Abstract: The present invention relates to a method for the production of drill holes in difficult to machine materials, in which a removal of material takes place in order to produce a drill hole by electrochemical erosion of material by an electrode that is moved in the longitudinal direction of the drill hole being produced in the direction onto the material to be processed at a feed rate, wherein the drilling has at least two steps, wherein, in the first step, the electrochemical processing takes place, and wherein, in a second step, the further processing of the drill hole to the final diameter takes place by machining processing or by erosion or by an electrochemical processing.

Abstract: Graphene has been used in nanocomposites as constituents/doping in plastics or epoxy providing dramatic enhancement of the mechanical properties but have not progressed past the laboratory level novelty. This invention can provide a graphene based composite structure with a density less that 1.9 g/cm3 for a fiber, yarn, rope or cable and a density less that 1.5 g/cm3 for a sheet both structure have tensile and shear strength greater than either Aluminum or Steel; thus providing a graphene material that is both much lighter and stronger.

Abstract: Methods for electropolishing and coating aluminum on a surface of an air and/or moisture sensitive substrate, including: in a vessel, submerging the substrate in a first molten salt bath and applying an anodizing current to the substrate at a first temperature to electropolish the surface of the substrate; wherein the first molten salt bath includes one of a first organic salt bath and first inorganic salt bath; wherein, when used, the first organic salt bath includes one of (a) aluminum halide and ionic liquid, (b) a combination of an aluminum halide and halogenatedmethylphenylsulfone (C6(H5-y,Xy)SO2CX3, where y is a number from 0-5), (c) a combination of an aluminum halide, an ionic liquid, and halogenatedmethylphenylsulfone (C6(H5-y,Xy)SO2CX3), and (d) AlF3-organofluoride-hydrofluoric acid adduct; wherein, when used, the first inorganic salt bath includes aluminum halide and alkali metal halide; and wherein the anodizing current is 10-30 mA/cm2.

Abstract: A method for supplying hydrogen gas for consumption in at least one downstream process, the method comprising: electrolysing water to provide hydrogen gas; compressing the hydrogen gas in a multistage compression system to provide compressed hydrogen gas; and feeding at least a portion of the compressed hydrogen gas to the downstream process(es); wherein the multistage compression system comprises at least one centrifugal compression stage; wherein the hydrogen gas is dosed with nitrogen gas upstream of the centrifugal compression stage(s); and wherein the nitrogen gas is present in the compressed hydrogen gas when fed to the downstream process(es).

Abstract: The disclosure relates to an electrolysis cell for producing hydrogen. The cell comprises an electrolyte compartment and an electrolyte disposed therein. The electrolyte comprises an aqueous alkaline solution comprising a transition metal ion or p block metal ion. The cell further comprises first and second spaced apart electrodes at least partially disposed in the electrolyte.

Abstract: A method for forming an atomically smooth surface on a copper electrode through electropolishing and the atomically smooth surface are provided. An exemplary method for forming an atomically smooth surface by electropolishing includes placing a copper foil in an electrolyte solution including ethylene glycol and phosphoric acid. The copper foil is coupled to a current source. Current is applied to the copper foil to electropolish the copper foil. The electropolishing is stopped when the electropolishing is completed.

Abstract: A reduction electrode of an embodiment includes a metal base material and a plurality of metal nanowires provided on the metal base material. The plurality of metal nanowires include metal nanowires whose average height of contour curve of surface is 20 nm or less for 50% or more in a number ratio. The plurality of metal nanowires are formed by reducing a plurality of metal oxides each having a nanowire shape formed on the metal base material by an electrochemical reduction method. A reduction process of the metal oxides includes a first process of passing a current under a constant current condition where an absolute value is 5 mA/cm2 or more through the plurality of metal oxides, and a second process of passing a current under a constant potential condition through the plurality of metal oxides.

Abstract: An electrochemical plating apparatus for depositing a conductive material on a wafer includes a cell chamber. The plating solution is provided from a bottom of the cell chamber into the cell chamber. A plurality of openings passes through a sidewall of the cell chamber. A flow regulator is arranged with each of the plurality of openings configured to regulate an overflow amount of the plating solution flowing out through the each of the plurality of openings. The electrochemical plating apparatus further comprises a controller to control the flow regulator such that overflow amounts of the plating solution flowing out through the plurality of openings are substantially equal to each other.

Abstract: Provided are electrochemical cells and methods for generating hydrogen gas and oxygen gas.

Abstract: An ion-exchange membrane electrolysis device includes an ion-exchange membrane electrolytic cell and an integrally formed integrated flow channel device. The ion-exchange membrane electrolytic cell generates a gas comprising hydrogen. The integrated flow channel device has a first setting structure, a water tank structure, a gas flow channel system and a water flow channel system. The water tank structure accommodates water. The first setting structure is configured for removably fixing the ion-exchange membrane electrolytic cell to the integrated flow channel device. The water flow channel system connects the water tank structure and the first setting structure for inputting the water in the water tank structure into the ion-exchange membrane electrolytic cell. The gas flow channel system is connected to the first setting structure for receiving and transporting the gas comprising hydrogen.

Abstract: The present invention relates to a method for producing hydrogen in a polymer electrolyte membrane (PEM) water electrolyser cell. A direct electric current is applied to the water electrolyser cell. Water molecules are allowed to diffuse from a cathode compartment through a polymer electrolyte membrane into an anode compartment, to oxidize water molecules at an anode catalyst layer into protons, oxygen and electrons. The protons are allowed to migrate through a polymer electrolyte membrane into the cathode compartment and the protons are reduced at a cathode catalyst layer to produce hydrogen. The cell is supplied with water to the cathode compartment, and humidified air is supplied to the anode compartment. The invention also relates to a polymer electrolyte membrane (PEM) water electrolyser cell, a polymer electrolyte membrane (PEM) water electrolyser stack and a polymer electrolyte membrane (PEM) water electrolyser system.

Abstract: The invention relates to a method for making nanopores in thin layers or monolayers of transition metal dichalcogenides that enables accurate and controllable formation of pore within those thin layer(s) with sub-nanometer precision.

Abstract: Methods are provided for modifying a porous surface of an implantable medical device by subjecting the porous surface to a modified micro-arc oxidation process to improve the ability of the medical device to resist microbial growth, to improve the ability of the medical device to adsorb a bioactive agent or a therapeutic agent, and to improve tissue in-growth and tissue on-growth of the implantable medical device.

Abstract: A novel cell for generating ozonated water including an integrated ozone concentration detector. The cell comprises a nafion membrane separating a diamond coated anode, and a gold surfaced cathode enclosed within a cell housing with the catalyst side of the nafion membrane facing the cathode. The cell housing has a cathode housing portion and an anode housing portion separated by the membrane. The cathode and anode have an array of holes allowing fluid to penetrate to the surface of the niobium membrane. Ozonated water from the anode is channeled to a spectrophotometer integrated within the housing. The spectrophotometer creates a signal representative of the ozone concentration in the ozonated water which is utilized by control circuitry in a closed loop to maintain a stable target concentration. A bubble trap may be integrated within the housing through which the ozonated water passes before entering the spectrophotometer to remove bubbles form the ozonated water.

Abstract: A novel system for generating ozonated water, for example, for sterilization of medical equipment. The system comprises an ozone generating cell including a nafion membrane separating an anode, and a cathode enclosed within a cell housing. The cell housing has a cathode housing portion and an anode housing portion separated by the membrane. The housing also incorporates an integrated spectrophotometer including a bubble trap. The system includes a hydrogen water reservoir for receiving water from the cathode and an ozone water reservoir for receiving generated ozonated water from the anode. Control circuitry controls a set of pumps, and controls ozone generation in a closed loop using the spectrophotometer to provide a selected ozone concentration in the ozonated water from the anode. An output port coupled to the ozone water reservoir allows ozonated water to flow out of the system for external use.

Abstract: The present invention relates to a process for the fabrication of cobalt interconnections and to an electrolyte which enables the implementation thereof. The electrolyte which has a pH below 4.0 comprises cobalt ions, chloride ions and at most two organic additives of low molecular weight. One of these additives may be an alpha-hydroxy carboxylic acid or a compound having a pKa value ranging from 1.8 to 3.5.

Abstract: A system includes a device disposed within a storage tank. The device includes a cyclonic separator and an electrostatic coalescer. The cyclonic separator is configured to receive and separate phases of a multi-phase fluid stream. The cyclonic separator is configured to induce cyclonic flow of the multi-phase fluid stream to separate the multi-phase fluid stream into a gas stream and a liquid stream. The liquid stream includes a first liquid phase and a second liquid phase. The cyclonic separator is configured to discharge at least a portion of the gas stream and at least a portion of the liquid stream. The electrostatic coalescer is downstream of and fluidically connected to the second outlet of the cyclonic separator. The electrostatic coalescer is configured to demulsify the liquid stream by causing coalescence of liquid droplets of one of the first or second liquid phases.

Abstract: Methods for providing laminated coatings on metal articles using electroplating methods such as barrel plating, vibratory plating, rocker plating or other non-rack methods that involve movement of articles to be plated in a containment apparatus, as well as articles made from such processes. Embodiments of such processes involve mass-transfer modulation to provide compositionally modulated coatings.

Abstract: The chamber frame element of the present invention, which has a smaller amount of voltage drop, consumes less reactive power than the prior art, and exhibits no metal corrosion, is a chamber frame element (14) for an electrolyzer or an electrodialysis cell. The chamber frame element (14) includes: a bag body (141); a frame (142) housed in an interior space of the bag body (141); and an inlet (143) and an outlet (144) to which piping can be attached, which are formed on the outer side of a region where the frame is housed in the bag body (141).

Abstract: A method of preparing a modified-metal surface by attaching a phosphorous-based acid to a surface of a metal: preparing a solution of the phosphorous-based acid in a protic solvent; immersing a strip of a metal work piece into the solution of the phosphorous-based acid, immersing a strip of a reference metal into the solution of the phosphorous-based acid, supplying a voltage for a duration of time, removing the metal work piece, cleaning the metal work piece, and drying the cleaned metal work piece under an inert atmosphere to obtain a modified metal work piece.