Patents Examined by Harry I. Moatz
  • Patent number: 3963759
    Abstract: Citraconic anhydride is made by the vanadium-catalyzed gas-phase air oxidation of mesityl oxide at about 200-500.degree.C. and atmospheric pressure with a contact time of less than 1 second. Preferred catalysts are vanadium oxide and vanadate salts. Preferred O.sub.2 /mesityl oxide molar ratios are about 10:1 to 100:1.
    Type: Grant
    Filed: June 7, 1973
    Date of Patent: June 15, 1976
    Assignee: The Dow Chemical Company
    Inventor: Edwin J. Strojny
  • Patent number: 3963743
    Abstract: A strong, clean phthalocyanine pigment is prepared by conditioning the crude pigment with 4-sulfophthalic acid or the anhydride thereof.
    Type: Grant
    Filed: October 1, 1973
    Date of Patent: June 15, 1976
    Assignee: Chemetron Corporation
    Inventor: James Dial Stepp
  • Patent number: 3962284
    Abstract: A series of 3-(5-aryl-2-furyl)-3-hydroxypropionic acids and ethyl esters are useful as antiinflammatory agents.
    Type: Grant
    Filed: August 20, 1975
    Date of Patent: June 8, 1976
    Assignee: Morton-Norwich Products, Inc.
    Inventor: Stanford S. Pelosi, Jr.
  • Patent number: 3960900
    Abstract: Viscous polybutenes of number average molecular weight (M.sub.n) in the range of about 300 to about 3000 have improved reactivity with intramolecular anhydrides of unsaturated aliphatic dicarboxlyic acids when such polybutenes contain rather small amounts, i.e., 5 to 200 ppm, of halogenated, preferably chlorinated and/or brominated aliphatic or aromatic hydrocarbons. Preference is given to such halogen containing compounds having a sufficient vapor pressure at a temperature in the range of 100.degree. to 300.degree.C to be substantially completely removed at absolute pressures in the range of 5 to 760 mm Hg.
    Type: Grant
    Filed: May 10, 1973
    Date of Patent: June 1, 1976
    Assignee: Standard Oil Company
    Inventors: Imre Puskas, John A. Cengel
  • Patent number: 3960891
    Abstract: (3-amino-2-hydroxy propyloxy) thiochromans of the formula ##SPC1##Wherein A is hydrogen or halogen, R.sub.1 is hydrogen or lower alkyl, and R.sub.2 is lower alkyl or cyclo lower alkyl.These compounds possess cardiovascular properties and may be used as blockers of cardiac .beta. adrenergic receptors.
    Type: Grant
    Filed: March 31, 1971
    Date of Patent: June 1, 1976
    Assignee: Science-Union et Cie
    Inventors: Charles Malen, Michel Laubie
  • Patent number: 3960901
    Abstract: High purity citraconic acid is prepared in good yield by the thermolysis, in the presence of a catalyst, of citramalic acid, 3-methylmalic acid, paraconic acid, mesaconic acid and mixtures thereof.
    Type: Grant
    Filed: April 7, 1975
    Date of Patent: June 1, 1976
    Assignee: Pfizer Inc.
    Inventor: Rudolph G. Berg
  • Patent number: 3960858
    Abstract: A new class of 2,3-benzoxazepine compounds of the formula ##SPC1##In the formula, R is heterocyclic acyl or heterocyclic acetyl. The compounds have central nervous system and anti-inflammatory activity.
    Type: Grant
    Filed: November 14, 1974
    Date of Patent: June 1, 1976
    Assignee: Gruppo Lepetit S.p.A.
    Inventors: Giorgio Pifferi, Amedeo Omodei-Sale', Pietro Consonni
  • Patent number: 3960869
    Abstract: A process is provided for the preparation of 2-chloropyridine by the liquid phase hydrogenolysis of 2,6-dichloropyridine in the presence of a selected transition metal catalyst and a strong base.
    Type: Grant
    Filed: March 4, 1974
    Date of Patent: June 1, 1976
    Assignee: Olin Corporation
    Inventor: Roland R. Kyi
  • Patent number: 3959370
    Abstract: Novel compounds, N-acetyl-polychlorobenzamides, are prepared by treating corresponding polychlorobenzonitrile compounds with acetic acid in a closed reactor at an elevated temperature above the boiling point of the acetic acid. These new compounds have been found to be useful biological chemicals, particularly in controlling undesirable vegetation, and also useful as chemical intermediates.
    Type: Grant
    Filed: July 16, 1973
    Date of Patent: May 25, 1976
    Assignee: Jefferson Chemical Company, Inc.
    Inventor: Lewis William Watts, Jr.
  • Patent number: 3959273
    Abstract: The disclosure relates to new 2-aryloxymethylmorpholine derivatives which possess antidepressant properties, and to processes for the manufacture of the said morpholine derivatives, to pharmaceutical compositions containing them, and to a method of preventing or relieving depression in warm-blooded animals including man. Typical of the morpholine derivatives disclosed is 2-(o-ethoxyphenoxymethyl)morpholine.
    Type: Grant
    Filed: September 27, 1974
    Date of Patent: May 25, 1976
    Assignee: Imperial Chemical Industries Limited
    Inventors: Keith Blakeney Mallion, Ralph William Turner, Alexander Henry Todd
  • Patent number: 3957480
    Abstract: Compounds of the formula: ##SPC1##Wherein R.sub.1 and R.sub.2 are the same or different and are hydrogen, alkyl of from 1 to 6 carbon atoms, inclusive, or phenyl; R.sub.3 is hydrogen, alkyl of from 1 to 8 carbon atoms, inclusive, phenyl, or benzyl; R.sub.4 is hydrogen or alkyl of from 1 to 6 carbon atoms, inclusive, and R.sub.3 and R.sub.4 can be joined together to form a heterocyclic ring selected from the group consisting of morpholine, pyrrolidine or piperidine; X is oxygen or sulfur; A and B are the same or different, and are hydrogen, alkyl of from 1 to 6 carbon atoms inclusive, cycloalkyl of from 3 to 7 carbon atoms, inclusive, haloalkyl, and halogen; Z is an alkyl group of from 1 to 6 carbon atoms, inclusive, or a cycloalkyl group of from 3 to 7 carbon atoms provided that when A and B are halogen, Z is located at the 4 or 5 positions.
    Type: Grant
    Filed: December 23, 1974
    Date of Patent: May 18, 1976
    Assignee: The Upjohn Company
    Inventor: Gabriel Kornis
  • Patent number: 3957792
    Abstract: Process for the manufacture of 2-ethyl-pyridine from 2-methyl-pyridine and methanol in the gaseous phase with a catalyst consisting essentially of silicon dioxide and oxides of metals of the second and/or third main group or subgroup and/or the fifth main group of the periodic system of elements at elevated temperatures.
    Type: Grant
    Filed: June 6, 1974
    Date of Patent: May 18, 1976
    Assignee: Hoechst Aktiengesellschaft
    Inventors: Hans-Jurgen Arpe, Hansjorg Hey
  • Patent number: 3958005
    Abstract: Novel tetrahydrofuran derivatives of the formula ##EQU1## wherein R is a branched or linear alkyl of 1 to 10 carbon atoms and R.sub.1 is alkyl of 1 to 5 carbon atoms and X is selected from the group consisting of chlorine, bromine, --OH and alkylcarbonyloxy of 2 to 5 carbon atoms useful as insecticides and their preparation.
    Type: Grant
    Filed: February 3, 1975
    Date of Patent: May 18, 1976
    Assignee: Roussel Uclaf
    Inventors: Daniel Hainaut, Jean-Pierre Demoute, Pierre Girault
  • Patent number: 3956323
    Abstract: Compounds represented by the following formula ##EQU1## wherein A is a substituted or unsubstituted heterocyclic radical and T is a C.sub.2 -C.sub.5 alkyl, alkenyl, cyclopropylmethyl, cyclobutylmethyl or cyclopentyl groupA process for their preparation and novel intermediates therefor are disclosed. These compounds are useful antibiotics.
    Type: Grant
    Filed: August 2, 1974
    Date of Patent: May 11, 1976
    Assignee: Hoffmann-La Roche Inc.
    Inventors: Andre Furlenmeier, Peter Quitt, Karl Vogler, Paul Lanz
  • Patent number: 3956318
    Abstract: A process for producing a substituted tetrahydrofuran which comprises contacting an epoxide with molecular hydrogen and a Group VIII metal hydrogenation catalyst at a temperature between 50.degree. and 250.degree.C and a pressure between 10 and 5000 psig, wherein the contacting is carried out in the liquid phase and in the presence of a protonic acid, and the epoxide has the formula ##EQU1## wherein R.sup.1 is a methyl, ethyl, propyl or butyl group and wherein R.sup.2 is hydrogen, methyl, ethyl, propyl or butyl.
    Type: Grant
    Filed: January 29, 1975
    Date of Patent: May 11, 1976
    Assignee: Chevron Research Company
    Inventor: Shigeto Suzuki
  • Patent number: 3956386
    Abstract: cis-N,N,N',N'-Tetramethylcyclopropane-1,2-dicarboxamide as a new chemical compound, and the use thereof in the regulation of plant growth.
    Type: Grant
    Filed: May 26, 1971
    Date of Patent: May 11, 1976
    Assignee: Monsanto Company
    Inventor: Charles F. Hobbs
  • Patent number: 3954812
    Abstract: Viscous polybutenes of number average molecular weight (M.sub.n) in the range of about 300 to about 3000 have improved reactivity with intramolecular anhydrides of unsaturated aliphatic dicarboxylic acids when such polybutenes contain rather small amounts, i.e., 5 to 200 ppm, of halogenated, preferably chlorinated and/or brominated carboxylic or sulfonic acid. Preference is given to such halogen containing compounds having a sufficient vapor pressure at a temperature in the range of 100.degree. to 300.degree.C to be substantially completely removed at absolute pressures in the range of 5 to 760 mm Hg. Use of such polybutenes containing such halogenated compounds in the addition reaction with said unsaturated anhydrides can reduce formation of undesired tarry product resulting from polymerization and/or thermal decomposition of the unsaturated anhydrides and enhance yield of desired alkenyl-substituted anhydride.
    Type: Grant
    Filed: May 10, 1973
    Date of Patent: May 4, 1976
    Assignee: Standard Oil Company
    Inventors: Imre Puskas, John A. Cengel
  • Patent number: 3954796
    Abstract: Tetra-(alkylsulphamoyl)-copper phthalocyanines of the formula ##EQU1## WHEREIN CuPc denotes a copper phthalocyanine radical, R.sub.1, R.sub.2 and R.sub.3 denote alkyl radicals with a total of 7 - 12 C atoms, R.sub.4, R.sub.5 and R.sub.6 denote alkyl radicals with a total of 11 - 13 C atoms and n denotes 0 - 4 have a good solubility an alcohol and are particularly suitable for dyeing alcoholic solutions of film-forming polymers.
    Type: Grant
    Filed: July 10, 1974
    Date of Patent: May 4, 1976
    Assignee: Ciba-Geigy Corporation
    Inventor: Werner Kuster
  • Patent number: 3954795
    Abstract: Improved process for the preparation of copper phthalocyanine in pigmentary form by viscous salt milling crude copper phthalocyanine in the presence of an organic conditioning agent and FeCl.sub.3 followed by acid extraction. This process requires substantially less energy than conventional viscous salt milling and produces a highly dispersible, very strong .beta.-phase copper phthalocyanine which is useful as a pigment in a variety of applications.
    Type: Grant
    Filed: May 2, 1975
    Date of Patent: May 4, 1976
    Assignee: E. I. Du Pont de Nemours and Company
    Inventor: Julius Jackson
  • Patent number: 3954813
    Abstract: This invention relates to therapeutically active 2,5-furane derivatives, wherein the substituent in the 2-position is a lower alkyl group or a group ROOC--(CH.sub.2).sub.7 --, in which R is hydrogen or lower alkyl, the 5-substituent being an alkyl or alkylene group of 4 to 13 carbon atoms, which may be substituted with an oxygen atom, a hydroxy group or a lower alkyl group at the third carbon atom, counted from the furane ring, and to the production thereof.
    Type: Grant
    Filed: June 19, 1974
    Date of Patent: May 4, 1976
    Assignee: Aktieselskabet Grindstedvaerket
    Inventors: Poul Nedenskov, Karol Alster