to acquire a spectrum; a calculation unit configured to execute quantitative analysis for an element included in the sample based on a peak included in the spectrum; and an evaluation unit configured to calculate a plurality of evaluation values obtained using different calculation methods for a series of processes, being the process of acquiring the spectrum by the spectrum acquisition unit, and the process of executing the quantitative analysis by the calculation unit, and to calculate a comprehensive evaluation value obtained by composing the plurality of evaluation values.Type: GrantFiled: November 30, 2020Date of Patent: March 21, 2023Assignee: Rigaku CorporationInventor: Shinya Kikuta
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Patent number: 11598369Abstract: Only an outer spacer (33) is cooled by an outer spacer cooling structure, thereby causing a temperature difference between an inner spacer (32) and the outer spacer (33). According to this temperature difference, an inner ring (37) of a bearing (31) is displaced relatively to an outer ring (38) in a direction in which a preload inside the bearing (31) decreases.Type: GrantFiled: May 6, 2021Date of Patent: March 7, 2023Assignee: RIGAKU CORPORATIONInventors: Yasuyuki Shimazaki, Shinichi Oya
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Patent number: 11594393Abstract: Provided is an X-ray tube, including: an electron-beam emitting unit; a target having a first surface and a second surface; a solid heat diffusion member fixed onto the second surface of the target; and a flow-path forming member, which is arranged on a side of the solid heat diffusion member, the side being opposite to the target, and that is configured to define a film flow path in which a cooling fluid forms a film flow that is parallel to a surface shape of the solid heat diffusion member. A protruding portion protrudes toward the side of the solid heat diffusion member, which is opposite to the target. The film flow path has a shape extending along at least a part of a surface of the protruding portion.Type: GrantFiled: February 8, 2021Date of Patent: February 28, 2023Assignee: RIGAKU CORPORATIONInventor: Masaaki Yamakata
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Patent number: 11585769Abstract: A quantitative analysis method, which is performed by an X-ray fluorescence spectrometer, includes: a step of acquiring a plurality of spectra at least having a first peak at a first energy position from a sample containing a plurality of elements under different measurement conditions; a step of designating, from among the plurality of spectra, a primary spectrum and a secondary spectrum having a second peak at a second energy position; a first fitting step of performing a fitting on the first peak included in the secondary spectrum to calculate a background intensity at the second energy position due to the first peak; and a second fitting step of performing a fitting on the first peak of the primary spectrum and performing a fitting on the second peak of the secondary spectrum under a condition that the calculated background intensity is included at the second energy position.Type: GrantFiled: July 10, 2020Date of Patent: February 21, 2023Assignee: RIGAKU CORPORATIONInventor: Shin Tanaka
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Publication number: 20230044361Abstract: An X-ray fluorescence spectrometer of the present invention includes: a determination module (21) configured to determine, with respect to every one of measurement lines that correspond to secondary X-rays having intensities to be measured, whether or not a ratio of a theoretical intensity in thin film calculated on the basis of an assumed thickness and known contents of respective components to a theoretical intensity in bulk calculated on the basis of the known contents of the respective components exceeds a predetermined threshold; and a saturation thickness quantification module (23) configured to, according to a positive determination by the determination module (21), calculate a saturation thickness with respect to each of the measurement lines, at which the theoretical intensity saturates, on the basis of the known contents of the respective components and to adopt a largest saturation thickness as a quantitative value of a thickness.Type: ApplicationFiled: September 10, 2021Publication date: February 9, 2023Applicant: RIGAKU CORPORATIONInventors: Shinya HARA, Yasujiro YAMADA, Hisashi HOMMA
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Patent number: 11543367Abstract: There is provided an acquiring method of a projection image of a sample whose shape is uneven with respect to a rotation center, the method comprising the steps of setting the sample S0 at a position of the rotation center C0 provided between an X-ray source 116a and a detector 117, and acquiring the projection image of the sample S0 at each different rotation angle for each different magnification ratio over a rotation angle of 180° or more by rotating the sample S0 around the rotation center C0, and by relatively changing a separation distance between the X-ray source and the rotation center, or a separation distance between the rotation center and the detector in an optical axis direction according to the shape of the sample S0 and the rotation angle of the sample S0.Type: GrantFiled: April 10, 2020Date of Patent: January 3, 2023Assignee: RIGAKU CORPORATIONInventor: Yoshihiro Takeda
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Publication number: 20220414955Abstract: The angle error estimating apparatus 310 comprises a storing section 315 for storing a series of projection data of an X-ray CT and control values of projection angles respectively associated with the projection data, a temporary correction section 330 for correcting the control values of the projection angles to temporary correction values with an error model using an assumed parameter, a temporary reconstruction section 332 for reconstructing a plurality of temporarily corrected images using the temporary correction values of the projection angles for each of different projection data sets composed of a part of the series of projection data, a consistency evaluating section 340 for evaluating consistency of the plurality of temporarily corrected images, and a parameter determining section 345 for determining an optimum parameter used for the error model based on the evaluated consistency.Type: ApplicationFiled: June 22, 2022Publication date: December 29, 2022Applicant: Rigaku CorporationInventor: Takumi OTA
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Patent number: 11525790Abstract: A sample holder (10) filled with a sample is held in a base member (20), and an airtight member (30) is mounted on the base member (20) so as to cover the surroundings of the sample holder (10), thereby forming a sample holding structure in a closed space. The airtight member (30) includes a fitting portion (35) which is configured to be fitted and mounted in a mounting portion (21).Type: GrantFiled: August 13, 2020Date of Patent: December 13, 2022Assignee: RIGAKU CORPORATIONInventor: Koichiro Ito
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Publication number: 20220390394Abstract: A quantitative analysis apparatus, a method, a program, and a manufacturing control system are provided. A WPPF section 320 for determining parameters of theoretical diffraction intensity by performing whole powder pattern fitting with respect to an X-ray diffraction profile to be analyzed, a scale factor acquiring section 325 for acquiring a scale factor of a test component among the determined parameters, a calibration curve storing section 350 for storing a calibration curve indicating a correlation between scale factors of the test component acquired with respect to a standard sample and content ratios of the test component in the standard sample, and a conversion section 370 for converting the scale factor of the test component acquired with respect to an objective sample into the content ratio of the test component in the objective sample using the stored calibration curve, are comprised.Type: ApplicationFiled: June 2, 2022Publication date: December 8, 2022Applicant: Rigaku CorporationInventors: Takahiro KUZUMAKI, Tetsuya OZAWA, Miki KASARI, Akihiro HIMEDA, Atsushi OHBUCHI, Takayuki KONYA
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Patent number: 11513086Abstract: A sequential X-ray fluorescence spectrometer according to the present invention includes a total analysis time display unit configured to measure, for each kind of analytical sample, a standard sample which contains a component at a known content as a standard value to determine a measured intensity of each measurement line corresponding to the component. The total analysis time display unit is further configured to calculate, for each component, a counting time which gives a specified analytical precision by using the standard value and the measured intensity and to calculate a total counting time as a sum of the counting times of respective components. The total analysis time display unit is configured to calculate a total analysis time as a sum of the total counting time and a total non-counting time and to output the calculated total analysis time and the calculated counting times of the respective components.Type: GrantFiled: April 29, 2022Date of Patent: November 29, 2022Assignee: Rigaku CorporationInventors: Yoshiyuki Kataoka, Yasuhiko Nagoshi
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Publication number: 20220347679Abstract: A sample holder unit 400 capable of quickly and easily soaking a sample in a crystalline sponge, and of quickly and accurately performing single-crystal X-ray structure analysis, is provided. The sample holder unit comprises a sample holder 214 and an applicator 300. The applicator 300 comprises an opening 302 and a storing space in which the sample holder is stored; a seal part 304 provided on a contact surface with the sample holder stored in the storing space; and a pull-out prevention part 305 that prevents the sample holder from being pulled out from the opening 302, the pull-out prevention part engaged with the sample holder stored in the storing space.Type: ApplicationFiled: November 21, 2019Publication date: November 3, 2022Applicant: Rigaku CorporationInventor: Takashi SATO
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Patent number: 11487043Abstract: An X-ray image generation device includes a moving mechanism that moves an object relative to a grating part in a direction crossing X-rays emitted toward the grating part. The grating part includes N (2?N) regions along the direction of movement by the moving mechanism. A cyclic direction of a grating structure in each of the plurality of gratings belonging to an ith (1?i?N?1) region out of the N regions and a cyclic direction of a grating structure in each of the plurality of gratings belonging to an (i+1)th region out of the N regions are different directions. The plurality of gratings are configured so that moiré interference fringes generated in the N regions have a cyclic intensity fluctuation measurable by the detector and of at least one cycle or more in the direction of movement by the moving mechanism.Type: GrantFiled: June 3, 2021Date of Patent: November 1, 2022Assignee: Rigaku CorporationInventors: Masashi Kageyama, Kenichi Okajima, Kouichi Katou
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Publication number: 20220307994Abstract: A tolerance error estimating apparatus, method, program, reconstruction apparatus and control apparatus capable of estimating a deviation of a drive axis from a reference position with respect to driving time are provided. A tolerance error estimating apparatus (processing apparatus 300) X-ray analysis apparatus comprises a specific position calculating section 320 for obtaining a specific position of a reference sample at each rotation driving time from X-ray detection images and a deviation amount calculating section 330 for calculating the deviation amount ?x in the x direction and ?y in the y direction of the center position of a rotation drive shaft as the rotation drive axis at each rotation driving time from the reference position based on the specific position, when the z direction of the orthogonal coordinate system fixed to the sample is set the direction parallel to the rotation drive axis.Type: ApplicationFiled: March 24, 2022Publication date: September 29, 2022Applicant: Rigaku CorporationInventor: Takumi OTA
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Publication number: 20220278381Abstract: A structure for battery analysis of the present invention includes a pressurizing unit (30) having a pressurizing mechanism, and a pressure receiving unit (10) for receiving pressure acting on a sample battery (S), and pressurizes the sample battery (S) accommodated in a hollow portion of a battery accommodation unit (20) between the pressurizing unit (30) and the pressure receiving unit (10) to suppress expansion and contraction of the sample battery (S).Type: ApplicationFiled: March 30, 2020Publication date: September 1, 2022Applicant: RIGAKU CORPORATIONInventors: Koichiro Ito, Suguru Sasaki